CN110323019B - R-t-b系烧结磁铁 - Google Patents

R-t-b系烧结磁铁 Download PDF

Info

Publication number
CN110323019B
CN110323019B CN201910238251.6A CN201910238251A CN110323019B CN 110323019 B CN110323019 B CN 110323019B CN 201910238251 A CN201910238251 A CN 201910238251A CN 110323019 B CN110323019 B CN 110323019B
Authority
CN
China
Prior art keywords
sintered magnet
phase
oxide
magnet according
grain boundary
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201910238251.6A
Other languages
English (en)
Chinese (zh)
Other versions
CN110323019A (zh
Inventor
藤原真理子
三轮将史
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TDK Corp
Original Assignee
TDK Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TDK Corp filed Critical TDK Corp
Publication of CN110323019A publication Critical patent/CN110323019A/zh
Application granted granted Critical
Publication of CN110323019B publication Critical patent/CN110323019B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C30/00Alloys containing less than 50% by weight of each constituent
    • C22C30/02Alloys containing less than 50% by weight of each constituent containing copper
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/16Both compacting and sintering in successive or repeated steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/04Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/005Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/032Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
    • H01F1/04Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
    • H01F1/047Alloys characterised by their composition
    • H01F1/053Alloys characterised by their composition containing rare earth metals
    • H01F1/055Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
    • H01F1/057Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
    • H01F1/0571Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
    • H01F1/0575Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
    • H01F1/0577Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together sintered
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • B22F2003/248Thermal after-treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2201/00Treatment under specific atmosphere
    • B22F2201/01Reducing atmosphere
    • B22F2201/013Hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2301/00Metallic composition of the powder or its coating
    • B22F2301/35Iron
    • B22F2301/355Rare Earth - Fe intermetallic alloys
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00Aspects linked to processes or compositions used in powder metallurgy
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C2202/00Physical properties
    • C22C2202/02Magnetic
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/032Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
    • H01F1/04Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
    • H01F1/047Alloys characterised by their composition
    • H01F1/053Alloys characterised by their composition containing rare earth metals
    • H01F1/055Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
    • H01F1/057Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
    • H01F1/0571Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
    • H01F1/0575Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
    • H01F1/0576Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together pressed, e.g. hot working

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Power Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Hard Magnetic Materials (AREA)
  • Powder Metallurgy (AREA)
  • Manufacturing Cores, Coils, And Magnets (AREA)
CN201910238251.6A 2018-03-28 2019-03-27 R-t-b系烧结磁铁 Active CN110323019B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2018062776A JP7110662B2 (ja) 2018-03-28 2018-03-28 R‐t‐b系焼結磁石
JP2018-062776 2018-03-28

Publications (2)

Publication Number Publication Date
CN110323019A CN110323019A (zh) 2019-10-11
CN110323019B true CN110323019B (zh) 2021-03-26

Family

ID=68057240

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910238251.6A Active CN110323019B (zh) 2018-03-28 2019-03-27 R-t-b系烧结磁铁

Country Status (3)

Country Link
US (1) US11145444B2 (enExample)
JP (1) JP7110662B2 (enExample)
CN (1) CN110323019B (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111243812B (zh) * 2020-02-29 2022-04-05 厦门钨业股份有限公司 一种r-t-b系永磁材料及其制备方法和应用
JP7214043B2 (ja) * 2020-04-08 2023-01-27 三菱電機株式会社 希土類焼結磁石および希土類焼結磁石の製造方法、回転子並びに回転機
CN118486518B (zh) * 2024-07-16 2024-10-18 南通正海磁材有限公司 R-t-b-m系永磁材料及其制备方法和应用

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1501411A (zh) * 2002-11-14 2004-06-02 ��Խ��ѧ��ҵ��ʽ���� R-Fe-B烧结磁体
JP2016027643A (ja) * 2014-06-27 2016-02-18 日立金属株式会社 コイル部品
CN107077965A (zh) * 2015-07-30 2017-08-18 日立金属株式会社 R‑t‑b系烧结磁体的制造方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62291902A (ja) * 1986-06-12 1987-12-18 Toshiba Corp 永久磁石の製造方法
US5405455A (en) * 1991-06-04 1995-04-11 Shin-Etsu Chemical Co. Ltd. Rare earth-based permanent magnet
JPH05226129A (ja) * 1992-02-18 1993-09-03 Kobe Steel Ltd 高耐食性希土類磁石の製造方法
AU2001275775A1 (en) * 2000-08-03 2002-02-18 Sanei Kasei Co., Limited Nanocomposite permanent magnet
US20030130129A1 (en) * 2001-07-13 2003-07-10 Massachusetts Institute Of Technology Vacuum processing for fabrication of superconducting films fabricated by metal-organic processing
EP1562203A4 (en) 2003-03-12 2009-08-05 Hitachi Metals Ltd R-T-B SINTERED MAGNET AND PROCESS FOR ITS MANUFACTURE
JP2005260098A (ja) * 2004-03-12 2005-09-22 Tdk Corp 希土類磁石およびその製造方法
EP1744331B1 (en) 2004-03-31 2016-06-29 TDK Corporation Rare earth magnet and method for manufacturing same
JP5115511B2 (ja) 2008-03-28 2013-01-09 Tdk株式会社 希土類磁石
US8823478B2 (en) * 2010-03-30 2014-09-02 Tdk Corporation Rare earth sintered magnet, method for producing same, motor and automobile
EP2444985B1 (en) * 2010-10-25 2018-07-11 Toyota Jidosha Kabushiki Kaisha Production method of rare earth magnet
JP5572673B2 (ja) 2011-07-08 2014-08-13 昭和電工株式会社 R−t−b系希土類焼結磁石用合金、r−t−b系希土類焼結磁石用合金の製造方法、r−t−b系希土類焼結磁石用合金材料、r−t−b系希土類焼結磁石、r−t−b系希土類焼結磁石の製造方法およびモーター
JP6238444B2 (ja) 2013-01-07 2017-11-29 昭和電工株式会社 R−t−b系希土類焼結磁石、r−t−b系希土類焼結磁石用合金およびその製造方法
JP6303480B2 (ja) * 2013-03-28 2018-04-04 Tdk株式会社 希土類磁石
US10109403B2 (en) * 2013-08-09 2018-10-23 Tdk Corporation R-T-B based sintered magnet and motor
JP6511844B2 (ja) 2015-02-10 2019-05-15 Tdk株式会社 R−t−b系焼結磁石
JP6759649B2 (ja) * 2016-03-23 2020-09-23 Tdk株式会社 希土類磁石及びモーター
JP7387992B2 (ja) * 2019-03-20 2023-11-29 Tdk株式会社 R-t-b系永久磁石

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1501411A (zh) * 2002-11-14 2004-06-02 ��Խ��ѧ��ҵ��ʽ���� R-Fe-B烧结磁体
JP2016027643A (ja) * 2014-06-27 2016-02-18 日立金属株式会社 コイル部品
CN107077965A (zh) * 2015-07-30 2017-08-18 日立金属株式会社 R‑t‑b系烧结磁体的制造方法

Also Published As

Publication number Publication date
JP2019176011A (ja) 2019-10-10
JP7110662B2 (ja) 2022-08-02
US20190304639A1 (en) 2019-10-03
CN110323019A (zh) 2019-10-11
US11145444B2 (en) 2021-10-12

Similar Documents

Publication Publication Date Title
CN110299237B (zh) R-t-b系烧结磁铁
RU2389098C2 (ru) Функционально-градиентный редкоземельный постоянный магнит
EP2590181B1 (en) Process of manufacturing an r-t-b based rare earth permanent magnet
RU2377680C2 (ru) Редкоземельный постоянный магнит
RU2359352C2 (ru) Функционально усовершенствованный редкоземельный постоянный магнит
CN106024253B (zh) R-Fe-B烧结磁体及制备方法
EP2752857B1 (en) R-T-B rare earth sintered magnet
CN104395971B (zh) 烧结磁铁
RU2697266C2 (ru) Спеченный магнит r-fe-b и способ его изготовления
KR101482816B1 (ko) 표면 개질된 희토류계 소결 자석의 제조 방법 및 표면 개질된 희토류계 소결 자석
EP2779179B1 (en) R-T-B-based rare earth magnet particles, process for producing the R-T-B-based rare earth magnet particles, and bonded magnet
EP3121821B1 (en) Permanent magnet, motor, and generator
EP2608224A1 (en) Rare earth-iron-nitrogen system alloy material, method for producing rare earth-iron-nitrogen system alloy material, rare earth-iron system alloy material, and method for producing rare earth-iron system alloy material
CN111261353B (zh) R-t-b系永磁体
CN113450983B (zh) R-t-b系永久磁铁
JP7247670B2 (ja) R-t-b系永久磁石およびその製造方法
CN110323019B (zh) R-t-b系烧结磁铁
CN111710489B (zh) R-t-b系永久磁铁
JP2005150503A (ja) 焼結磁石の製造方法
JP4702548B2 (ja) 傾斜機能性希土類永久磁石
CN111724955B (zh) R-t-b系永久磁铁
JP5359383B2 (ja) 磁石成形体及びその製造方法
JP7188172B2 (ja) R‐t‐b系永久磁石
CN111724961B (zh) R-t-b系永久磁铁
CN113838621A (zh) R-t-b系永久磁铁及电动机

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant