CN110183696A - A kind of preparation method of the quick-fried pearl lapping of cigarette - Google Patents
A kind of preparation method of the quick-fried pearl lapping of cigarette Download PDFInfo
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- CN110183696A CN110183696A CN201910416518.6A CN201910416518A CN110183696A CN 110183696 A CN110183696 A CN 110183696A CN 201910416518 A CN201910416518 A CN 201910416518A CN 110183696 A CN110183696 A CN 110183696A
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- fried pearl
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2305/00—Characterised by the use of polysaccharides or of their derivatives not provided for in groups C08J2301/00 or C08J2303/00
- C08J2305/08—Chitin; Chondroitin sulfate; Hyaluronic acid; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2401/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2401/08—Cellulose derivatives
- C08J2401/26—Cellulose ethers
- C08J2401/28—Alkyl ethers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2405/00—Characterised by the use of polysaccharides or of their derivatives not provided for in groups C08J2401/00 or C08J2403/00
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2489/00—Characterised by the use of proteins; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/05—Alcohols; Metal alcoholates
- C08K5/053—Polyhydroxylic alcohols
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
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Abstract
The present invention relates to a kind of cigarette preparation methods of quick-fried pearl lapping, belong to tobacco curing field of material technology.The present invention uses polished rice, minced fillet for raw material, cigarette is prepared with quick-fried pearl lapping, these Interaction of substituents, to maintain the stabilization of albumen membrane structure, and then have preferable mechanical performance, protein and plasticizer is molten into deionized water by a certain percentage, protein denaturation is made by heat treatment again, space structure spread apart comes, and forms fine and close space net structure, improves the toughness of the quick-fried pearl lapping of cigarette.The present invention uses chitosan, carragheen, gellan gum for modified feedstock, prepare composite edible film, carragheen is capable of forming film after being heat-treated, it can effectively avoid microorganism to cigarette generation pollution inside quick-fried pearl, block-water performance is improved simultaneously, it can be effectively prevented the quick-fried pearl moisture absorption of cigarette, chitosan has the high grade of transparency, toughness good and the feature of high oxygen barrier, can effectively improve the weatherability of cigarette lapping.
Description
Technical field
The present invention relates to a kind of cigarette preparation methods of quick-fried pearl lapping, belong to tobacco curing field of material technology.
Background technique
Quick-fried pearl, also referred to as fragrance dripping pill, brittleness capsule etc., are referred to and are embedded in one of cigarette filter liquid in the form of capsule
The small glue bead of body, by wrapping up the liquid solvent of diverse fragrant flavour, it is pinched brokenly with hand extruding during the smoking process, is made by smoker
Perfume liquid flows out in pearl, and flavor component is released under cigarette mainstream flue gas effect.Application of the quick-fried pearl in cigarette filter rod,
The adjustable of cigarette odor-absorbing is realized, flavouring humectation effect is obvious, can satisfy the consumer for pursuing cigarette individual character note, is relaxed
Suitable sense, the suction experience for returning sweet tea sense, the pleasants such as sense of promoting the production of body fluid；The vision that quick-fried pearl has the sound, transparent visual etc. powerful simultaneously
Output assigns the function that cigarette product play one.In recent years, the country has many tobacco enterprises and researches and develops and manufacture quick-fried pearl volume
Cigarette achieves certain achievement in terms of breaking through quick-fried pearl key technology barrier.In conjunction with practical condition, existing skill is being used
In art, quick-fried pearl is produced using dropping preparation method and is had the following deficiencies: in dripping pill drying after formation, screening and filter stick telescopiny
It is easy rubbed, squeeze and fracture phenomena occurs, the oily perfume in soft capsule is easy exudation, the adhesion between dripping pill occurs
The phenomenon that situation, after storing a period of time, dripping pill brittleness is reduced, and will appear hair mist once in a while, when pinching brokenly dripping pill with hand, it is difficult to hear
" " clear and melodious sound, seriously affect the exterior quality and practical application effect of dripping pill.This may be due to rubber thinner thickness,
Moisture content is unstable, rubber matrix occurs caused by the reasons such as putrid and deteriorated.
The wall material raw material that traditional technology prepares soft capsule is mostly gelatin, is mainly extracted from the skin, bone of certain animals
It obtains.Gelatin is a kind of mixture of water soluble protein, is the partial denaturation product of collagen.Since gelatin is produced from natural
Object, and because of its appearance gloss, has the ability for undertaking dyestuff, easy to operate, and as a kind of good drug overcoats material,
The solid dosage forms being widely used in medicine, including hard, Perle and gelatine glaze piece.But since gelatin intensity is low,
Brittleness is big, easily water absorption and swelling and intensity and elasticity modulus are low after being swollen, and makes gelatin directly using being restricted.So in order to
Solve the problems, such as gelatin soft capsule, needing to develop a kind of high performance cigarette with quick-fried pearl lapping improves consumer experience
Feel bad problem.
Summary of the invention
The technical problems to be solved by the invention: it is poor for existing quick-fried pearl weatherability, it is easy rubbed, squeeze and occur
Fracture phenomena " is pinched and is not broken " after the moisture absorption or the problem of " pinch and do not ring ", provides a kind of preparation method of quick-fried pearl lapping of cigarette.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:
(1) ethyl cellulose is added to absolute ethanol, 20 ~ 30min is stirred with 200 ~ 300r/min revolving speed under room temperature, obtains ethyl
Cellulosic ethanol solution；
(2) rice protein concentrate, carragheen, gellan gum, chitosan and minced fillet are added in deionized water, in 60 ~ 80 DEG C of water
40 ~ 60min is stirred with 300 ~ 350r/min revolving speed under bath, obtains mixture；
(3) glycerine, ethyl cellulose ethanol solution are added in mixture, homogeneous obtains homogenate；
(4) by homogenate, 20 ~ 25min of magnetic agitation, adjusting pH to 3 ~ 4 obtain gel under 40 ~ 50 DEG C of water-baths；
(5) gel is placed in 60 ~ 65 DEG C of water-baths in 200 ~ 250r/min, 30 ~ 40min of tachyphylaxis, room temperature still aging 24 ~
26h, then it is placed at 100 ~ 120 DEG C dry 20 ~ for 24 hours, film forming obtains cigarette with quick-fried pearl lapping.
It is the rice protein concentrate, carragheen, gellan gum, chitosan, minced fillet, ethyl cellulose, glycerine, anhydrous
Ethyl alcohol, deionized water parts by weight be 10 ~ 20 parts of rice protein concentrates, 10 ~ 20 parts of carragheens, 10 ~ 20 parts of gellan gums, 30 ~
40 parts of chitosans, 20 ~ 30 parts of minced fillets, 10 ~ 20 parts of ethyl celluloses, 40 ~ 50 parts of glycerine, 60 ~ 80 parts of dehydrated alcohols, 100 ~
120 parts of deionized waters,
The acetic acid that it is 1% using mass fraction that pH described in step (4), which is adjusted,.
Cigarette described in step (5) is with quick-fried pearl lapping with a thickness of 0.4 ~ 0.6mm.
The specific preparation step of rice protein concentrate described in step (2) are as follows:
(1) sodium hydroxide is added in deionized water, 10 ~ 15min is stirred with 150 ~ 200r/min revolving speed under room temperature, obtains sodium hydroxide
Solution；
(2) milled rice flour is added in sodium hydroxide solution, 30 ~ 40min is stirred with 200 ~ 300r/min revolving speed under room temperature, must be mixed
Liquid；
(3) mixed liquor is placed in a centrifuge and 5 ~ 10min is centrifugated with 5000 ~ 6000r/min revolving speed, take supernatant liquor, adjusted
PH to 4.5 ~ 5.5 is saved, reaction clear liquid is obtained；
(4) reaction clear liquid is centrifugated under 5000 ~ 6000r/min revolving speed 10min, lower layer's deposit is taken, by sediment
Matter is added in deionized water, adjusts pH to 6.5 ~ 7.5, obtains mechanism liquid；
(5) regulation mechanism liquid pH to 4.5 ~ 5.5 obtains reaction mechanism liquid；
(6) reaction mechanism liquid is placed in a centrifuge under room temperature and 5 ~ 10min is centrifugated with 6000 ~ 7000r/min revolving speed, removed
Layer solid, room temperature dry, and obtain rice protein concentrate.
The rice flour, sodium hydroxide, deionized water parts by weight be 20 ~ 30 parts of milled rice flours, 4 ~ 6 parts of sodium hydroxides, 40 ~
60 parts of deionized waters.
PH described in step (3) adjusts the hydrochloric acid using mass concentration 1%.
Deposit described in step (4) and deionized water quality ratio are 1:5, and pH is adjusted using mass concentration 1%
Sodium hydroxide solution.
The hydrochloric acid that it is 1% using mass concentration that pH described in step (5), which is adjusted,.
The specific preparation step of milled rice flour described in step (2) are as follows:
Polished rice is placed in ball mill under room temperature with 300 ~ 350r/min revolving speed 1 ~ 2h of ball milling, 60 ~ 80 meshes is crossed, obtains milled rice flour.
The present invention is compared with other methods, and advantageous effects are:
(1) present invention uses polished rice, minced fillet for raw material, prepares the quick-fried pearl lapping of cigarette, and minced fillet is a kind of novel aquatic products tune
Raw material is managed, minced fillet is cut after mixing, adds auxiliary material to carry out arena and bursts, at heating after sticky pasted fish meat reshaping, becomes that there is elasticity
Gelinite, the protein in minced fillet muscle is generally divided into salt soluble protein, water soluble protein and insoluble protein three
Class, and it can be dissolved in neutral salt solution, and can form the protein with resilient gel after the heating is mainly salting-in protein
Matter, i.e. myofibrillar protein, it is made of myosin, actin and actomyosin, is that minced fillet forms elastic coagulate
The main component of colloid, gel phenomenon are actin advanced knots after heated after being fully dissolved out because of salting-in protein
Structure is unlocked, and is mutually wound fibrous macromolecular by hydrogen bond between molecule and is constituted stable reticular structure, due to flesh
Globulin has extremely strong hydrophily in process in leaching, thus a large amount of free water is contained in the reticular structure of formation
Point, after being thermally formed gel, just constitutes than more uniform reticular structure and make product that there is extremely strong elasticity, polished rice,
There are a large amount of disulfide bond, hydrogen bond and hydrophobic bond etc., these Interaction of substituents, to tie up inside protein molecule in minced fillet
Hold the stabilization of albumen membrane structure, and then have preferable mechanical performance, protein and plasticizer it is molten by a certain percentage to go from
In sub- water, then protein denaturation made by heat treatment, space structure spread apart comes, so that the hydrophobic grouping of protein interior is sudden and violent
It exposes outside, fine and close space net structure is formed, and then maintain the stability of protein film, to improve cigarette with quick-fried pearl lapping
Toughness；
(2) present invention prepares the quick-fried pearl lapping of cigarette by addition chitosan, carragheen, gellan gum, and carragheen is carrying out heat
It is capable of forming film after processing, can effectively avoid microorganism to cigarette generation pollution inside quick-fried pearl, while improving water preventing ability
Can, it can be effectively prevented the quick-fried pearl moisture absorption of cigarette, chitosan is with the high grade of transparency, toughness is good and the feature of high oxygen barrier, can
It is effectively prevent the quick-fried pearl ingress of air of cigarette, gellan gum is heat-resisting, acid resistance is good, and it is also high to the stability of enzyme, it can effectively improve
The weatherability of cigarette lapping；
(3) present invention prepares the quick-fried pearl lapping of cigarette, ethyl cellulose is the ethyl of cellulose by addition ethyl cellulose
Ether, is not easy the moisture absorption, and ethyl cellulose has good film forming, thin film can be quickly formed on lapping, due to second
Base hydrophobic cellulose is good, and film can effectively improve the cigarette tolerance and humidity resistance of quick-fried pearl lapping.
Specific embodiment
Polished rice is placed in ball mill under room temperature with 300 ~ 350r/min revolving speed 1 ~ 2h of ball milling, 60 ~ 80 meshes is crossed, obtains polished rice
Powder weighs 20 ~ 30 parts of milled rice flours, 4 ~ 6 parts of sodium hydroxides, 40 ~ 60 parts of deionized waters, by hydroxide according to parts by weight respectively
Sodium is added in deionized water, stirs 10 ~ 15min under room temperature with 150 ~ 200r/min revolving speed, obtains sodium hydroxide solution, by milled rice flour plus
Enter in sodium hydroxide solution, under room temperature with 200 ~ 300r/min revolving speed stir 30 ~ 40min, obtain mixed liquor, by mixed liquor be placed in from
5 ~ 10min is centrifugated with 5000 ~ 6000r/min revolving speed in scheming, takes supernatant liquor, mass concentration 1% is added dropwise into clear liquid
Salt acid for adjusting pH obtains reaction clear liquid to 4.5 ~ 5.5, and reaction clear liquid is centrifugated 10min under 5000 ~ 6000r/min revolving speed,
Lower layer's deposit is taken, deposit is added in deionized water 1:5 in mass ratio, and the sodium hydroxide that mass concentration 1% is added dropwise is molten
Liquid adjusts pH to 6.5 ~ 7.5, obtains mechanism liquid, and the salt acid for adjusting pH of mass concentration 1% is added dropwise into mechanism liquid to 4.5 ~ 5.5, obtains instead
Mechanism liquid is answered, reaction mechanism liquid is placed in a centrifuge under room temperature, 5 ~ 10min is centrifugated with 6000 ~ 7000r/min revolving speed, taken
Lower layer's solid, room temperature dry, and obtain rice protein concentrate, according to parts by weight, weigh 10 ~ 20 parts of rice protein concentrations respectively
Object, 10 ~ 20 parts of carragheens, 10 ~ 20 parts of gellan gums, 30 ~ 40 parts of chitosans, 20 ~ 30 parts of minced fillets, 10 ~ 20 parts of ethyl celluloses, 40
~ 50 parts of glycerine, 60 ~ 80 parts of dehydrated alcohols, 100 ~ 120 parts of deionized waters, ethyl cellulose are added to absolute ethanol, room temperature
Under with 200 ~ 300r/min revolving speed stir 20 ~ 30min, ethyl cellulose ethanol solution is obtained, by rice protein concentrate, OK a karaoke club
Glue, gellan gum, chitosan and minced fillet are added in deionized water, under 60 ~ 80 DEG C of water-baths with 300 ~ 350r/min revolving speed stirring 40 ~
60min obtains mixture, glycerine, ethyl cellulose ethanol solution is added in mixture, homogeneous obtains homogenate, by homogenate 40
20 ~ 25min of magnetic agitation under ~ 50 DEG C of water-baths, the acetic acid solution that mass concentration 1% is added dropwise adjust pH to 3 ~ 4, gel are obtained, by gel
It is placed in 60 ~ 65 DEG C of water-baths in 200 ~ 250r/min, 30 ~ 40min of tachyphylaxis, the still aging 24 ~ 26h of room temperature, then it is placed in 100 ~
Dry 20 at 120 DEG C ~ for 24 hours, film forming obtains cigarette with quick-fried pearl lapping.
Example 1
Ethyl cellulose is added to absolute ethanol, 20min is stirred with 200r/min revolving speed under room temperature, obtains ethyl cellulose ethyl alcohol
Solution；By rice protein concentrate, carragheen, gellan gum, chitosan and minced fillet be added deionized water in, under 60 DEG C of water-baths with
300r/min revolving speed stirs 40min, obtains mixture；Glycerine, ethyl cellulose ethanol solution are added in mixture, homogeneous,
Obtain homogenate；By homogenate, magnetic agitation 20min, adjusting pH to 3 obtain gel under 40 DEG C of water-baths；Gel is placed in 60 DEG C of water-baths
In 200r/min tachyphylaxis 30min, room temperature is still aging for 24 hours, then is placed at 100 DEG C dry 20h, and film forming obtains cigarette with quick-fried pearl
Lapping.Rice protein concentrate, carragheen, gellan gum, chitosan, minced fillet, ethyl cellulose, glycerine, dehydrated alcohol,
The parts by weight of deionized water are 10 parts of rice protein concentrates, 10 parts of carragheens, 10 parts of gellan gums, 30 parts of chitosans, 20 portions of fishes
Gruel, 10 parts of ethyl celluloses, 40 parts of glycerine, 60 parts of dehydrated alcohols, 100 parts of deionized waters, pH are adjusted using quality point
The acetic acid that number is 1%.Cigarette is with quick-fried pearl lapping with a thickness of 0.4mm.The specific preparation step of rice protein concentrate are as follows: will
Sodium hydroxide is added in deionized water, stirs 10min under room temperature with 150r/min revolving speed, obtains sodium hydroxide solution；By milled rice flour plus
Enter in sodium hydroxide solution, 30min is stirred with 200r/min revolving speed under room temperature, obtains mixed liquor；Mixed liquor is placed in a centrifuge
It is centrifugated 5min with 5000r/min revolving speed, takes supernatant liquor, pH to 4.5 is adjusted, obtains reaction clear liquid；Reaction clear liquid is existed
Be centrifugated 10min under 5000r/min revolving speed, take lower layer's deposit, will deposit be added deionized water in, adjust pH to
6.5, obtain mechanism liquid；Regulation mechanism liquid pH to 4.5 obtains reaction mechanism liquid；By reaction mechanism liquid be placed in a centrifuge under room temperature with
6000r/min revolving speed is centrifugated 5min, takes lower layer's solid, room temperature dries, and obtains rice protein concentrate.Rice flour, sodium hydroxide,
The parts by weight of deionized water are 20 parts of milled rice flours, 4 parts of sodium hydroxides, 40 parts of deionized waters.PH is adjusted using mass concentration
1% hydrochloric acid.Deposit and deionized water quality ratio are 1:5, and pH adjusts molten using the sodium hydroxide of mass concentration 1%
Liquid.The hydrochloric acid that it is 1% using mass concentration that pH, which is adjusted,.The specific preparation step of milled rice flour are as follows: polished rice is placed in ball mill
With 300r/min revolving speed ball milling 1h under room temperature, 60 meshes are crossed, milled rice flour is obtained.
Example 2
Ethyl cellulose is added to absolute ethanol, 25min is stirred with 250r/min revolving speed under room temperature, obtains ethyl cellulose ethyl alcohol
Solution；By rice protein concentrate, carragheen, gellan gum, chitosan and minced fillet be added deionized water in, under 70 DEG C of water-baths with
325r/min revolving speed stirs 50min, obtains mixture；Glycerine, ethyl cellulose ethanol solution are added in mixture, homogeneous,
Obtain homogenate；By homogenate, magnetic agitation 23min, adjusting pH to 3.5 obtain gel under 45 DEG C of water-baths；Gel is placed in 63 DEG C of water-baths
In in 225r/min tachyphylaxis 35min, the still aging 25h of room temperature, then be placed at 110 DEG C dry 22h, film forming obtains cigarette with quick-fried
Pearl lapping.Rice protein concentrate, carragheen, gellan gum, chitosan, minced fillet, ethyl cellulose, glycerine, anhydrous second
Alcohol, deionized water parts by weight be 15 parts of rice protein concentrates, 15 parts of carragheens, 15 parts of gellan gums, 35 parts of chitosans, 25 parts
Minced fillet, 15 parts of ethyl celluloses, 45 parts of glycerine, 70 parts of dehydrated alcohols, 110 parts of deionized waters, pH are adjusted using quality
The acetic acid that score is 1%.Cigarette is with quick-fried pearl lapping with a thickness of 0.5mm.The specific preparation step of rice protein concentrate are as follows:
Sodium hydroxide is added in deionized water, 13min is stirred with 175r/min revolving speed under room temperature, obtains sodium hydroxide solution；By milled rice flour
It is added in sodium hydroxide solution, 35min is stirred with 250r/min revolving speed under room temperature, obtains mixed liquor；Mixed liquor is placed in centrifuge
In 7min is centrifugated with 5500r/min revolving speed, take supernatant liquor, adjust pH to 5.0, obtain reaction clear liquid；Reaction clear liquid is existed
Be centrifugated 10min under 5500r/min revolving speed, take lower layer's deposit, will deposit be added deionized water in, adjust pH to
7.0, obtain mechanism liquid；Regulation mechanism liquid pH to 5.0 obtains reaction mechanism liquid；By reaction mechanism liquid be placed in a centrifuge under room temperature with
6500r/min revolving speed is centrifugated 7min, takes lower layer's solid, room temperature dries, and obtains rice protein concentrate.Rice flour, sodium hydroxide,
The parts by weight of deionized water are 25 parts of milled rice flours, 5 parts of sodium hydroxides, 50 parts of deionized waters.PH is adjusted using mass concentration
1% hydrochloric acid.Deposit and deionized water quality ratio are 1:5, and pH adjusts molten using the sodium hydroxide of mass concentration 1%
Liquid.The hydrochloric acid that it is 1% using mass concentration that pH, which is adjusted,.The specific preparation step of milled rice flour are as follows: polished rice is placed in ball mill
With 325r/min revolving speed ball milling 1.5h under room temperature, 70 meshes are crossed, milled rice flour is obtained.
Example 3
Ethyl cellulose is added to absolute ethanol, 30min is stirred with 300r/min revolving speed under room temperature, obtains ethyl cellulose ethyl alcohol
Solution；By rice protein concentrate, carragheen, gellan gum, chitosan and minced fillet be added deionized water in, under 80 DEG C of water-baths with
350r/min revolving speed stirs 60min, obtains mixture；Glycerine, ethyl cellulose ethanol solution are added in mixture, homogeneous,
Obtain homogenate；By homogenate, magnetic agitation 25min, adjusting pH to 4 obtain gel under 50 DEG C of water-baths；Gel is placed in 65 DEG C of water-baths
In 250r/min tachyphylaxis 40min, the still aging 26h of room temperature, then it is placed in drying at 120 DEG C and for 24 hours, forms a film, obtain cigarette with quick-fried pearl
Lapping.Rice protein concentrate, carragheen, gellan gum, chitosan, minced fillet, ethyl cellulose, glycerine, dehydrated alcohol,
The parts by weight of deionized water are 20 parts of rice protein concentrates, 20 parts of carragheens, 20 parts of gellan gums, 40 parts of chitosans, 30 portions of fishes
Gruel, 20 parts of ethyl celluloses, 50 parts of glycerine, 80 parts of dehydrated alcohols, 120 parts of deionized waters, pH are adjusted using quality point
The acetic acid that number is 1%.Cigarette is with quick-fried pearl lapping with a thickness of 0.6mm.The specific preparation step of rice protein concentrate are as follows: will
Sodium hydroxide is added in deionized water, stirs 15min under room temperature with 200r/min revolving speed, obtains sodium hydroxide solution；By milled rice flour plus
Enter in sodium hydroxide solution, 40min is stirred with 300r/min revolving speed under room temperature, obtains mixed liquor；Mixed liquor is placed in a centrifuge
It is centrifugated 10min with 6000r/min revolving speed, takes supernatant liquor, pH to 5.5 is adjusted, obtains reaction clear liquid；Reaction clear liquid is existed
Be centrifugated 10min under 6000r/min revolving speed, take lower layer's deposit, will deposit be added deionized water in, adjust pH to
7.5, obtain mechanism liquid；Regulation mechanism liquid pH to 5.5 obtains reaction mechanism liquid；By reaction mechanism liquid be placed in a centrifuge under room temperature with
7000r/min revolving speed is centrifugated 10min, takes lower layer's solid, room temperature dries, and obtains rice protein concentrate.Rice flour, hydroxide
Sodium, deionized water parts by weight be 30 parts of milled rice flours, 6 parts of sodium hydroxides, 60 parts of deionized waters.PH adjusts dense using quality
The hydrochloric acid of degree 1%.Deposit and deionized water quality ratio are 1:5, and pH adjusts molten using the sodium hydroxide of mass concentration 1%
Liquid.The hydrochloric acid that it is 1% using mass concentration that pH, which is adjusted,.The specific preparation step of milled rice flour are as follows: polished rice is placed in ball mill
With 350r/min revolving speed ball milling 2h under room temperature, 80 meshes are crossed, milled rice flour is obtained.
The moisture content of quick-fried pearl lapping is detected to pearl quick-fried in above-described embodiment using HR73/HG53 moisture detector,
Drying temperature is 105 DEG C, and heating mode is soft heating, heating-up time 1:20min.By the quick-fried pearl of dripping in temperature 20 ± 2
DEG C, moisture absorption 48h under the conditions of relative humidity 85%~95% detects quick-fried pearl lapping moisture such as table 1 before and after the moisture absorption respectively.
The hardness for being detected quick-fried pearl to pearl quick-fried in above-described embodiment using DPYD-A dripping pill tablet hardness meter, quick-fried pearl is put
It sets among the sample tray of hardness analyzer, and is close proximity on fixed baffle, open tester switch, push rod is with 1mm/s's
Fixed speed advances, and squeezes quick-fried pearl, records the push rod pressure when rupture of quick-fried pearl, i.e. hardness, testing result such as table 1:
Quick-fried pearl moisture absorption front and back moisture content and Hardness results in 1 embodiment of table
Test two: quick-fried pearl hydrothermal aging test
The quick-fried pearl of dripping in each embodiment is subjected to hydrothermal aging cyclic test, circulation time in high/low temperature hydrothermal aging case
48h observes quick-fried pearl appearance and detects the hardness after the quick-fried pearl moisture absorption.
Experiment condition is as follows:
(1) cryogenic conditions: 20 DEG C × 12h of -20 DEG C × 12h
(2) hot conditions: 22 DEG C × 12h, 40 DEG C × 12h
Relative humidity maintains (93 ± 3) % under above-mentioned higher temperature, remaining time is not less than 95% in recycling, and circulation is real
Test middle result such as table 2:
Quick-fried pearl carries out hydrothermal aging cyclic test in high/low temperature hydrothermal aging case in the implementation of table 2
The quick-fried pearl lapping performance characterization of 1 cigarette of table
2 cigarette of table is characterized with quick-fried pearl lapping heat and moisture aging resistance
The quick-fried pearl lapping of cigarette prepared by the present invention as shown in Table 1, quick-fried pearl equilibrium moisture content reduce, and the moisture absorption performance of quick-fried pearl mentions
Height, quick-fried pearl is strong to environmental adaptability, good weatherability.
Claims (10)
1. a kind of cigarette preparation method of quick-fried pearl lapping, which is characterized in that specific preparation step are as follows:
(1) ethyl cellulose is added to absolute ethanol, 20 ~ 30min is stirred with 200 ~ 300r/min revolving speed under room temperature, obtains ethyl
Cellulosic ethanol solution；
(2) rice protein concentrate, carragheen, gellan gum, chitosan and minced fillet are added in deionized water, in 60 ~ 80 DEG C of water
40 ~ 60min is stirred with 300 ~ 350r/min revolving speed under bath, obtains mixture；
(3) glycerine, ethyl cellulose ethanol solution are added in mixture, homogeneous obtains homogenate；
(4) by homogenate, 20 ~ 25min of magnetic agitation, adjusting pH to 3 ~ 4 obtain gel under 40 ~ 50 DEG C of water-baths；
(5) gel is placed in 60 ~ 65 DEG C of water-baths in 200 ~ 250r/min, 30 ~ 40min of tachyphylaxis, room temperature still aging 24 ~
26h, then it is placed at 100 ~ 120 DEG C dry 20 ~ for 24 hours, film forming obtains cigarette with quick-fried pearl lapping.
2. a kind of cigarette according to claim 1 preparation method of quick-fried pearl lapping, which is characterized in that the rice
Protein concentrate, carragheen, gellan gum, chitosan, minced fillet, ethyl cellulose, glycerine, 6 dehydrated alcohols, deionized water weight
Amount part is 10 ~ 20 parts of rice protein concentrates, 10 ~ 20 parts of carragheens, 10 ~ 20 parts of gellan gums, 30 ~ 40 parts of chitosans, 20 ~ 30 parts
Minced fillet, 10 ~ 20 parts of ethyl celluloses, 40 ~ 50 parts of glycerine, 60 ~ 80 parts of dehydrated alcohols, 100 ~ 120 parts of deionized waters.
3. a kind of cigarette according to claim 1 preparation method of quick-fried pearl lapping, which is characterized in that step (4) institute
The acetic acid that it is 1% using mass fraction that the pH stated, which is adjusted,.
4. a kind of cigarette according to claim 1 preparation method of quick-fried pearl lapping, which is characterized in that step (5) institute
The cigarette stated is with quick-fried pearl lapping with a thickness of 0.4 ~ 0.6mm.
5. a kind of cigarette according to claim 1 preparation method of quick-fried pearl lapping, which is characterized in that step (2) institute
The specific preparation step for the rice protein concentrate stated are as follows:
(1) sodium hydroxide is added in deionized water, 10 ~ 15min is stirred with 150 ~ 200r/min revolving speed under room temperature, obtains sodium hydroxide
Solution；
(2) milled rice flour is added in sodium hydroxide solution, 30 ~ 40min is stirred with 200 ~ 300r/min revolving speed under room temperature, must be mixed
Liquid；
(3) mixed liquor is placed in a centrifuge and 5 ~ 10min is centrifugated with 5000 ~ 6000r/min revolving speed, take supernatant liquor, adjusted
PH to 4.5 ~ 5.5 is saved, reaction clear liquid is obtained；
(4) reaction clear liquid is centrifugated under 5000 ~ 6000r/min revolving speed 10min, lower layer's deposit is taken, by sediment
Matter is added in deionized water, adjusts pH to 6.5 ~ 7.5, obtains mechanism liquid；
(5) regulation mechanism liquid pH to 4.5 ~ 5.5 obtains reaction mechanism liquid；
(6) reaction mechanism liquid is placed in a centrifuge under room temperature and 5 ~ 10min is centrifugated with 6000 ~ 7000r/min revolving speed, removed
Layer solid, room temperature dry, and obtain rice protein concentrate.
6. a kind of cigarette according to claim 5 preparation method of quick-fried pearl lapping, which is characterized in that the rice
Powder, sodium hydroxide, deionized water parts by weight be 20 ~ 30 parts of milled rice flours, 4 ~ 6 parts of sodium hydroxides, 40 ~ 60 parts of deionized waters.
7. a kind of cigarette according to claim 5 preparation method of quick-fried pearl lapping, which is characterized in that step (3) institute
The pH stated adjusts the hydrochloric acid using mass concentration 1%.
8. a kind of cigarette according to claim 5 preparation method of quick-fried pearl lapping, which is characterized in that step (4) institute
The deposit and deionized water quality ratio stated are 1:5, and pH adjusts the sodium hydroxide solution using mass concentration 1%.
9. a kind of cigarette according to claim 5 preparation method of quick-fried pearl lapping, which is characterized in that step (5) institute
The hydrochloric acid that it is 1% using mass concentration that the pH stated, which is adjusted,.
10. a kind of cigarette according to claim 5 preparation method of quick-fried pearl lapping, which is characterized in that step (2) institute
The specific preparation step for the milled rice flour stated are as follows:
Polished rice is placed in ball mill under room temperature with 300 ~ 350r/min revolving speed 1 ~ 2h of ball milling, 60 ~ 80 meshes is crossed, obtains milled rice flour.
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| CN201910416518.6A CN110183696A (en) | 2019-05-20 | 2019-05-20 | A kind of preparation method of the quick-fried pearl lapping of cigarette |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910416518.6A CN110183696A (en) | 2019-05-20 | 2019-05-20 | A kind of preparation method of the quick-fried pearl lapping of cigarette |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111728124A (en) * | 2020-07-08 | 2020-10-02 | 江苏宏远药业有限公司 | Food-grade white pigment with high safety |
| CN113367383A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Water blasting bead |
| CN113367378A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Preparation method of water blasting bead |
| CN113367379A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Tobacco product |
-
2019
- 2019-05-20 CN CN201910416518.6A patent/CN110183696A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113367383A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Water blasting bead |
| CN113367378A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Preparation method of water blasting bead |
| CN113367379A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Tobacco product |
| CN111728124A (en) * | 2020-07-08 | 2020-10-02 | 江苏宏远药业有限公司 | Food-grade white pigment with high safety |
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