CN109646360A - A kind of facial treatment milk and preparation method thereof with white-skinned face function - Google Patents
A kind of facial treatment milk and preparation method thereof with white-skinned face function Download PDFInfo
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Abstract
The invention discloses a kind of facial treatment milk and preparation method thereof with white-skinned face function.The raw material of the facial treatment milk is made of polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract, Ascorbyl Tetraisopalmitate, kojic dipalmitate, thymol, polyacrylic acid etc..The preparation method of the facial treatment milk with white-skinned face function is specifically that the first mixture is made through homogeneous, heating stirring in cetostearyl alcohol, hydrolyzed wheat protein etc., adding Ascorbyl Tetraisopalmitate, kojic dipalmitate etc., vacuum homogeneous obtains the second mixture in a heated condition, then stand heat preservation, be placed in emulsion pot again and thymol be added stage by stage, polygonum cuspidate root extract obtains final mixture, be eventually adding additive and stir to get finished emulsion.The facial treatment milk with white-skinned face function has significant whitening effect, and non-stimulated to skin, there is preferable application prospect in face skin nursing.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of facial treatment milk with white-skinned face function and its preparation
Method.
Background technique
In the aesthetic conceptions of most of compatriots, fair complexion is standard of beauty.Contain 4% in the basal layer cell of human epidermal
~5% chromatophore.The color of human skin is not depend on melanocyte quantity, but depends on the number of melanosome
Amount, size, distribution and melanocyte degree.And tyrosinase is the first step rate-limiting enzyme and key enzyme of B16 cell.Therefore, greatly
All contain tyrosinase inhibitor in most whitening agents, formation, the transfer etc. by influencing melanosome achieve the effect that whitening.
Tyrosinase is a kind of cupric aerobic enzyme, in the reaction process that tyrosine is converted into DOPA, it is necessary to have oxygen radical participation.?
That is oxygen radical is both initiator and reactant, the process of the catalysis oxidation of tyrosinase is clear in fact and in human body
Except the process of free radical.The removing of oxygen radical can block the catalysis of tyrosinase to react, so that oxidizing tyrosine be made to react
Remitted its fury.Although current market sales of whitening product has certain whitening effect after, in these products
Mostly containing there are many ingredients for being easy to produce side effect.If any cosmetics in contain heavy metal component, if be used for a long time meeting
Damage is generated to skin, leads to the generation of skin aging and wrinkle.And often due to chemicals, strong acid and strong base, chemistry are anti-
The problems such as rotten agent, cannot not only achieve the purpose that fundamentally to protect skin, can also make skin generation dependence or have to skin
Intense stimulus.Therefore, the trend that skin-protection product has become cosmetic field is prepared using phytochemicals production.
Summary of the invention
Consumer demand is not able to satisfy still in terms of whitening effect and to skin irritation based on contemporary skin care lotion to ask
Topic, the present invention provide a kind of facial treatment milk and preparation method thereof with white-skinned face function.
A kind of facial treatment milk with white-skinned face function, the raw material of the facial treatment milk by mass percentage, form as follows:
Polygonum cuspidate root extract 2.5~3.5%
Angelica Dahurica extract 0.8~1.6%
Leonurus extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Hydrolyzed wheat protein 1.8~3.8%
Glycerol 8.5~9.5%
Ascorbyl Tetraisopalmitate 3.5~5.5%
Kojic dipalmitate 2.5~5.5%
Dimethyl silicone polymer 2.5~3.5%
Thymol 1.6~1.8%
Polyacrylic acid 0.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
The above-mentioned facial treatment milk with white-skinned face function contains polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract, musk deer
The functional components such as vanilla phenol, hydrolyzed wheat protein, each functional components are in addition to playing basic effect possessed by itself, also
Synergistic function unexpectedly is shown, human endocrine and function can be adjusted from body metabolism level, fundamentally risen
To whitening function.The facial treatment milk has whitening effect good, the low feature of irritation, suitable for there is the crowd of whitening demand use.
The preparation side of the polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract in one of the embodiments,
Method are as follows:
Polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, be sieved, be added to weight be 30 times, volumetric concentration be 70~
In 80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering,
Again by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
To polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract.
The raw material of the facial treatment milk by mass percentage, forms as follows in one of the embodiments:
Polygonum cuspidate root extract 3.0%
Angelica Dahurica extract 1.2%
Leonurus extract 1.0%
Cetostearyl alcohol 5.0%
Hydrolyzed wheat protein 2.8%
Glycerol 9.0%
Ascorbyl Tetraisopalmitate 4.5%
Kojic dipalmitate 4.0%
Dimethyl silicone polymer 3.0%
Thymol 1.7%
Polyacrylic acid 0.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
The essence is any one in ginger extrait, flavoring rose essence, lavender oil in one of the embodiments,
Kind.
The antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro pyrrole in one of the embodiments,
Any one muttered in triol.
Any one of the preservative in Nipasol, sorbic acid, triclosan in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned facial treatment milk with white-skinned face function, comprise the steps of:
(1) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 2000~
3000 revs/min of rate is stirred homogeneous 10~20 minutes, and mixed liquor is then warming up to 75~80 DEG C, according to 1200~
1500 revs/min of rate stirs 20~30 minutes, obtains the first mixture；
(2) step (1) institute is added in Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer
In the first mixture obtained, continue to heat mixed liquor to 88~92 DEG C, under vacuum conditions according to 1600~1800 revs/min
Rate homogeneous 8~12 minutes again, obtain the second mixture；
(3) the second mixture for obtaining step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to
Thymol is added in emulsion pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature drop to be mixed
When to 65~70 DEG C, polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract are added into emulsion pot, according to 1500~
1700 revs/min of rate stirs 8~10 minutes, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15~25 minutes according to 100~120 revs/min of rates, finished emulsion is obtained after discharging.
The preparation method of the above-mentioned facial treatment milk with white-skinned face function, process conditions are mild, controllability is strong, and product quality is steady
Fixed, production cost economy is suitable for large-scale production.
Homogeneous is carried out under the vacuum condition of -0.08~-0.1MPa in the step (2) in one of the embodiments,.
The present invention also provides application of the facial treatment milk with white-skinned face function in face skin nursing.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment,
The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair
It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of facial treatment milk with white-skinned face function, the raw material of the facial treatment milk by mass percentage, form as follows:
Polygonum cuspidate root extract 2.5~3.5%
Angelica Dahurica extract 0.8~1.6%
Leonurus extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Hydrolyzed wheat protein 1.8~3.8%
Glycerol 8.5~9.5%
Ascorbyl Tetraisopalmitate 3.5~5.5%
Kojic dipalmitate 2.5~5.5%
Dimethyl silicone polymer 2.5~3.5%
Thymol 1.6~1.8%
Polyacrylic acid 0.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
Wherein, polygoni cuspidati,radix is the rhizomes of Polygonum, and extract is mainly made of resveratrol and rheum emodin, resveratrol
Significant anti-oxidation characteristics are known as with rheum officinale, thus have the effects that good antibacterial, anti-inflammatory, anti-oxidant, antiviral.In addition,
Polygonum cuspidate root extract to and chromatophore activity have good inhibiting effect, while having facilitation to macrophage activity, it is right
There is excellent effect in skin-whitening.
Wherein, the root of Dahurain angelica is the dry root of the perennial tall and big herbaceous plant root of Dahurain angelica of Umbelliferae or Radix angelicae dahuricae.The root of Dahurain angelica is from ancient times
The beauty medicine of doctor's happiness has effects that dispel pathogenic wind and remove dampness, reduces swelling, removes acne, fine and smooth skin, whitening face.
Wherein, motherwort removing blood stasis for promoting tissue regeneration, promoting blood circulation for regulating menstruation, swelling and pain relieving also can be used for itchy skin eruption.Chang Yinke promoting blood circulationization
The stasis of blood enhances endocrine function and cutaneous immunisation power, slows down skin aging.Leonurus extract can effectively remove face's grease, kill
Bacterium disinfection, glabrous skin have certain effect to treatment dark sore.
Wherein, thymol is the main component of thyme oil, and the bactericidal range of thymol is wide, effect is good.Thyme
Phenol still has anti-oxidant and anti-inflammatory effect, and there are some researches prove the oxidation resistances of thymol to be higher than vitamin E.
Wherein, hydrolyzed wheat protein has moisturizing, antioxidation and soft refinement skin, has special moisturizing ingredient, changes
Kind wrinkle.It using to after on skin, infiltrates into the minute crack of cuticula, is sustained effect of each component to skin, thus
Each component is reduced to the irritation of skin.
The above-mentioned facial treatment milk with white-skinned face function contains polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract, musk deer
The functional components such as vanilla phenol, hydrolyzed wheat protein, each functional components are in addition to playing basic effect possessed by itself, also
Synergistic function unexpectedly is shown, human endocrine and function can be adjusted from body metabolism level, fundamentally risen
To whitening function.The facial treatment milk has whitening effect good, the low feature of irritation, suitable for there is the crowd of whitening demand use.
In a preferred embodiment, the preparation of the polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract
Method are as follows:
Polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, be sieved, be added to weight be 30 times, volumetric concentration be 70~
In 80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering,
Again by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
To polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract.
In a preferred embodiment, the raw material of the facial treatment milk by mass percentage, forms as follows:
Polygonum cuspidate root extract 3.0%
Angelica Dahurica extract 1.2%
Leonurus extract 1.0%
Cetostearyl alcohol 5.0%
Hydrolyzed wheat protein 2.8%
Glycerol 9.0%
Ascorbyl Tetraisopalmitate 4.5%
Kojic dipalmitate 4.0%
Dimethyl silicone polymer 3.0%
Thymol 1.7%
Polyacrylic acid 0.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
In a preferred embodiment, the essence is any in ginger extrait, flavoring rose essence, lavender oil
It is a kind of.
In a preferred embodiment, the antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro
Any one in pyrans triol.
In a preferred embodiment, the preservative is any one in Nipasol, sorbic acid, triclosan
Kind.
The present invention also provides the preparation methods of the above-mentioned facial treatment milk with white-skinned face function, comprise the steps of:
(1) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 2000~
3000 revs/min of rate is stirred homogeneous 10~20 minutes, and mixed liquor is then warming up to 75~80 DEG C, according to 1200~
1500 revs/min of rate stirs 20~30 minutes, obtains the first mixture；
(2) step (1) institute is added in Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer
In the first mixture obtained, continue to heat mixed liquor to 88~92 DEG C, under vacuum conditions according to 1600~1800 revs/min
Rate homogeneous 8~12 minutes again, obtain the second mixture；
(3) the second mixture for obtaining step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to
Thymol is added in emulsion pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature drop to be mixed
When to 65~70 DEG C, polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract are added into emulsion pot, according to 1500~
1700 revs/min of rate stirs 8~10 minutes, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15~25 minutes according to 100~120 revs/min of rates, finished emulsion is obtained after discharging.
In a preferred embodiment, it is carried out under the vacuum condition of -0.08~-0.1MPa in the step (2) equal
Matter.
The present invention also provides application of the above-mentioned facial treatment milk with white-skinned face function in face skin nursing.
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality
Apply example.
Embodiment 1
The facial treatment milk formula with white-skinned face function of the present embodiment is as follows:
Polygonum cuspidate root extract 2.5%
Angelica Dahurica extract 0.8%
Leonurus extract 0.5%
Cetostearyl alcohol 4.8%
Hydrolyzed wheat protein 1.8%
Glycerol 8.5%
Ascorbyl Tetraisopalmitate 3.5%
Kojic dipalmitate 2.5%
Dimethyl silicone polymer 2.5%
Thymol 1.6%
Polyacrylic acid 0.12%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The facial treatment milk with white-skinned face function of the present embodiment is prepared as follows:
(1) polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, is sieved, being added to weight is 30 times, and volumetric concentration is
In 70% ethanol solution, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering, then
By filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried to obtain
Polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract
(2) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 2000
Rev/min rate be stirred homogeneous 10 minutes, mixed liquor is then warming up to 75 DEG C, according to 1200 revs/min of rate
Stirring 20 minutes, obtains the first mixture；
(3) step (2) institute is added in Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer
In the first mixture obtained, continue to heat mixed liquor to 88 DEG C, according to 1600 revs/min under the vacuum condition of -0.08MPa
Rate homogeneous 8 minutes again, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 30 minutes, is subsequently placed in emulsion pot, and to emulsification
Thymol is added in pot, is stirred 10 minutes according to 2200 revs/min of rates, when liquid temperature to be mixed is down to 65 DEG C, to cream
Change and polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract are added in pot, stirs 8 points according to 1500 revs/min of rates
Clock obtains final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15 minutes according to 100 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S1.
Embodiment 2
The facial treatment milk formula with white-skinned face function of the present embodiment is as follows:
Polygonum cuspidate root extract 3.0%
Angelica Dahurica extract 1.2%
Leonurus extract 1.0%
Cetostearyl alcohol 5.0%
Hydrolyzed wheat protein 2.8%
Glycerol 9.0%
Ascorbyl Tetraisopalmitate 4.5%
Kojic dipalmitate 4.0%
Dimethyl silicone polymer 3.0%
Thymol 1.7%
Polyacrylic acid 0.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
The facial treatment milk with white-skinned face function of the present embodiment is prepared as follows:
(1) polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, is sieved, being added to weight is 30 times, and volumetric concentration is
In 70% ethanol solution, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering, then
By filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried to obtain
Polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract
(2) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 2500
Rev/min rate be stirred homogeneous 15 minutes, mixed liquor is then warming up to 77.5 DEG C, according to 1350 revs/min of speed
Rate stirs 25 minutes, obtains the first mixture；
(3) step (2) institute is added in Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer
In the first mixture obtained, continue to heat mixed liquor to 90 DEG C, according to 1700 revs/min under the vacuum condition of -0.09MPa
Rate homogeneous 10 minutes again, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 35 minutes, is subsequently placed in emulsion pot, and to emulsification
Thymol is added in pot, is stirred 12.5 minutes according to 2300 revs/min of rates, when liquid temperature to be mixed is down to 67.5 DEG C,
Polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract are added into emulsion pot, stirs 8 according to 1600 revs/min of rates
~10 minutes, obtain final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 20 minutes according to 110 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S2.
Embodiment 3
The facial treatment milk formula with white-skinned face function of the present embodiment is as follows:
Polygonum cuspidate root extract 3.5%
Angelica Dahurica extract 1.6%
Leonurus extract 1.5%
Cetostearyl alcohol 5.2%
Hydrolyzed wheat protein 3.8%
Glycerol 9.5%
Ascorbyl Tetraisopalmitate 5.5%
Kojic dipalmitate 5.5%
Dimethyl silicone polymer 3.5%
Thymol 1.8%
Polyacrylic acid 0.12%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The facial treatment milk with white-skinned face function of the present embodiment is prepared as follows:
(1) polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, is sieved, being added to weight is 30 times, and volumetric concentration is
In 70% ethanol solution, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering, then
By filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried to obtain
Polygonum cuspidate root extract, Angelica Dahurica extract and Leonurus extract
(2) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 3000
Rev/min rate be stirred homogeneous 20 minutes, mixed liquor is then warming up to 80 DEG C, according to 1500 revs/min of rate
Stirring 30 minutes, obtains the first mixture；
(3) step (2) institute is added in Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer
In the first mixture obtained, continue to heat mixed liquor to 92 DEG C, according to 1800 revs/min under the vacuum condition of -0.1MPa
Rate homogeneous 12 minutes again, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 40 minutes, is subsequently placed in emulsion pot, and to emulsification
Thymol is added in pot, is stirred 15 minutes according to 2400 revs/min of rates, when liquid temperature to be mixed is down to 70 DEG C, to cream
Change and polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract are added in pot, stirs 10 points according to 1700 revs/min of rates
Clock obtains final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 25 minutes according to 120 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S3.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the facial treatment milk of this comparative example, does not add polygonum cuspidate
Root extract, final facial treatment milk obtained are denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the facial treatment milk of this comparative example, does not add the root of Dahurain angelica
Extract, final facial treatment milk obtained are denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the facial treatment milk of this comparative example, does not add beneficial mother
Careless extract, final facial treatment milk obtained are denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the facial treatment milk of this comparative example, does not add Moschus
Careless phenol, final facial treatment milk obtained are denoted as C4.
Comparative example 5
Substantially with embodiment 1, difference is the formula and preparation method of the facial treatment milk of this comparative example, does not add hydrolysis
Wheat gluten, final facial treatment milk obtained are denoted as C5.
Performance test
Facial treatment milk prepared by Examples 1 to 3 and comparative example 1~5 is subjected to using effect performance test.
Select the age at 25~45 years old, the women population that the colour of skin is dim, not pale is randomly divided into 8 groups as test object,
Every group of 15 people, each group skin of face situation, in terms of the difference that there are no significant, 1~8 group respectively daily
Early, two periods of evening smear facial treatment milk S1~S3 that the embodiment of the present invention 1~3 is prepared and comparative example 1~5 is prepared into
Facial treatment milk C1~the C5 arrived is each primary, after being used continuously one month, carries out effect assessment using the method for marking.Full marks are
5 points, 4~5 points of expression improvements are splendid；3~4 points of expression improvements are good；2~3 points of expression improvements are general；2 points
Following presentation is not affected significantly effect, and last each group is made even respectively, and the specific situation that scores is as shown in table 1:
Table 1
| The scoring of user's colour of skin improvement | Irritation | |
| S1 | 4.5 | It is non-stimulated |
| S2 | 4.8 | It is non-stimulated |
| S3 | 4.4 | It is non-stimulated |
| C1 | 2.9 | It is non-stimulated |
| C2 | 2.7 | It is non-stimulated |
| C3 | 3.2 | It is non-stimulated |
| C4 | 3.7 | It is non-stimulated |
| C5 | 3.9 | Low stimulation |
Test result is as shown above, the facial treatment milk of embodiment S1~S3 group and the facial treatment milk of comparative example C1~C5 group
It compares, more excellent whitening effect is all had for user, and the facial treatment milk of embodiment S2 is with most excellent
Using effect.It can be seen that from the case where embodiment and comparative example in the facial treatment milk ingredient with white-skinned face function of the invention
Polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract, thymol, hydrolyzed wheat protein to using effect generate
It significantly affects, and in the case that mentioned component is used in conjunction with, using effect has compared to lacking any one ingredient
It is extremely obviously improved, it is seen that produce synergistic effect between above-mentioned several ingredients, have a good application prospect.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.
Claims (9)
1. a kind of facial treatment milk with white-skinned face function, which is characterized in that the raw material of the facial treatment milk by mass percentage,
It forms as follows:
Polygonum cuspidate root extract 2.5~3.5%
Angelica Dahurica extract 0.8~1.6%
Leonurus extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Hydrolyzed wheat protein 1.8~3.8%
Glycerol 8.5~9.5%
Ascorbyl Tetraisopalmitate 3.5~5.5%
Kojic dipalmitate 2.5~5.5%
Dimethyl silicone polymer 2.5~3.5%
Thymol 1.6~1.8%
Polyacrylic acid 0.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
2. the facial treatment milk according to claim 1 with white-skinned face function, which is characterized in that the polygonum cuspidate root extract,
Angelica Dahurica extract and Leonurus extract the preparation method comprises the following steps:
Polygoni cuspidati,radix, root of Dahurain angelica root and motherwort are crushed respectively, are sieved, being added to weight is 30 times, and volumetric concentration is 70~80%
Ethanol solution in, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W, then take supernatant centrifugation, filtering, then will
Filtrate rotary evaporation under conditions of vacuum degree is -0.08MPa, obtains extract concentrated solution, finally freeze-dried to obtain tiger
Cane root extract, Angelica Dahurica extract and Leonurus extract.
3. the facial treatment milk according to claim 1 with white-skinned face function, which is characterized in that the raw material of the facial treatment milk
By mass percentage, it forms as follows:
Polygonum cuspidate root extract 3.0%
Angelica Dahurica extract 1.2%
Leonurus extract 1.0%
Cetostearyl alcohol 5.0%
Hydrolyzed wheat protein 2.8%
Glycerol 9.0%
Ascorbyl Tetraisopalmitate 4.5%
Kojic dipalmitate 4.0%
Dimethyl silicone polymer 3.0%
Thymol 1.7%
Polyacrylic acid 0.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
4. described in any item facial treatment milk with white-skinned face function according to claim 1~3, which is characterized in that the essence
Any one in ginger extrait, flavoring rose essence, lavender oil.
5. described in any item facial treatment milk with white-skinned face function according to claim 1~3, which is characterized in that the antioxygen
Any one of agent in butylated hydroxy anisole, allantoin, hydroxypropyl oxinane triol.
6. described in any item facial treatment milk with white-skinned face function according to claim 1~3, which is characterized in that the anti-corrosion
Any one of agent in Nipasol, sorbic acid, triclosan.
7. a kind of preparation method of the facial treatment milk as described in any one of claims 1 to 6 with white-skinned face function, feature exist
In comprising the steps of:
(1) cetostearyl alcohol, hydrolyzed wheat protein, glycerol, polyacrylic acid are added into deionized water, according to 2000~3000
Rev/min rate be stirred homogeneous 10~20 minutes, mixed liquor is then warming up to 75~80 DEG C, according to 1200~1500
Rev/min rate stir 20~30 minutes, obtain the first mixture；
(2) Ascorbyl Tetraisopalmitate, kojic dipalmitate, dimethyl silicone polymer addition step (1) is resulting
In first mixture, continue to heat mixed liquor to 88~92 DEG C, under vacuum conditions according to 1600~1800 revs/min of rate
Homogeneous 8~12 minutes again obtain the second mixture；
(3) the second mixture obtained step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to emulsification
Thymol is added in pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature to be mixed is down to 65
At~70 DEG C, into emulsion pot be added polygonum cuspidate root extract, Angelica Dahurica extract, Leonurus extract, according to 1500~1700 turns/
The rate of minute stirs 8~10 minutes, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, according to 100
~120 revs/min of rate stirs 15~25 minutes, and finished emulsion is obtained after discharging.
8. the preparation method of the facial treatment milk according to claim 7 with white-skinned face function, which is characterized in that the step
(2) homogeneous is carried out under the vacuum condition of -0.08~-0.1MPa in.
9. described in any item answering in face skin nursing of the facial treatment milk with white-skinned face function according to claim 1~6
With.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110368336A (en) * | 2019-07-16 | 2019-10-25 | 广东海洋大学 | A kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application |
| CN114469799A (en) * | 2021-11-02 | 2022-05-13 | 广州古泉生物科技有限公司 | Skin care cream and preparation method thereof |
-
2019
- 2019-02-16 CN CN201910118480.4A patent/CN109646360A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110368336A (en) * | 2019-07-16 | 2019-10-25 | 广东海洋大学 | A kind of Fructus Platycaryae strobilaceac preface facial treatment milk and its preparation method and application |
| CN110368336B (en) * | 2019-07-16 | 2022-04-12 | 广东海洋大学 | Skin-care lotion containing platycarya strobilacea infructescence as well as preparation method and application of skin-care lotion |
| CN114469799A (en) * | 2021-11-02 | 2022-05-13 | 广州古泉生物科技有限公司 | Skin care cream and preparation method thereof |
| CN114469799B (en) * | 2021-11-02 | 2023-08-18 | 广州古泉生物科技有限公司 | Skin care cream and preparation method thereof |
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Application publication date: 20190419 |