CN110101609A - A kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil - Google Patents

A kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil Download PDF

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CN110101609A
CN110101609A CN201910496112.3A CN201910496112A CN110101609A CN 110101609 A CN110101609 A CN 110101609A CN 201910496112 A CN201910496112 A CN 201910496112A CN 110101609 A CN110101609 A CN 110101609A
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parts
camellia seed
phase component
seed oil
mild
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王文概
刘光中
蔡煌莉
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • A61K2800/34Free of silicones
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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Abstract

The present invention provides a kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil, it is related to cosmetic technical field, the raw material including following parts by weight: A phase component: 45-55 parts of water, 8-10 parts of lauroyl oat amino acid sodium, 6-10 parts of dodecanamide propyl hydroxy sulfo lycine, 5-8 parts of C12-13 alcohol phosphate potassium, 5-7 parts of lauryl glucoside, 0.01-0.03 parts of EDETATE SODIUM;B phase component: 6-8 parts of saponin(e, 5-10 parts of camellia seed extract, 4.2-6 parts of camellia seed oil, 0.05-0.1 parts of Polyquaternium-10,0.03-0.08 parts of citric acid;C phase component: 0.2-0.3 parts of decoyl hydroximic acid, 0.1-0.2 parts of Sensiva SC50,1,0.2-0.3 parts of 2- hexylene glycol, the present invention is using surfactants such as camellia seeds series, the amino acid systems such as camellia seed oil, camellia seed extract, tsubakisaponin, the novel organic acid of decoyl hydroximic acid replaces traditional preservatives to develop for main component, it is product safety, natural, mild, it is an ideal shampoo used also as bath lotion, it is virgin is especially suitable for pregnant baby.

Description

A kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil And preparation method thereof.
Background technique
Shampoo used also as bath lotion belongs to family daily necessity, mostly uses be made using industrial chemicals of main component currently on the market, long Phase use can generate harm to skin and hair.These ingredients include: 1) to synthesize silicone oil, it can block the pore on scalp, make At scalp itch, in some instances it may even be possible to cause to shave one's head, the sequelae of alopecia;2) laruyl alcohol sodium sulfovinate, laureth sodium sulfovinate Deng for principal surfactant, the stimulation living of this table is big, degreasing power is strong, is not easy to be flush with water, long-time stimulus causes scalp It is also easy to produce red and swollen, inflammation, and is easy also to take off scalp protection grease together, causes hair follicles damage;3) first thiazolinone, methyl Chloroisothiazole quinoline class preservative: Yi Yinqi Contact hyper sensitization, dermatitis etc..
As the improvement of people's living standards, health perception is constantly reinforced, especially infant group, skin development is endless Entirely, skin barrier ability is weak, extremely sensitive to outside stimulus, therefore people have natural, safe, mild shampoo used also as bath lotion Strong demand.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the mild no silicone oil shampoo used also as bath lotion that the present invention provides a kind of containing camellia seed oil and Preparation method, it is living using surfaces such as the camellia seeds such as camellia seed oil, camellia seed extract, tsubakisaponin series, amino acid systems Property agent, the novel organic acid of decoyl hydroximic acid replaces traditional preservatives to develop for main component, product safety, natural, mild, It is an ideal shampoo used also as bath lotion, it is virgin is especially suitable for pregnant baby.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
A kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil, the raw material including following parts by weight:
1) A phase component
45-55 parts of water, 8-10 parts of lauroyl oat amino acid sodium, 6-10 parts of dodecanamide propyl hydroxy sulfo lycine, 5-8 parts of C12-13 alcohol phosphate potassium, 5-7 parts of lauryl glucoside, 0.01-0.03 parts of EDETATE SODIUM;
2) B phase component
6-8 parts of saponin(e, 5-10 parts of camellia seed extract, 4.2-6 parts of camellia seed oil, 0.05-0.1 parts of Polyquaternium-10, lemon 0.03-0.08 parts of lemon acid;
3) C phase component
0.2-0.3 parts of decoyl hydroximic acid, 0.1-0.2 parts of Sensiva SC50,0.2-0.3 parts of 1,2- hexylene glycol.
Further, the raw material including following parts by weight:
1) A phase component
47-52 parts of water, 9-10 parts of lauroyl oat amino acid sodium, 7-9 parts of dodecanamide propyl hydroxy sulfo lycine, C12- 13 6-7 parts of alcohol phosphate potassium, 5-6 parts of lauryl glucoside, 0.02-0.03 parts of EDETATE SODIUM;
2) B phase component
7-8 parts of saponin(e, 5-7 parts of camellia seed extract, 4.2-5 parts of camellia seed oil, 0.06-0.08 parts of Polyquaternium-10, lemon 0.04-0.06 parts of lemon acid;
3) C phase component
0.22-0.25 parts of decoyl hydroximic acid, 0.1-0.2 parts of Sensiva SC50,0.2-0.3 parts of 1,2- hexylene glycol.
Further, the raw material including following parts by weight:
1) A phase component
50 parts of water, 9 parts of lauroyl oat amino acid sodium, 8 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol phosphoric acid 7 parts of ester potassium, 6 parts of lauryl glucoside, 0.03 part of EDETATE SODIUM;
2) B phase component
8 parts of saponin(e, 5 parts of camellia seed extract, 4.2 parts of camellia seed oil, 0.07 part of Polyquaternium-10,0.05 part of citric acid;
3) C phase component
0.25 part of decoyl hydroximic acid, 0.15 part of Sensiva SC50,0.25 part of 1,2- hexylene glycol.
Steps are as follows for the preparation method of the above-mentioned mild no silicone oil shampoo used also as bath lotion containing camellia seed oil:
1) first emulsion pot is heated, when emulsification kettle temperature reaches 40-60 DEG C, then sequentially adds A phase group into emulsion pot Part, using positive and negative rotation alternate agitation method, stirring is warming up to 70-75 DEG C, and 25-35min, mixing speed 20- are stirred in moisturizing 30rpm;
2) each material of B phase component is sequentially added in oily mutually system material pot, is heated to 70-75 DEG C, is stirred dissolution Uniformly, 25-35min is kept the temperature, it is ensured that solid sufficiently dissolves;
3) B phase component obtained in step 2) is pumped into emulsion pot, stirs evenly pre-emulsification 8-12min, then carries out 5-10min homogeneous, insulated and stirred 4-6min, mixing speed 25-35rpm;
4) defoaming cooling is carried out to emulsion pot under vacuum conditions, when being cooled to 40-45 DEG C, C phase is added into emulsion pot Component stirs evenly;
5) pH value is adjusted as 5.5-7.0, is discharged, is sealed with 200 mesh filter screens, weighing is sent between semi-finished product standing, to Inspection is aged 48 hours or more between room temperature is 26 DEG C of standing after the assay was approved, obtains product.
Further, in step 4), vacuum degree 0.3-0.5MPa, cooling rate is 0.4-0.6 DEG C/min.
Further, in step 4), mixing time 10-20min, mixing speed 20-30rpm.
(3) beneficial effect
The present invention provides a kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil, present invention production Product use mild surfactant, and safe and non-stimulating, skin-friendly is very good, and without using the excessive chemistry such as chemical foaming characteristic Additive, not will cause scalp and skin disturbs situations such as itching, and be very suitable to the sensibility skin such as pregnant baby child.The present invention adds camellia Seed oil component can not only moisten scalp, anti-dandruff, moreover it is possible to prevent hair loss, antipruritic formation skin protective film the effects of.Product of the present invention It is not added with traditional preservation formulations system, using decoyl hydroximic acid organic acid antipathogenic composition, substantially reduces preservative to the thorn of skin Swash effect, during the preparation process, the temperature of emulsification is 70-75 DEG C, has both guaranteed good emulsifying effectiveness, also can avoid generating oxidation The loss of phenomenon and active constituent.
Product of the present invention uses natural component, mild formulation, does not add silicone oil, alcohol, soap base, essence pigment, preservative Equal ingredients integrate safety, mild, naturally, are the excellent selections that day common hair washing is taken a shower, be especially suitable for pregnant woman, infant, Sensibility skin, the elderly etc. are used for a long time.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making Every other embodiment obtained, shall fall within the protection scope of the present invention under the premise of creative work.
Embodiment 1:
A kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil, the raw material including following parts by weight:
1) A phase component
45 parts of water, 10 parts of lauroyl oat amino acid sodium, 10 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol phosphorus 8 parts of acid esters potassium, 7 parts of lauryl glucoside, 0.02 part of EDETATE SODIUM;
2) B phase component
7 parts of saponin(e, 6 parts of camellia seed extract, 6 parts of camellia seed oil, 0.1 part of Polyquaternium-10,0.08 part of citric acid;
3) C phase component
0.3 part of decoyl hydroximic acid, 0.2 part of Sensiva SC50,0.3 part of 1,2- hexylene glycol.
The preparation method step of the above-mentioned mild no silicone oil shampoo used also as bath lotion containing camellia seed oil are as follows:
1) first emulsion pot is heated, when emulsification kettle temperature reaches 40 DEG C, then sequentially adds A phase component into emulsion pot, Using positive and negative rotation alternate agitation method, stirring is warming up to 70 DEG C, and 25min, mixing speed 20rpm are stirred in moisturizing;
2) each material of B phase component is sequentially added in oily mutually system material pot, is heated to 70 DEG C, it is equal is stirred dissolution It is even, keep the temperature 25min, it is ensured that solid sufficiently dissolves;
3) B phase component obtained in step 2) is pumped into emulsion pot, stirs evenly pre-emulsification 8min, then carries out 5min Homogeneous, insulated and stirred 4min, mixing speed 25rpm;
4) defoaming cooling carried out to emulsion pot under vacuum conditions, vacuum degree 0.3MPa, cooling rate is 0.4 DEG C/ Min when being cooled to 40 DEG C, C phase component is added into emulsion pot, stirs evenly, mixing time 10min, mixing speed is 20rpm;
5) adjusting pH value is 5.5, is discharged with 200 mesh filter screens, is sealed, weighing, is sent between semi-finished product standing, to be checked, inspection After testing qualification, it is aged 48 hours or more between room temperature is 26 DEG C of standing, obtains product.
Embodiment 2:
A kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil, the raw material including following parts by weight:
1) A phase component
50 parts of water, 9 parts of lauroyl oat amino acid sodium, 8 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol phosphoric acid 7 parts of ester potassium, 6 parts of lauryl glucoside, 0.03 part of EDETATE SODIUM;
2) B phase component
8 parts of saponin(e, 5 parts of camellia seed extract, 4.2 parts of camellia seed oil, 0.07 part of Polyquaternium-10,0.05 part of citric acid;
3) C phase component
0.25 part of decoyl hydroximic acid, 0.15 part of Sensiva SC50,0.25 part of 1,2- hexylene glycol.
The preparation method step of the above-mentioned mild no silicone oil shampoo used also as bath lotion containing camellia seed oil are as follows:
1) first emulsion pot is heated, when emulsification kettle temperature reaches 50 DEG C, then sequentially adds A phase component into emulsion pot, Using positive and negative rotation alternate agitation method, stirring is warming up to 70 DEG C, and 30min, mixing speed 25rpm are stirred in moisturizing;
2) each material of B phase component is sequentially added in oily mutually system material pot, is heated to 70 DEG C, it is equal is stirred dissolution It is even, keep the temperature 30min, it is ensured that solid sufficiently dissolves;
3) B phase component obtained in step 2) is pumped into emulsion pot, stirs evenly pre-emulsification 10min, then carries out 10min homogeneous, insulated and stirred 5min, mixing speed 30rpm;
4) defoaming cooling, vacuum degree 0.4MPa are carried out to emulsion pot under vacuum conditions, cooling rate is 0.5 DEG C, drop When temperature is to 40 DEG C, C phase component is added into emulsion pot, stirs evenly, mixing time 15min, mixing speed 25rpm;
5) adjusting pH value is 6, is discharged with 200 mesh filter screens, is sealed, weighing, is sent between semi-finished product standing, to be checked, is examined After qualification, it is aged 48 hours or more between room temperature is 26 DEG C of standing, obtains product.
Embodiment 3:
A kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil, the raw material including following parts by weight:
1) A phase component
55 parts of water, 8 parts of lauroyl oat amino acid sodium, 6 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol phosphoric acid 5 parts of ester potassium, 5 parts of lauryl glucoside, 0.01 part of EDETATE SODIUM;
2) B phase component
6 parts of saponin(e, 10 parts of camellia seed extract, 4.5 parts of camellia seed oil, 0.05 part of Polyquaternium-10, citric acid 0.03 Part;
3) C phase component
0.2 part of decoyl hydroximic acid, 0.1 part of Sensiva SC50,0.2 part of 1,2- hexylene glycol.
Steps are as follows for the preparation method of the above-mentioned mild no silicone oil shampoo used also as bath lotion containing camellia seed oil:
1) first emulsion pot is heated, when emulsification kettle temperature reaches 60 DEG C, then sequentially adds A phase component into emulsion pot, Using positive and negative rotation alternate agitation method, stirring is warming up to 75 DEG C, and 35min, mixing speed 30rpm are stirred in moisturizing;
2) each material of B phase component is sequentially added in oily mutually system material pot, is heated to 75 DEG C, it is equal is stirred dissolution It is even, keep the temperature 35min, it is ensured that solid sufficiently dissolves;
3) B phase component obtained in step 2) is pumped into emulsion pot, stirs evenly pre-emulsification 12min, then carries out 10min homogeneous, insulated and stirred 6min, mixing speed 35rpm;
4) defoaming cooling carried out to emulsion pot under vacuum conditions, vacuum degree 0.5MPa, cooling rate is 0.6 DEG C/ Min when being cooled to 45 DEG C, C phase component is added into emulsion pot, stirs evenly, mixing time 20min, mixing speed is 20rpm;
5) pH value is adjusted as 5.5-7.0, is discharged, is sealed with 200 mesh filter screens, weighing is sent between semi-finished product standing, to Inspection is aged 48 hours or more between room temperature is 26 DEG C of standing after the assay was approved, obtains product.
Testing experiment:
1) cleaning and soothing effect test
This test uses 2 product of example and commercially available supermarket's brand product, selects 50 objects (0-6 years old 20,6-12 years old 20,12-30 years old 10) be divided into 2 groups, every group of each 25 people, respectively from antidandruff efficacy, wash the submissive degree of rear scalp, wash The dry and comfortable degree of skin and itch degree compare afterwards, and the results are shown in Table 1.
Table 1:
Test result show embodiment 2 in anti-dandruff, wash after the submissive degree of scalp, wash after the dry and comfortable degree of skin and itch Effect is in degree far more than commercial product.
2) acute eye irritation/corrosion test
Experimental animal: regular grade New Zealand White rabbit 4, Guangdong Medical Lab Animal Center's (three water basely) is (real Test animal productiong licensing number: SCXK (Guangdong) 2014-0035) it provides.Experimental animal weight 2.3-2.4kg.
Using product made from the embodiment of the present invention 2 as tested material.
Test procedure: taking tested material 0.1mL to instill in the conjunctival sac of rabbit left side, upper and lower eyelid made passively to be closed 1s, until the With normal saline flushing 30s when 30s.Rabbit right branch hole eyeball is not handled as control.1h after instilling tested material, for 24 hours, 48h, Animal eyes were checked in 72h and the 4th day and the 7th day.If 72h does not occur stimulate the reaction, then termination test.To tested Animal corneal after object, iris or conjunctiva it is each it is comfortable for 24 hours, the top mean value of the stimulate the reaction of 48h or 72h observation time point and extensive Multiple Time evaluation carries out eye damage scoring by method related content and records.
Test result: after tested material is added, only observing that Eye irritation reacts in 1h, remaining observation time point does not observe rabbit Eye irritation reaction.For 24 hours, 48h, 72h are respectively observed in time point, and conjunctival congestion top mean value is 0, and chemosis top is equal Value is 0, and iris top mean value is 0, and cornea top mean value is 0.Horn film, iris, conjunctiva integral are instilling 0 is down to after tested material for 24 hours.
Test result: grade scale is reacted according to the Eye irritation in method, which once contacts rabbit and cause house The reaction of rabbit eye irritation
To sum up, the embodiment of the present invention have the following beneficial effects: product made from 1-3 of the embodiment of the present invention anti-dandruff, It washes the submissive degree of rear scalp, wash in the dry and comfortable degree of rear skin and itch degree effect far more than commercial product, and by acute Eye irritation/corrosion test proves product produced by the present invention, nonirritant, is the excellent selection that day common hair washing is taken a shower, It is especially suitable for pregnant woman, infant, sensibility skin, the elderly etc. to be used for a long time.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that There is also other identical elements in process, method, article or equipment including the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation Technical solution documented by example is modified or equivalent replacement of some of the technical features;And these modification or Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.

Claims (6)

1. a kind of mild no silicone oil shampoo used also as bath lotion containing camellia seed oil, which is characterized in that the raw material including following parts by weight:
1) A phase component
45-55 parts of water, 8-10 parts of lauroyl oat amino acid sodium, 6-10 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 5-8 parts of alcohol phosphate potassium, 5-7 parts of lauryl glucoside, 0.01-0.03 parts of EDETATE SODIUM;
2) B phase component
6-8 parts of saponin(e, 5-10 parts of camellia seed extract, 4.2-6 parts of camellia seed oil, 0.05-0.1 parts of Polyquaternium-10, citric acid 0.03-0.08 parts;
3) C phase component
0.2-0.3 parts of decoyl hydroximic acid, 0.1-0.2 parts of Sensiva SC50,0.2-0.3 parts of 1,2- hexylene glycol.
2. the mild no silicone oil shampoo used also as bath lotion containing camellia seed oil as described in claim 1, which is characterized in that including following heavy Measure the raw material of part:
1) A phase component
47-52 parts of water, 9-10 parts of lauroyl oat amino acid sodium, 7-9 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol 6-7 parts of phosphate potassium, 5-6 parts of lauryl glucoside, 0.02-0.03 parts of EDETATE SODIUM;
2) B phase component
7-8 parts of saponin(e, 5-7 parts of camellia seed extract, 4.2-5 parts of camellia seed oil, 0.06-0.08 parts of Polyquaternium-10, citric acid 0.04-0.06 parts;
3) C phase component
0.22-0.25 parts of decoyl hydroximic acid, 0.1-0.2 parts of Sensiva SC50,0.2-0.3 parts of 1,2- hexylene glycol.
3. the mild no silicone oil shampoo used also as bath lotion containing camellia seed oil as claimed in claim 2, which is characterized in that including following heavy Measure the raw material of part:
1) A phase component
50 parts of water, 9 parts of lauroyl oat amino acid sodium, 8 parts of dodecanamide propyl hydroxy sulfo lycine, C12-13 alcohol phosphate potassium 7 parts, 6 parts of lauryl glucoside, 0.03 part of EDETATE SODIUM;
2) B phase component
8 parts of saponin(e, 5 parts of camellia seed extract, 4.2 parts of camellia seed oil, 0.07 part of Polyquaternium-10,0.05 part of citric acid;
3) C phase component
0.25 part of decoyl hydroximic acid, 0.15 part of Sensiva SC50,0.25 part of 1,2- hexylene glycol.
4. the mild no silicone oil shampoo used also as bath lotion as described in any one of claims 1-3 containing camellia seed oil, which is characterized in that should Steps are as follows for the preparation method of shampoo used also as bath lotion:
1) first emulsion pot is heated, when emulsification kettle temperature reaches 40-60 DEG C, then sequentially adds A phase component into emulsion pot, adopts With positive and negative rotation alternate agitation method, stirring is warming up to 70-75 DEG C, and 25-35min, mixing speed 20-30rpm are stirred in moisturizing;
2) each material of B phase component is sequentially added in oily mutually system material pot, is heated to 70-75 DEG C, is stirred and is uniformly dissolved, Keep the temperature 25-35min, it is ensured that solid sufficiently dissolves;
3) B phase component obtained in step 2) is pumped into emulsion pot, stirs evenly pre-emulsification 8-12min, then carries out 5- 10min homogeneous, insulated and stirred 4-6min, mixing speed 25-35rpm;
4) defoaming cooling is carried out to emulsion pot under vacuum conditions, when being cooled to 40-45 DEG C, C phase component is added into emulsion pot, It stirs evenly;
5) pH value is adjusted as 5.5-7.0, is discharged, is sealed with 200 mesh filter screens, and weighing is sent between semi-finished product standing, to be checked, inspection After testing qualification, it is aged 48 hours or more between room temperature is 26 DEG C of standing, obtains product.
5. the mild no silicone oil shampoo used also as bath lotion containing camellia seed oil as claimed in claim 4, which is characterized in that in step 4), Vacuum degree is 0.3-0.5MPa, and cooling rate is 0.4-0.6 DEG C/min.
6. the mild no silicone oil shampoo used also as bath lotion containing camellia seed oil as claimed in claim 4, which is characterized in that in step 4), Mixing time is 10-20min, mixing speed 20-30rpm.
CN201910496112.3A 2019-06-10 2019-06-10 A kind of mild no silicone oil shampoo used also as bath lotion and preparation method thereof containing camellia seed oil Pending CN110101609A (en)

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CN107569404A (en) * 2017-02-17 2018-01-12 杭州千岛湖天鑫有限公司 A kind of camellia oil shampoo used also as bath lotion and preparation method thereof
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CN108904331A (en) * 2018-08-29 2018-11-30 她芙医美(厦门)科技有限公司 A kind of infant's camellia oil shampoo used also as bath lotion and preparation method thereof

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CN107693436A (en) * 2017-11-21 2018-02-16 郑生华 A kind of baby's soapberry protects shower cream and preparation method thereof again
CN108904331A (en) * 2018-08-29 2018-11-30 她芙医美(厦门)科技有限公司 A kind of infant's camellia oil shampoo used also as bath lotion and preparation method thereof

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