CN110476982A - A kind of biological agricultural chemical insecticide and preparation method thereof containing biological agglutinin - Google Patents

A kind of biological agricultural chemical insecticide and preparation method thereof containing biological agglutinin Download PDF

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Publication number
CN110476982A
CN110476982A CN201910761927.XA CN201910761927A CN110476982A CN 110476982 A CN110476982 A CN 110476982A CN 201910761927 A CN201910761927 A CN 201910761927A CN 110476982 A CN110476982 A CN 110476982A
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China
Prior art keywords
agglutinin
biological
vegetable oil
mass percent
agricultural chemical
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CN201910761927.XA
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Chinese (zh)
Inventor
赖燕华
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Guangdong Everrise Agricultural Technology Co Ltd
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Guangdong Everrise Agricultural Technology Co Ltd
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Priority to CN201910761927.XA priority Critical patent/CN110476982A/en
Publication of CN110476982A publication Critical patent/CN110476982A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A01N37/46N-acyl derivatives
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses: a kind of biological agricultural chemical insecticide containing biological agglutinin, including vegetable oil, biological agglutinin, emulsifier and surfactant, each mass percent of the vegetable oil, biological agglutinin, emulsifier and surfactant are as follows: the vegetable oil of 10%-80% mass percent, the biological agglutinin of 1%-80% mass percent, the emulsifier and surfactant of 10%-30% mass percent, are related to technical field of pesticide.The biological agricultural chemical insecticide and preparation method thereof containing biological agglutinin, form biological pesticide, so that insect pest is not easy to produce resistance it, sustainable use, it does not stimulate other pests to occur simultaneously, is not easy to kill natural enemy, is the favourable agents of integrated control, pure biological source, it is low to environmental organism lethality to safety of human and livestock, and it can be decomposed by microorganisms into water and carbon dioxide in a short time, without Environmental Residues, achieved the purpose that it is easy to produce, the process proportion rationally, it is easy to operate, implement to produce on a large scale convenient for factory, practicability is stronger.

Description

A kind of biological agricultural chemical insecticide and preparation method thereof containing biological agglutinin
Technical field
The present invention relates to technical field of pesticide, specially a kind of biological agricultural chemical insecticide and its preparation containing biological agglutinin Method.
Background technique
Pesticide is meant for preventing and treating the harmful organism (pest, harmful mite, nematode, pathogen, the weeds that endanger agriculture forest and husbandry production And mouse.After, by the production and life process of longer development, gradually recognize some natural in prevention and treatment farming and animal husbandry The performance of harmful organism.To 17 classes etc.) and coordinate plant growth chemicals and biologics.Usually for health and change In the various auxiliary agents of kind effective component physico-chemical property are also included within.
Agricultural is still in the majority with chemicals at present, sprays chemical pesticide to crops, is easy to environment and food safety Have an impact, and pest and disease damage is easy to produce resistance to chemical pesticide.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of biological agricultural chemical insecticide and its system containing biological agglutinin Preparation Method, it is still in the majority with chemicals for solving in agricultural at present, sprays chemical pesticide to crops, is easy to environment and food The problem of product have an impact safely, and pest and disease damage is easy to produce resistance to chemical pesticide.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of biology containing biological agglutinin Agricultural chemical insecticide, including biological agglutinin, vegetable oil, emulsifier and surfactant, the biology agglutinin, vegetable oil, cream Each mass percent of agent and surfactant are as follows: the biological agglutinin of 1%-80% mass percent, 10%-80% mass The vegetable oil of percentage, the emulsifier and surfactant of 10%-30% mass percent.
Preferably, the biological agglutinin includes: insect agglutinin and phytolectin, the insect agglutinin includes: Maduca sexta agglutinin, bollworm agglutinin, Ostrinia furnacalis agglutinin, Drosophila melanogaster agglutinin etc.;The plant lectin Element includes: pisum sativum agglutinin, lanatechead saussurea herb with flower agglutinin etc.;The vegetable oil is mainly the vegetable oil containing unsaturated fatty acid, institute Stating the vegetable oil containing unsaturated fatty acid includes: soybean oil, corn oil, coconut oil etc..
Preferably, the biological agglutinin can be used as agricultural agent and use when bucket is mixed spraying with other pestsides synthesis.
Preferably, the emulsifier and surfactant include and are not limited to diglycerol sodium laurate, castor oil polyoxy second Alkene ether etc..
A kind of preparation method of the biological agricultural chemical insecticide containing biological agglutinin, comprising the following steps:
Step 1: taking the vegetable oil of 10-80% mass percent spare, then takes the biology of 1-80% mass percent again Agglutinin is spare, finally takes 10-30% emulsifier and surfactant spare;
Step 2: simultaneously by the vegetable oil of 10-80% mass percent and the biological agglutinin of 1-80% mass percent It is added in reaction kettle and carries out heating reaction, form the mixed liquor of vegetable oil and biological agglutinin;
Step 3: 10-30% emulsifier and surfactant are added to the vegetable oil produced in step 2 and biology coagulates It in the mixed liquor for collecting element, and is reacted by reaction kettle, forms the mixed of vegetable oil, biological agglutinin, emulsifier and surfactant Close liquid;
Step 4: to the mixed liquor of the vegetable oil produced in step 3, biological agglutinin, emulsifier and surfactant It is sufficiently stirred, high speed shear can be made into biological agricultural chemical insecticide to being completely dissolved.
Preferably, temperature need to be controlled at 40 DEG C -50 DEG C in reaction kettle in the step 2.
Preferably, duration being stirred in the step 4 need to control at 30-45 minutes.
Preferably, the biological agricultural chemical insecticide produced in the step 4, which need to be stood, to be cooled to room temperature, and can case preservation.
(3) beneficial effect
The invention has the following advantages:
(1), the biological agricultural chemical insecticide and preparation method thereof for containing biological agglutinin passes through the biological agglutinin packet Contain: insect agglutinin and phytolectin, the insect agglutinin includes: maduca sexta agglutinin, bollworm agglutinin, Asia Corn borer agglutinin, Drosophila melanogaster agglutinin etc.;The phytolectin includes: pisum sativum agglutinin, lanatechead saussurea herb with flower agglutinin etc. Deng;The vegetable oil is mainly the vegetable oil containing unsaturated fatty acid, and the vegetable oil containing unsaturated fatty acid includes: soybean Oil, corn oil, coconut oil etc., the emulsifier and surfactant include and are not limited to diglycerol sodium laurate, castor oil gathers Ethylene oxide ether etc. forms biological pesticide, so that insect pest is not easy to produce resistance it, sustainable use, and while other evils are not stimulated Worm occurs, and is not easy to kill natural enemy, is the favourable agents of integrated control, pure biological source kills safety of human and livestock to environmental organism Overstrain is low, and can be decomposed by microorganisms into water and carbon dioxide in a short time, no Environmental Residues.
(2), the biological agricultural chemical insecticide and preparation method thereof for containing biological agglutinin, passes through step 1: taking 10-80% matter The vegetable oil for measuring percentage is spare, then takes the biological agglutinin of 1-80% mass percent spare again, finally takes 10-30% newborn Agent and surfactant are spare;Step 2: by the life of the vegetable oil of 10-80% mass percent and 1-80% mass percent Object agglutinin is added in reaction kettle carries out heating reaction simultaneously, forms the mixed liquor of vegetable oil and biological agglutinin;Step 3: 10-30% emulsifier and surfactant are added in the mixed liquor of the vegetable oil produced in step 2 and biological agglutinin, And reacted by reaction kettle, form the mixed liquor of vegetable oil, biological agglutinin, emulsifier and surfactant;Step 4: to step The mixed liquor of vegetable oil, biological agglutinin, emulsifier and the surfactant produced in rapid three is sufficiently stirred, and is cut at a high speed Be switched to be completely dissolved and can be made into biological agricultural chemical insecticide, achieved the purpose that it is easy to produce, the process proportion rationally, operation letter It is single, implement to produce on a large scale convenient for factory, practicability is stronger.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
The embodiment of the present invention provides a kind of technical solution: a kind of biological agricultural chemical insecticide containing biological agglutinin, including plants Object oil, biological agglutinin, emulsifier and surfactant, the vegetable oil, biological agglutinin, emulsifier and surfactant Each mass percent are as follows: the vegetable oil of 10%-80% mass percent, the biological agglutinin of 1%-80% mass percent, The emulsifier and surfactant of 10%-30% mass percent.
The biology agglutinin includes: insect agglutinin and phytolectin, the insect agglutinin includes: maduca sexta Agglutinin, bollworm agglutinin, Ostrinia furnacalis agglutinin, Drosophila melanogaster agglutinin etc.;The phytolectin includes: pea Beans agglutinin, lanatechead saussurea herb with flower agglutinin etc.;The vegetable oil is mainly the vegetable oil containing unsaturated fatty acid, described containing unsaturation The vegetable oil of fatty acid includes: soybean oil, corn oil, coconut oil etc..
Biological agglutinin is one group of protein component being widely present in plant tissue, in storage organ and organ of multiplication In content it is especially abundant, there are many critically important physiological actions to plant for biological agglutinin, wherein in crop pest prevention and treatment side The effect that face can be shown is defencive function, i.e., in each stage of plant growth, biological agglutinin is protected in different ways Plant is protected from the infringement of pest, result of study shows that biological agglutinin is primarily present in the albuminous granules of plant cell, once Ingested by pest, biological agglutinin will release in the alimentary canal of insect, and with the glycoprotein phase on enteron aisle funnel In conjunction with influencing the normal absorption of nutriment.Simultaneously it is also possible to induce lesion in the alimentary canal of insect, promote in alimentary canal The proliferation of bacterium causes to cause harm to pest itself, to achieve the purpose that desinsection.
The biology agglutinin can be used as agricultural agent and use when bucket is mixed spraying with other pestsides synthesis, can play raising The effect of drug effect, the usage amount of reduction pesticide.
The emulsifier and surfactant include and are not limited to diglycerol sodium laurate, castor oil polyoxyethylene ether etc..
A kind of preparation method of the biological agricultural chemical insecticide containing biological agglutinin, comprising the following steps:
Step 1: taking the vegetable oil of 10-80% mass percent spare, then takes the biology of 1-80% mass percent again Agglutinin is spare, finally takes 10-30% emulsifier and surfactant spare, if taken raw material pure free from admixture, it keeps away Exempt to influence the quality of biological pesticide;
Step 2: simultaneously by the vegetable oil of 10-80% mass percent and the biological agglutinin of 1-80% mass percent It is added in reaction kettle and carries out heating reaction, the mixed liquor for forming vegetable oil and biological agglutinin should cooperate when heating is reacted The synchronous stirring of blender;
Step 3: 10-30% emulsifier and surfactant are added to the vegetable oil produced in step 2 and biology coagulates It in the mixed liquor for collecting element, and is reacted by reaction kettle, forms the mixed of vegetable oil, biological agglutinin, emulsifier and surfactant Close liquid;
Step 4: to the mixed liquor of the vegetable oil produced in step 3, biological agglutinin, emulsifier and surfactant It is sufficiently stirred, high speed shear can be made into biological agricultural chemical insecticide to being completely dissolved.
Temperature need to be controlled at 40 DEG C -50 DEG C in reaction kettle in the step 2, and extremes of temperature will affect product matter Amount.
Duration is stirred in the step 4 need to control at 30-45 minutes, it is ensured that be sufficiently stirred.
The biological agricultural chemical insecticide produced in the step 4 need to stand and be cooled to room temperature, and can case preservation.
Compared with the relevant technologies, the biological agricultural chemical insecticide and preparation method thereof provided by the invention containing biological agglutinin It has the following beneficial effects:
Include by the biological agglutinin: insect agglutinin and phytolectin, the insect agglutinin includes: tobacco Hawkmoth agglutinin, bollworm agglutinin, Ostrinia furnacalis agglutinin, Drosophila melanogaster agglutinin etc.;The phytolectin packet Contain: pisum sativum agglutinin, lanatechead saussurea herb with flower agglutinin etc.;The vegetable oil is mainly the vegetable oil containing unsaturated fatty acid, described to contain The vegetable oil of unsaturated fatty acid includes: soybean oil, corn oil, coconut oil etc., the emulsifier and surfactant include and Be not limited to diglycerol sodium laurate, castor oil polyoxyethylene ether etc., form biological pesticide so that insect pest it is not likely to produce it is anti- Property, sustainable use, while other pests not being stimulated to occur, it is not easy to kill natural enemy, is the favourable agents of integrated control, it is pure Biological source, it is low to environmental organism lethality to safety of human and livestock, and it can be decomposed by microorganisms into water and titanium dioxide in a short time Carbon, no Environmental Residues, passes through step 1: taking the vegetable oil of 10-80% mass percent spare, then takes 1-80% mass hundred again Divide the biological agglutinin of ratio spare, finally takes 10-30% emulsifier and surfactant spare;Step 2: by 10-80% matter The biological agglutinin of the vegetable oil and 1-80% mass percent of measuring percentage is added in reaction kettle simultaneously heat instead It answers, forms the mixed liquor of vegetable oil and biological agglutinin;Step 3: 10-30% emulsifier and surfactant are added to step It in the mixed liquor of the vegetable oil and biological agglutinin that are produced in rapid two, and is reacted by reaction kettle, forms vegetable oil, biology agglutination The mixed liquor of element, emulsifier and surfactant;Step 4: to the vegetable oil produced in step 3, biological agglutinin, emulsification The mixed liquor of agent and surfactant is sufficiently stirred, and high speed shear can be made into biological agricultural chemical insecticide to being completely dissolved, Achieved the purpose that it is easy to produce, the process proportion rationally, it is easy to operate, implement to produce on a large scale convenient for factory, practicability It is relatively strong.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (8)

1. a kind of biological agricultural chemical insecticide containing biological agglutinin, including vegetable oil, biological agglutinin, emulsifier and surface-active Agent, it is characterised in that: each mass percent of the vegetable oil, biological agglutinin, emulsifier and surfactant are as follows: 10%- The vegetable oil of 80% mass percent, the biological agglutinin of 1%-80% mass percent, the cream of 10%-30% mass percent Agent and surfactant.
2. a kind of biological agricultural chemical insecticide containing biological agglutinin according to claim 1, it is characterised in that: the biology Agglutinin includes: insect agglutinin and phytolectin, and the insect agglutinin includes: maduca sexta agglutinin, bollworm are solidifying Collect element, Ostrinia furnacalis agglutinin, Drosophila melanogaster agglutinin etc.;The phytolectin: pisum sativum agglutinin, lanatechead saussurea herb with flower agglutination Element etc.;The vegetable oil is mainly the vegetable oil containing unsaturated fatty acid, and the vegetable oil containing unsaturated fatty acid includes: Soybean oil, corn oil, coconut oil etc..
3. a kind of biological agricultural chemical insecticide containing biological agglutinin according to claim 1, it is characterised in that: the biology Agglutinin can be used as agricultural agent and use when bucket is mixed spraying with other pestsides synthesis.
4. a kind of biological agricultural chemical insecticide containing biological agglutinin according to claim 1, it is characterised in that: the emulsification Agent and surfactant include and are not limited to diglycerol sodium laurate, castor oil polyoxyethylene ether.
5. a kind of preparation method of the biological agricultural chemical insecticide containing biological agglutinin, it is characterised in that: the following steps are included:
Step 1: taking the vegetable oil of 10-80% mass percent spare, then takes the biology agglutination of 1-80% mass percent again Element is spare, finally takes 10-30% emulsifier and surfactant spare;
Step 2: the biological agglutinin of the vegetable oil of 10-80% mass percent and 1-80% mass percent is added simultaneously Heating reaction is carried out into reaction kettle, forms the mixed liquor of vegetable oil and biological agglutinin;
Step 3: 10-30% emulsifier and surfactant are added to the vegetable oil produced in step 2 and biological agglutinin Mixed liquor in, and reacted by reaction kettle, form the mixed liquor of vegetable oil, biological agglutinin, emulsifier and surfactant;
Step 4: the mixed liquor of the vegetable oil produced in step 3, biological agglutinin, emulsifier and surfactant is carried out It is sufficiently stirred, high speed shear can be made into biological agricultural chemical insecticide to being completely dissolved.
6. a kind of preparation method of biological agricultural chemical insecticide containing biological agglutinin according to claim 5, feature exist In: temperature need to be controlled at 40 DEG C -50 DEG C in reaction kettle in the step 2.
7. a kind of preparation method of biological agricultural chemical insecticide containing biological agglutinin according to claim 5, feature exist In: duration is stirred in the step 4 need to control at 30-45 minutes.
8. a kind of preparation method of biological agricultural chemical insecticide containing biological agglutinin according to claim 5, feature exist In: the biological agricultural chemical insecticide produced in the step 4 need to stand and be cooled to room temperature, and can case preservation.
CN201910761927.XA 2019-08-19 2019-08-19 A kind of biological agricultural chemical insecticide and preparation method thereof containing biological agglutinin Pending CN110476982A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112889825A (en) * 2021-01-22 2021-06-04 王启吉 Composite ecological pesticide and preparation method thereof

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CN112889825A (en) * 2021-01-22 2021-06-04 王启吉 Composite ecological pesticide and preparation method thereof

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Application publication date: 20191122