CN108904329A - A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof - Google Patents
A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof Download PDFInfo
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- CN108904329A CN108904329A CN201810942671.8A CN201810942671A CN108904329A CN 108904329 A CN108904329 A CN 108904329A CN 201810942671 A CN201810942671 A CN 201810942671A CN 108904329 A CN108904329 A CN 108904329A
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- polyacid
- hand cleanser
- environment friendly
- friendly bacteriostatic
- deionized water
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The present invention relates to a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof, belong to technical field of daily necessities.The present invention, which utilizes, contains a large amount of saponin(e substance in the pod of Chinese honey locust, saponin(e substance has multiple biological activities and pharmacological action, such as anti-inflammatory, antiallergy, it is antiviral, a variety of diseases such as anticancer, saponin(e is very good natural nonionic surfactant again simultaneously, to the skin of majority, eyes are non-stimulated, the characteristics of on ecological environment without influencing, it is supported on the polyacid compound of metallic silver ion doping, prepare the growth that anti-biotic material is killed and inhibits harmful bacteria, breeding, realize the health of the product for civilian use and cleaning for living environment, play the multi-efficiency of silver ion and polyacid nanocomposite Synergistic antimicrobial.
Description
Technical field
The present invention relates to a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof, belong to technical field of daily necessities.
Background technique
As a kind of infectious disease for seriously threatening human health, the infection sources of Flu-A is illness and symptomless infection
Animal and people, route of transmission mainly have 2 kinds, are coughed by patient and symptomless infection person or the droplet of sneezing generation is through breathing
Road is propagated, and passes through the environment of the respiratory secretions of contact patient and symptomless infection person, alimentary canal excreta and pollution
Behind communal facility surface, then contact itself oral cavity, nasal cavity, eyes etc. mucous membrane propagated.Crowd is generally susceptible, generally
Symptoms are mild by people, can get well by short, but some people at highest risk are poor to influenza resistance, after infection, symptom compared with
Weight, is easy to appear multiple complications, can lead to death when serious.People at highest risk mainly includes：Pregnancy women, with breathing system
The crowd of system disease, disease of cardiovascular system chronic diseases, children and the elderly etc..
Harm of the influenza A virus to crowd is reduced, takes effective precautionary measures particularly important, that takes at present arranges
Apply including：Control the infection sources, cutting route of transmission and protection healthy population.It is rear two that crowd, which protects the main path of own health,
Kind, it can be realized by some simple methods, for example form good personal hygiene habit, abundance sleep is diligent in tempering body
Body reduces pressure, and sufficient nutrition avoids contact with the respiratory disease patients such as influenza-like symptom or pneumonia, pays attention to personal hygiene,
It washes one's hands commonly using soap and clear water, especially after cough or sneezing, avoids contact with the animal that may propagate influenza, avoid
Go to crowded place etc..In addition inoculation influenza vaccines are also a kind of effective method, but influenza virus is still constantly sending out
It changes different, once generating new antigenicity, currently available vaccines, existing vaccines is by there is no the effect of prevention & protection, and in addition vaccine inoculation may
Cause different degrees of adverse reaction, if injection site is ached, rubescent, influenza-like symptom, Nausea and vomiting, stomachache, diarrhea, head
It is dizzy, cause some mild reactions such as hypersensitivity, serious person will appear carcinogenic, teratogenesis, permanent or significant disability, even result in
It is dead.
Washing one's hands is method that most convenient effectively cuts off transmission approach.Hand can touch diversified in environment
Pathogenic microorganism, hand have a large amount of sebaceous glands and a hair follicle, secrete grease and sweat, conducive to the adherency of bacterial virus, and hand
Temperature humidity is suitble to many bacterial viruses growths and long-term surviving, and contaminated hand is easy when touching other positions of body will be sick
Substance is propagated over together, causes disease.Prevent disease by washing one's hands, not only it is noted that the frequency of use and method of hand cleanser,
Effective hand lotion is more used, in face of constantly attacking for influenza and other communicable diseases, reinforces personal hygiene and likes, use
Effective hand lotion, often washes one's hands, and can effectively cut off route of transmission, is a kind of active and effective method.
Summary of the invention
The technical problems to be solved by the invention：For hand cleanser higher cost in the prior art, product is used for a long time
There is the problem of injury to the skin of people, provides a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof.
In order to solve the above technical problems, the technical solution adopted by the present invention is that：
A kind of environment friendly bacteriostatic polyacid hand cleanser, the hand cleanser chemical composition and weight percent content are as follows：
10~12% dodecyl polyoxyethylene ether sodium sulphate, 12~15% neopelexes, 1~3% coco-nut oil fatty acid
Diglycollic amide, 0.6~1.2% sodium chloride, 1~2% glycerol, 0.1~0.2% essence, 0.05~0.20% antimicrobial factors, deionization
Water surplus.
The antimicrobial factors be silver nitrate dissolve in deionized water with after heteropoly acid hybrid reaction be added ammonium oxalate, Chinese honey locust
Volatile oil, polyethylene glycol 400 are uniformly mixed and dry obtained after hydro-thermal reaction.
Described weight of material part be 0.5~1.0 part of silver nitrate, 100~150 parts of deionized waters, 1.2~3.2 parts of heteropoly acids,
0.1~0.5 part of ammonium oxalate, 1~2 part of Chinese honey locust volatile oil, 4~8 parts of polyethylene glycol 400s.
The heteropoly acid is one or more of phosphotungstic acid, phosphomolybdic acid, silico-tungstic acid.
The hybrid reaction process is to be heated with stirring to 60~80 DEG C under nitrogen atmosphere and continue 1~4h of stirring.
The hydrothermal temperature is 120~240 DEG C.
The Chinese honey locust volatile oil is to crush to be laid on filter paper after air-drying Chinese honey locust, is placed in 3~5cm above deionized water
On the bracket at place, steam is passed through in condenser pipe by heating deionized water to boiling, and standing takes upper oil, and with anhydrous sulphur
Sour magnesium dehydration is made.
A kind of preparation method of the environment friendly bacteriostatic polyacid hand cleanser, the specific steps are：
（1）It crushes and is laid on filter paper after Chinese honey locust is air-dried, is placed on the bracket above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to boiling, and standing takes upper oil, and is dehydrated with anhydrous magnesium sulfate, is obtained Chinese honey locust and is waved
Hair oil；
（2）It takes silver nitrate to be added in deionized water to stir, ammonium oxalate, Chinese honey locust volatilization is added after adding heteropoly acid hybrid reaction
Oil, polyethylene glycol 400 are uniformly mixed and dry after hydro-thermal reaction, obtain antimicrobial factors；
（3）Dodecyl polyoxyethylene ether sodium sulphate, neopelex is taken to be added in deionized water, with 300~400r/
Min is heated with stirring to 50~60 DEG C, 20~30min of insulated and stirred, and coco-nut oil fatty acid diethanol acyl is added after being cooled to room temperature
Amine, sodium chloride, glycerol continue 20~30min of stirring, add essence, antimicrobial factors, add after 30~40min of insulated and stirred and go
Ionized water obtains environment friendly bacteriostatic polyacid hand cleanser to 100g.
The present invention is compared with other methods, and advantageous effects are：
（1）The present invention has multiple biological activities and medicine using a large amount of saponin(e substance, saponin(e substance is contained in the pod of Chinese honey locust
Reason effect, such as anti-inflammatory, antiallergy, antiviral, a variety of diseases of anticancer, while saponin(e are very good natural nonionic table again
Face activating agent, it is non-stimulated to skin, the eyes of majority, on ecological environment without influence the characteristics of, be supported on metallic silver from
On the polyacid compound of son doping, prepares anti-biotic material and kill and inhibit the growth of harmful bacteria, breeding, realize the product for civilian use
Health and living environment clean, and play the multi-efficiency of silver ion and polyacid nanocomposite Synergistic antimicrobial；
（2）Product of the present invention exposure be not in for a long time in air it is mouldy, rotten, spoiled, property stablize, do not need to be added
Antiseptic kind substance, product are not in lamination by freezing heating repeatedly, and property is reliable, and reaches chemical industry hand cleanser and go out
Bacterium effect.
Specific embodiment
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 50~100g Chinese honey locust powder is taken to be laid in filter paper
On, it being placed on the bracket above deionized water at 3~5cm, steam is passed through in condenser pipe by heating deionized water to boiling,
Continuous heating grease into condenser pipe is not further added by, stand 1~2h after take upper oil, into grease be added 20~
30g anhydrous magnesium sulfate stands filtering removal anhydrous magnesium sulfate after 20~30min, obtains Chinese honey locust volatile oil, take 0.5~1.0g nitric acid
Silver is added in 100~150g deionized water, stirs 20~30min under the conditions of being protected from light with 300~400r/min, adds 1.2
~3.2g heteropoly acid, is heated with stirring to 60~80 DEG C under nitrogen atmosphere, and 0.1~0.5g oxalic acid is added after persistently stirring 1~4h
Ammonium, 1~2g Chinese honey locust volatile oil, 4~8g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing, at 120~240 DEG C
4~8h is reacted, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2~3 times is washed with deionized and is placed in drying box, 60
Dry 3~5h, obtains antimicrobial factors, takes 10~12g dodecyl polyoxyethylene ether sodium sulphate, 12~15g dodecane at~80 DEG C
Base benzene sulfonic acid sodium salt is added in 50~60g deionized water, is heated with stirring to 50~60 DEG C with 300~400r/min, insulated and stirred 20
~30min, addition 1~3g cocoanut fatty acid diethanolamide, 0.6~1.2g sodium chloride, 1~2g are sweet after being cooled to room temperature
Oil continues 20~30min of stirring, adds 0.1~0.2g essence, 0.05~0.20g antimicrobial factors, and insulated and stirred 30~
After 40min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 50g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 3cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 1h, and 20g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 20min, obtains Chinese honey locust volatile oil, takes 0.5g silver nitrate, is added in 100g deionized water, is keeping away
20min is stirred with 300r/min under the conditions of light, 1.2g heteropoly acid is added, is heated with stirring to 60 DEG C under nitrogen atmosphere, is continued
0.1g ammonium oxalate, 1g Chinese honey locust volatile oil is added after stirring 1h, 4g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
4h is reacted at 120 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2 times is washed with deionized and is placed in drying box,
Dry 3h, obtains antimicrobial factors, takes 10g dodecyl polyoxyethylene ether sodium sulphate, 12g neopelex adds at 60 DEG C
Enter in 50g deionized water, be heated with stirring to 50 DEG C, insulated and stirred 20min with 300r/min, 1g coconut is added after being cooled to room temperature
Fatty acid oil diglycollic amide, 0.6g sodium chloride, 1g glycerol continue to stir 20min, add 0.1g essence, 0.05g antibacterial because
Son, after insulated and stirred 30min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 80g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 4cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 1h, and 25g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 25min, obtains Chinese honey locust volatile oil, takes 0.8g silver nitrate, is added in 120g deionized water, is keeping away
20min is stirred with 300r/min under the conditions of light, 2g heteropoly acid is added, is heated with stirring to 70 DEG C under nitrogen atmosphere, persistently stirs
0.3g ammonium oxalate, 1g Chinese honey locust volatile oil is added after mixing 3h, 6g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
6h is reacted at 200 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2 times is washed with deionized and is placed in drying box, 70
Dry 4h, obtains antimicrobial factors at DEG C, takes 10g dodecyl polyoxyethylene ether sodium sulphate, and 15g neopelex is added
In 60g deionized water, 60 DEG C, insulated and stirred 30min are heated with stirring to 400r/min, 3g coconut oil is added after being cooled to room temperature
Fatty diglycollic amide, 0.8g sodium chloride, 2g glycerol continue to stir 25min, add 0.1g essence, 0.1g antimicrobial factors,
After insulated and stirred 30min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 100g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 5cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 2h, and 30g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 30min, obtains Chinese honey locust volatile oil, takes 1.0g silver nitrate, is added in 150g deionized water, is keeping away
30min is stirred with 400r/min under the conditions of light, 3.2g heteropoly acid is added, is heated with stirring to 80 DEG C under nitrogen atmosphere, is continued
0.5g ammonium oxalate, 2g Chinese honey locust volatile oil is added after stirring 4h, 8g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
8h is reacted at 240 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 3 times is washed with deionized and is placed in drying box,
Dry 5h, obtains antimicrobial factors, takes 12g dodecyl polyoxyethylene ether sodium sulphate, 15g neopelex adds at 80 DEG C
Enter in 60g deionized water, be heated with stirring to 60 DEG C, insulated and stirred 30min with 400r/min, 3g coconut is added after being cooled to room temperature
Fatty acid oil diglycollic amide, 1.2g sodium chloride, 2g glycerol continue to stir 30min, add 0.2g essence, 0.20g antibacterial because
Son, after insulated and stirred 40min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
Reference examples：The environment friendly bacteriostatic polyacid hand cleanser of Shandong company production.
The environment friendly bacteriostatic polyacid hand cleanser that example and reference examples are prepared is detected, specific test result such as table 1.
1 performance characterization contrast table of table
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| pH | 6.5 | 6.3 | 6.1 | 4.2 |
| Sterilizing rate % | 98 | 98 | 99 | 88 |
| Total plate count CFU/g | 10 | 9 | 11 | 50 |
| Excrement colibacillus group CFU/g | 0 | 0 | 0 | 0 |
As shown in Table 1, environment friendly bacteriostatic polyacid hand cleanser prepared by the present invention has good bacteriostasis property.
Claims (8)
1. a kind of environment friendly bacteriostatic polyacid hand cleanser, which is characterized in that the hand cleanser chemical composition and weight percent content are such as
Under：
10~12% dodecyl polyoxyethylene ether sodium sulphate, 12~15% neopelexes, 1~3% coco-nut oil fatty acid
Diglycollic amide, 0.6~1.2% sodium chloride, 1~2% glycerol, 0.1~0.2% essence, 0.05~0.20% antimicrobial factors, deionization
Water surplus.
2. a kind of environment friendly bacteriostatic polyacid hand cleanser as described in claim 1, which is characterized in that the antimicrobial factors are silver nitrate
Dissolution with addition ammonium oxalate, Chinese honey locust volatile oil, polyethylene glycol 400 after heteropoly acid hybrid reaction, is uniformly mixed in deionized water
And it is dry obtained after hydro-thermal reaction.
3. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that described weight of material part is 0.5
~1.0 parts of silver nitrates, 100~150 parts of deionized waters, 1.2~3.2 parts of heteropoly acids, 0.1~0.5 part of ammonium oxalate, 1~2 portion of Chinese honey locust
Volatile oil, 4~8 parts of polyethylene glycol 400s.
4. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the heteropoly acid be phosphotungstic acid,
One or more of phosphomolybdic acid, silico-tungstic acid.
5. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the hybrid reaction process be
It is heated with stirring to 60~80 DEG C under nitrogen atmosphere and continues 1~4h of stirring.
6. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the hydrothermal temperature is
120~240 DEG C.
7. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the Chinese honey locust volatile oil is by soap
Pod crushes after air-drying and is laid on filter paper, is placed on the bracket above deionized water at 3~5cm, heating deionized water to boiling
It rises, steam is passed through in condenser pipe, standing takes upper oil, and is dehydrated and is made with anhydrous magnesium sulfate.
8. a kind of preparation method of environment friendly bacteriostatic polyacid hand cleanser as described in claim 1~7 any one, feature exist
In, the specific steps are：
（1）It crushes and is laid on filter paper after Chinese honey locust is air-dried, is placed on the bracket above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to boiling, and standing takes upper oil, and is dehydrated with anhydrous magnesium sulfate, is obtained Chinese honey locust and is waved
Hair oil；
（2）It takes silver nitrate to be added in deionized water to stir, ammonium oxalate, Chinese honey locust volatilization is added after adding heteropoly acid hybrid reaction
Oil, polyethylene glycol 400 are uniformly mixed and dry after hydro-thermal reaction, obtain antimicrobial factors；
（3）Dodecyl polyoxyethylene ether sodium sulphate, neopelex is taken to be added in deionized water, with 300~400r/
Min is heated with stirring to 50~60 DEG C, 20~30min of insulated and stirred, and coco-nut oil fatty acid diethanol acyl is added after being cooled to room temperature
Amine, sodium chloride, glycerol continue 20~30min of stirring, add essence, antimicrobial factors, add after 30~40min of insulated and stirred and go
Ionized water obtains environment friendly bacteriostatic polyacid hand cleanser to 100g.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810942671.8A CN108904329A (en) | 2018-08-17 | 2018-08-17 | A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof |
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| CN201810942671.8A CN108904329A (en) | 2018-08-17 | 2018-08-17 | A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof |
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Cited By (2)
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| CN111281826A (en) * | 2018-12-10 | 2020-06-16 | 哈尔滨源麻科技有限公司 | Antibacterial washing liquid containing cannabis polyphenol extract |
| CN112791075A (en) * | 2020-12-29 | 2021-05-14 | 新乡医学院 | Explosive wound and body surface cleaning and sterilizing liquid and preparation method and application thereof |
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| CN111281826A (en) * | 2018-12-10 | 2020-06-16 | 哈尔滨源麻科技有限公司 | Antibacterial washing liquid containing cannabis polyphenol extract |
| CN112791075A (en) * | 2020-12-29 | 2021-05-14 | 新乡医学院 | Explosive wound and body surface cleaning and sterilizing liquid and preparation method and application thereof |
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Application publication date: 20181130 |
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| WD01 | Invention patent application deemed withdrawn after publication |