CN110438802A - It is a kind of to have effects that the purified cotton cloth of disinfection and sterilization and its preparation process - Google Patents
It is a kind of to have effects that the purified cotton cloth of disinfection and sterilization and its preparation process Download PDFInfo
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- CN110438802A CN110438802A CN201910671608.XA CN201910671608A CN110438802A CN 110438802 A CN110438802 A CN 110438802A CN 201910671608 A CN201910671608 A CN 201910671608A CN 110438802 A CN110438802 A CN 110438802A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/1845—Aromatic mono- or polycarboxylic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- General Chemical & Material Sciences (AREA)
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Abstract
The present invention relates to functional cloth technical fields, specially a kind of to have effects that the purified cotton cloth of disinfection and sterilization and its preparation process；Elder, passionflower, rosemary and camomile extract in the present invention mutually cooperate with, not only have effects that good antibacterial and sterilization, and strengthen the function of skin metabolism, increase the activity of skin surface cell and the wettability of skin surface, accelerates skin renewal；It is mutually cooperateed between no foul smell garlic powder, high mallow and mustard seed section plant, good antibacterial action can not only be played, and there is anti-inflammatory and its soft and moist smooth surface skin, while there is certain anti-corrosion function.Cationic surfactant and ultrasonic mixing cooperate so that medical fluid mixes more uniform, raising drug effect.The use of sterile silver-series antibacterial agent, further increases antibiotic effect.High mallow, no foul smell garlic powder and preservative cooperate, and not only improve the holding time of drug effect, moreover it is possible to which the toxin for removing skin surface further increases the effect of bactericidal antiphlogistic.
Description
Technical field
The present invention relates to functional cloth technical field, specially it is a kind of have effects that the purified cotton cloth of disinfection and sterilization and its
Preparation process.
Background technique
Health care is increasingly paid attention to now with people, not only to carry out skin before every medical treatment and nursing operation
Disinfection, also increasingly pay attention to disinfection treatment in people's daily life, disinfection cotton increasingly becomes a kind of indispensable
Daily necessities, a kind of its promotion product as paper handkerchief, cloths for cleaning in our daily lifes has cleaning, disinfection function, and
It is easy to carry, using simple.The cleaning of aseptic cotton, disinfection function determine that it manufactures raw material and must have soft, water imbibition
By force, anti-inflammatory, sterilization, it is ensured that the surface to be cleaned does not have the residual objects such as slag wool, silk weaving hair and water mark.As people increasingly field is raw
Deposit exploration, unavoidably will appear it is some abrade the small wounds bled, such as use it is portable, using simple and there is anti-inflammatory to kill virus function
The pure cotton cloth of effect, can avoid when because of injury that anti-inflammation and sterilization measure is not in place, occurs secondary inflammatory complication afterwards, increases patient's energy
Pain.
Applicant retrieves the prior art 1 (CN106474350) and discloses a kind of plant antibiotic compound spray by retrieval
Agent and preparation method thereof, mainly by Rhizoma Gastrodiae, radix scutellariae, viola mandshurica, kuh-seng, the fruit of summer cypress, favus skin, calyx meto, granatum, garden burnet
And surfactant, cosurfactant etc. are constituted.Plant antibiotic compound spray of the invention, be it is a kind of significant in efficacy and
The skin preparation for external use not recurred does not add any Western medicine element, and residual hazard pollution-free to human and environment.Clinical test of the present invention
It is completed, obvious effective rate reaches 95% or more；Total is effectively 99% or more.Pass through the synergistic effect between each raw material, antibacterial anti-inflammatory effect
Fruit is good, has no stimulation of the skin, without allergic phenomena.It can be used for treating tinea pedis, burn and scald and acne, simultaneously for body
Also there is good curative effect at other positions by fungus-caused tinea scabies and skin disease.
A kind of preparation method of plant antibiotic compound spray, it is characterised in that the following steps are included:
1) surfactant, cosurfactant, Rhizoma Gastrodiae, radix scutellariae, viola mandshurica, the kuh-seng, summer cypress of formula rate are weighed
Son, favus skin, calyx meto, granatum, garden burnet, sodium chloride, 50% ethyl alcohol, methyl p-hydroxybenzoate are spare；
2) Chinese medicine is put into reflux unit, the water of 10-20 times of Chinese medicine weight, heating and refluxing extraction is added into container
1.5-3h, filtering, the dregs of a decoction add the water of 10-20 times of Chinese medicine total weight, and heating and refluxing extraction 1.5-3h merges gained filter twice
Liquid concentrates the filtrate to the raw medicine concentration of 0.2-0.8g/ml, through 8000rpm, is centrifuged in 10min, takes supernatant, spare；
3) surfactant of 25-40 parts by weight is added in Xiang Shangshu Chinese medicine extract, stirs 30min, adds 10-20
The cosurfactant of parts by weight, the sodium chloride of 5-10 parts by weight continue stirring and make it completely dissolved, obtains solution A；
4) it takes 50% ethyl alcohol of 2-10 parts by weight, is added the methyl p-hydroxybenzoate of 0.6-1.2 parts by weight, under 200rpm
20min is stirred, solution B is obtained；
5) B solution is poured into solution A, stirs 30min under 200rpm, mixes well above-mentioned substance, at 115-121 DEG C
Sterilize 10-20min；Self be cooled to room temperature after be distributed into aerosol bottle to get.
Above-mentioned antibiotic compound spray in the prior art can not be used for cotton, and antibacterial effect is bad, currently, city
Few on field to sell the pure cotton cloth with disinfection and sterilization, the pure cotton function of the disinfection and sterilization effect not only sold is more single
One, and anti-inflammation and sterilization effect is poor, is not suitable for hospital and field exploration.
Based on this, the present invention devise it is a kind of have effects that the purified cotton cloth of disinfection and sterilization and its preparation process, with solve
The above problem.
Summary of the invention
In view of the above problems, the present invention provides a kind of moisturizing antimicrobial form wet tissues and preparation method thereof, for solving
Certainly proposed in background technique the technical issues of.
To achieve the above object, the following technical solution is employed by the present invention:
A kind of have effects that the purified cotton cloth of disinfection and sterilization, the purified cotton cloth with disinfection and sterilization by substrate and
The arrangement medical fluid composition being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight: no foul smell garlic powder 15-
20 parts, plant 4-7 parts of mustard seed section, 6-10 parts of elder, 8-12 parts of rosemary, 6-12 parts of passionflower, 8-15 parts of high mallow, sterile silver
1-2 parts of series antibacterial agent, 5-9 parts of camomile extract, preservative O.5-1.0 part, 1.5-2.3 parts of cationic surfactant, chelating
0.3~0.6 part and 150~180 parts of deionized water of agent.
Further, the substrate selects fine fleece cotton.
Further, the preservative selects one of anesin, benzoic acid and sorbic acid.
Further, the cationic surfactant selects chlorobenzene bundle to press.
Further, the chelating agent selects disodium ethylene diamine tetraacetate.
Further, the camomile extract extraction process are as follows:
D, clean camomile is selected, 100-200 targeted fine powder is ground to after drying naturally, then by camomile fine powder and 50%
Ethanol solution 1: 20~40mg/mL in mass ratio mixing, through frequency be 20KHz ultrasonic echography extract, extraction 10min, then
It is filtered, obtains filtrate；
E, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, and elution speed is
0.8ml/min obtains the camomile extract of high-purity after recovered；
It f, is in mass ratio 1: 20~40 to mix to get camomile extraction by the camomile extract of high-purity and deionized water
Liquid.
A kind of preparation process with the purified cotton cloth of disinfection and sterilization:
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 10-20min in S1, soft and ventilative processing is carried out；
S3: it by mustard seed section plant, elder, rosemary, passionflower and high mallow with after clear water washes clean, is placed under sunlight
Naturally dry, then respectively through crushing and milled processed, obtaining partial size is the no foul smell garlic powder of 100~200 mesh, the plant of mustard seed section
Object, elder, rosemary, passionflower and the fine powder of high mallow, save respectively, spare；
S4: by the fine powder and no foul smell garlic powder of gained mustard seed section plant, elder, rosemary, passionflower and high mallow in S1
It is transferred in deionized water, and is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 30-40min, through filtration treatment
Afterwards, the dregs of a decoction are discarded, medical fluid is retained；
S5: load weighted sterile silver-series antibacterial agent being added after medical fluid is naturally cooling to 50-60 DEG C, and ultrasonic agitation 10~
20min, gained are denoted as mixed component；
S6: mixed component is naturally cooling to 30-40 DEG C, then remaining ingredient is transferred in mixed component, ultrasonic mixing
20~30min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
S8: carrying out natural-dehydration for the substrate after padding obtained by S7, and controls more than moisture that rate is in 10-20%, to de-
Substrate after water is being connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed, had by lower natural air drying
The purified cotton cloth finished product of disinfection and sterilization effect.
Using above-mentioned technical solution, the beneficial effect that the present invention reaches is:
1, elder, passionflower, rosemary and camomile extract mutually cooperate with, not only with good antibacterial and sterilization
Effect, and strengthen the function of skin metabolism, increase the activity of skin surface cell and the wettability of skin surface, accelerates
Skin renewal.After pure cotton cloth and injured skin sites contact, the tissue of medicine components and injury which has
Liquid combines, and accelerates sterilization of the medicine components to injury.
2, it is mutually cooperateed between no foul smell garlic powder, high mallow and mustard seed section plant, good antibacterial action can not only be played, and
And there is anti-inflammatory and its soft and moist smooth surface skin, while there is certain anti-corrosion function.Cationic surfactant and ultrasound
Mutual cooperation is mixed so that increasing the more uniform of medical fluid mixing, drug effect is improved, that is, improves and sterilize and anti-inflammatory effect.It is sterile
The use of silver-series antibacterial agent, further increases antibiotic effect.In addition, high mallow, no foul smell garlic powder and preservative cooperate, not only
The holding time for improving drug effect further increases the effect of bactericidal antiphlogistic moreover, the toxin of skin surface can be removed.
3, camomile is isolated and purified using NKA absorption resin, not only increases the purity of camomile extract, Er Qiejian
Change camomile extract extraction process, compared with traditional organic solvent extractionprocess, reduces the use of organic solvent, resin is repeatable
It utilizes, improves economic benefit.Meanwhile substrate is placed in and arranges second dipping and rolling in medical fluid, may make and arranges effective component in medical fluid
Into in the interval between substrate molecule, so that anti-inflammation and sterilization function is more lasting.
Furthermore 4, use fine fleece cotton to be made into plain weave cloth as substrate, not only can increase the aeration of pure cotton cloth, but also
When it is wrapped at patient injury, patient's sense can be made soft not thick and solid, increase comfort.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described.Based on the embodiment of the present invention, the common skill in this field
Art personnel every other embodiment obtained without creative efforts belongs to the model that the present invention protects
It encloses.
Embodiment 1:
A kind of have effects that the purified cotton cloth of disinfection and sterilization, the purified cotton cloth with disinfection and sterilization by substrate and
The arrangement medical fluid composition being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight: no foul smell garlic powder 15
It is part, 4 parts of mustard seed section plant, 8 parts of elder, 8 parts of rosemary, 10 parts of passionflower, 12 parts of high mallow, 1 part of sterile silver-series antibacterial agent, sweet
5 parts of chrysanthemum extracting solution, 0.7 part of preservative, 1.5 parts of cationic surfactant, 0.3 part of chelating agent and 150 parts of deionized water.
The substrate selects fine fleece cotton.
The preservative selects benzoic acid.
The cationic surfactant selects chlorobenzene bundle to press.
The chelating agent selects disodium ethylene diamine tetraacetate.
The camomile extract extraction process are as follows:
A, clean camomile is selected, 100 targeted fine powders are ground to after fried dry, it is then that the ethyl alcohol of camomile fine powder and 50% is molten
Liquid in mass ratio 1: 20mg/mL mixes, and is the extraction of 20KHz ultrasonic echography through frequency, extracting 10min must filter using filter
Liquid；
B, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, and elution speed is
0.8ml/min obtains filtrate using filter；
C, be in mass ratio with deionized water by the camomile extract of high-purity 1: 20mg/mL mix to get camomile extraction
Liquid.
A kind of preparation process with the purified cotton cloth of disinfection and sterilization:
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 10min in S1, soft and ventilative processing is carried out；
S3: it by mustard seed section plant, elder, rosemary, passionflower and high mallow with after clear water washes clean, is placed under sunlight
Naturally dry, then respectively through crushing and milled processed, obtaining partial size is the no foul smell garlic powder of 100 mesh, mustard seed section plant, synthetism
Wood, rosemary, passionflower and the fine powder of high mallow, save respectively, spare；
S4: by the fine powder and no foul smell garlic powder of gained mustard seed section plant, elder, rosemary, passionflower and high mallow in S1
It is transferred in deionized water, and is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 30min, after filtration treatment,
The dregs of a decoction are discarded, medical fluid is retained；
Load weighted sterile silver-series antibacterial agent: being added after medical fluid is naturally cooling to 50 DEG C, 10min be stirred by ultrasonic by S5,
Gained is denoted as mixed component；
S6: mixed component is naturally cooling to 30 DEG C, then remaining ingredient is transferred in mixed component, ultrasonic mixing
20min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
S8: carrying out natural-dehydration for the substrate after padding obtained by S7, and controls more than moisture that rate is 10%, after dehydration
Substrate be connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed by lower natural air drying, obtains having disinfection
The purified cotton cloth finished product of biocidal efficacies.
Embodiment 2:
A kind of have effects that the purified cotton cloth of disinfection and sterilization, the purified cotton cloth with disinfection and sterilization by substrate and
The arrangement medical fluid composition being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight: no foul smell garlic powder 20
Part, 6 parts of mustard seed section plant, 10 parts of elder, 12 parts of rosemary, 6 parts of passionflower, 15 parts of high mallow, sterile silver-series antibacterial agent 1.4
Part, 7 parts of camomile extract, 0.5 part of preservative, 1.8 parts of cationic surfactant, 0.5 part of chelating agent and deionized water 160
Part.
The substrate selects fine fleece cotton.
The preservative selects benzoic acid.
The cationic surfactant selects chlorobenzene bundle to press.
The chelating agent selects disodium ethylene diamine tetraacetate.
The camomile extract extraction process are as follows:
A, clean camomile is selected, 100 targeted fine powders are ground to after fried dry, it is then that the ethyl alcohol of camomile fine powder and 50% is molten
Liquid in mass ratio 1: 25mg/mL mixes, and is the extraction of 20KHz ultrasonic echography through frequency, extracting 10min must filter using filter
Liquid；
B, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, and elution speed is
0.8ml/min obtains filtrate using filter；
C, be in mass ratio with deionized water by the camomile extract of high-purity 1: 25mg/mL mix to get camomile extraction
Liquid.
A kind of preparation process with the purified cotton cloth of disinfection and sterilization:
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 15min in S1, soft and ventilative processing is carried out；
S3: it by mustard seed section plant, elder, rosemary, passionflower and high mallow with after clear water washes clean, is placed under sunlight
Naturally dry, then respectively through crushing and milled processed, obtaining partial size is the no foul smell garlic powder of 100 mesh, mustard seed section plant, synthetism
Wood, rosemary, passionflower and the fine powder of high mallow, save respectively, spare；
S4: by the fine powder and no foul smell garlic powder of gained mustard seed section plant, elder, rosemary, passionflower and high mallow in S1
It is transferred in deionized water, and is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 30min, after filtration treatment,
The dregs of a decoction are discarded, medical fluid is retained；
Load weighted sterile silver-series antibacterial agent: being added after medical fluid is naturally cooling to 55 DEG C, 15min be stirred by ultrasonic by S5,
Gained is denoted as mixed component；
S6: mixed component is naturally cooling to 35 DEG C, then remaining ingredient is transferred in mixed component, ultrasonic mixing
20min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
Substrate after padding obtained by S7 is carried out natural-dehydration by S8, and controls more than moisture that rate is 10%, after dehydration
Substrate be connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed by lower natural air drying, obtains having disinfection
The purified cotton cloth finished product of biocidal efficacies.
Embodiment 3:
A kind of have effects that the purified cotton cloth of disinfection and sterilization, the purified cotton cloth with disinfection and sterilization by substrate and
The arrangement medical fluid composition being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight: no foul smell garlic powder 18
It is part, 7 parts of mustard seed section plant, 6 parts of elder, 10 parts of rosemary, 12 parts of passionflower, 8 parts of high mallow, 2 parts of sterile silver-series antibacterial agent, sweet
9 parts of chrysanthemum extracting solution, 1.0 parts of preservative, 2.3 parts of cationic surfactant, 0.6 part of chelating agent and 170 parts of deionized water.
The substrate selects fine fleece cotton.
The preservative selects anesin.
The cationic surfactant selects chlorobenzene bundle to press.
The chelating agent selects disodium ethylene diamine tetraacetate.
The camomile extract extraction process are as follows:
A, clean camomile is selected, 100 targeted fine powders are ground to after fried dry, it is then that the ethyl alcohol of camomile fine powder and 50% is molten
Liquid in mass ratio 1: 30mg/mL mixes, and is the extraction of 20KHz ultrasonic echography through frequency, extracting 10min must filter using filter
Liquid；
B, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, and elution speed is
0.8ml/min obtains filtrate using filter；
C, be in mass ratio with deionized water by the camomile extract of high-purity 1: 30mg/mL mix to get camomile extraction
Liquid.
A kind of preparation process with the purified cotton cloth of disinfection and sterilization:
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 15min in S1, soft and ventilative processing is carried out；
S3: it by mustard seed section plant, elder, rosemary, passionflower and high mallow with after clear water washes clean, is placed under sunlight
Naturally dry, then respectively through crushing and milled processed, obtaining partial size is the no foul smell garlic powder of 100 mesh, mustard seed section plant, synthetism
Wood, rosemary, passionflower and the fine powder of high mallow, save respectively, spare；
S4: by the fine powder and no foul smell garlic powder of gained mustard seed section plant, elder, rosemary, passionflower and high mallow in S1
It is transferred in deionized water, and is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 30min, after filtration treatment,
The dregs of a decoction are discarded, medical fluid is retained；
Load weighted sterile silver-series antibacterial agent: being added after medical fluid is naturally cooling to 60 DEG C, 20min be stirred by ultrasonic by S5,
Gained is denoted as mixed component；
S6: mixed component is naturally cooling to 30 DEG C, then remaining ingredient is transferred in mixed component, ultrasonic mixing
30min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
S8: carrying out natural-dehydration for the substrate after padding obtained by S7, and controls more than moisture that rate is 15%, after dehydration
Substrate be connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed by lower natural air drying, obtains having disinfection
The purified cotton cloth finished product of biocidal efficacies.
Embodiment 4:
It is a kind of to have effects that the purified cotton cloth of disinfection and sterilization, it is characterised in that: described to have effects that the pure cotton of disinfection and sterilization
Cloth is made of substrate and the arrangement medical fluid being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight:
17 parts of no foul smell garlic powder, 5 parts of mustard seed section plant, 9 parts of elder, 11 parts of rosemary, 8 parts of passionflower, 10 parts of high mallow, sterile silver system
1.7 parts of antibacterial agent, 8 parts of camomile extract, 0.9 part of preservative, 2.O parts of cationic surfactant, 0.4 part of chelating agent and go from
180 parts of sub- water.
The substrate selects fine fleece cotton.
The preservative selects sorbic acid.
The cationic surfactant selects chlorobenzene bundle to press.
The chelating agent selects disodium ethylene diamine tetraacetate.
The camomile extract extraction process are as follows:
A, clean camomile is selected, 100 targeted fine powders are ground to after fried dry, it is then that the ethyl alcohol of camomile fine powder and 50% is molten
Liquid in mass ratio 1: 40mg/mL mixes, and is the extraction of 20KHz ultrasonic echography through frequency, extracting 10min must filter using filter
Liquid；
B, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, and elution speed is
0.8ml/min obtains filtrate using filter；
C, be in mass ratio with deionized water by the camomile extract of high-purity 1: 40mg/mL mix to get camomile extraction
Liquid.
A kind of preparation process with the purified cotton cloth of disinfection and sterilization:
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 20min in S1, soft and ventilative processing is carried out；
S3: it by mustard seed section plant, elder, rosemary, passionflower and high mallow with after clear water washes clean, is placed under sunlight
Naturally dry, then respectively through crushing and milled processed, obtaining partial size is the no foul smell garlic powder of 100 mesh, mustard seed section plant, synthetism
Wood, rosemary, passionflower and the fine powder of high mallow, save respectively, spare；
S4: by the fine powder and no foul smell garlic powder of gained mustard seed section plant, elder, rosemary, passionflower and high mallow in S1
It is transferred in deionized water, and is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 40min, after filtration treatment,
The dregs of a decoction are discarded, medical fluid is retained；
Load weighted sterile silver-series antibacterial agent: being added after medical fluid is naturally cooling to 50 DEG C, 10min be stirred by ultrasonic by S5,
Gained is denoted as mixed component；
S6: mixed component is naturally cooling to 30 DEG C, then remaining ingredient is transferred in mixed component, ultrasonic mixing
30min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
S8: carrying out natural-dehydration for the substrate after padding obtained by S7, and controls more than moisture that rate is 20%, after dehydration
Substrate be connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed by lower natural air drying, obtains having disinfection
The purified cotton cloth finished product of biocidal efficacies.
Properties of product detection:
Purified cotton cloth and commercially available pure cotton prepared by embodiment 1, embodiment 2, embodiment 3 and embodiment 4 in the present invention
Cloth carries out anti-microbial property test, described in test result is as follows table:
As seen from the above table, the antibiotic property of cloth prepared by the present invention is substantially better than comparative example.Show production prepared by the present invention
Product overall performance is more preferable than comparative example, has better market popularization value.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these modification or
Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.
Claims (6)
1. a kind of have effects that the purified cotton cloth of disinfection and sterilization, it is characterised in that: described to have effects that the pure cotton cloth of disinfection and sterilization
Material is made of substrate and the arrangement medical fluid being carried on the substrate；The arrangement medical fluid is grouped as by the group of following parts by weight: nothing
Smelly garlic powder 15-20 parts, plant 4-7 parts of mustard seed section, 6-10 parts of elder, 8-12 parts of rosemary, 6-12 parts of passionflower, high mallow 8-
15 parts, silver-series antibacterial agent 1-2 parts sterile, 5-9 parts of camomile extract, 0.5-1.0 parts of preservative, cationic surfactant 1.5-
2.3 parts, 0.3~0.6 part of chelating agent and 150~180 parts of deionized water；
The camomile extract extraction process are as follows:
A, clean camomile is selected, 100-200 targeted fine powder is ground to after drying naturally, then by camomile fine powder and 50% second
Alcoholic solution 1: 20~40mg/mL in mass ratio mixing is the extraction of 20KHz ultrasonic echography through frequency, extracts 10min, using
Filter, obtains filtrate；
B, filtrate is isolated and purified through NKA absorption resin, selecting 80% ethyl alcohol is eluant, eluent, elution speed 0.8ml/
Min obtains the camomile extract of high-purity after recovered；
It c, is in mass ratio that 1: 20~40mg/mL mixes to get camomile extraction with deionized water by the camomile extract of high-purity
Liquid.
A kind of has effects that the purified cotton cloth of disinfection and sterilization 2. according to claim 1, it is characterised in that: the substrate choosing
With fine fleece cotton.
A kind of has effects that the purified cotton cloth of disinfection and sterilization 3. according to claim 1, it is characterised in that: the preservative
Select one of anesin, benzoic acid and sorbic acid.
A kind of has effects that the purified cotton cloth of disinfection and sterilization 4. according to claim 1, it is characterised in that: the cation
Surfactant selects chlorobenzene bundle to press.
A kind of has effects that the purified cotton cloth of disinfection and sterilization 5. according to claim 1, it is characterised in that: the chelating agent
Select disodium ethylene diamine tetraacetate.
6. a kind of preparation process with the purified cotton cloth of disinfection and sterilization according to claim 1, it is characterised in that:
It is described.
S1: fine fleece cotton is made into plain weave cloth；
S2: after gained plain weave cloth is soaked in ethanol solution 10-20min in S1, soft and ventilative processing is carried out；
S3: mustard seed section plant, elder, rosemary, passionflower and high mallow is natural with after clear water washes clean, being placed under sunlight
Dry, then respectively through crush and milled processed, obtain partial size be 100~200 mesh no foul smell garlic powder, mustard seed section plant, connect
Bone wood, rosemary, passionflower and high mallow fine powder, save respectively, it is spare；
S4: the fine powder and no foul smell garlic powder of gained mustard seed section plant in S1, elder, rosemary, passionflower and high mallow are transferred to
In deionized water, and it is heated to fluidized state, and ultrasonic vibration simultaneously, digestion time 30-40min is abandoned after filtration treatment
The dregs of a decoction are removed, medical fluid is retained；
S5: load weighted sterile silver-series antibacterial agent being added after medical fluid is naturally cooling to 50-60 DEG C, and ultrasonic agitation 10~
20min, gained are denoted as mixed component；
S6: being naturally cooling to 30-40 DEG C for mixed component, then remaining ingredient be transferred in mixed component, and ultrasonic mixing 20~
30min, gained are to arrange medical fluid；
S7: gained substrate in S2 is put into and arranges second dipping and rolling in medical fluid；
S8: carrying out natural-dehydration for the substrate after padding obtained by S7, and controls more than moisture that rate is in 10-20%, after dehydration
Substrate be connected with the sterile N of high temperature2Substrate is taken out later and sealed, sterile is packed by lower natural air drying, obtains having disinfection
The purified cotton cloth finished product of biocidal efficacies.
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| CN201910671608.XA CN110438802A (en) | 2019-07-24 | 2019-07-24 | It is a kind of to have effects that the purified cotton cloth of disinfection and sterilization and its preparation process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112376269A (en) * | 2020-11-17 | 2021-02-19 | 国佳新材湖北环保凝胶产业园有限公司 | Aerogel composite fiber felt structural member and preparation method thereof |
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| CN112376269A (en) * | 2020-11-17 | 2021-02-19 | 国佳新材湖北环保凝胶产业园有限公司 | Aerogel composite fiber felt structural member and preparation method thereof |
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