CN107456403A - A kind of BB frosts and preparation method thereof - Google Patents
A kind of BB frosts and preparation method thereof Download PDFInfo
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- CN107456403A CN107456403A CN201710810084.9A CN201710810084A CN107456403A CN 107456403 A CN107456403 A CN 107456403A CN 201710810084 A CN201710810084 A CN 201710810084A CN 107456403 A CN107456403 A CN 107456403A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of BB frosts and preparation method thereof, it is related to cosmetic technical field.Wherein BB frosts include the component of following percentage by weight：Ring five dimethyl silicone polymer 5 15%；Sun-screening agent 0 5%；The dimethyl silicone polymers 1 1.5% of PEG 10；Sorbitan sesquioleate 0.2 0.5%；Phytosterol/octyl dodecanol lauroyl glutamate ester 0 2.5%；Thickener 0.2 1%；Preservative 0 1%；Colouring agent 2 15%；Filler 0 2%；Water 65 75%.The present invention reduces the dosage of emulsifying agent, improves the water-resistance and grease resistance of product, raising adornment imitates persistence, is not easy dizzy adornment, while ensures the stability of BB frosts, reduces excitant by ultrasonic emulsification technique；Effectively kill bacterium；PCA Na, hyaluronic acid and the three's Synergistic of polyquaternium 51, and the bionical moisture film of natural skin is formed, the moisture retention of product is improved, makes skin water profit smooth.
Description
Technical field
The present invention relates to cosmetic technical field, more specifically, it relates to a kind of BB frosts and preparation method thereof.
Background technology
In recent years, with cosmetics continuous development and the women that likes to be beautiful demand increase, BB frosts are increasingly pursued by people
And turn into fashion trend.Its underlying cause is that BB frosts are not only easy to use, and has foundation cream, sun-proof and isolated product concurrently
Effect.The women to like to be beautiful only need to possess flawless skin quality and skin sense using BB frost cans.BB frosts can allow female friend
Go out in proud array；It can more help the women to like to be beautiful to make perfect bottom adornment, persistently keep the dressing of one day.
Disclosed in Publication No. CN104546651A Chinese invention patent a kind of with photosensitive even color, the frivolous screening flaw
The air cushion BB frosts of effect, its each component percentage by weight are：Ozocerite 5-10%, NMF 24-44%, lubricant 6-
12%th, oils 8-14%, emulsifying agent 6-10%, dispersant 11-21%, preservative 0.2%, hydrophobic pigment 1-4%, thickener
2-9%, superfine pearl powder 4-8%, saualane 4-8%, ring five dimethyl silicone polymer 1-3%, octyl salicylate 8-10%, two
Titanium oxide 4-6%, alumina 1-3%, deionized water surplus.
For above-mentioned BB frosts in order to ensure emulsion stability, emulsifying agent addition is up to 6-10%, because surfactant has
There is amphipathic property, the addition of emulsifying agent is high, adornment when easily being dissolved by the grease of skin secretion and sweat, while can reduce use
The persistence of effect；And emulsifying agent has stronger excitant therefore emulsifying agent addition crosses the excitant that conference improves product.
It is, therefore, desirable to provide a kind of new scheme solves the above problems.
The content of the invention
In view of the deficienciess of the prior art, the purpose of the present invention one is to provide a kind of BB frosts, by using a small amount of breast
Agent adds ultrasonic emulsification technique, while stability is ensured, reduces the usage amount of emulsifying agent, solves of the prior art
BB frosts adornment imitates unabiding problem, and it has, and adornment effect persistence is strong, strong, the bland advantage that is not easy dizzy adornment, stability.
To achieve the above object one, the invention provides following technical scheme：
A kind of BB frosts, include the component of following percentage by weight：
Ring five dimethyl silicone polymer 5-15%；
Sun-screening agent 0-5%；
KF6017 1-1.5%；
Sorbitan sesquioleate 0.2-0.5%；
Phytosterol/octyl dodecanol lauroyl glutamate ester 0-2.5%；
Thickener 0.2-1%；
Preservative 0-1%；
Colouring agent 2-15%；
Filler 0-2%；
Water 65-75%.
Further, the BB frosts also include the NMF that percentage by weight is 3.51-9.02%.
Further, the NMF includes butanediol, Sodium Hyaluronate, Anjidew NL50, polyquaternium -51, according to BB frosts
Total amount meter, the butanediol, Sodium Hyaluronate, Anjidew NL50, the percentage by weight of polyquaternium -51 are respectively：2-5%, 0.01-
0.02%th, 0.5-2%, 1-2%.
Further, the BB frosts also include the skin conditioning agent that percentage by weight is 4-15.5%.
Further, the skin conditioning agent includes two octanoic acids of butanediol/dicaprate, tridecanol isononoate, angle
Shark alkane, phenyl trimethicone, pungent glycol, according to the total amount meter of BB frosts, two octanoic acids of the butanediol/dicaprate, ten
Three alkanol isononoates, saualane, phenyl trimethicone, the percentage by weight of pungent glycol are respectively：2-5%, 1-
3%th, 0-2%, 2-5%, 0-0.5%.
Further, the preservative includes Phenoxyethanol, methyl hydroxybenzoate, according to the total amount meter of BB frosts, the benzene oxygen second
Alcohol, the percentage by weight of methyl hydroxybenzoate are respectively：0-0.8%, 0-0.2%.
Further, the colouring agent includes iron oxides, titanium dioxide, according to the total amount meter of BB frosts, the iron oxide
Class, the percentage by weight of titanium dioxide are respectively：0-2%, 2-13%.
Further, the sun-screening agent is ethylhexyl methoxy cinnamate, and the thickener is distearyl dimethylammonium lithium
Montmorillonite, the filler are mica.
The purpose of the present invention two is to provide a kind of preparation method of BB frosts have adornment effect using the BB frosts of this method preparation
Persistence is strong, strong, the bland advantage that is not easy dizzy adornment, stability.
To achieve the above object two, the invention provides following technical scheme：
A kind of preparation method of BB frosts, comprises the following steps：
Step 1, by ring five dimethyl silicone polymer, two octanoic acids of butanediol/dicaprate, tridecanol isononoate, spiny dogfish
Alkane, phenyl trimethicone, pungent glycol, ethylhexyl methoxy cinnamate, KF6017, sorb are smooth
Sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium hectorite, Phenoxyethanol add
Enter to emulsify in pot and be well mixed, and be heated to 80-85 DEG C, heat while stirring, be heated to melting, form A phases；
Step 2, iron oxides, titanium dioxide, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, water, butanediol, Sodium Hyaluronate, Anjidew NL50, polyquaternium -51, methyl hydroxybenzoate are well mixed, and are heated to
80-85 DEG C, heat while stirring to being completely dissolved, form C phases；
Step 4, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly pumped into C phases, added while stirring, treat to add completely
After entering, vacuumize and reach -0.08MPa, open ultrasonic wave homogenizer, continuous homogenizing is emulsified, and BB frosts are obtained after the completion of emulsification.
Ring five dimethyl silicone polymer can dilute thick and heavy, greasy organosilicon, and KF6017 mixes
Close and use, improve lubricity, water proofing property and reflecting feel.
Two octanoic acids of butanediol/dicaprate is splendid ductility emollient, has the skin sense of salubrious non-greasy.
Phenyl trimethicone reduces surface tension, makes BB frosts are salubrious easily to smear, not glutinous greasy.
Ethylhexyl methoxy cinnamate can effectively prevent 280-310nm ultraviolet, and absorptivity as sun-screening agent
Height, non-stimulated to skin, security is good.
Phytosterol/octyl dodecanol lauroyl glutamate ester forms stratiform liquid crystal structure in skin surface, maintains skin
Barrier function, reach high-quality moistening effect.
Sodium Hyaluronate is the sodium salt of hyaluronic acid, and its theoretical water retention value is up to more than 500ml/g, in connective tissue
Actual water retention value is about 80ml/g.Therefore its distinctive water retention makes that skin is flexible, high resilience；Sufficient moisture makes skin
Smooth delicacy.It can play a part of supplementing and storing moisture of skin using the cosmetics containing hyaluronic acid, recover and keep skin
Youth gloss.Sodium Hyaluronate can be removed in epidermis in sunlight ultraviolet irradiation caused by active oxygen radical, keep
Skin does harm to from it, is referred to as efficient free radical " street cleaner ".Skin is regenerated, repaired simultaneously.
Sodium Hyaluronate belongs to high molecular polymer, has very strong lubrication sense and film forming sense.Skin care containing Sodium Hyaluronate
Lubrication sense is obvious when product are smeared, and feel is good.After being applied to skin, one layer of ventilative hydrated films can be formed in skin surface, made
Skin produces good smooth feeling and moist feeling, and skin is played a protective role, and has repair to damage skin.
Anjidew NL50 is naturally occurring material in skin, is amino acid derivativges, has stronger hygroscopicity, Ke Yicong
Moisture content is absorbed in air, its moisture-retaining capacity will be strong than glycerine, propane diols, sorbierite these traditional NMFs, while and its
Its NMF also has good concertedness.
Polyquaternium -51 is the artificial cell membrane for imitating cell membrane to design, and is protected than hyaluronic acid with more preferably moisture absorption
It is moist, the moisture of skin can be more pinned, more permanent moist and smooth sense is given, it is good to suppress chapped skin effect.
In summary, the invention has the advantages that：
(1) it has been investigated that, using KF6017, sorbitan sesquioleate as emulsifying agent, by super
Sound wave emulsification function, the average grain diameter of emulsion is reduced, increase the interfacial tension of emulsion, so as to greatly reduce PEG-10 poly- two
The usage amount of methylsiloxane, sorbitan sesquioleate, because emulsifying agent has amphipathic property, reduce emulsifier
Afterwards, the water-resistance and grease resistance of product are improved, adornment effect persistence is improved, is not easy dizzy adornment, while ensure the stability of BB frosts；
(2) due to using ultrasonic technique, reducing emulsifier, reducing the excitant of emulsifying agent；
(3) due to there is cavitation using ultrasonic technique, ultrasonic wave, eucaryotic cell structure or smudge cells can be destroyed, effectively
Kill bacterium；
(4) PCA Na, hyaluronic acid and the three's Synergistic of polyquaternium -51, and the bionical moisture film of natural skin is formed, greatly
The big moisture retention for improving product, make skin water profit smooth.
Brief description of the drawings
Fig. 1 is the process chart of the present invention.
Embodiment
With reference to the accompanying drawings and examples, the present invention will be described in detail.
Embodiment 1：As shown in figure 1, a kind of BB frosts, each component and its corresponding percentage by weight are as shown in table 1, and pass through
Following steps prepare：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, two octanoic acids of butanediol/dicaprate, tridecanol
Isononoate, saualane, phenyl trimethicone, pungent glycol, ethylhexyl methoxy cinnamate, PEG-10 poly dimethyls
Siloxanes, sorbitan sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium lithium cover de-
Stone, Phenoxyethanol are added in emulsification pot and are well mixed, and are heated to 80-85 DEG C, are heated while stirring, 60 revs/min of mixing speed
Clock, it is heated to melting, forms A phases；
Step 2, the iron oxides of corresponding parts by weight, titanium dioxide, mica are well mixed, B is formed after pulverizer crushes
Phase；
Step 3, the water of corresponding parts by weight, butanediol, Sodium Hyaluronate, Anjidew NL50, polyquaternium -51, methyl hydroxybenzoate are mixed
Close uniformly, and be heated to 80-85 DEG C, heat while stirring, 60 revs/min of mixing speed, to being completely dissolved, form C phases；Step
Four, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and C phases are slowly pumped into, add, after the entry to be completely, take out while stirring
Vacuum reaches -0.08MPa, opens ultrasonic wave homogenizer, and continuous homogenizing is emulsified for 30 minutes, and BB frosts are obtained after the completion of emulsification.
Wherein, iron oxides, titanium dioxide, mica are purchased from Shanghai Rong Yu new materials Science and Technology Ltd., iron oxides
The trade mark is 73 34 FM of FM, Inno-BK of FM, Inno-YL of Inno-Red 75.
Embodiment 2-5：A kind of BB frosts, are, each component and its corresponding percentage by weight with the difference of embodiment 1
As shown in table 1.
Each component and its percentage by weight in the embodiment 1-5 of table 1
Embodiment 6-15：A kind of BB frosts, are, each component and its corresponding weight percent are such as with the difference of embodiment 3
Shown in table 2.
Each component and its percentage by weight in the embodiment 6-15 of table 2
Embodiment 16-26：A kind of BB frosts, are, each component and its corresponding percentage by weight with the difference of embodiment 14
As shown in table 3.
Each component and its percentage by weight in the embodiment 16-26 of table 3
Comparative example 1：A kind of BB frosts, are with the difference of embodiment 3, are added without KF6017 and sorb
Smooth sesquioleate.
Comparative example 2：A kind of BB frosts, are with the difference of embodiment 3, are added without sorbitan sesquioleate, and lead to
Following steps are crossed to prepare：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, ethylhexyl methoxy cinnamate, PEG-10 poly- two
Methylsiloxane, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium hectorite, Phenoxyethanol add
Enter to emulsify in pot and be well mixed, and be heated to 80-85 DEG C, heat while stirring, 60 revs/min of mixing speed, be heated to melting,
Form A phases；
Step 2, the titanium dioxide of corresponding parts by weight, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly added into the water of corresponding parts by weight, while stirring
Add, after the entry to be completely, be uniformly mixing to obtain BB frosts.
Comparative example 3：A kind of BB frosts, are with the difference of comparative example 2, are added without sorbitan sesquioleate, and lead to
Following steps are crossed to prepare：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, ethylhexyl methoxy cinnamate, the smooth sesquialter of sorb
Oleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium hectorite, Phenoxyethanol add breast
Change in pot and be well mixed, and be heated to 80-85 DEG C, heat while stirring, 60 revs/min of mixing speed, be heated to melting, formed
A phases；
Step 2, the titanium dioxide of corresponding parts by weight, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly added into the water of corresponding parts by weight, while stirring
Add, after the entry to be completely, be uniformly mixing to obtain BB frosts.
Comparative example 4：A kind of BB frosts, are with the difference of embodiment 3, are added without sorbitan sesquioleate.
Comparative example 5：A kind of BB frosts, are with the difference of embodiment 3, are added without KF6017
Comparative example 6：A kind of BB frosts, are with the difference of embodiment 3, acquisition are made by the steps：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, ethylhexyl methoxy cinnamate, PEG-10 poly- two
Methylsiloxane, sorbitan sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium lithium
Montmorillonite, Phenoxyethanol are added in emulsification pot and are well mixed, and are heated to 80-85 DEG C, are heated while stirring, mixing speed 60
Rev/min, it is heated to melting, forms A phases；
Step 2, the titanium dioxide of corresponding parts by weight, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly added into the water of corresponding parts by weight, while stirring
Add, after the entry to be completely, be uniformly mixing to obtain BB frosts.
Comparative example 7：A kind of BB frosts, are, KF6017 and sorb are smooth with the difference of embodiment 3
The percentage by weight of sesquioleate is 5%, and other components and its percentage by weight are same as Example 3.And by as follows
Step prepares：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, ethylhexyl methoxy cinnamate, PEG-10 poly- two
Methylsiloxane, sorbitan sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium lithium
Montmorillonite, Phenoxyethanol are added in emulsification pot and are well mixed, and are heated to 80-85 DEG C, are heated while stirring, mixing speed 60
Rev/min, it is heated to melting, forms A phases；
Step 2, the titanium dioxide of corresponding parts by weight, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly added into the water of corresponding parts by weight, while stirring
Add, after the entry to be completely, be uniformly mixing to obtain BB frosts.
Comparative example 8：A kind of BB frosts, are, KF6017 and sorb are smooth with the difference of embodiment 3
The percentage by weight of sesquioleate is 5%, and other components and its percentage by weight are same as Example 3.And by as follows
Step prepares：
Step 1, by the ring five dimethyl silicone polymer of corresponding parts by weight, ethylhexyl methoxy cinnamate, PEG-10 poly- two
Methylsiloxane, sorbitan sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium lithium
Montmorillonite, Phenoxyethanol are added in emulsification pot and are well mixed, and are heated to 80-85 DEG C, are heated while stirring, mixing speed 60
Rev/min, it is heated to melting, forms A phases；
Step 2, the titanium dioxide of corresponding parts by weight, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly added into the water of corresponding parts by weight, while stirring
Adding, after the entry to be completely, vacuumize and reach -0.08MPa, open ultrasonic wave homogenizer, continuous homogenizing is emulsified for 30 minutes,
BB frosts are obtained after the completion of emulsification.
Comparative example 9：A kind of BB frosts, are, the weight of KF6017 with the difference of comparative example 8
Percentage is 1.2%, and the percentage by weight of sorbitan sesquioleate is 5%.
Comparative example 10：A kind of BB frosts, are, the weight of KF6017 with the difference of comparative example 8
It is 5% to measure percentage, and the percentage by weight of sorbitan sesquioleate is 0.35%.
Test water resistant grease resistance test
Test specimen：Test specimen 1-26 is used as using the BB frosts obtained in embodiment 1-26, using being obtained in comparative example 1-10
BB frosts be used as control sample 1-10, be used as control sample 11 using the common BB of certain commercially available money is white.
Test method：
1st, water-resistance is tested
The material film for taking test specimen 1-26 and control sample 1-11 to be grown in the wide 10mm of human body skin of dorsum of hand surface smear 3mm respectively,
A small amount of clear water coating film, smearing number when record material film starts shedding off are picked with finger belly, every group of sample repeats experiment 10 times,
Give up every group of maximum and minimum value, it is remaining to take its average value.
2nd, grease resistance is tested
The material film for taking test specimen 1-26 and control sample 1-11 to be grown in the wide 10mm of human body skin of dorsum of hand surface smear 3mm respectively,
A small amount of vegetable oil coating film, smearing number when record material film starts shedding off are picked with finger belly, every group of sample repeats experiment 10
It is secondary, give up every group of maximum and minimum value, it is remaining to take its average value.
Result of the test：Test specimen 1-26 and control sample 1-11 water-resistance and grease resistance test result are as shown in table 4.By
Table 4 understands that the water-resistance and grease resistance of control sample 1,2,3,11 are worst, after ultrasonic emulsification step, control sample 4,
5th, 8,9,10 water-resistance and grease resistance are significantly lifted, still, with KF6017, the smooth sesquialter of sorb
The increase of oleate percentage by weight, the water-resistance of control sample 8,9,10 are compared test specimen 3 with grease resistance and decreased,
In selection KF6017, the optimal proportion of sorbitan sesquioleate and after coordinating ultrasonic emulsification step,
Test specimen 1-26 water-resistance and grease resistance is substantially improved.After reducing emulsifier, adornment effect persistence is improved, is not easy to swoon
Adornment, and the excitant to skin can be reduced.
The test specimen 1-26 of table 4 and control sample 1-11 test result
Test two stability tests
Test specimen：Using the water resistant oil resistant eye-liner obtained in embodiment 1-26 as test specimen 1-26, using comparative example
The water resistant oil resistant eye-liner obtained in 1-10 is as control sample 1-10, using certain commercially available eye-liner as control sample 11.
Test method：
1st, it is accurate to measure test specimen 1-26, each 10mL of control sample 1-11, add in the centrifuge tube that numbering is respectively 1-37, so
10min is centrifuged under 4000r/min centrifugal speeds afterwards, discards supernatant liquor, sediment removes moisture, accurately weighs deposit
Amount, every group weighs 3 times and averages, and rate of deposition is calculated using formula：
Rate of deposition (%)=sediment weight (g)/10ml sample weights (g) * 100%；
2nd, it is accurate to measure test specimen 1-26, each 10mL of control sample 1-11, add in the centrifuge tube that numbering is respectively 1-37, so
10min is centrifuged under 4000r/min centrifugal speeds afterwards, sediment has been seen whether after standing 1 day.
Result of the test：Test specimen 1-26 and control sample 1-11 centrifugation rate and delamination is as shown in table 5.By
Table 5 is understood, with the increase of KF6017, sorbitan sesquioleate percentage by weight, control sample 8-
10 stability is slightly lifted compared to test specimen 3, but after using ultrasonic emulsification step, even if substantially reduce the number PEG-10
The addition of dimethyl silicone polymer, sorbitan sesquioleate, the stabilization of test specimen 3, control sample 9 and control sample 10
Property, which is not affected by, to be significantly affected；And test specimen 1-26 does not occur obvious layering and floccule, there is preferable emulsion stability, no
Easily influenceed by centrifugal action；The emulsion stability of control sample 1-7 and control sample 11 is worst, with reference to the data in table 4, explanation
The present invention improves the water-resistance and grease resistance of BB frosts, while ensure that material body dispersion stabilization.
The test specimen 1-26 of table 5 and control sample 1-11 centrifugation rate and delamination
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-described embodiment,
All technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
For those of ordinary skill, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (9)
1. a kind of BB frosts, it is characterised in that include the component of following percentage by weight：
Ring five dimethyl silicone polymer 5-15%；
Sun-screening agent 0-5%；
KF6017 1-1.5%；
Sorbitan sesquioleate 0.2-0.5%；
Phytosterol/octyl dodecanol lauroyl glutamate ester 0-2.5%；
Thickener 0.2-1%；
Preservative 0-1%；
Colouring agent 2-15%；
Filler 0-2%；
Water 65-75%.
2. BB frosts according to claim 1, it is characterised in that the BB frosts are 3.51-9.02% also including percentage by weight
NMF.
3. BB frosts according to claim 2, it is characterised in that the NMF includes butanediol, Sodium Hyaluronate, PCA
Sodium, polyquaternium -51, according to the total amount meter of BB frosts, the butanediol, Sodium Hyaluronate, Anjidew NL50, the weight of polyquaternium -51
Percentage is respectively：2-5%、0.01-0.02%、0.5-2%、1-2%.
4. BB frosts according to claim 3, it is characterised in that it is 4-15.5%'s that the BB frosts, which also include percentage by weight,
Skin conditioning agent.
5. BB frosts according to claim 4, it is characterised in that the skin conditioning agent includes two octanoic acids of butanediol/didecyl
Acid esters, tridecanol isononoate, saualane, phenyl trimethicone, pungent glycol, it is described according to the total amount meter of BB frosts
Two octanoic acids of butanediol/dicaprate, tridecanol isononoate, saualane, phenyl trimethicone, the weight of pungent glycol
Percentage is respectively：2-5%、1-3%、0-2%、2-5%、0-0.5%.
6. BB frosts according to claim 5, it is characterised in that the preservative includes Phenoxyethanol, methyl hydroxybenzoate, according to
The total amount meter of BB frosts, the Phenoxyethanol, the percentage by weight of methyl hydroxybenzoate are respectively：0-0.8%、0-0.2%.
7. BB frosts according to claim 6, it is characterised in that the colouring agent includes iron oxides, titanium dioxide, according to
The total amount meter of BB frosts, the iron oxides, the percentage by weight of titanium dioxide are respectively：0-2%、2-13%.
8. BB according to claim 7 frost, it is characterised in that the sun-screening agent is ethylhexyl methoxy cinnamate, institute
It is distearyl dimethylammonium hectorite to state thickener, and the filler is mica.
9. a kind of preparation method of BB frosts, it is characterised in that comprise the following steps：
Step 1, by ring five dimethyl silicone polymer, two octanoic acids of butanediol/dicaprate, tridecanol isononoate, spiny dogfish
Alkane, phenyl trimethicone, pungent glycol, ethylhexyl methoxy cinnamate, KF6017, sorb are smooth
Sesquioleate, phytosterol/octyl dodecanol lauroyl glutamate ester, distearyl dimethylammonium hectorite, Phenoxyethanol add
Enter to emulsify in pot and be well mixed, and be heated to 80-85 DEG C, heat while stirring, be heated to melting, form A phases；
Step 2, iron oxides, titanium dioxide, mica are well mixed, B phases are formed after pulverizer crushes；
Step 3, water, butanediol, Sodium Hyaluronate, PCA sodium, polyquaternium -51, methyl hydroxybenzoate are well mixed, and heated
To 80-85 DEG C, heat while stirring to being completely dissolved, form C phases；
Step 4, B phases are pumped into emulsification pot inside holding to 80-85 DEG C, and are slowly pumped into C phases, added while stirring, treat to add completely
After entering, vacuumize and reach -0.08MPa, open ultrasonic wave homogenizer, continuous homogenizing is emulsified, and BB frosts are obtained after the completion of emulsification.
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| CN201710810084.9A CN107456403A (en) | 2017-09-09 | 2017-09-09 | A kind of BB frosts and preparation method thereof |
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Cited By (3)
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| CN108309861A (en) * | 2018-04-10 | 2018-07-24 | 广东卡维达商务集团有限公司 | A kind of adornment supports the preparation method of the long-acting BB frosts for holding adornment of unification |
| CN114848515A (en) * | 2021-06-03 | 2022-08-05 | 安婕妤化妆品科技股份有限公司 | Flawless cosmetic emulsion and preparation method thereof |
| CN115252463A (en) * | 2022-06-14 | 2022-11-01 | 上海科黛生物科技有限公司 | Sustained-release composition with anti-irritation effect and preparation method and application thereof |
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| CN115252463A (en) * | 2022-06-14 | 2022-11-01 | 上海科黛生物科技有限公司 | Sustained-release composition with anti-irritation effect and preparation method and application thereof |
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