CN114469825B - Bath foam special for pets and preparation method thereof - Google Patents
Bath foam special for pets and preparation method thereof Download PDFInfo
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- CN114469825B CN114469825B CN202111682941.4A CN202111682941A CN114469825B CN 114469825 B CN114469825 B CN 114469825B CN 202111682941 A CN202111682941 A CN 202111682941A CN 114469825 B CN114469825 B CN 114469825B
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Classifications
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- A—HUMAN NECESSITIES
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Abstract
The invention discloses bath foam special for pets and a preparation method thereof, and relates to the technical field of pet supplies. The special bath foam for the pets comprises the following raw material components in percentage by mass: 15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant miticide, 2-4% of compound enzyme preparation, 2-4% of hair softening and bulking agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water; wherein the complex enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme. According to the invention, the plant surfactant and the complex enzyme preparation are compounded, and the plant surfactant and the complex enzyme preparation are synergistic, so that various stains on the pet can be cleaned rapidly and efficiently; the special bath foam for pets can sterilize and expel parasites by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine plant miticide are both plant sources, and have high safety, mild ingredients and no irritation, so that the bath foam special for pets is safe and nontoxic and does not lick.
Description
Technical Field
The invention relates to the technical field of pet supplies, in particular to bath foam special for pets and a preparation method thereof.
Background
With the economic development and rising income level, the pet is raised to be a mental support, many people regard the pet as family members, the pet owners translate self life modes to lovers, and demand upgrading and consumption upgrading are formed in the basic consumption field, so that the comfort, safety and functionality of the clean product of the pet are more and more paid attention to in the pet raising process.
In order to achieve the cleaning effect, a surfactant is generally added into the bathing product, and the surfactant is selected from chemical reagents such as sodium dodecyl sulfate, ethoxylated alkyl sodium sulfate and the like, which are greatly irritated to eyes and skin of the pet and easily cause the discomfort and diseases of the pet. In addition, most bath products are mainly cleaned, have few sterilizing functions, have most of effective components such as chemical components, and the like, have low sterilizing efficiency, have toxic, corrosive and pungent smell, have certain damage to skin and hair, cannot eliminate the peculiar smell, have great stimulation to pets, and easily cause the inspirations and diseases of the pets.
Disclosure of Invention
The invention mainly aims to provide a bath foam special for pets and a preparation method thereof, and aims to provide the bath foam special for pets, which has good cleaning effect, can sterilize and expel worms and is not stimulated by component temperature.
In order to achieve the above purpose, the invention provides a bath foam special for pets, which comprises the following raw material components in percentage by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant miticide, 2-4% of compound enzyme preparation, 2-4% of hair softening and bulking agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water;
wherein the complex enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme.
Optionally, the plant surfactant comprises a sapogenin extract of fructus gleditsiae and a peel extract of fructus soapberry.
Optionally, the mass ratio of the small fruit gleditsia sinensis saponin extract to the soapberry peel extract is 1-2: 1 to 4.
Optionally, the Chinese herbal medicine plant miticide comprises at least one of stemona root extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, peppermint extract, ginger root extract and motherwort extract.
Optionally, the Chinese herbal medicine plant miticide is the stemona root extract, the cnidium fruit extract, the pricklyash peel extract, the lilac flower extract, the peppermint extract, the ginger root extract and the motherwort extract;
the mass ratio of the stemona root extract, the cnidium fruit extract, the pricklyash peel extract, the lilac flower extract, the peppermint extract, the ginger root extract and the motherwort herb extract is 7-9: 3.5 to 4.5:3.5 to 4.5:3:3:3:2.
optionally, the complex enzyme preparation is obtained by compounding the lipase, the protease, the cellulase and the lysozyme, and the mass ratio of the lipase to the protease to the cellulase to the lysozyme is 0.5-1.2: 0.8 to 2.5:0.1 to 0.5:0.05 to 0.5; and/or the number of the groups of groups,
the hair softening and bulking agent comprises at least one of bionic phospholipid, hair care grease, hydrolyzed wheat protein, guar gum and polyquaternium-7.
Optionally, the biological enzyme stabilizer comprises a metal compound, a saccharide, and a polyol.
Optionally, the metal compound includes at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate, and potassium chloride; and/or the number of the groups of groups,
the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the number of the groups of groups,
the polyalcohol comprises at least one of glycerol, 1, 3-propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
Optionally, the thickening stabilizer comprises at least one of PEG-120 methyl glucose dioleate, cocoamide methyl MEA, polyethylene glycol distearate and fatty alcohol polyoxyethylene ether acrylic acid copolymer; and/or the number of the groups of groups,
the preservative comprises pinacol and phenoxyethanol.
Based on the above purpose, the invention also provides a preparation method of the bath foam special for pets, which comprises the following steps:
dissolving a plant surfactant in deionized water to obtain a mixed solution;
adding Chinese herbal medicine plant mite-killing agent into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain mixed solution;
under the stirring condition, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution to obtain a solution A;
and (3) cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the special bath foam is 6.5-7.8, and the viscosity of the special bath foam is 3500-8000 cps.
According to the technical scheme provided by the invention, the special bath foam for pets is prepared from the raw materials of the plant surfactant, the Chinese herbal medicine plant miticide, the complex enzyme preparation, the hair softening and bulking agent, the biological enzyme stabilizer, the thickening stabilizer, the preservative and the deionized water, and the plant surfactant and the complex enzyme preparation are compounded to synergistically increase the two, so that various stains on the pets can be cleaned rapidly and efficiently; the special bath foam for pets can sterilize and expel parasites by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine plant miticide are both plant sources, and have high safety, mild ingredients and no irritation, so that the bath foam special for pets is safe and nontoxic and does not lick.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention more clear, the technical solutions of the embodiments of the present invention will be clearly and completely described below. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
In addition, the meaning of "and/or" as it appears throughout includes three parallel schemes, for example "A and/or B", including the A scheme, or the B scheme, or the scheme where A and B are satisfied simultaneously. In addition, the technical solutions of the embodiments may be combined with each other, but it is necessary to base that the technical solutions can be realized by those skilled in the art, and when the technical solutions are contradictory or cannot be realized, the combination of the technical solutions should be regarded as not exist and not within the protection scope of the present invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The invention provides a bath foam special for pets, and aims to provide a bath foam special for pets, which can sterilize and expel worms and has no stimulation to component temperature. In one embodiment, the special bath foam for pets comprises the following raw material components in percentage by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant acaricide, 2-4% of compound enzyme preparation, 2-4% of hair softening and bulking agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water.
Wherein the complex enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme. By selecting at least two of the above substances, the addition of the complex enzyme preparation can be synergistic with the plant surfactant, thereby having good cleaning effect. Meanwhile, the synergistic effect is better through the design of the addition amount of the plant surfactant and the complex enzyme preparation.
According to the technical scheme provided by the invention, the special bath foam for pets is prepared from the raw materials of the plant surfactant, the Chinese herbal medicine plant miticide, the complex enzyme preparation, the hair softening and bulking agent, the biological enzyme stabilizer, the thickening stabilizer, the preservative and the deionized water, and the plant surfactant and the complex enzyme preparation are compounded to synergistically increase the two, so that various stains on the pets can be cleaned rapidly and efficiently; the special bath foam for pets can sterilize and expel parasites by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine plant miticide are both plant sources, and have high safety, mild ingredients and no irritation.
The present invention is not limited to the specific choice of the plant surfactant, as long as it can function as a surfactant, and preferably, the plant surfactant includes saponaria saponin extract and soapberry peel extract.
The gleditsia sinensis saponin extract is a natural product of gleditsia sinensis seeds of leguminous plants, the basic structure of the gleditsia sinensis saponin extract is a combined natural product formed by triterpene aglycone ligand and structural sugar and organic acid, and the aglycone ligand structure belongs to pentacyclic triterpene compounds, wherein the most important aglycone compounds are five glycoside compounds. The gleditsia sinensis saponin molecule consists of hydrophilic glycosyl and hydrophobic saponin coordination group, so that the gleditsia sinensis saponin has various surface active properties such as emulsification, dispersion, wetting, decontamination, foaming and the like, and is a nonionic natural surfactant with good performance. In addition, the gleditsia sinensis saponin also has obvious effects of anti-inflammatory, phlegm eliminating, pain relieving, sterilization, insect killing and the like.
The soapberry (SAPINDUS MUKOROSSI) pericarp extract contains rich glycoside substances, mainly triterpene saponin (I) and sesquiterpene glycoside (II), has strong surface activity, is a natural nonionic surfactant, has strong detergency, is easy to degrade, has no harmful residue, is easy to wash, has rich foam, fine and smooth handfeel and strong detergency, and has the characteristics of antibiosis, environmental protection, no public hazard, rich foam, dirt removal, antibiosis, beauty maintenance, skin tendering, whitening, freckle removal, acne removal, skin disease prevention and the like; meanwhile, the hair conditioner contains a large amount of natural nutrition conditioning substances, has no stimulation to hair and skin, and has the effects of conditioning, removing dandruff, relieving itching and the like.
The invention combines the small fruit gleditsia sinensis saponin extract and the soapberry peel extract, so that the plant surfactant has good cleaning effect, low foam and easy cleaning, and has certain sterilization and insect-repellent effects; in addition, the substances are easy to degrade, and the degraded substances are safe and environment-friendly.
More preferably, the mass ratio of the small fruit gleditsia sinensis saponin extract to the soapberry peel extract is 1-2: 1-4, thus, the plant surfactant obtained by compounding has better cleaning effect.
The invention does not limit the specific source of the gleditsia sinensis saponin extract, and the gleditsia sinensis saponin extract can be obtained through purchase or self-preparation, and the steps are as follows: pulverizing semen Gleditsiae Abnormalis, leaching with water (ultrasonic assisted extraction), sequentially centrifuging, hydrolyzing with enzyme, decolorizing, centrifuging, evaporating, concentrating, and drying to obtain fructus Gleditsiae Abnormalis saponin extract.
The invention also does not limit the specific source of the soapberry pericarp extract, and the soapberry pericarp extract can be obtained by purchase or prepared by self, and the preparation method is as follows: 1. selecting soapberry peel, drying at 60 ℃, and crushing for later use; 2. soaking soapberry peel powder in methanol solution, and extracting with ultrasonic assistance; 3. concentrating under reduced pressure to separate methanol to obtain extract of sapindus fruit peel; 4. freezing the extractive solution at 4deg.C for 24 hr, cooling for crystallization, and centrifuging to obtain fructus Sapindi Mukouossi pericarp extract.
In the embodiment, the gleditsia sinensis saponin extract and the soapberry peel extract both adopt an ultrasonic auxiliary extraction technology, so that the solvent can more easily permeate into plants under the ultrasonic condition, the active ingredients can be completely dissolved in the solvent, the extraction is more thorough, and the active ingredients of the extracting solution are higher and more effective.
By adding the Chinese herbal medicine, namely the plant acaricide, the prepared bath foam special for pets has the effects of sterilizing and expelling parasites. In this embodiment, the Chinese herbal medicine plant miticide includes at least one of a stemona root extract, a cnidium fruit extract, a pricklyash fruit extract, a lilac flower extract, a peppermint extract, a ginger root extract and a motherwort extract, so that the Chinese herbal medicine plant miticide has mild and non-irritating components and good sterilizing and insect-expelling effects.
In a preferred embodiment, the Chinese herbal medicine plant miticide is composed of the stemona root extract, the fructus cnidii extract, the fructus zanthoxyli extract, the flos caryophylli extract, the mint extract, the ginger root extract and the herba leonuri extract, and the mass ratio of the stemona root extract to the fructus cnidii extract to the fructus zanthoxyli extract to the flos caryophylli extract to the mint extract is 7-9: 3.5 to 4.5:3.5 to 4.5:3:3:3:2, more preferably, the mass ratio is 8:4:4:3:3:3:2.
the components of the Chinese herbal medicine plant miticide can be purchased or prepared by self, and the steps are as follows: (1) sorting: removing impurities in the medicinal materials, and bad parts such as staleness, mildew or insect diet; (2) cleaning and airing: rinsing the medicinal materials with clear water, and sun-drying; (3) sterilization and disinfection: sterilizing the dried medicinal materials with ultraviolet lamp light; (4) crushing treatment: putting the sterilized medicinal materials into a pulverizer for pulverizing treatment until the medicinal materials pass through a 50-mesh sieve; (5) primary soaking: immersing the crushed medicinal materials into white vinegar for soaking for 12 hours, wherein the mass ratio of the medicinal materials to the white vinegar is 1: 2-1: 3, a step of; boiling the soaked mixed solution with strong fire, and stewing with slow fire until white vinegar is boiled; (6) secondary soaking: soaking the medicinal materials after boiling the white vinegar for 8 hours by using deionized water as a solvent, wherein the dosage of the solvent is 6-8 times of that of the medicinal materials, and the extraction temperature is 65 ℃; (7) concentrating: precipitating the obtained medicinal liquid for 5 hr, filtering, and concentrating the filtrate to obtain extract with relative density of 1.2-1.35; (8) an article: and (3) freeze-drying the prepared extract in a freezer at the temperature of minus 50 ℃ for 0.5 to 5 hours, and vacuum drying to obtain the plant extract.
In order to make the cleaning effect of the bath foam special for pets better, in a preferred embodiment, the complex enzyme preparation is prepared by compounding the lipase, the protease, the cellulase and the lysozyme, and the mass ratio of the lipase to the protease to the cellulase to the lysozyme is 0.5-1.2: 0.8 to 2.5:0.1 to 0.5:0.05 to 0.5. In addition, lysozyme can also play a certain role in sterilization.
The enzyme in the complex enzyme preparation is easy to inactivate, and in order to make the enzyme in the complex enzyme preparation fully play the role, the special bath foam for pets is added with a biological enzyme stabilizer. In this embodiment, the bio-enzyme stabilizer includes a metal compound, a saccharide, and a polyol. In a preferred embodiment, the bio-enzyme stabilizer is composed of a metal compound, a saccharide and a polyalcohol, so that the effect of stabilizing the enzyme is good.
Wherein the metal compound comprises at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate and potassium chloride; and/or the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the polyalcohol comprises at least one of glycerol, 1, 3-propanediol, propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
In a preferred embodiment, the metal compound is calcium chloride, the saccharide is glucose, and the polyol is a mixture of glycerol and polyethylene glycol. Further, the polyethylene glycol (PEG) has a molecular weight of 1000.
The hair softening and bulking agent is added, so that the special bath foam for pets has the effect of caring hair, and the hair of pets is easy to comb and smooth. In this embodiment, the hair softening and bulking agent comprises at least one of bionic phospholipid, hair care grease, hydrolyzed wheat protein, guar gum and polyquaternium-7, and by selecting the above substances, the hair care effect is better, and the ingredients of the bath foam special for pets are mild and no irritation.
By adding the thickening stabilizer, the system of the prepared bath foam special for the pets is stable, and turbidity, precipitation or layering are not easy to occur. In this embodiment, the thickening stabilizer includes at least one of PEG-120 methylglucdioleate, cocamidomethyl MEA, polyethylene glycol distearate, and fatty alcohol-polyoxyethylene ether acrylic acid copolymer.
Preferably, the thickening stabilizer is compounded from PEG-120 methyl glucose dioleate and cocoamide methyl MEA. Further, the molecular weight of the polyethylene glycol distearate is 6000.
In this embodiment, the preservative includes pinacol and phenoxyethanol. Preferably, the preservative is compounded by pinus koraiensis and phenoxyethanol, so that the prepared special bath foam for pets has longer preservation time.
The bath foam special for pets can be used for most animals, and in view of the fact that the market of cats and dogs is the pet market with the largest standard, the example is given here. The skin thickness of the cat is 0.4-2 mm, the skin thickness of the dog is 0.5-5 mm (the skin thickness of the human body is 0.5-4 mm); the skin tissue structure of the cat and the dog is simple, and the skin layers (10 to 15 layers of people) are 3 to 5 layers, namely, the skin tissue structure of the cat and the dog is single, the structure is fragile and easy to damage; meanwhile, the pH value of the skin of the cat and the dog is about 7.0. The pH value of the prior bath foam special for pets is 5.5-6.4, and the pH value of the bath foam special for pets is greatly different from that of skins of cats and dogs, and the prior bath foam is used for easily damaging sebaceous glands of the cats and dogs, so that the self protection of the cats and dogs is reduced, the cats and dogs are easily affected by skin diseases, and the fur is rough, dull and even falls off. In the embodiment, the pH value of the bath foam special for the pet is about 6.5-7.8 and is closer to the pH value of the skin of the pet by designing the components and the proportion of the bath foam special for the pet, so that the bath foam special for the pet is mild and does not irritate the skin of the pet.
In addition, cats and dogs lick the fur, and therefore, the residual ingredients of the washing product are also important for the safety of pets. The bath foam special for pets is safe and nontoxic and lick-free by selecting the specific substances, and the selected natural source raw materials are high in safety and easy to degrade.
In conclusion, the special bath foam for the pets, provided by the invention, has the advantages that the pH of the product is 6.5-7.8 through the design of the raw material components and the proportion, the pH is closer to the pH of the skin of the pets, and the special bath foam for the pets is mild and does not irritate the skin of the pets; the natural-source green surfactant compound biological enzyme plays a synergistic effect, quickly and efficiently eliminates various stains such as proteins, fats, saccharides, sweat, excrement and the like on pets, and plays a certain role in sterilization and insect expelling; on the basis of cleaning, the principle of the theoretical formulation of 'monarch, minister, assistant and guide' of the traditional Chinese medicine is followed, and the Chinese herbal medicine plant miticide and miticide are added to prevent and treat Demodex, sterilize and expel worms; in addition, the bath foam is prepared from natural source raw materials which are high in safety and easy to degrade, does not contain alcohol, synthetic spice masking agents or chemical disinfectants, and is safe, nontoxic and harmless to lick.
Further, the invention also provides a preparation method of the bath foam special for pets, which comprises the following steps of:
s10, dissolving a plant surfactant in deionized water to obtain a mixed solution;
s20, adding Chinese herbal medicine plant mite-killing agent into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain mixed solution;
s30, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution under the stirring condition to obtain a solution A;
s40, cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the special bath foam is 6.5-7.8, and the viscosity of the special bath foam is 3500-8000 cps.
In one embodiment, the bath foam special for pets is prepared by the following steps: adding 50% of the total mass of deionized water into a batching pot, and slowly starting a stirrer with stirring frequency of 15-30 r/min; putting the plant surfactant into a batching pot, and stirring until the plant surfactant is completely dissolved; putting the Chinese herbal medicine plant miticide into a batching pot, starting a heater to heat to 50-60 ℃, and stirring at the frequency of 45-65 r/min until the Chinese herbal medicine plant miticide is uniformly mixed; adding the thickening stabilizer into a batching pot, and stirring until the thickening stabilizer is completely dissolved uniformly; putting the hair softening and fluffing agent into a batching pot, and stirring until the hair softening and fluffing agent is uniformly mixed; adding the biological enzyme stabilizer into a batching pot, and stirring until the biological enzyme stabilizer is uniformly mixed; adding the rest deionized water, and starting to cool; accurately weighing the compound enzyme preparation when the temperature of the materials in the pot is reduced to be lower than 35 ℃, and putting the compound enzyme preparation into a material mixing pot, wherein the stirring speed is reduced, and the stirring frequency is 10-20 r/min; the preservative is put into a batching pot and stirred until being uniformly mixed, so that the special bath foam for pets is obtained, which is light yellow transparent liquid, has the pH value of 6.5-7.8 and the viscosity of 3500-8000 cps.
The following description of the embodiments of the present invention will be presented in further detail with reference to the examples, which should be understood as being merely illustrative of the present invention and not limiting.
In the following examples, the source information of the partial raw materials used is as follows:
in the hair relaxer: the bionic phospholipid is the product of CRODA in England, and has the product of SAPILUB PTC and the chemical name of cocamidopropyl PG-dimethyl ammonium chloride phosphate; the hair care oil is CRODA product of England with trade name CROMOLLIENT SCE-LQ- (MH) and chemical name of bis (PPG-2 myristyl oleyl polyether-10) adipate; the hydrolyzed wheat protein is potassium of undecylenoyl hydrolyzed wheat protein which is the Chongqing sea sail biochemical technology Co., ltd; guar gum is a product of Sorvy under the trade nameExcel, chemical name guar hydroxypropyl trimethyl ammonium chloride; polyquaternium-7 is a ropeProducts of Erwei, trade name +.>550SBF。
The thickener comprises the following components: the manufacturer of PEG-120 methyl glucose dioleate is Lipurun in America, and the trade name is GLUCAMATE DOE-120; the manufacturer of cocoamidomethyl MEA is Guangzhou flower fine chemical Co., ltd, and has the trade name CMMEA.
Among the preservatives: the trade name of the kathon is mulberry K15 (SupGuard K15); phenoxyethanol is commercially available under the name ofPE 9010。
Example 1
The special bath foam for the pets comprises the following raw material components in percentage by mass:
15% of a plant surfactant, wherein the plant surfactant is prepared by compounding a gleditsia sinensis saponin extract and a soapberry peel extract in a mass ratio of 2:1;
the Chinese herbal medicine plant acaricide 15%, wherein the Chinese herbal medicine plant acaricide is prepared from radix stemonae extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, peppermint extract, ginger root extract and motherwort extract according to the mass ratio of 8:4:4:3:3:3:2, compounding to obtain the compound;
2% of a compound enzyme preparation, wherein the compound enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1:0.8:0.1:0.1;
2% of hair softening and bulking agent, wherein the hair softening and bulking agent is prepared by compounding bionic phospholipid, hair care grease and hydrolyzed wheat protein according to the mass ratio of 0.6:0.4:1;
4% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is prepared by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.01:1:8:2;
a thickening stabilizer 3%, specifically PEG-120 methylglucdioleate;
0.75% of preservative, wherein the preservative is prepared by compounding pinus koraiensis and phenoxyethanol according to the mass ratio of 0.1:0.65;
58.25% of deionized water.
Example 2
The special bath foam for the pets comprises the following raw material components in percentage by mass:
23% of a plant surfactant, wherein the mass ratio of the plant surfactant is 1.875:1, a small fruit gleditsia sinensis saponin extract and a soapberry peel extract are compounded to obtain the compound Chinese medicinal preparation;
20% of Chinese herbal medicine plant miticide, wherein the Chinese herbal medicine plant miticide is prepared from radix stemonae extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, peppermint extract, ginger root extract and motherwort extract according to the mass ratio of 8:4:4:3:3:3:2, compounding to obtain the compound;
2.35% of a complex enzyme preparation, wherein the complex enzyme preparation comprises lipase, protease, cellulase and lysozyme according to the mass ratio of 0.5:1.5:0.1:0.25 of the components;
3% of hair softening and bulking agent, wherein the hair softening and bulking agent is prepared by compounding bionic phospholipid, hair care grease and hydrolyzed wheat protein according to a mass ratio of 1:1:1;
8% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is prepared by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.01:5:2:5;
1% of thickening stabilizer, specifically PEG-120 methyl glucose dioleate;
1.65% of preservative, wherein the preservative is prepared by compounding pinus koraiensis and phenoxyethanol according to the mass ratio of 0.3:1.35;
41% of deionized water.
Example 3
The special bath foam for the pets comprises the following raw material components in percentage by mass:
25% of a plant surfactant, wherein the plant surfactant is prepared by compounding a gleditsia sinensis saponin extract and a soapberry peel extract in a mass ratio of 1:4;
the Chinese herbal medicine plant acaricide is 8%, wherein the Chinese herbal medicine plant acaricide is prepared from radix stemonae extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, peppermint extract, ginger root extract and motherwort extract according to the mass ratio of 8:4:4:3:3:3:2, compounding to obtain the compound;
4% of a compound enzyme preparation, wherein the compound enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1:2.5:0.35:0.05;
4% of hair softening and bulking agent, wherein the hair softening and bulking agent is prepared by compounding bionic phospholipid, hair care grease and polyquaternium-7 according to the mass ratio of 1.5:1:1.5;
2% of biological enzyme stabilizer, wherein the biological enzyme stabilizer is prepared by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.05:5:2:5;
thickening stabilizer 2%, specifically polyethylene glycol distearate;
2% of preservative, wherein the preservative is prepared by compounding pinus koraiensis and phenoxyethanol according to the mass ratio of 0.15:1.85;
53% of deionized water.
Example 4
The special bath foam for the pets comprises the following raw material components in percentage by mass:
30% of a plant surfactant, wherein the plant surfactant is prepared by compounding a gleditsia sinensis saponin extract and a soapberry peel extract in a mass ratio of 1:1;
the Chinese herbal medicine plant acaricide 10%, wherein the Chinese herbal medicine plant acaricide is prepared from radix stemonae extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, peppermint extract, ginger root extract and motherwort extract according to the mass ratio of 8:4:4:3:3:3:2, compounding to obtain the compound;
3.4% of a compound enzyme preparation, wherein the compound enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1.2:1.2:0.5:0.5;
2.8% of hair softening and bulking agent, wherein the hair softening and bulking agent is prepared by compounding bionic phospholipid, guar gum and polyquaternium-7 according to the mass ratio of 1.5:0.3:1;
6% of biological enzyme stabilizer, wherein the biological enzyme stabilizer is prepared by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.05:2:6:2;
3% of thickening stabilizer, wherein the thickening stabilizer is prepared by compounding polyethylene glycol distearate and cocoamide methyl MEA according to a mass ratio of 2:1;
0.5% of preservative, wherein the preservative is prepared by compounding pinus koraiensis and phenoxyethanol according to the mass ratio of 0.08:0.42;
44.3% of deionized water.
Example 5
Except that the Chinese herbal medicine plant mite-killing agent is replaced by a stemona root extract, a fructus cnidii extract and a pricklyash peel extract according to the mass ratio of 8:4:4, and the rest components and proportions are the same as in example 1.
Example 6
The other components and proportions are the same as in example 1 except that the Chinese herbal medicine plant mite-killing agent is replaced by a compound of stemona root extract, fructus cnidii extract, flos caryophylli extract and mint extract according to a mass ratio of 3:2:4:2.
Example 7
(1) The formula of the bath foam special for pets is the same as that of the example 1;
(2) Adding 50% of the total mass of deionized water into a batching pot, and slowly starting a stirrer with stirring frequency of 15-30 r/min; putting the plant surfactant into a batching pot, and stirring until the plant surfactant is completely dissolved; putting the Chinese herbal medicine plant miticide into a batching pot, starting a heater to heat to 50-60 ℃, and stirring at the frequency of 45-65 r/min until the Chinese herbal medicine plant miticide is uniformly mixed; adding the thickening stabilizer into a batching pot, and stirring until the thickening stabilizer is completely dissolved uniformly; putting the hair softening and fluffing agent into a batching pot, and stirring until the hair softening and fluffing agent is uniformly mixed; adding the biological enzyme stabilizer into a batching pot, and stirring until the biological enzyme stabilizer is uniformly mixed; adding the rest deionized water, and starting to cool; accurately weighing the compound enzyme preparation when the temperature of the materials in the pot is reduced to be lower than 35 ℃, and putting the compound enzyme preparation into a material mixing pot, wherein the stirring speed is reduced, and the stirring frequency is 10-20 r/min; the preservative is put into a batching pot and stirred until being uniformly mixed, so that the special bath foam for pets is obtained, which is light yellow transparent liquid, has the pH value of 6.5-7.8 and the viscosity of 3500-8000 cps.
Example 8
The procedure was the same as in example 7, except that the formulation of the pet-specific bath foam was replaced with the formulation of example 2.
Example 9
The procedure was the same as in example 7, except that the formulation of the pet-specific bath foam was replaced with the formulation of example 3.
Example 10
The procedure was the same as in example 7, except that the formulation of the pet-specific bath foam was replaced with the formulation of example 4.
Example 11
The procedure was the same as in example 7, except that the formulation of the pet-specific bath foam was replaced with the formulation of example 5.
Example 12
The procedure was the same as in example 7, except that the formulation of the pet-specific bath foam was replaced with the formulation of example 6.
Example 13
(1) The formulation was the same as in example 1 except that the complex enzyme preparation was replaced with a 1:2 formulation of lipase and protease.
(2) The same as in step (2) in example 7.
Comparative example 1
The other components and proportions, and preparation steps were the same as in example 7, except that the plant surfactant was replaced with a chemical surfactant, which was compounded from sodium dodecyl sulfate and ethoxylated alkyl sodium sulfate in a mass ratio of 4:1.
Comparative example 2
The remaining components and proportions, and preparation procedure were the same as in example 7, except that the plant surfactant was replaced with conventional surfactants, sodium fatty alcohol polyoxyethylene ether sulfate (AES) and sodium alpha-alkenyl sulfonate (AOS), wherein the mass ratio of AES to AOS was 3:2.
Comparative example 3
Except that the complex enzyme preparation was not added, the addition amount of deionized water was modified to 60.25%, and the other components and proportions, and the preparation steps were the same as in example 7.
The pet-specific body washes prepared in examples 7 to 10 and comparative example 1 were tested as follows:
1. safety test
1. The testing method comprises the following steps: in vitro ocular irritation assay-modified CAMVA method.
2. The evaluation method comprises the following steps:
(1) The CAMVA stimulation response included ghosting, congestion, bleeding, etc., which phenomena and stimulation scores are shown in table 1 below.
TABLE 1CAMVA stimulus response phenomenon and scoring table thereof
(2) According to the scores of table 1, 60 effective chick embryos are divided into 6 groups of 10 chick embryos, the irritation evaluation of the samples is recorded, the average value is obtained, and the average irritation score (AS) of the samples is obtained, wherein the corresponding relation between the AS value and the eye irritation of the samples is shown in table 2 below.
TABLE 2 evaluation criteria for eye irritation
| Stimulation scoring | Stimulation level |
| 0≤AS＜0.5 | No irritation |
| 0.5≤AS＜1.5 | Microstimulation |
| 1.5≤AS＜3.5 | Light irritation |
| 3.5≤AS＜5 | Moderate irritation |
| 5.0≤AS＜6.0 | Strong irritation/corrosiveness |
(3) The pet-specific body washes prepared in examples 7 to 10 and the body washes prepared in comparative examples 1 and 2 were applied to 6 groups of chick embryos (10 pieces per group), respectively, and the results of CAMVA test observations are shown in Table 3 below.
TABLE 3CAMVA test observations
From the evaluation criteria of tables 1 and 2 and the results of the CAMVA test observations of Table 3, the CAMVA test observations scoring table shown in Table 4 below was obtained.
Table 4 CAMVA test observation scoring table
As can be seen from Table 4, the results of the in vitro eye irritation test show that the average eye irritation of the bath foam special for pets prepared by any embodiment of the invention is less than 1.1, and the average eye irritation of the bath foam prepared by comparative examples 1 and 2 is 2.8 and 2.3 respectively, and the average eye irritation is light, which shows that the components of the bath foam special for pets prepared by the invention are mild, the irritation is small and the safety is high by selecting the plant surfactant.
It should be noted that, the preparation principles of examples 11-13 are similar to those of examples 7-10, and the pH is also similar and is between 6.5 and 7.8, so that the irritation is similar to that of examples 7-10, and detailed description thereof is omitted.
2. Mite killing performance test
1. Mite killing performance test according to the method for testing the efficacy of insecticidal indoor for sanitary use and for pesticide registration of NY/T1151.2-2006 and evaluation part 2: mite killing and repelling agents.
2. Mite killing test:
(1) Taking 7 culture dishes, putting 6 of the culture dishes into the special bath foam for pets prepared in the examples 7-12 according to the using method, and uniformly smearing a mixture of white oil and Vaseline on the upper edge of the inner wall of each culture dish without putting the bath foam to be tested into the other culture dish as a control.
(2) 200 insects are put in the center of each culture dish, 0.5g of mite feed is put in the center of each culture dish at 30min, and then the culture dishes are placed in a water-proof incubator.
(3) The number of dead mites was checked and recorded for 48 h.
3. Result calculation
The mite killing rate is calculated according to a formula and expressed as a percentage (%):
P＝R/N×100.................(1)
wherein:
p-mite killing rate;
r is death test number;
n-number of test insects.
When the mite mortality rate of the control group is less than 5%, correction is not needed; when the mite mortality rate of the control group is between 5% and 20%, the corrected mortality rate is calculated according to the following formula (2), expressed as a percentage (%); when mite mortality rate of the control group is more than 20%, the test is carried out again.
Pt＝(Py-Px)/(1-Px)..............(2)
Wherein:
pt-correct mite kill rate;
py—test group mite killing rate;
px-mite killing rate of control group.
Test insects: dust mites (Dermatophagoides farinae), male and female adults
Test conditions:
temperature: 25 ℃ +/-2 DEG C
Relative humidity: 75% ± 5%
4. The results of the mite-killing rate test are shown in the following table 5.
TABLE 5 mite-killing test results
| Examples | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 |
| Mite killing rate (%) | 96.8 | 98.2 | 97.6 | 99.1 | 95.6 | 95.4 |
5. The evaluation criteria of the miticidal effect are shown in Table 6 below.
TABLE 6 evaluation criteria for miticidal efficacy
As can be seen from the combination of Table 5 and Table 6, the mite-killing rates of the bath foam special for pets prepared in examples 7-12 of the invention reach the B level, which shows that the mite-killing effect of the bath foam special for pets prepared by the invention is good through the design of the raw material components and the proportion.
Wherein the mite-killing rate of the special bath foam for pets in examples 7-10 is above 96.8%, the mite-killing rates of the special bath foam for pets prepared in examples 11 and 12 are 95.6% and 95.4%, respectively, and the herbal medicine plant mite-killing agent is prepared by compounding the stemona root extract, the fructus cnidii extract, the fructus zanthoxyli extract, the flos caryophylli extract, the mint extract, the ginger root extract and the motherwort extract, and the mass ratio of the two is 7-9: 3.5 to 4.5:3.5 to 4.5:3:3:3:2, the mite killing effect is better.
3. Antibacterial property test
According to the test method of the quantitative sterilization test of suspension in the disinfection technical Specification (2002 edition), the Escherichia coli (ATCC 25922), staphylococcus aureus (ATCC 6538) and candida albicans (ATCC 10231) are tested for killing, and the test method of each example is as follows: setting two identical culture dishes (containing culture mediums), placing an equal amount of test bacteria, taking one culture dish as an experimental group, adding a special pet bath foam diluent (the special pet bath foam diluent is obtained by mixing the special pet bath foam prepared by the embodiment with deionized water according to the mass ratio of 1:5), taking the other culture dish as a control group (the special pet bath foam of the invention is not added, deionized water with the same amount as the special pet bath foam diluent of the experimental group is added), culturing for the same time under the same culture condition, and then testing the survival bacteria of the control group and the experimental group respectively, wherein the action time is as follows: 5min; the test results are shown in Table 7 below.
TABLE 7 antibacterial Property test results
As can be seen from Table 7, the sterilizing rates of the special bath foam for pets prepared in examples 7-12 on escherichia coli, staphylococcus aureus and candida albicans all reach more than 99%, so that the special bath foam for pets provided by the invention has excellent antibacterial effect through the design of components and proportions. The sterilization rates of examples 7 to 10 are higher than those of examples 11 and 12, and the sterilization rate of example 12 is higher than that of example 11, and the herbal medicine plant miticide is prepared by compounding the stemona root extract, the fructus cnidii extract, the fructus zanthoxyli extract, the flos caryophylli extract, the peppermint extract, the ginger root extract and the motherwort extract, and the mass ratio of the two is 7 to 9:3.5 to 4.5:3.5 to 4.5:3:3:3:2, the sterilization effect is better.
4. Detergency test
The detergency test is carried out according to GB/T13174-2008 test of detergency and cycle washing performance of the detergent for clothing, the detergency test concentration is 0.1% (1000 times of bath foam dilution), and the pH is between 6.8 and 7.2. JB-01-carbon black dirty cloth; JB-02-protein dirt cloth; JB-03-sebum dirt cloth; standard parameter index requires that all three test dirty cloth of JB-01, JB-02 and JB-03 are larger than or equal to standard liquid, and the test dirty cloth is qualified.
Table 8 detergency test results
| Detergency (%) JB-01 | Detergency (%) JB-02 | DecontaminationForce (%) JB-03 | |
| Standard solution | 1.0 | 1.0 | 1.0 |
| Comparative example 1 | 1.9 | 1.5 | 1.7 |
| Comparative example 2 | 1.5 | 1.0 | 0.9 |
| Comparative example 3 | 1.8 | 1.3 | 1.1 |
| Example 7 | 2.2 | 1.8 | 2.0 |
| Example 8 | 2.1 | 1.6 | 2.5 |
| Example 9 | 2.5 | 2.2 | 1.9 |
| Example 10 | 2.1 | 3.2 | 2.0 |
| Example 13 | 2.0 | 1.6 | 1.8 |
As can be seen from Table 8, the detergency of the bath foam for pets prepared in any embodiment to the test soiling cloth of JB-01, JB-02 and JB-03 is higher than that of the comparative example, which shows that the bath foam for pets has excellent cleaning effect by designing the components and the proportion of the plant surfactant. As can be seen by comparing example 7 with example 13, when the complex enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme, the mass ratio of them is 0.5-1.2: 0.8 to 2.5:0.1 to 0.5: when the detergency of the bath foam special for pets is 0.05 to 0.5, the prepared bath foam special for pets has the best detergency.
As can be seen from comparison of comparative example 3 with inventive example 7, the combination of the complex enzyme preparation and the plant surfactant plays an important role in improving detergency, and if the complex enzyme preparation is absent, detergency is lowered, which means that the plant surfactant and the complex enzyme in the bath foam special for pets of the invention have a synergistic effect, and can rapidly and efficiently remove various stains such as proteins, fats, saccharides, sweat, excrement and the like on pets.
The foregoing is merely a preferred embodiment of the present invention and is not intended to limit the scope of the present invention, but various modifications and variations will be apparent to those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (6)
1. The special bath foam for the pets is characterized by comprising the following raw material components in percentage by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant miticide, 2-4% of compound enzyme preparation, 2-4% of hair softening and bulking agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water;
the plant surfactant comprises a gleditsia sinensis saponin extract and a soapberry pericarp extract;
the mass ratio of the small fruit gleditsia sinensis saponin extract to the soapberry peel extract is 1-2: 1 to 4;
the Chinese herbal medicine plant miticide is radix stemonae extract, fructus cnidii extract, fructus zanthoxyli extract, flos caryophylli extract, mint extract, ginger root extract and motherwort extract;
the mass ratio of the stemona root extract, the cnidium fruit extract, the pricklyash peel extract, the lilac flower extract, the peppermint extract, the ginger root extract and the motherwort herb extract is 8:4:4:3:3:3:2;
the complex enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme, wherein the mass ratio of the lipase to the protease to the cellulase to the lysozyme is 0.5-1.2: 0.8 to 2.5:0.1 to 0.5:0.05 to 0.5;
the pH value of the bath foam special for the pets is 6.5-7.8.
2. The pet-specific body wash of claim 1, wherein the hair softening and bulking agent comprises at least one of biomimetic phospholipids, hair care oils, hydrolyzed wheat protein, guar gum, and polyquaternium-7.
3. The pet-specific body wash of claim 1, wherein the bio-enzyme stabilizer comprises a metal compound, a saccharide, and a polyol.
4. The pet-specific body wash of claim 3, wherein the metal compound comprises at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate, and potassium chloride; and/or the number of the groups of groups,
the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the number of the groups of groups,
the polyalcohol comprises at least one of glycerol, 1, 3-propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
5. The pet-specific body wash of claim 1, wherein the thickening stabilizer comprises at least one of PEG-120 methyl glucdioleate, cocoamidomethyl MEA, polyethylene glycol distearate, and fatty alcohol polyoxyethylene ether acrylic acid copolymer; and/or the number of the groups of groups,
the preservative comprises pinacol and phenoxyethanol.
6. A method for preparing the bath foam for pets according to any of claims 1 to 5, comprising the steps of:
dissolving a plant surfactant in deionized water to obtain a mixed solution;
adding Chinese herbal medicine plant mite-killing agent into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain mixed solution;
under the stirring condition, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution to obtain a solution A;
and (3) cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the special bath foam is 6.5-7.8, and the viscosity of the special bath foam is 3500-8000 cps.
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