CN110106603A - A kind of Graphene antibiosis fabric and preparation method thereof - Google Patents
A kind of Graphene antibiosis fabric and preparation method thereof Download PDFInfo
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- CN110106603A CN110106603A CN201910330442.5A CN201910330442A CN110106603A CN 110106603 A CN110106603 A CN 110106603A CN 201910330442 A CN201910330442 A CN 201910330442A CN 110106603 A CN110106603 A CN 110106603A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/94—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of other polycondensation products
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- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
- D02G3/04—Blended or other yarns or threads containing components made from different materials
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/40—Fibres of carbon
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- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/10—Inorganic fibres based on non-oxides other than metals
- D10B2101/12—Carbon; Pitch
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- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
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- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
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Abstract
The invention discloses a kind of Graphene antibiosis fabrics, it contains the following parts by weight: 80-140 parts of graphene composite fibres, 10-15 parts of bamboo charcoal fibers, 6-12 portions of PTT, 30-50 portions of cottons, 8-12 parts of antibacterial agent, wherein, graphene composite fibre includes 0.6-1.5 parts of graphenes, 79.4-138.5 parts of fibrous matrixes；The preparation method of graphene composite fibre includes the following steps: S1, pretreatment, S2, dry-mixed, S3, granulation, S4, melt spinning, S5, drafting forming is blended, to obtain graphene composite fibre；The preparation method of Graphene antibiosis fabric, comprising: S1, scribbled, S2, mercerising, S3, warping weaving, S4, face weave, S5, antibiotic finish, S6, the final finishing for carrying out dyeing and finishing, washing, sizing, preshrunk.Graphene antibiosis fabric of the invention has comfortable soft, ventilative nice and cool, the advantage that anti-microbial property is lasting, efficient.
Description
Technical field
The present invention relates to fabric processing technique field, in particular to a kind of Graphene antibiosis fabric and preparation method thereof.
Background technique
Fabric is the material for making clothes, can not only annotate the style of clothes as one of clothes three elements
And characteristic, and it is directly related to the expression effect of clothing color, moulding.With being gradually increased for people's living standard, people
The requirement of more and more functional and style aspects is proposed to fabric, therefore conventional fabric can no longer meet market
Demand.
Functional fiber specifically includes that modified fibre, such as in the modified acquisition anti-pilling, antistatic property, parent of feed stage
Aqueous, anti-flammability etc.；Functional topical finishing generally comprises: comfort finishing, be embodied in ventilative, moisture-inhibiting, it is slim and graceful, smooth, prevent it is quiet
The arrangement of electricity etc..Wholesomeness arranges, and embodies its antibacterial and deodouring；Protective arranges, and is embodied in fire-retardant, uvioresistant, prevents
Radiation etc.；Health arranges, and is embodied in beauty pro-skin, far infrared；Easily keeping property arranges, and it is whole to be embodied in crease-resistant, mothproof function
Reason；The feature of environmental protection arranges, and is embodied in ring close friend, green non-pollution.
Existing application publication number is the Chinese invention patent of CN109137191A, discloses a kind of nice and cool yarn of Graphene antibiosis
The preparation method of line, yarn include the graphene polyamide fibre composite fibre that parts by weight are 70-90 parts, 10-18 parts of bamboo fibre, 5-
15 parts of viscose rayon, by mixed cotton, cotton carding, drafting, spun yarn, winder spinning at line.
Although having the fiber of anti-microbial property in prior art using graphene polyamide fibre composite fibre, bamboo fibre etc.,
But further antibiotic finish is not carried out to fabric, therefore the anti-microbial property of fabric will receive certain restrictions.
Summary of the invention
The purpose of the present invention is to provide a kind of Graphene antibiosis fabric and preparation method thereof, manufactured fabric has comfortable
Softness is breathed freely nice and cool, the advantage that anti-microbial property is lasting, efficient.
To achieve the above object, the present invention provides the following technical scheme that a kind of Graphene antibiosis fabric, includes following heavy
Measure the component of part:
80-140 parts of graphene composite fibres, 10-15 parts of bamboo charcoal fibers, 6-12 portions of PTT, 30-50 portions of cottons, 8-12 parts of antibacterial agent.
By using above-mentioned technical proposal, graphene composite fibre is a kind of that graphene is novel in conjunction with general fibre
Tec fiber can significantly improve fiber and antibacterial fabric using the excellent anti-microbial property of graphene, Low Temperature Far Infrared function
Performance.Relative to traditional inorganic, organic antibacterial agent, graphene is green safe, more suitable for human skin, has pro-skin foster skin
Effect；On the other hand, graphene conductive is high, in conjunction with general carbon fiber, the electric conductivity of fiber can be improved, and then increase and knit
The antistatic property of object.
Bamboo charcoal fiber is the tencel with honeycomb microporous structure formed using moso bamboo as Raw material processing, has and inhales
Penetrable ventilated, bacteriostasis antibiosis, anti-ultraviolet effect are ideal antibacterial fabric fibers, can effectively improve the ventilative of fabric
Hygroscopicity and anti-microbial property.
Ptt fiber is 1,3 propylene glycol ester fiber of poly terephthalic acid, and fiber anti-pollution is good, and stainability is good, feel is soft
Soft, high resilience, extensibility can spandex fibre shoulder to shoulder, but be more readily processed than elastomer spandex, be very suitable to make weaving clothes
Fill fabric.
Cotton fiber softness skin-friendly is good, moisture absorbing and sweat releasing and abundant raw materials are cheap, can be further improved the dress of fabric
Comfort level, while the processing cost of fabric can also be reduced.
Antibacterial agent is added in fabric antibiotic finish process, antibacterial agent can be adsorbed, be infiltrated into inside face liber, from
And further increase the anti-microbial property of fabric.
The present invention is further arranged to, and the graphene composite fibre includes 0.6-1.5 parts of graphenes, 79.4-138.5 parts
Fibrous matrix.
By using above-mentioned technical proposal, graphene and fibrous matrix are organically combined, so that fiber has the spy of graphene
Property and function, to assign the antibacterial of fabric persistent high efficiency, antistatic property.
The present invention is further arranged to, and the fibrous matrix is any one of terylene, spandex.
By using above-mentioned technical proposal, terylene constancy is good, elastic high, corrosion-resistant, and processing technology is mature, price phase
To lower；Elastomeric polyurethane fiber is excellent, and intensity is high, and line density is thinner, chemically-resistant degradation, resistance to acid and alkali, sweat proof, dry cleaning resistance and wear-resisting
Property is preferable, and for spandex since molecular structure is closer and amino acid molecular structure, skin-friendly comfort is good.
The present invention is further arranged to, and the preparation method of the graphene composite fibre includes the following steps:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 60-100 DEG C, when dry
Between be 8-15h；
It is S2, dry-mixed: graphene, fibrous matrix are put into high-speed mixer, adjust revolving speed 220-300rpm, mixes 1-3min, then
Revolving speed 800-1000rpm is adjusted, 1-2min is continuesd to mix, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 180-220 DEG C, revolving speed 80-160rpm, and the melt blending time is 3-6min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning, spinning temperature 180-230 are carried out to graphene fiber master batch using melt spinning machine
DEG C, winding speed is set as 1500-2800m/min, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 85-120 DEG C, and drafting multiple is 2-8 times,
Finally obtain graphene composite fibre.
By using above-mentioned technical proposal, graphene, the fibrous matrix after vacuum drying are carried out it is dry-mixed, can with when graphite
Alkene is uniformly mixed with fibrous matrix, obtains graphene-fibrous matrix mixture, then melt altogether by twin-screw blender
Mixed, so that graphene and fibrous matrix be made to carry out depth integration, graphene can evenly spread to fibrous inside, improve graphite
Fastness of the alkene in conjunction with fiber；Again by carrying out melt spinning to graphene fiber master batch, the higher graphene of dispersion degree is obtained
As-spun fibre, then degree of orientation when passing through drafting forming inside graphene as-spun fibre and crystallinity improve, to further mention
The intensity and elongation of high microsteping.
The present invention is further arranged to, and the antibacterial agent is silicone Quaternary Ammonium Salt Antimicrobial Agent.
By using above-mentioned technical proposal, organosilicon quaternary ammonium salt is the ideal antibacterial agent of a kind of comprehensive performance, finish fabric
When such antibacterial agent do not need high temperature baking, just can produce lasting antibacterial effect after general drying, the fabric after arrangement is not only
With excellent anti-microbial property, and be also equipped with good moisture absorption absorption of perspiration, flexibility, flatness, resilience, static electricity resistance and
Resistance tocrocking.
The present invention is further arranged to, the preparation method of the Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain graphene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 160- on sectional warper
180m/min, beaming speed are 115-140m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: configuration quality percentage concentration is the machine silicon quaternary ammonium salt antiseptic solution of 8%-12%, by the face of S4 step
Material is impregnated in antimicrobial, and bath raio is (4:1)-(5:1), and dip time is 30-60 minutes, after dipping at 75-85 DEG C
It is dried, drying time is 25-35 minutes；
S6, final finishing: the fabric of S5 step is subjected to final finishing.
It is blended to obtain graphene scribbled by using above-mentioned technical proposal, so that yarn has the compound of multifilament
Characteristic and function, so that providing basis for fabric is also permanent anti-microbial property；Mercerising improves fiber especially cotton fiber
Intensity and lustrous surface so that the colourability of fiber further increases；Antibacterial and final finishing are carried out to fabric, so that fabric is anti-
Bacterium performance, wrinkle resistance, feel etc. have further promotion.
The present invention is further arranged to, and the line density of the graphene composite fibre is 1-1.5D, fibre length 30-
42mm。
By using above-mentioned technical proposal, the graphene composite fibre fiber number of the specification is thinner, and fibre length is moderate, easily
In spinning processing.
The present invention is further arranged to, and the number of the graphene scribbled in the S1 step is 15-100 branch.
By using above-mentioned technical proposal, the graphene scribbled in the count range hangs down, and pliable, intensity is relatively high,
Face weave can be carried out well.
The present invention is further arranged to, and the finishing process in the S6 step includes dyeing and finishing, washing, sizing, preshrunk work
Sequence.
By using above-mentioned technical proposal, washing can be removed the loose colour of web surface and impurity, and pass through and be formed, is pre-
Contracting can effectively reduce the washing contraction distortion in the subsequent use process of fabric.
In conclusion the invention has the following advantages:
1. the graphene composite fibre in the present invention, by the way that graphene, fibrous matrix to be blended to granulation in twin-screw blender,
Graphene fiber master batch is formed, graphene fiber master batch is being formed into graphene composite fibre by melt spinning, so that graphite
Alkene obtains in conjunction with high degree of dispersion with fiber in molecular level, thus near permanent imparting fiber with the characteristic of graphene；
2. adding bamboo charcoal fiber in the fabric in the present invention, the anti-microbial property of fabric can be further improved, while also further
Improve flexibility, the sucting wet air permeability of fabric；
3. adding ptt fiber in the fabric in the present invention, the feature high using ptt fiber soil resistance, stainability is good be can be improved
The dyefastness of fabric and refuse the antifouling performance of oil；
4. the fabric in the present invention passes through the antibiotic finish of silicone Quaternary Ammonium Salt Antimicrobial Agent finishing fluid, so that antibacterial agent is adsorbed and soaked
Profit is into face liber, to achieve the effect that further increase fabric anti-microbial property.
Specific embodiment
Invention is further described in detail with reference to embodiments.
Embodiment
Embodiment 1:
A kind of Graphene antibiosis fabric, contains the following parts by weight:
80 parts of graphene composite fibres, 10 parts of bamboo charcoal fibers, 6 parts of PTT, 30 portions of cottons, 8 parts of antibacterial agents；Wherein, the compound fibre of graphene
Dimension includes 0.6 part of graphene, 79.4 parts of fibrous matrix.
The preparation step of graphene composite fibre is as follows:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 60 DEG C, and drying time is
8h；
It is S2, dry-mixed: graphene, fibrous matrix being put into high-speed mixer, revolving speed 220rpm is adjusted, mixes 1min, then adjust and turn
Fast 800rpm, continuess to mix 1min, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 180 DEG C, revolving speed 80rpm, and the melt blending time is 3min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning is carried out to graphene fiber master batch using melt spinning machine, spinning temperature is 180 DEG C, volume
It is set as 1500m/min around speed, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 85 DEG C, and drafting multiple is 2 times, final
It is 1D to line density, fibre length is the graphene composite fibre of 30mm.
The preparation method of Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, it is mixed to obtain 15 graphenes
Yarn；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 160m/ on sectional warper
Min, beaming speed are 115m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: the machine silicon quaternary ammonium salt antiseptic solution that configuration quality percentage concentration is 8% soaks the fabric of S4 step
Stain is in antimicrobial, bath raio 4:1, and dip time is 30 minutes, is dried at 75 DEG C after dipping, drying time is
25min；
S6, final finishing: the fabric of S5 step is carried out to the final finishing of dyeing and finishing, washing, sizing, preshrunk.
Embodiment 2:
A kind of Graphene antibiosis fabric, contains the following parts by weight:
92 parts of graphene composite fibres, 12 parts of bamboo charcoal fibers, 8 parts of PTT, 35 portions of cottons, 9 parts of antibacterial agents；Wherein, the compound fibre of graphene
Dimension includes 0.8 part of graphene, 91.2 parts of fibrous matrix.
The preparation step of graphene composite fibre is as follows:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 70 DEG C, and drying time is
10h；
It is S2, dry-mixed: graphene, fibrous matrix being put into high-speed mixer, revolving speed 240rpm is adjusted, mixes 2min, then adjust and turn
Fast 850rpm, continuess to mix 1min, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 190 DEG C, revolving speed 100rpm, and the melt blending time is 4min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning is carried out to graphene fiber master batch using melt spinning machine, spinning temperature is 190 DEG C, volume
It is set as 1800m/min around speed, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 95 DEG C, and drafting multiple is 4 times, final
It is 1-1.5D to line density, fibre length is the graphene composite fibre of 30-42mm.
The preparation method of Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain the graphite of 15-100 branch
Alkene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 165m/ on sectional warper
Min, beaming speed are 120m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: the machine silicon quaternary ammonium salt antiseptic solution that configuration quality percentage concentration is 9% soaks the fabric of S4 step
Stain is in antimicrobial, bath raio 4:1, and dip time is 35 minutes, is dried at 77 DEG C after dipping, drying time is
27min；
S6, final finishing: the fabric of S5 step is carried out to the final finishing of dyeing and finishing, washing, sizing, preshrunk.
Embodiment 3:
A kind of Graphene antibiosis fabric, contains the following parts by weight:
104 parts of graphene composite fibres, 13 parts of bamboo charcoal fibers, 10 parts of PTT, 40 portions of cottons, 10 parts of antibacterial agents；Wherein, graphene is multiple
Condensating fiber includes 1 part of graphene, 103 parts of fibrous matrix.
The preparation step of graphene composite fibre is as follows:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 80 DEG C, and drying time is
12h；
It is S2, dry-mixed: graphene, fibrous matrix being put into high-speed mixer, revolving speed 260rpm is adjusted, mixes 3min, then adjust and turn
Fast 900rpm, continuess to mix 1min, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 200 DEG C, revolving speed 120rpm, and the melt blending time is 5min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning is carried out to graphene fiber master batch using melt spinning machine, spinning temperature is 200 DEG C, volume
It is set as 2100m/min around speed, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 105 DEG C, and drafting multiple is 6 times, final
It is 1-1.5D to line density, fibre length is the graphene composite fibre of 30-42mm.
The preparation method of Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain the graphite of 15-100 branch
Alkene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 170m/ on sectional warper
Min, beaming speed are 125m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: the machine silicon quaternary ammonium salt antiseptic solution that configuration quality percentage concentration is 10% soaks the fabric of S4 step
Stain is in antimicrobial, bath raio 4:1, and dip time is 40 minutes, is dried at 79 DEG C after dipping, drying time is
29 minutes；
S6, final finishing: the fabric of S5 step is carried out to the final finishing of dyeing and finishing, washing, sizing, preshrunk.
Embodiment 4:
A kind of Graphene antibiosis fabric, contains the following parts by weight:
116 parts of graphene composite fibres, 14 parts of bamboo charcoal fibers, 11 parts of PTT, 45 portions of cottons, 11 parts of antibacterial agents；Wherein, graphene is multiple
Condensating fiber includes 1.2 parts of graphene, 114.8 parts of fibrous matrix.
The preparation step of graphene composite fibre is as follows:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 90 DEG C, and drying time is
14h；
It is S2, dry-mixed: graphene, fibrous matrix being put into high-speed mixer, revolving speed 280rpm is adjusted, mixes 3min, then adjust and turn
Fast 950rpm, continuess to mix 2min, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 210 DEG C, revolving speed 140rpm, and the melt blending time is 6min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning is carried out to graphene fiber master batch using melt spinning machine, spinning temperature is 210 DEG C, volume
It is set as 2400m/min around speed, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 115 DEG C, and drafting multiple is 8 times, final
It is 1-1.5D to line density, fibre length is the graphene composite fibre of 30-42mm.
The preparation method of Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain the graphite of 15-100 branch
Alkene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 175m/ on sectional warper
Min, beaming speed are 130m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: the machine silicon quaternary ammonium salt antiseptic solution that configuration quality percentage concentration is 11% soaks the fabric of S4 step
Stain is in antimicrobial, bath raio 4.5:1, and dip time is 50 minutes, is dried at 81 DEG C after dipping, drying time
For 32min；
S6, final finishing: the fabric of S5 step is carried out to the final finishing of dyeing and finishing, washing, sizing, preshrunk.
Embodiment 5:
A kind of Graphene antibiosis fabric, contains the following parts by weight:
140 parts of graphene composite fibres, 15 parts of bamboo charcoal fibers, 12 parts of PTT, 50 portions of cottons, 12 parts of antibacterial agents；Wherein, graphene is multiple
Condensating fiber includes 1.5 parts of graphene, 138.5 parts of fibrous matrix.
The preparation step of graphene composite fibre is as follows:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 100 DEG C, drying time
For 15h；
It is S2, dry-mixed: graphene, fibrous matrix being put into high-speed mixer, revolving speed 300rpm is adjusted, mixes 3min, then adjust and turn
Fast 1000rpm, continuess to mix 2min, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, melting is altogether
Mixed temperature is 220 DEG C, revolving speed 160rpm, and the melt blending time is 6min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning is carried out to graphene fiber master batch using melt spinning machine, spinning temperature is 230 DEG C, volume
It is set as 2800m/min around speed, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 120 DEG C, and drafting multiple is 8 times, final
It is 1-1.5D to line density, fibre length is the graphene composite fibre of 30-42mm.
The preparation method of Graphene antibiosis fabric, comprising the following steps:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain the graphite of 15-100 branch
Alkene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 180m/ on sectional warper
Min, beaming speed are 140m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: the machine silicon quaternary ammonium salt antiseptic solution that configuration quality percentage concentration is 12% soaks the fabric of S4 step
Stain is in antimicrobial, bath raio 5:1, and dip time is 60 minutes, is dried at 85 DEG C after dipping, drying time is
35min；
S6, final finishing: the fabric of S5 step is carried out to the final finishing of dyeing and finishing, washing, sizing, preshrunk.
Performance detection
The consistent sample fabric of 5 block specifications is respectively prepared according to the method for embodiment 1-5, and according to the following terms Indexs measure sample
Fabric, the test result of sample fabric as made from the same embodiment are averaged, and test result is as shown in table 1:
The indices test result of sample fabric made from 1 the above various embodiments of table
As can be seen from Table 1, the comfortable feel and pliability of 1-5 of embodiment of the present invention sample fabric are preferable, and embodiment 1-5
The grammes per square metre of sample fabric is relatively low, and illustrates that fabric of the invention is slim and graceful, is more suitable dress；It is strong in tensile strength and tearing
The testing result more stable homogeneous of degree aspect embodiment 1-5 sample fabric；In terms of color fastness, 1-5 sample of the embodiment of the present invention
Fabric reaches 3-4 grades of higher color fastness；In terms of anti-microbial property, since fabric is fine using graphene composite fibre and bamboo charcoal
Dimension, and pass through the final finishing of antibacterial agent finishing fluid, therefore achieve the effect that significantly improve fabric anti-microbial property.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (9)
1. a kind of Graphene antibiosis fabric, it is characterised in that: contain the following parts by weight:
80-140 parts of graphene composite fibres, 10-15 parts of bamboo charcoal fibers, 6-12 portions of PTT, 30-50 portions of cottons, 8-12 parts of antibacterial agent.
2. a kind of Graphene antibiosis fabric according to claim 1, it is characterised in that: the graphene composite fibre includes
0.6-1.5 parts of graphenes, 79.4-138.5 parts of fibrous matrixes.
3. a kind of Graphene antibiosis fabric according to claim 2, which is characterized in that the fibrous matrix is terylene, ammonia
Any one of synthetic fibre.
4. a kind of Graphene antibiosis fabric according to claim 2, which is characterized in that the system of the graphene composite fibre
Preparation Method includes the following steps:
S1, pretreatment: being put into graphene, fibrous matrix vacuum drying oven and be dried, and drying temperature is 60-100 DEG C, when dry
Between be 8-15h；
It is S2, dry-mixed: graphene, fibrous matrix are put into high-speed mixer, adjust revolving speed 220-300rpm, mixes 1-3min, then
Revolving speed 800-1000rpm is adjusted, 1-2min is continuesd to mix, obtains graphene-fibrous matrix premix；
S3, granulation is blended: graphene-fibrous matrix premix investment twin-screw blender is subjected to blending granulation, is melted
Blending temperature is 180-220 DEG C, revolving speed 80-160rpm, and the melt blending time is 3-6min, obtains graphene fiber master batch；
S4, melt spinning: melt spinning, spinning temperature 180-230 are carried out to graphene fiber master batch using melt spinning machine
DEG C, winding speed is set as 1500-2800m/min, obtains graphene as-spun fibre；
S5, drafting forming: carrying out drawing-off to graphene as-spun fibre, and drawing temperature is 85-120 DEG C, and drafting multiple is 2-8 times,
Finally obtain graphene composite fibre.
5. a kind of Graphene antibiosis fabric according to claim 1, which is characterized in that the antibacterial agent is organosilicone quaternary ammonium
Salt antibacterial agent.
6. the preparation method of Graphene antibiosis fabric according to claim 1-5, which is characterized in that including following
Step:
S1, scribbled: the progress of graphene composite fibre, bamboo charcoal fiber, PTT and cotton is blended, obtain graphene scribbled；
S2, mercerising: scribbled in S1 step is subjected to mercerization finish on Mercerising machines for yarns；
S3, warping weaving: the mercerized yarn that S2 step is obtained carries out warping, speed of beaming 160- on sectional warper
180m/min, beaming speed are 115-140m/min；
S4, face weave: warp thread and weft yarn that S3 step obtains are weaved；
S5, antibiotic finish: configuration quality percentage concentration is the machine silicon quaternary ammonium salt antiseptic solution of 8%-12%, by the fabric of S4 step
Be impregnated in antimicrobial, bath raio be (4:1)-(5:1), dip time be 30-60 minutes, after dipping at 75-85 DEG C into
Row drying, drying time are 25-35 minutes；
S6, final finishing: the fabric of S5 step is subjected to final finishing.
7. a kind of Graphene antibiosis fabric according to claim 4, it is characterised in that: the line of the graphene composite fibre
Density is 1-1.5D, fibre length 30-42mm.
8. a kind of preparation method of Graphene antibiosis fabric according to claim 6, it is characterised in that: in the S1 step
Graphene scribbled number be 15-100 branch.
9. a kind of preparation method of Graphene antibiosis fabric according to claim 6, it is characterised in that: in the S6 step
Finishing process include dyeing and finishing, washing, sizing, shrinking processes.
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| CN114277460A (en) * | 2021-08-03 | 2022-04-05 | 界首市圣通无纺布有限公司 | Preparation method for enhancing service performance of polyester hot melt yarn |
| CN115012094A (en) * | 2022-07-12 | 2022-09-06 | 席梦思床褥家具（苏州）有限公司 | Anti-splashing fabric for tencel graphene blended yarn |
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| CN115287803B (en) * | 2022-08-02 | 2023-08-11 | 晋江市联盛舒坦科技有限公司 | Antibacterial deodorizing self-heating functional liner cloth |
| CN115354426A (en) * | 2022-09-06 | 2022-11-18 | 朱财雄 | Preparation method of antibacterial graphene fabric |
| CN115679509A (en) * | 2022-10-18 | 2023-02-03 | 福建兆绅环保科技有限公司 | Rapid-heating antibacterial far-infrared fabric and preparation method thereof |
| CN115679509B (en) * | 2022-10-18 | 2023-11-17 | 福建兆绅环保科技有限公司 | Rapid-heating antibacterial far infrared fabric and preparation method thereof |
| CN118065024A (en) * | 2024-03-04 | 2024-05-24 | 广东七彩飞霞针织实业有限公司 | Modified polyester filament yarn-spandex blended yarn, preparation method and application |
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