CN110585106A - Dendrobium officinale barrier cream and preparation method thereof - Google Patents

Dendrobium officinale barrier cream and preparation method thereof Download PDF

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Publication number
CN110585106A
CN110585106A CN201911064261.9A CN201911064261A CN110585106A CN 110585106 A CN110585106 A CN 110585106A CN 201911064261 A CN201911064261 A CN 201911064261A CN 110585106 A CN110585106 A CN 110585106A
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parts
dendrobium officinale
silica
stirring
peg
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周涛
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Filang Biotechnology Hubei Co Ltd
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Filang Biotechnology Hubei Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The invention discloses dendrobium officinale makeup base cream and a preparation method thereof, wherein the dendrobium officinale makeup base cream is prepared by combining the following raw materials in parts by weight: water, CI 77891, CI77007, triethoxycaprylylsilane, aluminum hydroxide, mica, CI 77491, HDI/trimethylolhexylactone crosspolymer, silica, dimethylsilylated silica, cyclopentadimethylsiloxane, disteardimonium hectorite, hydrogenated polyisobutene, caprylic/capric triglyceride, cetostearyl ethylhexanoate, dimethicone, lauryl PEG-10 trisilicoethylmethylsiloxane, PEG-10 dimethicone, polyglyceryl-3 polyricinoleate, sorbitan isostearate, magnesium myristate, glycerin, propylene glycol, dendrobium officinale extract, magnesium sulfate, caprylyl glycol, ethylhexylglycerin. The sun screen disclosed by the invention is rich in abundant moisturizing components, and can be used for moisturizing and caring skin layer by layer, so that the skin can be kept moisture constantly to prevent dryness, and the moisture and the skin are made tender, and the skin is light and attractive due to the light faint scent of the formula.

Description

Dendrobium officinale barrier cream and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to dendrobium officinale barrier cream and a preparation method thereof.
Background
Isolation, as the name implies, is the isolation of the visceral material from the skin, preventing them from harming the skin. The dirt not only contains impurities in the air, but also comprises computer radiation, mobile phone radiation and the like, and the substances are isolated outside the skin, so that the damage to the skin can be reduced, and the elasticity of the skin can be kept; can also prevent the color cosmetics from blocking pores during makeup, do not irritate the skin and are protective films for the skin. The foundation cream has the effect of concealing flaws while insulating, can lighten spots, shrink pores, reduce fine lines and the like, and can brighten skin color to prevent the skin from being dark.
Disclosure of Invention
The invention aims to provide dendrobium officinale makeup base cream and a preparation method thereof, and aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a dendrobium officinale makeup base cream is prepared from the following raw materials in parts by weight: 58-78 parts of water, 0.1-0.5 part of CI 77891, 0.01-0.08 part of CI77007, 1-5 parts of triethoxyoctylsilane, 0.1-1 part of aluminum hydroxide, 0.1-0.8 part of mica, 0.1-0.5 part of CI 77491, 0.1-1 part of HDI/trimethylolhexyllactone crosspolymer, 0.1-1.5 parts of silica, 0.5-2.5 parts of dimethylsilylated silica, 1-3 parts of cyclopentyldimethicone, 0.1-1 part of disteardimonium hectorite, 1-5 parts of hydrogenated polyisobutene, 1-5 parts of caprylic/capric triglyceride, 1-5 parts of cetearyl ethyl hexanoate, 1-3 parts of polydimethylsiloxane, 1-5 parts of lauryl PEG-10 tris (trimethylsiloxy) silicon ethyl methicone, 1-3 parts of PEG-10 polydimethylsiloxane, 0.5-2.5 parts of polyglycerol-3 polyricinoleate, 1-5 parts of sorbitan isostearate, 0.5-2.5 parts of magnesium myristate, 1-5 parts of glycerol, 3-13 parts of propylene glycol, 0.1-1 part of DENDROBIUM officinale (Dendrobium CANDIDUM) extract, 0.1-1 part of magnesium sulfate, 1-3 parts of octaethylene glycol and 1-5 parts of ethylhexylglycerol.
As a further scheme of the invention: the composition is specifically prepared from the following raw materials in parts by weight: 58 parts of water, 0.1 part of CI 77891, 0.01 part of CI77007, 1 part of triethoxyoctylsilane, 0.1 part of aluminum hydroxide, 0.1 part of mica, 0.1 part of CI 77491, 0.1 part of HDI/trimethylolhexyllactone crosspolymer, 0.1 part of silica, 0.5 part of silica dimethylsilylate, 1 part of cyclopentyldimethicone, 0.1 part of hectorite of disteardimonium, 1 part of hydrogenated polyisobutene, 1 part of triglyceride octanoate/decanoate, 1 part of cetearyl ethyl hexanoate, 1 part of polydimethylsiloxane, 5 parts of lauryl PEG-10 tris (trimethylsiloxy) silicon ethyl methicone, 3 parts of PEG-10 dimethicone, 2.5 parts of polyglycerol-3 polyricinoleate, 5 parts of sorbitan isostearate, 2.5 parts of magnesium myristate, 5 parts of glycerol, 13 parts of propylene glycol, 1 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 1 part of magnesium sulfate, 3 parts of octyl glycol and 5 parts of ethylhexyl glycerol.
As a further scheme of the invention: the composition is specifically prepared from the following raw materials in parts by weight: 78 parts of water, 0.5 part of CI 77891, 0.08 part of CI77007, 5 parts of triethoxyoctylsilane, 1 part of aluminum hydroxide, 0.8 part of mica, 0.5 part of CI 77491, 1 part of HDI/trimethylolhexyllactone crosspolymer, 1.5 parts of silica, 2.5 parts of dimethylsilylated silica, 3 parts of cyclopentadimethylsiloxane, 1 part of distearyldimethylammonium hectorite, 5 parts of hydrogenated polyisobutene, 5 parts of caprylic/capric triglyceride, 5 parts of cetearyl ethylhexanoate, 3 parts of polydimethylsiloxane, 1 part of lauryl PEG-10 tris (trimethylsiloxy) silaethylmethicone, 1 part of PEG-10 polydimethylsiloxane, 0.5 part of polyglycerol-3 polyricinoleate, 1 part of sorbitan isostearate, 0.5 part of magnesium myristate, 1 part of glycerol, 3 parts of propylene glycol, 0.1 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.1 part of magnesium sulfate, 1 part of octyl glycol and 1 part of ethylhexyl glycerol.
As a further scheme of the invention: the composition is specifically prepared from the following raw materials in parts by weight: 62 parts of water, 0.2 parts of CI 77891, 0.03 parts of CI77007, 2 parts of triethoxyoctylsilane, 0.3 parts of aluminum hydroxide, 0.3 parts of mica, 0.2 parts of CI 77491, 0.2 parts of HDI/trimethylolhexyllactone crosspolymer, 0.3 parts of silica, 1.3 parts of dimethylsilylated silica, 2 parts of cyclopentyldimethicone, 0.4 parts of disteardimonium hectorite, 2 parts of hydrogenated polyisobutene, 2 parts of caprylic/capric triglyceride, 2 parts of cetearyl ethylhexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone, 2 parts of PEG-10 dimethicone, 1.1 part of polyglyceryl-3 polyricinoleate, 3 parts of sorbitan isostearate, 0.9 parts of magnesium myristate, 2 parts of glycerin, 7 parts of propylene glycol, 0.5 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.4 part of magnesium sulfate, 2 parts of octyl glycol and 3 parts of ethylhexyl glycerol.
As a further scheme of the invention: the composition is specifically prepared from the following raw materials in parts by weight: 72 parts of water, 0.4 parts of CI 77891, 0.07 parts of CI77007, 4 parts of triethoxyoctylsilane, 0.8 parts of aluminum hydroxide, 0.7 parts of mica, 0.4 parts of CI 77491, 0.8 parts of HDI/trimethylolhexyllactone crosspolymer, 1.3 parts of silica, 2.4 parts of dimethylsilylated silica, 2 parts of cyclopentyldimethicone, 0.9 parts of disteardimonium hectorite, 4 parts of hydrogenated polyisobutene, 4 parts of caprylic/capric triglyceride, 3 parts of cetearyl ethylhexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone, 2 parts of PEG-10 dimethicone, 2.1 parts of polyglyceryl-3 polyricinoleate, 4 parts of sorbitan isostearate, 2.3 parts of magnesium myristate, 4 parts of glycerin, 11 parts of propylene glycol, 0.9 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.9 part of magnesium sulfate, 2 parts of octyl glycol and 4 parts of ethylhexyl glycerol.
As a further scheme of the invention: the propylene glycol is one or a mixture of 1, 3-propylene glycol and 1, 2-propylene glycol.
The preparation method of the dendrobium officinale makeup base cream comprises the following steps:
s1, thoroughly cleaning and disinfecting related production equipment and related production tools, and preparing the following raw materials one by one according to the weight part ratio: water, CI 77891, CI77007, triethoxycaprylylsilane, aluminum hydroxide, mica, CI 77491, HDI/trimethylolhexyllactone crosspolymer, silica, dimethylsilylated silica, cyclopentadimethylsiloxane, disteardimonium hectorite, hydrogenated polyisobutene, caprylic/capric triglyceride, cetostearyl ethylhexanoate, dimethicone, lauryl PEG-10 tris (trimethylsiloxy) silylmethicone, PEG-10 dimethicone, polyglyceryl-3 polyricinoleate, sorbitan isostearate, magnesium myristate, glycerin, propylene glycol, Dendrobium officinale (Dendibumcandicum) extract, magnesium sulfate, caprylyl glycol, ethylhexyl glycerin;
s2, adding half of water into a single dissolving tank at normal temperature, and slowly and sequentially adding CI 77891, CI77007, triethoxyoctylsilane, aluminum hydroxide, mica, CI 77491, HDI/trihydroxymethylhexyl lactone crosspolymer, silica and dimethyl silylated silica while stirring by a stirrer to form a mixed solution;
s3, adding hydrogenated polyisobutene, caprylic/capric triglyceride, cetearyl ethyl hexanoate, polydimethylsiloxane, lauryl PEG-10 tri (trimethylsiloxy) silicon ethyl polymethylsiloxane, PEG-10 polydimethylsiloxane, polyglycerol-3 polyricinoleate, sorbitan isostearate and magnesium myristate into an emulsifying pot, heating to 75 +/-3 ℃, stirring by a stirrer while adding materials until the materials are completely dissolved, and cooling to 45 ℃;
s4, adding cyclopentadimethylsiloxane and disteardimonium hectorite into the emulsifying pot, adding the mixed solution formed in the step S2, and stirring by a stirrer while adding the materials until the materials are completely dispersed;
s5, adding the other half of water into the water phase dissolving tank at normal temperature, and slowly and sequentially adding glycerol, propylene glycol, herba Dendrobii (Dendrobii herba Dendrobii) extract, magnesium sulfate, octyl glycol and ethylhexyl glycerol while stirring with a stirrer until completely dissolving to form water phase liquid;
s6, adding the aqueous phase liquid formed in the step S5 into an emulsifying pot, stirring and stirring by a stirrer while adding materials, and pre-emulsifying;
s7, after pre-emulsification is finished, accelerating stirring and emulsifying;
s8, defoaming after emulsification is completed, and cooling the emulsifying pot to 30 ℃ to obtain semi-finished product of sun screen;
and S9, detecting the semi-finished product of the makeup base cream to be qualified, discharging, and sealing and storing to obtain the finished product of the makeup base cream.
As a further scheme of the invention: in the step S2, the stirring speed is 950-1050rpm, and the stirring time is 8-13 min; the stirring speed in the step S3 is 550-650rpm, and the stirring time is 4-7 min; in the step S4, the stirring speed is 2150-2250rpm, and the stirring time is 4-6 min; in the step S5, the stirring speed is 950-1050rpm, and the stirring time is 8-13 min; in the step S6, the stirring speed is 2950 and 3050rpm, and the stirring time is 4-7 min; in the step S7, the stirring speed is 2950 and 3050rpm, and the stirring time is 4-10 min; in the step S8, the stirring speed is 20-50rpm, and the vacuum degree is 60 Pa.
Compared with the prior art, the invention has the beneficial effects that: the sun screen disclosed by the invention is rich in abundant moisturizing components, and can be used for moisturizing and caring skin layer by layer, so that the skin can be constantly kept moisture to prevent dryness, and the moisture and the skin are made tender, and the skin is light and attractive due to the light faint scent of the formula; the inventive sun screen contains Dendrobium officinale extract, which can effectively resist the oxidation of the outside world to cells, effectively remove the accumulation and deposition of harmful substance free radicals on the skin, delay the aging of human cell tissues, repair damaged cells, and protect collagen, so that the skin is fresh and elastic, the young state is maintained, wrinkles are reduced, and aging is delayed; the inventive sun screen contains mica, has good shielding function to ultraviolet, and has no influence on skin ventilation, so that skin feels comfortable, and evaporation of skin moisture is inhibited.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1: the dendrobium officinale makeup base cream is specifically prepared from the following raw materials in parts by weight: 58 parts of water, 0.1 part of CI 77891, 0.01 part of CI77007, 1 part of triethoxyoctylsilane, 0.1 part of aluminum hydroxide, 0.1 part of mica, 0.1 part of CI 77491, 0.1 part of HDI/trimethylolhexyllactone crosspolymer, 0.1 part of silica, 0.5 part of silica dimethylsilylate, 1 part of cyclopentyldimethicone, 0.1 part of hectorite of disteardimonium, 1 part of hydrogenated polyisobutene, 1 part of triglyceride octanoate/decanoate, 1 part of cetearyl ethyl hexanoate, 1 part of polydimethylsiloxane, 5 parts of lauryl PEG-10 tris (trimethylsiloxy) silicon ethyl methicone, 3 parts of PEG-10 dimethicone, 2.5 parts of polyglycerol-3 polyricinoleate, 5 parts of sorbitan isostearate, 2.5 parts of magnesium myristate, 5 parts of glycerol, 13 parts of propylene glycol, 1 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 1 part of magnesium sulfate, 3 parts of octyl glycol and 5 parts of ethylhexyl glycerol.
Wherein the propylene glycol is 1, 3-propylene glycol.
A preparation method of dendrobium officinale makeup base cream comprises the following steps:
s1, thoroughly cleaning and disinfecting related production equipment and related production tools, and preparing the following raw materials one by one according to the weight part ratio: water, CI 77891, CI77007, triethoxycaprylylsilane, aluminum hydroxide, mica, CI 77491, HDI/trimethylolhexyllactone crosspolymer, silica, dimethylsilylated silica, cyclopentadimethylsiloxane, disteardimonium hectorite, hydrogenated polyisobutene, caprylic/capric triglyceride, cetostearyl ethylhexanoate, dimethicone, lauryl PEG-10 tris (trimethylsiloxy) silylmethicone, PEG-10 dimethicone, polyglyceryl-3 polyricinoleate, sorbitan isostearate, magnesium myristate, glycerin, propylene glycol, Dendrobium officinale (Dendibumcandicum) extract, magnesium sulfate, caprylyl glycol, ethylhexyl glycerin;
s2, adding half of water into a single dissolving tank at normal temperature, slowly and sequentially adding CI 77891, CI77007, triethoxyoctylsilane, aluminum hydroxide, mica, CI 77491, HDI/trihydroxymethyl hexyl lactone cross-linked polymer, silica and dimethyl silyl silica while stirring by a stirrer to form a mixed solution, wherein the stirring speed is 950 plus 1050rpm, and the stirring time is 8-13 min;
s3, adding hydrogenated polyisobutene, caprylic/capric triglyceride, cetearyl ethyl hexanoate, polydimethylsiloxane, lauryl PEG-10 tri (trimethylsiloxy) silicon ethyl polymethylsiloxane, PEG-10 polydimethylsiloxane, polyglycerol-3 polyricinoleate, sorbitan isostearate and magnesium myristate into an emulsifying pot, heating to 75 +/-3 ℃, stirring by a stirrer while adding materials until the materials are completely dissolved, cooling to 45 ℃, wherein the stirring speed is 550-650rpm, and the stirring time is 4-7 min;
s4, continuously adding cyclopentadimethylsiloxane and disteardimonium hectorite into the emulsifying pot, then adding the mixed solution formed in the step S2, stirring by using a stirrer while adding materials until the mixed solution is completely dispersed, wherein the stirring speed is 2150-2250rpm, the stirring time is 4-6min, and the temperature is kept at 45 ℃;
s5, adding the other half of water into the water phase dissolving tank at normal temperature, slowly and sequentially adding glycerol, propylene glycol, DENDROBIUM officinale (Dendrobium CANDIDUM) extract, magnesium sulfate, caprylyl glycol and ethylhexylglycerin while stirring by a stirrer until the glycerol, the propylene glycol, the DENDROBIUM officinale (Dendrobium CANDIDUM) extract, the magnesium sulfate, the caprylyl glycol and the ethylhexylglycerin are completely dissolved to form water phase liquid, wherein the stirring speed is 950 plus 1050rpm, and the stirring time is 8-13 min;
s6, adding the aqueous phase liquid formed in the step S5 into an emulsifying pot, stirring and stirring the aqueous phase liquid by a stirrer while adding the aqueous phase liquid, pre-emulsifying the aqueous phase liquid, wherein the stirring speed is 2950 and 3050rpm, the stirring time is 4-7min, and the temperature is kept at 45 ℃;
s7, after pre-emulsification is finished, accelerating stirring, emulsifying, wherein the stirring speed is 2950 and 3050rpm, the stirring time is 4-10min, and the temperature is kept at 45 ℃;
s8, defoaming after emulsification, and cooling an emulsifying pot to 30 ℃ to obtain semi-finished product isolating cream, wherein the stirring speed is 20-50rpm, and the vacuum degree is 60 Pa;
and S9, detecting the semi-finished product of the makeup base cream to be qualified, discharging, and sealing and storing to obtain the finished product of the makeup base cream.
Example 2: the dendrobium officinale makeup base cream is specifically prepared from the following raw materials in parts by weight: 78 parts of water, 0.5 part of CI 77891, 0.08 part of CI77007, 5 parts of triethoxyoctylsilane, 1 part of aluminum hydroxide, 0.8 part of mica, 0.5 part of CI 77491, 1 part of HDI/trimethylolhexyllactone crosspolymer, 1.5 parts of silica, 2.5 parts of dimethylsilylated silica, 3 parts of cyclopentadimethylsiloxane, 1 part of distearyldimethylammonium hectorite, 5 parts of hydrogenated polyisobutene, 5 parts of caprylic/capric triglyceride, 5 parts of cetearyl ethylhexanoate, 3 parts of polydimethylsiloxane, 1 part of lauryl PEG-10 tris (trimethylsiloxy) silaethylmethicone, 1 part of PEG-10 polydimethylsiloxane, 0.5 part of polyglycerol-3 polyricinoleate, 1 part of sorbitan isostearate, 0.5 part of magnesium myristate, 1 part of glycerol, 3 parts of propylene glycol, 0.1 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.1 part of magnesium sulfate, 1 part of octyl glycol and 1 part of ethylhexyl glycerol.
Wherein the propylene glycol is 1, 2-propylene glycol.
A preparation method of dendrobium officinale makeup base cream, which has the same specific implementation steps as example 1.
Example 3: the dendrobium officinale makeup base cream is specifically prepared from the following raw materials in parts by weight: 62 parts of water, 0.2 parts of CI 77891, 0.03 parts of CI77007, 2 parts of triethoxyoctylsilane, 0.3 parts of aluminum hydroxide, 0.3 parts of mica, 0.2 parts of CI 77491, 0.2 parts of HDI/trimethylolhexyllactone crosspolymer, 0.3 parts of silica, 1.3 parts of dimethylsilylated silica, 2 parts of cyclopentyldimethicone, 0.4 parts of disteardimonium hectorite, 2 parts of hydrogenated polyisobutene, 2 parts of caprylic/capric triglyceride, 2 parts of cetearyl ethylhexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone, 2 parts of PEG-10 dimethicone, 1.1 part of polyglyceryl-3 polyricinoleate, 3 parts of sorbitan isostearate, 0.9 parts of magnesium myristate, 2 parts of glycerin, 7 parts of propylene glycol, 0.5 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.4 part of magnesium sulfate, 2 parts of octyl glycol and 3 parts of ethylhexyl glycerol.
Wherein the propylene glycol is a mixture of 1, 3-propylene glycol and 1, 2-propylene glycol, and the 1, 3-propylene glycol accounts for 40%.
A preparation method of dendrobium officinale makeup base cream, which has the same specific implementation steps as example 1.
Example 4: the dendrobium officinale makeup base cream is specifically prepared from the following raw materials in parts by weight: 72 parts of water, 0.4 parts of CI 77891, 0.07 parts of CI77007, 4 parts of triethoxyoctylsilane, 0.8 parts of aluminum hydroxide, 0.7 parts of mica, 0.4 parts of CI 77491, 0.8 parts of HDI/trimethylolhexyllactone crosspolymer, 1.3 parts of silica, 2.4 parts of dimethylsilylated silica, 2 parts of cyclopentyldimethicone, 0.9 parts of disteardimonium hectorite, 4 parts of hydrogenated polyisobutene, 4 parts of caprylic/capric triglyceride, 3 parts of cetearyl ethylhexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone, 2 parts of PEG-10 dimethicone, 2.1 parts of polyglyceryl-3 polyricinoleate, 4 parts of sorbitan isostearate, 2.3 parts of magnesium myristate, 4 parts of glycerin, 11 parts of propylene glycol, 0.9 part of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.9 part of magnesium sulfate, 2 parts of octyl glycol and 4 parts of ethylhexyl glycerol.
Wherein the propylene glycol is a mixture of 1, 3-propylene glycol and 1, 2-propylene glycol, and the 1, 3-propylene glycol accounts for 70%.
A preparation method of dendrobium officinale makeup base cream, which has the same specific implementation steps as example 1.
200 female volunteers of 28-35 years old are selected and divided into 5 groups, 40 persons in each group are respectively tried on the finished sun screen of the embodiment 1, the embodiment 2, the embodiment 3 and the embodiment 4 and a blank group without the product, and the using method is as follows: after cleaning the face in the morning and evening every day, the face is firstly smeared at the position where two cheekbone bones protrude, the nose part is gently taken from top to bottom by using the middle finger and the ring finger from inside to outside, the nose wing part is smeared in a pressing mode by using a powder puff, then the chin and the lower part of the eyes are smeared in a circle drawing mode, the face is smeared in a pressing mode from the head to the tail of the eyes, and the belly of the middle finger and the ring finger is gently pressed. The effect after 15 days of use is shown in table 1; the effect after 30 days of use is shown in table 2; the effect after 45 days of use is shown in table 3.
Table 1: effect test table after using the product for sun screen for 15 days
Test items Example 1 Example 2 Example 3 Example 4 Blank group
Moisture of skin Increase by 6% Increase by 8 percent Increase by 6% The improvement is 9 percent Without change
Elasticity of skin Increase by 3 percent Increase by 4% Increase by 3 percent Increase by 5 percent Reduce by 1%
Wrinkle (wrinkle) Slightly reduced Slightly reduced Slightly reduced Reduction of Without change
Table 2: effect test table after using the product for sun screen for 30 days
Test items Example 1 Example 2 Example 3 Example 4 Blank group
Moisture of skin The improvement is 7 percent The improvement is 9 percent Increase by 8 percent The improvement is 10 percent Without change
Elasticity of skin Increase by 4% Increase by 5 percent Increase by 4% Increase by 5 percent Reduce by 1%
Wrinkle (wrinkle) Reduction of Reduction of Reduction of Reduction of Without change
Table 3: effect test table after using the product for sun screen for 45 days
Test items Example 1 Example 2 Example 3 Example 4 Blank group
Moisture of skin The improvement is 9 percent Increase by 11 percent The improvement is 10 percent The improvement is 12 percent Without change
Elasticity of skin Increase by 5 percent Increase by 6% The improvement is 7 percent Increase by 6% Without change
Wrinkle (wrinkle) Reduction of Is obviously reduced Is obviously reduced Is obviously reduced Without change
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.

Claims (8)

1. The dendrobium officinale makeup base cream is characterized by being prepared from the following raw materials in parts by weight: 58-78 parts of water, 0.1-0.5 part of CI 77891, 0.01-0.08 part of CI77007, 1-5 parts of triethoxyoctylsilane, 0.1-1 part of aluminum hydroxide, 0.1-0.8 part of mica, 0.1-0.5 part of CI 77491, 0.1-1 part of HDI/trimethylolhexyllactone crosspolymer, 0.1-1.5 parts of silica, 0.5-2.5 parts of dimethylsilylated silica, 1-3 parts of cyclopentyldimethicone, 0.1-1 part of disteardimonium hectorite, 1-5 parts of hydrogenated polyisobutene, 1-5 parts of caprylic/capric triglyceride, 1-5 parts of cetearyl ethyl hexanoate, 1-3 parts of dimethicone, 1-5 parts of lauryl PEG-10 trisilicoethyl methicone, 1-3 parts of PEG-10 polydimethylsiloxane, 0.5-2.5 parts of polyglycerol-3 polyricinoleate, 1-5 parts of sorbitan isostearate, 0.5-2.5 parts of magnesium myristate, 1-5 parts of glycerol, 3-13 parts of propylene glycol, 0.1-1 part of dendrobium officinale extract, 0.1-1 part of magnesium sulfate, 1-3 parts of caprylyl glycol and 1-5 parts of ethylhexyl glycerol.
2. The dendrobium officinale makeup base cream according to claim 1, which is prepared from the following raw materials in parts by weight: 58 parts of water, 0.1 part of CI 77891, 0.01 part of CI77007, 1 part of triethoxyoctylsilane, 0.1 part of aluminum hydroxide, 0.1 part of mica, 0.1 part of CI 77491, 0.1 part of HDI/trimethylolhexyllactone crosspolymer, 0.1 part of silica, 0.5 part of dimethylsilylated silica, 1 part of cyclopentyldimethicone, 0.1 part of disteardimonium hectorite, 1 part of hydrogenated polyisobutene, 1 part of caprylic/capric triglyceride, 1 part of cetearyl ethylhexanoate, 1 part of polydimethylsiloxane, 5 parts of lauryl PEG-10 trisilicoethylmethylsiloxane, 3 parts of PEG-10 polydimethylsiloxane, 2.5 parts of polyglyceryl-3 polyricinoleate, 5 parts of sorbitan isostearate, 2.5 parts of magnesium myristate, 5 parts of glycerol, 13 parts of propylene glycol, 1 part of dendrobium officinale extract, 1 part of magnesium sulfate, 3 parts of caprylyl glycol and 5 parts of ethylhexyl glycerin.
3. The dendrobium officinale makeup base cream according to claim 1, which is prepared from the following raw materials in parts by weight: 78 parts of water, 0.5 part of CI 77891, 0.08 part of CI77007, 5 parts of triethoxyoctylsilane, 1 part of aluminum hydroxide, 0.8 part of mica, 0.5 part of CI 77491, 1 part of HDI/trimethylolhexyllactone crosspolymer, 1.5 parts of silica, 2.5 parts of dimethylsilylated silica, 3 parts of cyclopentadimethylsiloxane, 1 part of disteardimonium hectorite, 5 parts of hydrogenated polyisobutene, 5 parts of caprylic/capric triglyceride, 5 parts of cetearyl ethylhexanoate, 3 parts of polydimethylsiloxane, 1 part of lauryl PEG-10 trisilicoethylmethylsiloxane, 1 part of PEG-10 polydimethylsiloxane, 0.5 part of polyglyceryl-3 polyricinoleate, 1 part of sorbitan isostearate, 0.5 part of magnesium myristate, 1 part of glycerol, 3 parts of propylene glycol, 0.1 part of dendrobium officinale extract, 0.1 part of magnesium sulfate, 1 part of octyl glycol and 1 part of ethylhexyl glycerol.
4. The dendrobium officinale makeup base cream according to claim 1, which is prepared from the following raw materials in parts by weight: 62 parts of water, 0.2 parts of CI 77891, 0.03 parts of CI77007, 2 parts of triethoxyoctylsilane, 0.3 parts of aluminum hydroxide, 0.3 parts of mica, 0.2 parts of CI 77491, 0.2 parts of HDI/trimethylolhexyllactone crosspolymer, 0.3 parts of silica, 1.3 parts of dimethylsilylated silica, 2 parts of cyclopentadimethicone, 0.4 parts of disteardimonium hectorite, 2 parts of hydrogenated polyisobutene, 2 parts of caprylic/capric triglyceride, 2 parts of cetearyl ethylhexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 trisilicoethylmethylsiloxane, 2 parts of PEG-10 polydimethylsiloxane, 1.1 part of polyglyceryl-3 polyricinoleate, 3 parts of sorbitan isostearate, 0.9 part of magnesium myristate, 2 parts of glycerol, 7 parts of propylene glycol, 0.5 part of dendrobium officinale extract, 0.4 part of magnesium sulfate, 2 parts of octyl glycol and 3 parts of ethylhexyl glycerol.
5. The dendrobium officinale makeup base cream according to claim 1, which is prepared from the following raw materials in parts by weight: 72 parts of water, 0.4 parts of CI 77891, 0.07 parts of CI77007, 4 parts of triethoxyoctylsilane, 0.8 parts of aluminum hydroxide, 0.7 parts of mica, 0.4 parts of CI 77491, 0.8 parts of HDI/trimethylolhexyllactone crosspolymer, 1.3 parts of silica, 2.4 parts of dimethylsilylated silica, 2 parts of cyclopentyldimethicone, 0.9 parts of disteardimonium hectorite, 4 parts of hydrogenated polyisobutene, 4 parts of caprylic/capric triglyceride, 3 parts of cetearyl ethyl hexanoate, 2 parts of polydimethylsiloxane, 3 parts of lauryl PEG-10 trisilicoethylmethylsiloxane, 2 parts of PEG-10 polydimethylsiloxane, 2.1 parts of polyglyceryl-3 polyricinoleate, 4 parts of sorbitan isostearate, 2.3 parts of magnesium myristate, 4 parts of glycerol, 11 parts of propylene glycol, 0.9 part of dendrobium officinale extract, 0.9 part of magnesium sulfate, 2 parts of octyl glycol and 4 parts of ethylhexyl glycerol.
6. The dendrobium officinale barrier cream as claimed in claim 1, wherein the propylene glycol is one or a mixture of 1, 3-propylene glycol and 1, 2-propylene glycol.
7. The preparation method of the dendrobium officinale isolation cream as set forth in any one of claims 1 to 6, which is characterized by comprising the following steps:
s1, thoroughly cleaning and disinfecting related production equipment and related production tools, and preparing the following raw materials one by one according to the weight part ratio: water, CI 77891, CI77007, triethoxycaprylylsilane, aluminum hydroxide, mica, CI 77491, HDI/trimethylolhexylactone crosspolymer, silica, dimethylsilylated silica, cyclopentadimethylsiloxane, disteardimonium hectorite, hydrogenated polyisobutene, caprylic/capric triglyceride, cetostearyl ethylhexanoate, dimethicone, lauryl PEG-10 trisilicoethylmethylsiloxane, PEG-10 dimethicone, polyglyceryl-3 polyricinoleate, sorbitan isostearate, magnesium myristate, glycerin, propylene glycol, Dendrobium officinale extract, magnesium sulfate, caprylyl glycol, ethylhexylglycerin;
s2, adding half of water into a single dissolving tank at normal temperature, and slowly and sequentially adding CI 77891, CI77007, triethoxyoctylsilane, aluminum hydroxide, mica, CI 77491, HDI/trihydroxymethylhexyl lactone crosspolymer, silica and dimethyl silylated silica while stirring by a stirrer to form a mixed solution;
s3, adding hydrogenated polyisobutene, caprylic/capric triglyceride, cetearyl ethyl hexanoate, polydimethylsiloxane, lauryl PEG-10 trisilicoethyl methylsiloxane, PEG-10 polydimethylsiloxane, polyglycerol-3 polyricinoleate, sorbitan isostearate and magnesium myristate into an emulsifying pot, heating to 75 +/-3 ℃, stirring by a stirrer while adding materials until the materials are completely dissolved, and cooling to 45 ℃;
s4, adding cyclopentadimethylsiloxane and disteardimonium hectorite into the emulsifying pot, adding the mixed solution formed in the step S2, and stirring by a stirrer while adding the materials until the materials are completely dispersed;
s5, adding the other half of water into the water phase dissolving tank at normal temperature, and slowly and sequentially adding glycerol, propylene glycol, the dendrobium officinale extract, magnesium sulfate, caprylyl glycol and ethylhexyl glycerol while stirring by a stirrer until the glycerol, the propylene glycol, the dendrobium officinale extract, the magnesium sulfate, the caprylyl glycol and the ethylhexyl glycerol are completely dissolved to form water phase liquid;
s6, adding the aqueous phase liquid formed in the step S5 into an emulsifying pot, stirring and stirring by a stirrer while adding materials, and pre-emulsifying;
s7, after pre-emulsification is finished, accelerating stirring and emulsifying;
s8, defoaming after emulsification is completed, and cooling the emulsifying pot to 30 ℃ to obtain semi-finished product of sun screen;
and S9, detecting the semi-finished product of the makeup base cream to be qualified, discharging, and sealing and storing to obtain the finished product of the makeup base cream.
8. The method for preparing the dendrobium officinale isolation cream as claimed in claim 7, wherein the stirring rotation speed in the step S2 is 950-1050rpm, and the stirring time is 8-13 min; the stirring speed in the step S3 is 550-650rpm, and the stirring time is 4-7 min; in the step S4, the stirring speed is 2150-2250rpm, and the stirring time is 4-6 min; in the step S5, the stirring speed is 950-1050rpm, and the stirring time is 8-13 min; in the step S6, the stirring speed is 2950 and 3050rpm, and the stirring time is 4-7 min; in the step S7, the stirring speed is 2950 and 3050rpm, and the stirring time is 4-10 min; in the step S8, the stirring speed is 20-50rpm, and the vacuum degree is 60 Pa.
CN201911064261.9A 2019-11-04 2019-11-04 Dendrobium officinale barrier cream and preparation method thereof Pending CN110585106A (en)

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CN111686057A (en) * 2020-06-28 2020-09-22 广州市澳莱化妆品有限公司 Formula and preparation method of dendrobium officinale repair and isolation cream
CN112156027A (en) * 2020-10-27 2021-01-01 广州德芙化妆品有限公司 Sunscreen cream with high sun protection value and preparation method thereof
CN114931538A (en) * 2022-05-24 2022-08-23 广州多多化妆品有限公司 Rainbow sugar eye shadow cream
CN115350108A (en) * 2022-08-24 2022-11-18 广州贝凯精细化工有限公司 Inorganic silicon composition and preparation method and application thereof

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Publication number Priority date Publication date Assignee Title
CN111686057A (en) * 2020-06-28 2020-09-22 广州市澳莱化妆品有限公司 Formula and preparation method of dendrobium officinale repair and isolation cream
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CN114931538A (en) * 2022-05-24 2022-08-23 广州多多化妆品有限公司 Rainbow sugar eye shadow cream
CN115350108A (en) * 2022-08-24 2022-11-18 广州贝凯精细化工有限公司 Inorganic silicon composition and preparation method and application thereof

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Application publication date: 20191220