CN110368336A - A kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application - Google Patents
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application Download PDFInfo
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- CN110368336A CN110368336A CN201910641574.XA CN201910641574A CN110368336A CN 110368336 A CN110368336 A CN 110368336A CN 201910641574 A CN201910641574 A CN 201910641574A CN 110368336 A CN110368336 A CN 110368336A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application.Present invention firstly provides a kind of Fructus Platycaryae strobilaceac preface skin care compositions, based on the skin care compositions, the present invention also provides a kind of Fructus Platycaryae strobilaceac preface facial treatment milk, it is prepared by the Fructus Platycaryae strobilaceac preface skin care compositions, pass through optimization reasonable mixture ratio of components collocation, the smell faint scent of the facial treatment milk, apparent condition, stretchability, exquisiteness, vicidity, salubrious property are good, hot and cold stability is good, with stronger antibiotic and sterilizing effect, content of microorganisms complies with standard, and moisture-keeping efficacy is brilliant, has stronger DPPH free radical scavenging ability.In addition, the preparation method of the facial treatment milk is simple, and it is at low cost, it is with a wide range of applications in the preparation of cosmetics.
Description
Technical field
The invention belongs to cosmetics research and development technology fields.More particularly, to a kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its
Preparation method and application.
Background technique
As the improvement of people's living standards, people especially pay attention to skin nursing, skin nursing products in daily life
It has been an indispensable daily necessities for modern female.But due to the growth at age and undesirable life
Mode and air-conditioning, environmental pollution, Seasonal conversion bring temperature change and pressure living, cause the skin condition of people to be deteriorated.
In order to meet the needs of people are to skin care, based on mineral oil, all kinds of chemical toilets for adding different natural flavors are in succession absurd fantastic
It is raw.However, conventional synthesis class cosmetics are due to often resulting in skin containing there are many ingredients such as chemical classes ingredient, heavy metal classes antibacterial agents
Skin damage is even disfeatured.It analyzes according to statistics, safety problem caused by chemical substance is exceeded is cosmetics especially skin care item safety
The main reason for problem, safety problem caused by such as light spot, oxidation resistant hydroquinone are exceeded account for 38%；The perboric acid of antibacterial
Sodium excessive problem accounts for 11.5%.Chemical classes whitening, anti-oxidant, antibacterial additives excessive uses endanger skin care item safety
Main problem.And plant extract has the inherent advantages such as functional activity is strong, toxic side effect is small, in replacement traditional skin care product
Learning has potential Development volue on additive.
Fructus Platycaryae strobilaceac preface is the fruit of juglandaceae plant Platycarya strobilacea (Plotytarya strohilacea Sieb et Zuce)
Sequence, infructescence strobiloid, ovate-elliptic to oblong cylinder.Natural Fructus Platycaryae strobilaceac preface as a kind of Common Chinese Herbs,
It with blood-activating and qi-promoting, detumescence, relieves pain, go tinea, desinsection antipruritic and other effects, be usually used in swollen internal injury chest, abdominal pain, traumatic injury, wet sore
Etc. illnesss.Existing research has significant antibacterial, clear it has been found that containing a large amount of polyphenol and flavones in infructescence of Platycarya strobilacea Sieb.et Zucc. Extract
Except free radical activity；In addition, Fructus Platycaryae strobilaceac preface has special fragrance, essence can be partially substituted.
Existing patent CN105534764A discloses a kind of for the compound pine peel composition of skin nursing and its preparation
A kind of compound pine has been prepared by selected a variety of Chinese herbal medicines and Chinese herbal medicine extract including dyetree fruit in method
Wood skin composition improves skin, and has and prevent and treat dermopathic effect.Existing patent CN107412098A is disclosed
A kind of nti-freckle reparation facial mask, the combination of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, Root of Buchtorm Libanotis extract and Radix et Rhizoma Smilacis Ripariae extract is prepared and is dispelled
Spot repairs facial mask, has effects that clean epidermis, whitening spot-removing.It but is to mention Fructus Platycaryae strobilaceac preface in the above existing patent
Object and other plurality of Chinese extract combinations are taken, skin care item are prepared, there is the problems such as preparation process is complicated, higher cost.
There has been no the reports being individually applied to infructescence of Platycarya strobilacea Sieb.et Zucc. Extract in cosmetics at present.
Summary of the invention
The technical problem to be solved by the present invention is to overcome individually be applied to change by infructescence of Platycarya strobilacea Sieb.et Zucc. Extract in the prior art
Blank in cosmetic provides a kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application.
The object of the present invention is to provide a kind of Fructus Platycaryae strobilaceac preface skin care compositions.
It is a further object of the present invention to provide the Fructus Platycaryae strobilaceac preface skin care compositions to prepare the application in cosmetics.
It is yet another object of the invention to provide a kind of Fructus Platycaryae strobilaceac preface facial treatment milk.
Another object of the present invention is to provide the preparation method of above-mentioned facial treatment milk.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
It is in parts by weight, composed of the following components: 18 present invention firstly provides a kind of Fructus Platycaryae strobilaceac preface skin care compositions
4~10 parts of alcohol, 0.5~3 part of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4~10 parts of 1,3 butylene glycol, Glycerin, mixed triester with caprylic acid capric acid (GTCC) 1~5
Part, 1~3 part of polyoxyethylene (2) stearyl ether (Brij721), 1~3 part of monoglyceride, 0.5~1.5 part of dimethicone, essence
0.1~0.3 part, (bi-imidazolidinyl urea-iodo propinyl butyl methylamine acid esters-propylene glycol is compound by preservative Germall plus
Object) 0.1~0.3 part, 100 parts are complemented to water.
Octadecyl alcolol is the base stock of cosmetics cream, facial treatment milk, and it is one that the performance for thickening emulsion is stronger than hexadecanol
Kind emulsion stabilizer；Infructescence of Platycarya strobilacea Sieb.et Zucc. Extract will affect the performances such as the appearance of facial treatment milk, skin sense, stability；1,3- fourth two
Alcohol is the raw material of plasticizer, can be used as surfactant, plasticiser, Chang Yingyong is in skin care milk.
Preferably, the Fructus Platycaryae strobilaceac preface skin care compositions, it is in parts by weight, composed of the following components: octadecyl alcolol 4~6
Part, 1~3 part of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4~6 parts of 1,3 butylene glycol, 2~4 parts of Glycerin, mixed triester with caprylic acid capric acid (GTCC), polyoxyethylene
(2) 1.5~2.5 parts of stearyl ether (Brij721), 1.5~2.5 parts of monoglyceride, 0.8~1.2 part of dimethicone, essence 0.15
~0.25 part, preservative Germall plus (bi-imidazolidinyl urea-iodo propinyl butyl methylamine acid esters-propanediol complexes)
0.15~0.25 part, 100 parts are complemented to water.
It is highly preferred that the Fructus Platycaryae strobilaceac preface skin care compositions, in parts by weight, composed of the following components: octadecyl alcolol 6
Part, 3 parts of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4 parts of 1,3 butylene glycol, 3 parts of Glycerin, mixed triester with caprylic acid capric acid (GTCC), polyoxyethylene (2) stearyl
2 parts of ether (Brij721), 2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, preservative Germall plus (double imidazolidines
Base urea-iodo propinyl butyl methylamine acid esters-propanediol complexes) 0.2 part, 100 parts are complemented to water.
Above-mentioned Fructus Platycaryae strobilaceac preface skin care compositions is preparing the application in cosmetics, also should protection scope of the present invention it
It is interior.
The present invention also provides a kind of Fructus Platycaryae strobilaceac preface facial treatment milk, by Fructus Platycaryae strobilaceac preface skin care compositions preparation
At.
The present invention also provides the preparation methods of the facial treatment milk, comprising the following steps:
S1. by the parts by weight take octadecyl alcolol, Glycerin, mixed triester with caprylic acid capric acid, polyoxyethylene (2) stearyl ether (Brij721),
Monoglyceride and dimethicone are uniformly mixed, obtain mixture A, take infructescence of Platycarya strobilacea Sieb.et Zucc. Extract and 1,3-BDO, and mixing is equal
It is even, mixture B is obtained, essence and preservative Germall plus are taken, is uniformly mixed, is obtained mixture C, be kept in dark place；
S2. mixture A is heated to 80 DEG C~90 DEG C, and mixture B is heated to 85 DEG C~95 DEG C, by mixture A and mixture B
Mixing is stirred, and is cooled to 35 DEG C~45 DEG C after homogeneous, and mixture C and water is then added, is cooled to room temperature, can be obtained described
Facial treatment milk.
Preferably, the speed of stirring described in step S2 is 40~60rpm.
When mixing speed too fast (> 60rpm), the lotion in this stage have fraction condensation generate gel, be also easy to produce bubble and
Demulsifying phenomenon, stability decline；When mixing speed excessively slow (< 40rpm), the lotion in this stage has fraction is cruelly poly- to generate agglomeration,
It is poor to form emulsion form ability, stability decline.
It is highly preferred that the speed of stirring described in step S2 is 55rpm.
Preferably, the speed of homogeneous described in step S2 is 1000~3000rpm.
When homogeneous excessive velocities (> 3000rpm), the emulsion viscosity in this stage declines, and excessively dilute thick, emulsion system is unstable
It is fixed；When homogeneous speed excessively slow (< 1000rpm), the emulsion viscosity in this stage increases, and homogeneous is insufficient, and emulsion system is unstable
It is fixed.
It is highly preferred that the speed of homogeneous described in step S2 is 2500rpm.
Preferably, in step S2, mixture A is heated to 85 DEG C.
When the heating temperature of mixture A excessively high (90 DEG C of >), the mixture A in this stage accelerates boiling, generates a large amount of gas
Bubble, component content are sharply reduced, are easily evaporated, and cause prepared facial treatment milk stability to decline, emulsion system is unstable；It is mixed
The heating temperature for closing object A is too low (at 80 DEG C of <), and the mixture A in this stage has a small amount of ingredient not melt completely, and reaction is incomplete,
Prepared facial treatment milk stability is caused to decline, emulsion system is unstable.
Preferably, in step S2, mixture B is heated to 90 DEG C.
When the heating temperature of mixture B excessively high (95 DEG C of >), the mixture B in this stage accelerates boiling, generates more gas
Bubble, component content are reduced, and cause prepared facial treatment milk stability to decline, emulsion system is unstable；Mixture B's
Heating temperature is too low (at 80 DEG C of <), and the mixture B in this stage has a small amount of ingredient not melt completely, and reaction not exclusively, leads to institute
The facial treatment milk stability of preparation declines, and emulsion system is unstable.
Preferably, in step S2,40 DEG C are cooled to after homogeneous.
Preferably, the temperature being kept in dark place is 3 DEG C~5 DEG C.
It is highly preferred that the temperature being kept in dark place is 4 DEG C.
The invention has the following advantages:
The present invention provides a kind of Fructus Platycaryae strobilaceac preface skin care compositions, are based on the skin care compositions, the present invention also provides
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk passes through optimization reasonable mixture ratio of components collocation, the gas of obtained Fructus Platycaryae strobilaceac preface facial treatment milk
Taste faint scent, apparent condition, stretchability, exquisiteness, vicidity, salubrious property are good, and smell faint scent, hot and cold stability is good, have relatively strong
Antibiotic and sterilizing effect, content of microorganisms complies with standard, and moisture-keeping efficacy is brilliant, has stronger DPPH free radical scavenging ability.
Wherein, infructescence of Platycarya strobilacea Sieb.et Zucc. Extract is rich in flavones, polyphenol, and the ability with stronger antibacterial and removing free radical can play
The effect of sterilization, moisturizing, delay skin aging.In addition, the preparation method of the facial treatment milk is simple, and it is at low cost, in cosmetics
It is with a wide range of applications in preparation.
Detailed description of the invention
Fig. 1 is the appearance character result figure for the mixture that comparative example 1~3 is prepared；Wherein, figure a is prepared by comparative example 1
The appearance character result figure of obtained mixture；Figure b is the appearance character result figure for the mixture that comparative example 2 is prepared；Scheme c
It is the appearance character result figure for the mixture that comparative example 3 is prepared.
Fig. 2 is the fungistatic effect and inhibition zone size comparison result figure of Fructus Platycaryae strobilaceac preface facial treatment milk；Wherein, being of A figure
Bacteriostasis of the perfume tree infructescence facial treatment milk to pseudomonas aeruginosa；B figure is Fructus Platycaryae strobilaceac preface facial treatment milk to golden yellow grape
The bacteriostasis of coccus；
Fig. 3 is Fructus Platycaryae strobilaceac preface facial treatment milk moisturizing Dependence Results figure in saturation sulfate solution (RH=81%).
Fig. 4 is Fructus Platycaryae strobilaceac preface facial treatment milk moisturizing Dependence Results figure in unsaturated carbonate potassium solution (RH=43%).
Fig. 5 is clearance rate result figure of the infructescence of Platycarya strobilacea Sieb.et Zucc. Extract to DPPH free radical.
Specific embodiment
Further illustrate the present invention below in conjunction with specific embodiment, but embodiment the present invention is not done it is any type of
It limits.Unless stated otherwise, the present invention uses reagent, method and apparatus is the art conventional reagents, method and apparatus.
Unless stated otherwise, following embodiment agents useful for same and material are commercially available.
The preparation of 1 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 10 parts of octadecyl alcolol, Platycarya strobilacea
0.5 part of infructescence extract, 10 parts of 1,3 butylene glycol, 1 part of GTCC, 3 parts of Brij721,1 part of monoglyceride, dimethicone 1.5
Part, 0.1 part of preservative Germall plus, complements to 100 parts with water at 0.3 part of essence.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment, comprising the following steps:
S1. octadecyl alcolol, Brij721, monoglyceride and dimethicone are taken by the parts by weight, is uniformly mixed, must mixes
Object A, takes infructescence of Platycarya strobilacea Sieb.et Zucc. Extract and 1,3-BDO, is uniformly mixed, obtains mixture B, take essence and preservative Germall
Plus is uniformly mixed, obtains mixture C, 4 DEG C are kept in dark place；
S2. mixture A is heated to 85 DEG C, and mixture B is heated to 90 DEG C, and mixture A and mixture B is mixed, stirring,
It is cooled to 40 DEG C after matter, mixture C is then added, is cooled to room temperature, facial treatment milk A1 can be obtained.
The preparation of 2 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 4 parts of octadecyl alcolol, Platycarya strobilacea
3 parts of infructescence extract, 4 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, essence
0.2 part, 0.2 part of preservative Germall plus, 100 parts are complemented to water.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment is same as Example 1, and skin care milk is prepared
Liquid A2.
The preparation of 3 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 4 parts of octadecyl alcolol, Platycarya strobilacea
1 part of infructescence extract, 6 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, essence
0.2 part, 0.2 part of preservative Germall plus, 100 parts are complemented to water.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment is same as Example 1, and skin care milk is prepared
Liquid A3.
The preparation of 4 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 4 parts of octadecyl alcolol, Platycarya strobilacea
3 parts of infructescence extract, 6 parts of 1,3 butylene glycol, 5 parts of GTCC, 1 part of Brij721,3 parts of monoglyceride, 0.5 part of dimethicone, perfume
0.1 part of essence, complements to 100 parts with water at 0.3 part of preservative Germall plus.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment, in addition to mixture A is heated to 80 DEG C, mixture
B is heated to 85 DEG C, and mixture A and mixture B is mixed, stirring, is cooled to 35 DEG C after homogeneous, remaining is same as Example 1,
Facial treatment milk A4 is prepared.
The preparation of 5 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 6 parts of octadecyl alcolol, Platycarya strobilacea
1 part of infructescence extract, 4 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, essence
0.2 part, 0.2 part of preservative Germall plus, 100 parts are complemented to water.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment is same as Example 1, and skin care milk is prepared
Liquid A5.
The preparation of 6 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 6 parts of octadecyl alcolol, Platycarya strobilacea
3 parts of infructescence extract, 4 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, essence
0.2 part, 0.2 part of preservative Germall plus, 100 parts are complemented to water.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment is same as Example 1, and skin care milk is prepared
Liquid A6.
The preparation of 7 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 6 parts of octadecyl alcolol, Platycarya strobilacea
0.5 part of infructescence extract, 6 parts of 1,3 butylene glycol, 5 parts of GTCC, 1 part of Brij721,3 parts of monoglyceride, 0.5 part of dimethicone,
0.1 part of essence, complements to 100 parts with water at 0.3 part of preservative Germall plus.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment, in addition to mixture A is heated to 90 DEG C, mixture
B is heated to 95 DEG C, and mixture A and mixture B is mixed, stirring, is cooled to 45 DEG C after homogeneous, remaining is same as Example 1,
Facial treatment milk A7 is prepared.
The preparation of 8 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
A kind of Fructus Platycaryae strobilaceac preface facial treatment milk is grouped as by following group according to parts by weight: 10 parts of octadecyl alcolol, Platycarya strobilacea
3 parts of infructescence extract, 10 parts of 1,3 butylene glycol, 1 part of GTCC, 3 parts of Brij721,1 part of monoglyceride, 1.5 parts of dimethicone,
0.3 part of essence, complements to 100 parts with water at 0.1 part of preservative Germall plus.
The preparation method of Fructus Platycaryae strobilaceac preface facial treatment milk described in the present embodiment is heated to 90 DEG C in addition to mixture A, mixture B
85 DEG C are heated to, mixture A and mixture B is mixed, is stirred, is cooled to 35 DEG C after homogeneous, remaining is same as Example 1,
Facial treatment milk A8 is prepared.
The composition difference for Fructus Platycaryae strobilaceac preface facial treatment milk A1~A8 that above embodiments 1~8 are prepared is as shown in table 1:
The group for the Fructus Platycaryae strobilaceac preface facial treatment milk that 1 Examples 1 to 8 of table is prepared is grouped as
Comparative example 1
1, experimental method
A kind of mixture is grouped as by following group according to parts by weight: it is grouped as by following group according to parts by weight:
3 parts of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, dimethicone 1
Part, 0.2 part of preservative Germall plus, complements to 100 parts with water at 0.2 part of essence.
The preparation method of mixture described in this comparative example is heated to 100 DEG C in addition to mixture A, and mixture B is heated to 75 DEG C,
Remaining is same as Example 1.
2, experimental result
Shown in a figure of the appearance character result figure for the mixture that this comparative example 1 is prepared as shown in figure 1, it can be seen that should
The not formed emulsion form of mixture, demulsifying phenomenon is serious, and at starchiness, stability is very poor；And glossiness is dark and consolidation in appearance
It is difficult, poor without wire drawing sense, spreadability to provoke provoking property on the stage for difference；Its smearing stage upper heavy feeling is big, is difficult to absorb, without refreshing
It is sliding to feel, is not sticky；Moistening effect is poor.
Comparative example 2
1, experimental method
A kind of mixture is grouped as by following group according to parts by weight: 6 parts of octadecyl alcolol, 4 parts of 1,3-BDO, GTCC
3 parts, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, 0.2 part of preservative Germall plus, with
Water complements to 100 parts.
The preparation method of mixture described in this comparative example is heated to 70 DEG C in addition to mixture A, and mixture B is heated to 105 DEG C,
Remaining is same as Example 1.
2, experimental result
Shown in the b figure of the appearance character result figure for the mixture that this comparative example 2 is prepared as shown in figure 1, it can be seen that should
Mixture is without infructescence fragrant, in the heat-resisting and cold tolerance of 1d, 7d, 14d, 21d and 28d, cold cycling performance and centrifugation
Afterwards without there is lamination, stability is preferable；And glossiness is brighter in appearance and consolidation is preferable, provokes and provokes on the stage
Property is easier to, wire drawing sense is general, spreadability is good；It smears that stage upper heavy feeling is larger, absorbability is general, without smooth sense, more sticky；
Moistening effect is declined.
Comparative example 3
1, experimental method
A kind of mixture is grouped as by following group according to parts by weight: 6 parts of octadecyl alcolol, infructescence of Platycarya strobilacea Sieb.et Zucc. Extract 3
Part, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, preservative Germall plus
0.2 part, 100 parts are complemented to water.
The preparation method of mixture described in this comparative example is heated to 100 DEG C in addition to mixture A, and mixture B is heated to 105
DEG C, remaining is same as Example 1.
2, experimental result
Shown in the c figure of the appearance character result figure for the mixture that this comparative example 3 is prepared as shown in figure 1, it can be seen that should
Easily there is demulsifying phenomenon in mixture, and stability is poor；And glossiness is darker in appearance and consolidation is poor, provokes and chooses on the stage
Rising property is difficult, wire drawing sense is poor, spreadability is general；It smears the stage, and above heavy feeling is big, absorbability is poor, without smooth sense, vicidity
It is poor；Moistening effect is declined.
Comparative example 4
1, experimental method
A kind of mixture is grouped as by following group according to parts by weight: 1 part of octadecyl alcolol, infructescence of Platycarya strobilacea Sieb.et Zucc. Extract 0.1
Part, 2 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, anti-corrosion
0.2 part of agent Germall plus, 100 parts are complemented to water.
The preparation method of mixture described in this comparative example is heated to 70 DEG C in addition to mixture A, and mixture B is heated to 75 DEG C,
Remaining is same as Example 1.
2, experimental result
The mixture that this comparative example 4 is prepared keeps emulsion form ability poor, and stability is poor, is also easy to produce demulsifying phenomenon；
And glossiness is brighter in appearance and consolidation is poor, provokes on the stage that provoking property is general, wire drawing sense is general, spreadability is poor；It is applied
Smearing the stage, above heavy feeling is larger, absorbability is general, smooth sense is preferable, vicidity is stronger；Moistening effect is poor.
Comparative example 5
1, experimental method
A kind of mixture is grouped as by following group according to parts by weight: 15 parts of octadecyl alcolol, infructescence of Platycarya strobilacea Sieb.et Zucc. Extract 5
Part, 15 parts of 1,3 butylene glycol, 3 parts of GTCC, 2 parts of Brij721,2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, anti-corrosion
0.2 part of agent Germall plus, 100 parts are complemented to water.
The preparation method of mixture described in this comparative example is heated to 100 DEG C in addition to mixture A, and mixture B is heated to 105
DEG C, remaining is same as Example 1.
2, experimental result
Mixture that this comparative example 5 is prepared forms that emulsion form ability is poor, and demulsifying phenomenon is more serious, muddy and excessively
Glossy sense, stability are poor；Glossiness is very dark in appearance and consolidation is poor for it, provoke provoking property on the stage is more difficult, wire drawing sense compared with
Difference, spreadability are poor；Its smearing stage is upper, and heavy feeling is larger, be not easy to absorb, smooth sense is general, vicidity is extremely strong；Moistening effect compared with
Difference.
It can be seen that the sense organ for the mixture that comparative example 1~5 is prepared, stabilization from the result of the above comparative example 1~5
The requirement of facial treatment milk is not achieved in property, appearance character, moistening effect etc..
Fructus Platycaryae strobilaceac preface facial treatment milk A1~A8 that above embodiments 1~8 are prepared is tested for the property, comprising:
Sensory evaluation, stability experiment, fungistatic effect test, content of microorganisms measurement, moisture-keeping efficacy test and radicals scavenging effect
Test, specific experiment method and experimental result are as follows:
The sensory evaluation of 9 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
1, experimental method
Using the form of Blind Test, random selection without skin medical history, without the Healthy Youth volunteer of cosmetic allergic contact dermatitis history, male,
Each 12 people of female takes a small amount of configured Fructus Platycaryae strobilaceac preface facial treatment milk sample to be applied to volunteer's inboard arm (3cm × 3cm mark
Remember area) with after ear, whether observation volunteer there is allergic reaction afterwards for 24 hours.
8 sample stochastic averaginas are distributed into 24 volunteers, corresponding 3 volunteers of each sample, with (1 ± 0.1) mg/
cm2Be applied to each volunteer's marked region, after score by indices, indices are evaluated as grading scheme: excellent 9-10
Point；Good 7-8 points；Middle 5-6 points；Poor 3-4 points；Very poor 1-2 point, Score index includes apparent condition, stretchability, exquisiteness, sticky
Property, salubrious property, the average value that each index takes 3 people to score, general comment is the average value of the sum of indices score.
2, experimental result
The Analyses Methods for Sensory Evaluation Results of Fructus Platycaryae strobilaceac preface facial treatment milk is as shown in table 2, it can be seen that Fructus Platycaryae strobilaceac preface facial treatment milk
The Analyses Methods for Sensory Evaluation Results of A2, A3, A5, A6 are all larger than 8.00 points, illustrate the sense organ of Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5, A6
Effect is good.
The Analyses Methods for Sensory Evaluation Results of 2 Fructus Platycaryae strobilaceac preface facial treatment milk of table
The stability experiment of 10 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
According to 9 sensory evaluation of embodiment as a result, using Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5, A6 as sample, test
Whether there is lamination after the heat-resisting and cold tolerance of 1d, 7d, 14d, 21d and 28d, cold cycling performance and centrifugation, has
Body experimental method and experimental result are as follows:
1, experimental method
(1) heat resistance test experiments
Two parts of equivalent samples are respectively taken from Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5 and A6, a copy of it is placed in 40 ±
It in 1 DEG C of constant incubator, is taken out respectively at 1d, 7d, 14d, 21d and 28d, after restoring room temperature, is often placed in room temperature with another
Sample be compared, observe its whether have it is thinning, discoloration, layering phenomena such as.
(2) cold tolerance test experiments
Two parts of equivalent samples are respectively taken from Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5 and A6, and a copy of it is placed in ice
It in case -5 ± 1 DEG C, is taken out respectively at 1d, 7d, 14d, 21d and 28d, after restoring room temperature, the sample of room temperature is often placed in another
Product are compared, and observe whether it has phenomena such as thinning, discoloration, layering.
(3) cold cycling performance test is tested
Two parts of equivalent samples are respectively taken from Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5 and A6, a copy of it is placed in 40 ±
It 1 day in 1 DEG C of constant incubator, is then placed in again in refrigerator -5 ± 1 DEG C 1 day, after so alternately placing 28 days, after restoring room temperature
The sample that room temperature is often placed in another is compared, and observes whether it has phenomena such as thinning, discoloration, layering.
(4) centrifugation rear stability performance test experiment
Two parts of equivalent samples are respectively taken from Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5 and A6, and a copy of it is placed in centrifugation
About 2/3 height of sample is injected in pipe, after being put into 38 DEG C of baking ovens holding 1h, is moved into centrifuge immediately, is revolved with the revolving speed of 2000r/min
After turning 30min, after restoring room temperature, the sample that room temperature is often placed in another is compared, and observes separation, the layering shape of sample
Condition.
2, experimental result
The stability result of Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5, A6 are as shown in table 3, as can be seen from the results, Platycarya strobilacea
There is lamination, Fructus Platycaryae strobilaceac preface facial treatment milk in heat-resisting, cold-resistant and thermocycling experiment later period in infructescence facial treatment milk A2
There is lamination in the later period of heat-resistant experiment in A3；These results suggest that: the stability of Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3
Difference, and Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 do not occur lamination, excellent in stability.
The stability result of table 3 Fructus Platycaryae strobilaceac preface facial treatment milk A2, A3, A5, A6
Note: "+" indicates layering, and "-" indicates not stratified.
The fungistatic effect test experiments of 11 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
According to 10 stability experiment of embodiment as a result, using Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 as sample, testization is fragrant
The fungistatic effect of infructescence facial treatment milk is set, specific experiment method and experimental result are as follows:
1, experimental method
Each strain respective liquid culture medium of pseudomonas aeruginosa, staphylococcus aureus is prepared into bacteria suspension, uses enzyme
It is 1 that mark instrument, which measures and adjusts bacteria suspension OD value, draws 100 μ L bacteria suspensions and is uniformly applied on corresponding plate using rubbing method, will
Oxford cup is placed on plate, draws 200 μ L for reagent liquid (experimental group: Fructus Platycaryae strobilaceac preface extracting solution, control group: red with liquid-transfering gun
Mycin) after, it is added in Oxford cup, it is parallel that every kind of medical fluid makees 3 samples, then, by pseudomonas aeruginosa, Staphylococcus aureus
Bacterium and escherichia coli, which are placed in 37 DEG C of biochemical cultivation cases, cultivates for 24 hours, measures antibacterial circle diameter with vernier caliper.
2, experimental result
The fungistatic effect and inhibition zone size comparison result of Fructus Platycaryae strobilaceac preface facial treatment milk can be seen as shown in Fig. 2 and table 4
Out, Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 all have significant fungistatic effect to pseudomonas aeruginosa, staphylococcus aureus,
Fructus Platycaryae strobilaceac preface extracting solution is 5mg/mL to the minimal inhibitory concentration (MIC) of pseudomonas aeruginosa, staphylococcus aureus, most
Small bacteriocidal concentration (MBC) is respectively 5mg/mL, 10mg/mL；Therefore, inhibition of the Fructus Platycaryae strobilaceac preface extracting solution to pseudomonas aeruginosa
Ability is most strong.
4 Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 inhibition zone size comparison result of table
The content of microorganisms measurement experiment of 12 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
According to the experimental result of embodiment 10,11, using Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 as sample, Platycarya strobilacea is tested
The content of microorganisms of infructescence facial treatment milk measures effect, and specific experiment method and experimental result are as follows:
1, experimental method
In 2007 editions " cosmetics health specifications " " Micro biological Tests method ", Fructus Platycaryae strobilaceac preface facial treatment milk is examined
Total plate count, yeast and mold sum, colibacillus of excrement sum, staphylococcus aureus sum, P. aeruginosa in A5, A6
Bacterium sum.
2, experimental result
The content of microorganisms measurement result of Fructus Platycaryae strobilaceac preface facial treatment milk is as shown in table 5, it can be seen that Fructus Platycaryae strobilaceac preface shield
Total plate count, yeast and mold sum in skin latex A 5, A6, colibacillus of excrement sum, staphylococcus aureus sum, copper
Green pseudomonad sum meets the standard of limit value, illustrates that Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 are qualified.
The content of microorganisms measurement result of table 5 Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6
The moisture-keeping efficacy test experiments of 13 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment
1, experimental method
By Fructus Platycaryae strobilaceac preface facial treatment milk A5, A6 respectively even application in the 5cm × 5cm glass for posting micropore ventilating adhensive plaster
On plate, applying amount 0.2000g is placed in the drier for filling saturation sulfate solution (RH=81%) and to fill saturated potassium carbonate molten
In the drier of liquid (RH=43%), it is placed in 25 DEG C of constant incubators and keeps constant temperature, claim after 1h, 2h, 4h, 8h, 12h respectively
Weight, calculates its moisturizing rate, and blank assay is arranged by above-mentioned steps in the facial treatment milk that infructescence of Platycarya strobilacea Sieb.et Zucc. Extract ingredient is not added,
It tests three times in parallel, takes its average value；
The calculation formula of moisturizing rate: Rr=Wt/Wo (Wt is different time sections sample quality, and Wo is original quality).
2, experimental result
Fructus Platycaryae strobilaceac preface facial treatment milk saturation sulfate solution (RH=81%) in moisturizing Dependence Results as shown in figure 3,
Fructus Platycaryae strobilaceac preface facial treatment milk is in unsaturated carbonate potassium solution (RH=43%) shown in moisturizing Dependence Results Fig. 4, from Fig. 3 and Fig. 4
As can be seen that the moisture-keeping efficacy of Fructus Platycaryae strobilaceac preface facial treatment milk A6 is better than Fructus Platycaryae strobilaceac preface facial treatment milk A5.In conclusion changing fragrant
The comprehensive performance for setting infructescence facial treatment milk A6 is best.
The radicals scavenging of 14 Fructus Platycaryae strobilaceac preface facial treatment milk of embodiment acts on test experiments
1, the experimental method of DPPH free radical scavenging activity measurement
(experimental group: Fructus Platycaryae strobilaceac preface extracts 0.1mmol/L DPPH solution, the 2.0mL for sequentially adding 2.0mL dehydrated alcohol
Liquid, control group: ddH2O), 2.0mL dehydrated alcohol shakes up, and dark place stands 30min at room temperature, and absorbance is measured at 517nm.
It is measured in parallel 3 times, is averaged, with ddH2O is negative control, and the calculation formula of DPPH free radical scavenging activity is as follows:
DPPH free radical scavenging activity (%)=(X0+X2-X1)/X0100%；
(X0 is the absorbance not added by test solution, and X1 is that the absorbance reacted after by test solution is added, and X2 is by test solution itself
Absorbance).
2, experimental result
The absorbance test result of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract is as shown in table 6, and the DPPH of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract is free
Base clearance rate test result is as shown in Fig. 5 and table 7, it can be seen that infructescence of Platycarya strobilacea Sieb.et Zucc. Extract has very significant free radical
Elimination effect, infructescence of Platycarya strobilacea Sieb.et Zucc. Extract is 3.25mg/mL to DPPH half elimination ratio (50%) concentration, and extracting solution is in skin care
The concentration applied in cream is higher than 10mg/mL, therefore, after facial treatment milk adds infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, has stronger DPPH
Free radical scavenging ability.
The absorbance test result of 6 infructescence of Platycarya strobilacea Sieb.et Zucc. Extract of table
The DPPH free radical scavenging activity test result of 7 infructescence of Platycarya strobilacea Sieb.et Zucc. Extract of table
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (8)
1. a kind of Fructus Platycaryae strobilaceac preface skin care compositions, which is characterized in that in parts by weight, composed of the following components: octadecyl alcolol 4~
10 parts, 0.5~3 part of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4~10 parts of 1,3 butylene glycol, 1~5 part of Glycerin, mixed triester with caprylic acid capric acid, polyoxyethylene
(2) 1~3 part of stearyl ether, 1~3 part of monoglyceride, 0.5~1.5 part of dimethicone, 0.1~0.3 part of essence, preservative
Germallplus0.1~0.3 part complements to 100 parts with water.
2. Fructus Platycaryae strobilaceac preface skin care compositions according to claim 1, which is characterized in that in parts by weight, by with the following group
It is grouped as: 4~6 parts of octadecyl alcolol, 1~3 part of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4~6 parts of 1,3 butylene glycol, Glycerin, mixed triester with caprylic acid capric acid 2~4
Part, 1.5~2.5 parts of polyoxyethylene (2) stearyl ether, 1.5~2.5 parts of monoglyceride, 0.8~1.2 part of dimethicone, essence
0.15~0.25 part, preservative Germallplus0.15~0.25 part, 100 parts are complemented to water.
3. Fructus Platycaryae strobilaceac preface skin care compositions according to claim 1, which is characterized in that in parts by weight, by with the following group
It is grouped as: 6 parts of octadecyl alcolol, 3 parts of infructescence of Platycarya strobilacea Sieb.et Zucc. Extract, 4 parts of 1,3 butylene glycol, 3 parts of Glycerin, mixed triester with caprylic acid capric acid, polyoxyethylene
(2) 2 parts of stearyl ether, 2 parts of monoglyceride, 1 part of dimethicone, 0.2 part of essence, Germallplus0.2 parts of preservative, with water
Complement to 100 parts.
4. any Fructus Platycaryae strobilaceac preface skin care compositions of claims 1 to 3 is preparing the application in cosmetics.
5. a kind of Fructus Platycaryae strobilaceac preface facial treatment milk, which is characterized in that by any Fructus Platycaryae strobilaceac preface skin care of claims 1 to 3
Composition is prepared.
6. the preparation method of facial treatment milk described in claim 5, which comprises the following steps:
S1. octadecyl alcolol, Glycerin, mixed triester with caprylic acid capric acid, polyoxyethylene (2) stearyl are taken by any parts by weight of claims 1 to 3
Ether, monoglyceride and dimethicone are uniformly mixed, obtain mixture A, take infructescence of Platycarya strobilacea Sieb.et Zucc. Extract and 1,3-BDO, mix
Uniformly, mixture B is obtained, essence and preservative Germall plus are taken, is uniformly mixed, is obtained mixture C, be kept in dark place；
S2. mixture A is heated to 80 DEG C~90 DEG C, and mixture B is heated to 85 DEG C~95 DEG C, and mixture A and mixture B are mixed
It closes, stirring, is cooled to 35 DEG C~45 DEG C after homogeneous, mixture C and water is then added, is cooled to room temperature, the shield can be obtained
Skin lotion.
7. preparation method according to claim 6, which is characterized in that the speed of stirring described in step S2 is 40~60rpm.
8. preparation method according to claim 6, which is characterized in that the speed of homogeneous described in step S2 be 1000~
3000rpm。
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| CN110755328A (en) * | 2019-12-02 | 2020-02-07 | 中国林业科学研究院林产化学工业研究所 | Beautifying, moisturizing and repairing composition and application thereof |
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