CN110115703A - A kind of sterilization toothpaste and preparation method thereof using betel nut as main material - Google Patents

A kind of sterilization toothpaste and preparation method thereof using betel nut as main material Download PDF

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Publication number
CN110115703A
CN110115703A CN201910453168.0A CN201910453168A CN110115703A CN 110115703 A CN110115703 A CN 110115703A CN 201910453168 A CN201910453168 A CN 201910453168A CN 110115703 A CN110115703 A CN 110115703A
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CN
China
Prior art keywords
betel nut
parts
extract
toothpaste
main material
Prior art date
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Pending
Application number
CN201910453168.0A
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Chinese (zh)
Inventor
郭眙铄
陈显利
周少萍
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Haining Daily Yuxing Chemical Co Ltd
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Haining Daily Yuxing Chemical Co Ltd
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Priority to CN201910453168.0A priority Critical patent/CN110115703A/en
Publication of CN110115703A publication Critical patent/CN110115703A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/02Local antiseptics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses

Abstract

Use betel nut for the sterilization toothpaste of main material the invention discloses a kind of, raw material mainly comprises the following components in parts by weight: 20-30 parts of betelnut extract, 3-7 parts of Chinese rhubarb extract, 3-7 parts of Scutellaria baicalensis extract, 3-7 parts of phellodendron extract, 3-7 parts of cinnamomum cassia extract, 10-12 parts of rubbing agent, 8-12 parts of wetting agent, 3-7 parts of adhesive, 6-8 parts of foaming agent, deionized water are several.The present invention is with betel nut for main raw material, its by extracting that its effective sterilizing oral ingredient is effectively is melted into tooth mug field, has stronger specific aim for sterilizing oral, cooperates other anti-inflammatory antipathogenic compositions, the construction that can be realized the intracavitary antibacterial environment of counterpart, facilitates human health.

Description

A kind of sterilization toothpaste and preparation method thereof using betel nut as main material
Technical field
It is specifically a kind of to use betel nut for the sterilization toothpaste of main material and its preparation side the present invention relates to a kind of toothpaste Method.
Background technique
The general multiple and internal environment of oral cavity of mouth disease is lacked of proper care, and is led to bacteria breed, is destroyed tooth, then induces periodontal disease Disease is common mouth disease, and symptom mainly has bleeding gums, swelling, pain.Periodontosis is not only to influence the health of tooth, It also will affect the health of whole body.Periodontosis has caused the concern of people to the influence of whole body health in recent years.Bacterial component and thin Bacterium product is easy to be diffused into attachment by oral pocket ulcer surface or is far apart organ, leads to or aggravate certain general diseases, is such as preced with The development of the diseases such as heart trouble, low class origin weight youngster, diabetes, pulmonary infection, seriously endangers human health.
Toothpaste, for cleaning tooth, protects the daily necessities of oral hygiene, consumer is accustomed to already every as a kind of The middle use of brushing teeth of day early, late.With the enhancing that consumer healthcare realizes, more healthcare function demands are proposed to toothpaste, Expectation can prevent and treat certain disease while brushing teeth, for example auxiliary prevents and treats mouth disease and cardiovascular and cerebrovascular disease The chronic diseases such as disease.Occur in toothpaste market at present it is many addition active ingredient of Chinese herbs functional toothpaste, as pseudo-ginseng toothpaste, Mica filled polypropylene etc., but the pseudo-ginseng distributional region of its functional component is few, and growth cycle is long and price is high.
Betel nut is as a kind of important Chinese medicine, and by the welcome of many people, but the mode of practical betel nut is endangered at present Evil is larger, so cause betel nut unsalable, but really containing the effective component for human oral cavity sterilization in betel nut, so by Bin Bulky toothpaste can adequately utilize the bactericidal effect of betel nut, while betel nut also has very big side to social development using the expansion of approach It helps.
Summary of the invention
The purpose of the present invention is to provide a kind of sterilization toothpaste and preparation method thereof for using betel nut as main material, with solution Certainly the problems mentioned above in the background art.
To achieve the above object, the invention provides the following technical scheme:
A kind of to use betel nut for the sterilization toothpaste of main material, raw material mainly comprises the following components in parts by weight: betel nut 20-30 parts of extract, 3-7 parts of Chinese rhubarb extract, 3-7 parts of Scutellaria baicalensis extract, 3-7 parts of phellodendron extract, cinnamomum cassia extract 3-7 Part, 10-12 parts of rubbing agent, 8-12 parts of wetting agent, 3-7 parts of adhesive, 6-8 parts of foaming agent, deionized water are several.
As a further solution of the present invention: the rubbing agent is one of calcite in powder, calcium monohydrogen phosphate, silica Or multiple combinations.
As a further solution of the present invention: the wetting agent is that glycerol, sorbierite, propylene glycol etc. are one such or more Kind combination.
As a further solution of the present invention: described adhesive is xanthan gum (xanthan gum), modified guar, carragheen etc. One such or multiple combinations.
As a further solution of the present invention: the foaming agent is laruyl alcohol sodium sulfovinate, lauryl sodium sulfate, laurel The one such or multiple combinations such as acylsarcosine sodium, dodecanoyl sodium sarcosinate.
It is a kind of to use betel nut for the preparation method for sterilizing toothpaste of main material, the specific steps of which are as follows:
(1) flower for cutting and falling off on flower and ground on betel nut tree branches and leaves is collected in spring, utilizes ultrasonic cleaning Device clean up it is spare, and under the sun under be exposed to the sun disinfection and drying;Betel nut is picked in the season of betel nut maturation simultaneously and is cleaned Clean then drying for standby;
(2) effective component extraction is carried out to betel nut flower and betel nut, specific extracting method is as follows:
A, betel nut flower and betel nut are subjected to low-temperature grinding, when crushing is kept for -5-0 degrees Celsius of temperature, avoids temperature excessively high It causes organic drug ingredient to be damaged, while can guarantee to be effectively split into solid-state under low temperature, be conducive to active principle and fiber Etc. materials separation;
B, the betel nut flower completed will be crushed and betel nut is individually stored and stood, 1-3 degrees Celsius of temperature of raising is simultaneously low Temperature stands 4-6 hours, and extractant is then directly added into powder;The raw material powder mixed in extractant is placed in centrifugation apparatus In be stirred centrifugation;
C, the extract liquor of previous step is separated and stays aqueous areca nut extract;
(3) rubbing agent, wetting agent, adhesive and foaming agent are added in blending tank and be mixed to get paste, and using go from Sub- water adjusts concentration, controls mixing temperature between 6-8 degrees Celsius;Then aqueous areca nut extract and Chinese rhubarb extract, scutellaria are mentioned It takes object, phellodendron extract, cinnamomum cassia extract to be mixed to get extract mixed liquor, extract mixed liquor and paste is mixed and obtain Bin Bulky toothpaste.
As a further solution of the present invention: the betel nut flower and betel nut obtained for the first time in the step (2) increases temperature 1-3 degrees Celsius and stand at low temperature 6-8 hours.
As a further solution of the present invention: the revolving speed of centrifugal mixer is 200-300rad/min in the step (2).
As a further solution of the present invention: the speed of agitator in the step (3) when mixing is 300-500rad/min, Mixing time 40-60 minutes.
Compared with prior art, the beneficial effects of the present invention are: the present invention with betel nut be main raw material, by extracting it Effective sterilizing oral ingredient be its effectively be melted into tooth mug field, there is stronger specific aim for sterilizing oral, cooperate Other anti-inflammatory antipathogenic compositions can be realized the construction of the intracavitary antibacterial environment of counterpart, facilitate human health.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Embodiment 1
A kind of to use betel nut for the sterilization toothpaste of main material in the embodiment of the present invention, raw material mainly includes following heavy Measure the component of part: 20 parts of betelnut extract, 3 parts of Chinese rhubarb extract, 3 parts of Scutellaria baicalensis extract, 3 parts of phellodendron extract, cortex cinnamomi are extracted 3 parts of object, 10 parts of rubbing agent, 8 parts of wetting agent, 3 parts of adhesive, 6 parts of foaming agent, deionized water are several.
It is a kind of to use betel nut for the preparation method for sterilizing toothpaste of main material, the specific steps of which are as follows:
(1) flower for cutting and falling off on flower and ground on betel nut tree branches and leaves is collected in spring, utilizes ultrasonic cleaning Device clean up it is spare, and under the sun under be exposed to the sun disinfection and drying;Betel nut is picked in the season of betel nut maturation simultaneously and is cleaned Clean then drying for standby;
(2) effective component extraction is carried out to betel nut flower and betel nut, specific extracting method is as follows:
A, betel nut flower and betel nut are subjected to low-temperature grinding, when crushing is kept for -5 degrees Celsius of temperature, avoids temperature is excessively high from making It is damaged at organic drug ingredient, while can guarantee to be effectively split into solid-state under low temperature, be conducive to active principle and fiber etc. Material separation;
B, the betel nut flower completed will be crushed and betel nut is individually stored and stood, increase 1 degree Celsius of temperature and low temperature 4 hours are stood, extractant is then directly added into powder;By the raw material powder mixed in extractant be placed in centrifugation apparatus into Row stirring centrifugation, the revolving speed of centrifugal mixer is 200rad/min, and main purpose is the Chinese medicine material by centrifugal force by crushing Interior effective component is thrown away and compatible with extract liquor;
C, the extract liquor of previous step is separated and stays aqueous areca nut extract;
(3) rubbing agent, wetting agent, adhesive and foaming agent are added in blending tank and be mixed to get paste, and using go from Sub- water adjusts concentration, controls mixing temperature between 6 degrees Celsius;Then aqueous areca nut extract and Chinese rhubarb extract, scutellaria are extracted Object, phellodendron extract, cinnamomum cassia extract are mixed to get extract mixed liquor, and extract mixed liquor and paste are mixed Object, speed of agitator when mixing is 300rad/min, mixing time 40 minutes, finally obtains betel nut toothpaste.
Embodiment 2
A kind of to use betel nut for the sterilization toothpaste of main material in the embodiment of the present invention, raw material mainly includes following heavy Measure the component of part: 25 parts of betelnut extract, 5 parts of Chinese rhubarb extract, 5 parts of Scutellaria baicalensis extract, 5 parts of phellodendron extract, cortex cinnamomi are extracted 5 parts of object, 11 parts of rubbing agent, 10 parts of wetting agent, 5 parts of adhesive, 7 parts of foaming agent, deionized water are several.
It is a kind of to use betel nut for the preparation method for sterilizing toothpaste of main material, the specific steps of which are as follows:
(1) flower for cutting and falling off on flower and ground on betel nut tree branches and leaves is collected in spring, utilizes ultrasonic cleaning Device clean up it is spare, and under the sun under be exposed to the sun disinfection and drying;Betel nut is picked in the season of betel nut maturation simultaneously and is cleaned Clean then drying for standby;
(2) effective component extraction is carried out to betel nut flower and betel nut, specific extracting method is as follows:
A, betel nut flower and betel nut are subjected to low-temperature grinding, when crushing is kept for -2 degrees Celsius of temperature, avoids temperature is excessively high from making It is damaged at organic drug ingredient, while can guarantee to be effectively split into solid-state under low temperature, be conducive to active principle and fiber etc. Material separation;
B, the betel nut flower completed will be crushed and betel nut is individually stored and stood, increase 2 degrees Celsius of temperature and low temperature 5 hours are stood, extractant is then directly added into powder;By the raw material powder mixed in extractant be placed in centrifugation apparatus into Row stirring centrifugation, the revolving speed of centrifugal mixer is 250rad/min, and main purpose is the Chinese medicine material by centrifugal force by crushing Interior effective component is thrown away and compatible with extract liquor;
C, the extract liquor of previous step is separated and stays aqueous areca nut extract;
(3) rubbing agent, wetting agent, adhesive and foaming agent are added in blending tank and be mixed to get paste, and using go from Sub- water adjusts concentration, controls mixing temperature between 7 degrees Celsius;Then aqueous areca nut extract and Chinese rhubarb extract, scutellaria are extracted Object, phellodendron extract, cinnamomum cassia extract are mixed to get extract mixed liquor, and extract mixed liquor and paste are mixed Object, speed of agitator when mixing is 400rad/min, mixing time 50 minutes, finally obtains betel nut toothpaste.
Embodiment 3
A kind of to use betel nut for the sterilization toothpaste of main material in the embodiment of the present invention, raw material mainly includes following heavy Measure the component of part: 30 parts of betelnut extract, 7 parts of Chinese rhubarb extract, 7 parts of Scutellaria baicalensis extract, 7 parts of phellodendron extract, cortex cinnamomi are extracted 7 parts of object, 12 parts of rubbing agent, 12 parts of wetting agent, 7 parts of adhesive, 8 parts of foaming agent, deionized water are several.
It is a kind of to use betel nut for the preparation method for sterilizing toothpaste of main material, the specific steps of which are as follows:
(1) flower for cutting and falling off on flower and ground on betel nut tree branches and leaves is collected in spring, utilizes ultrasonic cleaning Device clean up it is spare, and under the sun under be exposed to the sun disinfection and drying;Betel nut is picked in the season of betel nut maturation simultaneously and is cleaned Clean then drying for standby;
(2) effective component extraction is carried out to betel nut flower and betel nut, specific extracting method is as follows:
A, betel nut flower and betel nut are subjected to low-temperature grinding, when crushing is kept for 0 degree Celsius of temperature, avoids temperature is excessively high from causing Organic drug ingredient is damaged, while can guarantee to be effectively split into solid-state under low temperature, is conducive to the materials such as active principle and fiber Matter separation;
B, the betel nut flower completed will be crushed and betel nut is individually stored and stood, increase 3 degrees Celsius of temperature and low temperature 6 hours are stood, extractant is then directly added into powder;By the raw material powder mixed in extractant be placed in centrifugation apparatus into Row stirring centrifugation, the revolving speed of centrifugal mixer is 300rad/min, and main purpose is the Chinese medicine material by centrifugal force by crushing Interior effective component is thrown away and compatible with extract liquor;
C, the extract liquor of previous step is separated and stays aqueous areca nut extract;
(3) rubbing agent, wetting agent, adhesive and foaming agent are added in blending tank and be mixed to get paste, and using go from Sub- water adjusts concentration, controls mixing temperature between 8 degrees Celsius;Then aqueous areca nut extract and Chinese rhubarb extract, scutellaria are extracted Object, phellodendron extract, cinnamomum cassia extract are mixed to get extract mixed liquor, and extract mixed liquor and paste are mixed Object, speed of agitator when mixing is 500rad/min, mixing time 60 minutes, finally obtains betel nut toothpaste.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (9)

1. a kind of use betel nut for the sterilization toothpaste of main material, which is characterized in that its raw material mainly includes following parts by weight Component: 20-30 parts of betelnut extract, 3-7 parts of Chinese rhubarb extract, 3-7 parts of Scutellaria baicalensis extract, 3-7 parts of phellodendron extract, cortex cinnamomi mention Take 3-7 parts of object, 10-12 parts of rubbing agent, 8-12 parts of wetting agent, 3-7 parts of adhesive, 6-8 parts of foaming agent, deionized water several.
2. according to claim 1 use betel nut for the sterilization toothpaste of main material, which is characterized in that the rubbing agent is One of calcite in powder, calcium monohydrogen phosphate, silica or multiple combinations.
3. according to claim 1 use betel nut for the sterilization toothpaste of main material, which is characterized in that the wetting agent is One of glycerol, sorbierite, propylene glycol or multiple combinations.
4. according to claim 1 use betel nut for the sterilization toothpaste of main material, which is characterized in that described adhesive is One of xanthan gum, modified guar, carragheen or multiple combinations.
5. according to claim 1 use betel nut for the sterilization toothpaste of main material, which is characterized in that the foaming agent is One of laruyl alcohol sodium sulfovinate, lauryl sodium sulfate, sodium lauroyl sarcosine, dodecanoyl sodium sarcosinate or a variety of groups It closes.
6. a kind of preparation method of sterilization toothpaste for main material that uses betel nut according to claim 1, feature exists In, the specific steps of which are as follows:
(1) flower for cutting and falling off on flower and ground on betel nut tree branches and leaves is collected in spring, it is clear using ultrasonic cleaner Wash clean is spare, and under the sun under be exposed to the sun disinfection and drying;Betel nut is picked in the season of betel nut maturation simultaneously and is cleaned up Then drying for standby;
(2) effective component extraction is carried out to betel nut flower and betel nut, specific extracting method is as follows:
A, betel nut flower and betel nut are subjected to low-temperature grinding, when crushing is kept for -5-0 degrees Celsius of temperature, avoids temperature is excessively high from causing Organic drug ingredient is damaged, while can guarantee to be effectively split into solid-state under low temperature, is conducive to the materials such as active principle and fiber Matter separation;
B, the betel nut flower completed will be crushed and betel nut is individually stored and stood, increased 1-3 degrees Celsius of temperature and low temperature is quiet It sets 4-6 hours, extractant is then directly added into powder;By the raw material powder mixed in extractant be placed in centrifugation apparatus into Row stirring centrifugation;
C, the extract liquor of previous step is separated and stays aqueous areca nut extract;
(3) rubbing agent, wetting agent, adhesive and foaming agent are added in blending tank and are mixed to get paste, and utilize deionized water Concentration is adjusted, controls mixing temperature between 6-8 degrees Celsius;Then by aqueous areca nut extract and Chinese rhubarb extract, Scutellaria baicalensis extract, Phellodendron extract, cinnamomum cassia extract are mixed to get extract mixed liquor, and extract mixed liquor and paste are mixed and obtain betel nut tooth Cream.
7. according to claim 6 use betel nut for the preparation method for sterilizing toothpaste of main material, which is characterized in that institute It states the betel nut flower obtained for the first time in step (2) and betel nut increases 1-3 degrees Celsius of temperature and stand at low temperature 6-8 hours.
8. according to claim 6 use betel nut for the preparation method for sterilizing toothpaste of main material, which is characterized in that institute The revolving speed for stating centrifugal mixer in step (2) is 200-300rad/min.
9. according to claim 6 use betel nut for the preparation method for sterilizing toothpaste of main material, which is characterized in that institute Stating speed of agitator when mixing in step (3) is 300-500rad/min, mixing time 40-60 minutes.
CN201910453168.0A 2019-05-28 2019-05-28 A kind of sterilization toothpaste and preparation method thereof using betel nut as main material Pending CN110115703A (en)

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CN201910453168.0A CN110115703A (en) 2019-05-28 2019-05-28 A kind of sterilization toothpaste and preparation method thereof using betel nut as main material

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Application Number Priority Date Filing Date Title
CN201910453168.0A CN110115703A (en) 2019-05-28 2019-05-28 A kind of sterilization toothpaste and preparation method thereof using betel nut as main material

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105232403A (en) * 2015-11-11 2016-01-13 曹涛 Anti-allergy toothpaste capable of achieving prevention and adjuvant treatment of stomach illness
CN105687028A (en) * 2016-01-29 2016-06-22 海南宇星日用化工股份有限公司 Betel palm toothpaste

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105232403A (en) * 2015-11-11 2016-01-13 曹涛 Anti-allergy toothpaste capable of achieving prevention and adjuvant treatment of stomach illness
CN105687028A (en) * 2016-01-29 2016-06-22 海南宇星日用化工股份有限公司 Betel palm toothpaste

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Application publication date: 20190813

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