CN106479694A - A kind of agricultural chemicals cleaning agent and preparation method thereof - Google Patents

A kind of agricultural chemicals cleaning agent and preparation method thereof Download PDF

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Publication number
CN106479694A
CN106479694A CN201610832140.4A CN201610832140A CN106479694A CN 106479694 A CN106479694 A CN 106479694A CN 201610832140 A CN201610832140 A CN 201610832140A CN 106479694 A CN106479694 A CN 106479694A
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China
Prior art keywords
cleaning agent
agricultural chemicals
water
essence
chinese herbal
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CN201610832140.4A
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Chinese (zh)
Inventor
陈剑婷
黄飞必
谢文省
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Individual
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Individual
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Priority to CN201610832140.4A priority Critical patent/CN106479694A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/10Carbonates ; Bicarbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2093Esters; Carbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50Perfumes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Emergency Medicine (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention provides a kind of agricultural chemicals cleaning agent and preparation method thereof, is made up of by its weight portion following components:Chinese herbal medicine water extract, sodium acid carbonate, glucoside bactericide, antioxidant, essence, nano silicon, water.Prior art is compared, the cleaning agent raw material of the present invention is natural food ingredient, edible, safety, health, environmental protection, eat safety and Health efficiency high, elimination efficiency is high, common bacteria, general mould and parasite can be effectively killed, this product consumption is low, during cleaning fruits and vegetables, in every kilogram of water, need to only add about stoste 10ml, vegetables and fruits are immersed in 10 minutes in dilution, then flowing water cleans 23 times.

Description

A kind of agricultural chemicals cleaning agent and preparation method thereof
Technical field
The invention belongs to cleaning agent field, more particularly to a kind of agricultural chemicals cleaning agent and preparation method thereof.
Background technology
The definition of agricultural chemicals broad sense refer to for prevent, eliminate or control harm agricultural, the disease of forestry, worm, grass and other Harmful organism and purposefully regulation, control, impact plant and harmful organism metabolism, growth, development, the chemistry of reproductive process Synthesis or the mixing of a kind of material produced from biological, other natural products and Applied Biotechnology or several materials Thing and its preparation.Referred in the narrow sense in agricultural production, be the growth for ensureing, promoting plant and crops, the desinsection that is applied, A class medicine that is sterilized, killing harmful animal (or weeds) is referred to as.Refer in particular to agriculturally for preventing and treating disease pest and adjusting plant The medicaments such as growth, weeding.After food residues of pesticides show the direct applying pesticides preparation of crops, permeability agricultural chemicals is mainly attached on The crop surface such as veterinary antibiotics, major part can be washed away, and therefore the pesticide concentration of crop appearance is higher than inside.
Food security is to concern the forefront of human life's safety and Health, therefore, how to find a kind of safely and effectively agriculture Medicine scavenger is current urgent problem.
Content of the invention
In sum, the present invention is necessary to provide a kind of agricultural chemicals cleaning agent.
Additionally, there is a need to providing a kind of preparation method of above-mentioned agricultural chemicals cleaning agent.
A kind of agricultural chemicals cleaning agent, is made up of by its weight portion following components:
Chinese herbal medicine water extract 15-20 part
Sodium acid carbonate 0.3-0.8 part;
Glucoside bactericide 0.1-0.4 part;
Antioxidant 0.2-0.5 part;
Essence 0.1-0.3 part;
Nano silicon 5-7 part;
Water 80-90 part;
Wherein, the Chinese herbal medicine water extract is that the fleece-flower root, selfheal, the siccative of dandelion exist by following Mandragola In water
After extracting 12 hours, the powder of gained, wherein Mandragola, the fleece-flower root, selfheal, the weight ratio of dandelion is dry For
(1-2):(1-2):(1-2):(1-2).
Wherein, the antioxidant is Accutane sodium.
Wherein, the essence includes agrocybe essence and milk flavour, the preferably weight of agrocybe essence and milk flavour Than for 1: 1.
Wherein, the nano silicon is 600 mesh.
Wherein, the sodium acid carbonate is edible sodium bicarbonate.
A kind of method for preparing agricultural chemicals cleaning agent as described above, comprises the following steps:
1) by the weight ratio by Mandragola, the fleece-flower root, selfheal, the siccative mixing of dandelion, 12 are extracted little in water Shi Hou, extract obtain powder and are Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, Nano silicon and water are mixed by its weight portion.
Prior art is compared, the cleaning agent raw material of the present invention is natural food ingredient, edible, safety, health, environmental protection. Food safety and Health efficiency high, elimination efficiency are high.Common bacteria, general mould and parasite can effectively be killed.This product consumption is low, Only about stoste 10ml need to be added in every kilogram of water during cleaning fruits and vegetables, vegetables and fruits are immersed in 10 minutes in dilution, then flowing water cleaning 2-3 time.
Specific embodiment
Precipitation of protein of the present invention is extracted with reference to some specific embodiments.Specific embodiment is for further in detail The present invention is described, non-limiting protection scope of the present invention.
Used by embodiment, material derives from commercially available.
Method of testing
The detection method of caseinic acid sodium content:Execute according to GB10797.
The detection of residues of pesticides content:
In 1kg water, agricultural chemicals cleaning agent 10ml is added, will be immersed to embodiment and comparative example respectively with a batch of vegetables and fruits In the solution that is prepared, soak 10 minutes, then flowing water cleaning 3 times.
The detection method of the pesticide concentration after washing before washing, according to 19648 series of GB/T, a certain agricultural chemicals related chemistry Pesticides removal rate=(peak areaBefore washing- peak areaAfter washing)/peak areaBefore washing.
Bacteria Detection:GB4789.2.
Mould detects:GB4789.15.
Parasite detects:20 power microscope frame count checks.
Embodiment 1
Agricultural chemicals cleaning agent preparation method:
1) by Mandragola, the fleece-flower root, selfheal, the siccative by weight 1 of dandelion:1:1:1 mixing, extracts 12 in water After hour, extract obtains powder and is Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, The weight portion of nano silicon and water as shown in table 1 is mixed, and obtains agricultural chemicals cleaning agent;
Wherein, the specification of nano silicon used is 600 mesh.
Embodiment 2
Agricultural chemicals cleaning agent preparation method:
1) by Mandragola, the fleece-flower root, selfheal, the siccative by weight 1 of dandelion:2:1:1 mixing, extracts 12 in water After hour, extract obtains powder and is Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, The weight portion of nano silicon and water as shown in table 1 is mixed, and obtains agricultural chemicals cleaning agent;
Wherein, the specification of nano silicon used is 600 mesh.
Embodiment 3
Agricultural chemicals cleaning agent preparation method:
1) by Mandragola, the fleece-flower root, selfheal, the siccative by weight 1 of dandelion:1:2:1 mixing, extracts 12 in water After hour, extract obtains powder and is Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, The weight portion of nano silicon and water as shown in table 1 is mixed, and obtains agricultural chemicals cleaning agent;
Wherein, the specification of nano silicon used is 600 mesh.
Embodiment 4
Agricultural chemicals cleaning agent preparation method:
1) by Mandragola, the fleece-flower root, selfheal, the siccative by weight 1 of dandelion:1:1:2 mixing, extract 12 in water After hour, extract obtains powder and is Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, The weight portion of nano silicon and water as shown in table 1 is mixed, and obtains agricultural chemicals cleaning agent;
Wherein, the specification of nano silicon used is 600 mesh.
Embodiment 5
Agricultural chemicals cleaning agent preparation method:
1) by Mandragola, the fleece-flower root, selfheal, the siccative by weight 1 of dandelion:2:2:1 mixing, extracts 12 in water After hour, extract obtains powder and is Chinese herbal medicine water extract after drying;
2) by step 1) the Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, The weight portion of nano silicon and water as shown in table 1 is mixed, and obtains agricultural chemicals cleaning agent;
Wherein, the specification of nano silicon used is 600 mesh.
Comparative example 1
The weight portion of raw material used as shown in form 1, remaining preparation method are same as Example 1.
Comparative example 2
The weight portion of raw material used as shown in form 1, remaining preparation method are same as Example 2.
Comparative example 3
The weight portion of raw material used as shown in form 1, remaining preparation method are same as Example 3.
Comparative example 4
The weight portion of raw material used as shown in form 1, remaining preparation method are same as Example 4.
Comparative example 5
Nano silicon specification used is 200 mesh, and remaining preparation method is same as Example 5.
After agricultural chemicals cleaning agent obtained in above-described embodiment and comparative example is cleaned with a collection of fruit, detect by GB/T 19648 Residues of pesticides content, calculated structure are listed in Table 1 below.
Comparative example 6
Commercially common fruits and vegetables cleaning agent, is detected by the detection method of above-mentioned residues of pesticides content, its Pesticides removal rate is 68.2%.
Table 1
Embodiments of the invention are the foregoing is only, the scope of the claims of the present invention is not thereby limited, every using this Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks Domain, is included within the scope of the present invention.

Claims (6)

1. a kind of agricultural chemicals cleaning agent, is made up of by its weight portion following components:
Chinese herbal medicine water extract 15-20 part;
Sodium acid carbonate 0.3-0.8 part;
Glucoside bactericide 0.1-0.4 part;
Antioxidant 0.2-0.5 part;
Essence 0.1-0.3 part;
Nano silicon 5-7 part;
Water 80-90 part;
Wherein, the Chinese herbal medicine water extract is that the siccative of dandelion is in water by following Mandragola, the fleece-flower root, selfheal After extracting 12 hours, the powder of gained, wherein Mandragola is dry, the fleece-flower root, selfheal, the weight ratio of dandelion is(1-2): (1-2):(1-2):(1-2).
2. agricultural chemicals cleaning agent as claimed in claim 1, it is characterised in that:The antioxidant is Accutane sodium.
3. agricultural chemicals cleaning agent as claimed in claim 1, it is characterised in that:The essence includes agrocybe essence and milk perfume Essence.
4. agricultural chemicals cleaning agent as claimed in claim 1, it is characterised in that:The nano silicon is 600 mesh.
5. agricultural chemicals cleaning agent as claimed in claim 1, it is characterised in that:The sodium acid carbonate is edible sodium bicarbonate.
6. a kind of method for preparing agricultural chemicals cleaning agent as described in any one of claim 1-5, it is characterised in that comprise the following steps:
1)By the weight ratio by Mandragola, the fleece-flower root, selfheal, the siccative of dandelion mix, after extracting 12 hours in water, Extract obtains powder and is Chinese herbal medicine water extract after drying;
2)By step 1)The Chinese herbal medicine water extract of gained, sodium acid carbonate, glucoside bactericide, antioxidant, essence, nanometer Silica and water are mixed by its weight portion.
CN201610832140.4A 2016-09-19 2016-09-19 A kind of agricultural chemicals cleaning agent and preparation method thereof Pending CN106479694A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610832140.4A CN106479694A (en) 2016-09-19 2016-09-19 A kind of agricultural chemicals cleaning agent and preparation method thereof

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107865354A (en) * 2017-11-17 2018-04-03 江苏名芊生物科技有限公司 A kind of production method of new blackberry, blueberry magma
CN109777668A (en) * 2019-03-18 2019-05-21 浙江省食品药品检验研究院 A kind of the plant source cleaning agent and its application method residual for melon and fruit removal agriculture
CN111264522A (en) * 2018-12-05 2020-06-12 北京康为天生物科技有限公司 Pesticide residue remover and preparation method and application thereof
CN111264521A (en) * 2018-12-05 2020-06-12 北京康为天生物科技有限公司 Pesticide residue remover and preparation method and application thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563313A (en) * 2004-04-06 2005-01-12 中国计量学院 Natural scavenging agent for removing residual pesticide on vegetable and fruitage
CN102604757A (en) * 2012-03-21 2012-07-25 杨成玉 Chinese herbal preparation for removing nuisance pesticides on surface of fruits and vegetables
CN103858865A (en) * 2014-04-01 2014-06-18 杨成玉 Traditional Chinese medicine pesticide detoxification agent
CN104450225A (en) * 2014-11-03 2015-03-25 唐翊珲 Pesticide residue scavenging agent and preparation method thereof
CN104771857A (en) * 2014-01-13 2015-07-15 中国科学院上海微系统与信息技术研究所 Uses of mesoporous silicon oxide nanometer material
CN105238581A (en) * 2015-09-25 2016-01-13 山西振东家庭健康护理用品有限公司 Traditional Chinese medicine washing agent used for fruits and vegetables, and preparation method thereof
CN105779150A (en) * 2016-04-11 2016-07-20 安徽师范大学 Chinese herbal medicine type fruit and vegetable cleaning agent and preparing method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563313A (en) * 2004-04-06 2005-01-12 中国计量学院 Natural scavenging agent for removing residual pesticide on vegetable and fruitage
CN102604757A (en) * 2012-03-21 2012-07-25 杨成玉 Chinese herbal preparation for removing nuisance pesticides on surface of fruits and vegetables
CN104771857A (en) * 2014-01-13 2015-07-15 中国科学院上海微系统与信息技术研究所 Uses of mesoporous silicon oxide nanometer material
CN103858865A (en) * 2014-04-01 2014-06-18 杨成玉 Traditional Chinese medicine pesticide detoxification agent
CN104450225A (en) * 2014-11-03 2015-03-25 唐翊珲 Pesticide residue scavenging agent and preparation method thereof
CN105238581A (en) * 2015-09-25 2016-01-13 山西振东家庭健康护理用品有限公司 Traditional Chinese medicine washing agent used for fruits and vegetables, and preparation method thereof
CN105779150A (en) * 2016-04-11 2016-07-20 安徽师范大学 Chinese herbal medicine type fruit and vegetable cleaning agent and preparing method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107865354A (en) * 2017-11-17 2018-04-03 江苏名芊生物科技有限公司 A kind of production method of new blackberry, blueberry magma
CN107865354B (en) * 2017-11-17 2020-10-02 江苏名芊生物科技有限公司 Production method of blackberry raw pulp
CN111264522A (en) * 2018-12-05 2020-06-12 北京康为天生物科技有限公司 Pesticide residue remover and preparation method and application thereof
CN111264521A (en) * 2018-12-05 2020-06-12 北京康为天生物科技有限公司 Pesticide residue remover and preparation method and application thereof
CN109777668A (en) * 2019-03-18 2019-05-21 浙江省食品药品检验研究院 A kind of the plant source cleaning agent and its application method residual for melon and fruit removal agriculture

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Application publication date: 20170308