CN107007484A - The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method - Google Patents

The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method Download PDF

Info

Publication number
CN107007484A
CN107007484A CN201611103396.8A CN201611103396A CN107007484A CN 107007484 A CN107007484 A CN 107007484A CN 201611103396 A CN201611103396 A CN 201611103396A CN 107007484 A CN107007484 A CN 107007484A
Authority
CN
China
Prior art keywords
white fungus
extract
parts
fungus heteropolysaccharideand
hair
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611103396.8A
Other languages
Chinese (zh)
Inventor
骆峰
苏荣生
刘敏
周自华
杨海延
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Hui Wen Biotechnology Ltd By Share Ltd
Original Assignee
Shanghai Hui Wen Biotechnology Ltd By Share Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Hui Wen Biotechnology Ltd By Share Ltd filed Critical Shanghai Hui Wen Biotechnology Ltd By Share Ltd
Priority to CN201611103396.8A priority Critical patent/CN107007484A/en
Publication of CN107007484A publication Critical patent/CN107007484A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

Hair products and preparation method are washed the invention discloses the application on hair products are washed of white fungus heteropolysaccharideand and its extract, containing it.Wherein, the structure of white fungus heteropolysaccharideand is using α (1 3) mannoses as main chain, it is main to be made up of percentage by weight for 70 93% neutral total reducing sugar, 6 28% glucuronic acid and 0.1 3% associated proteins, mean molecule quantity is 85 160 ten thousand dalton, and its middle-molecular-weihydroxyethyl accounts for more than 90wt% more than 6000 dalton;Extract includes the above-mentioned white fungus heteropolysaccharideand that percentage by weight is 80 98%, 0.1 3.3% floating preteins and 0.5 8% ash content, and mean molecule quantity is 75 140 ten thousand dalton, and its middle-molecular-weihydroxyethyl accounts for 75 98wt% more than 6000 dalton.White fungus heteropolysaccharideand and its extract are applied to wash in hair products, plays a part of abundant foam, deep clean, repair damaged hair.

Description

The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method
Technical field
The present invention relates to the application of a kind of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method.
Background technology
With the extensive use of two-in-one shampoo, the shampoo of silicone-containing is accepted extensively.Siloxanes adds Plus it is very smooth after hair can be made dry, but precipitation of grease can be easily caused in scalp, influence skin of head breathing causes hair follicle Necrosis, alopecia can also give people the sensation not washed clean.
Meanwhile, surfactant with the system of human contact such as medicine, food, cosmetics and personal hygiene article Using more and more extensive.With the raising of human living standard, people are to surfactant in all kinds of formulas with human contact The increasing concern of toxic side effect input.For different purposes, the emphasis of Surfactant concern is concentrated mainly on to viscous The excitant of film, the sensitization to skin, toxicity, heredity, carcinogenicity, teratogenesis and hemolytic, the property digested and assimilated, biological drop In terms of solution property.The raw material of existing adjustment cardability is mainly guar gum, polyquaternary amine salt product, but its excitant is very Greatly, scalp itch can be made after use.
White fungus (TremellafaciformisBerk), also known as tremella, mulberry goose,《Qingyilu》.Belong to Tremellales (Tremellales), Tremellaceae (Tremellacease), Tremella (Tremella).With nourishing Yin and moistening lung, QI invigorating and blood it Effect.White fungus heteropolysaccharideand is a kind of acid heteroglycan that separation is extracted from Tremella fructification (or its microbial fermentation solution).In White fungus is referred to as senior tonic and medicine by state since ancient times, and the good merchantable brand of medicine-food two-purpose is the first-class food of nourishing in imperial palace.
Modern study shows that white fungus heteropolysaccharideand has and improves immunity, antitumor, anti-aging, hypoglycemic, blood fat, promotion egg The pharmacological actions such as the synthesis of white matter nucleic acid, antithrombotic.Japan widely applies to it in health products, cosmetics, medicine.Silver The development and application of ear, cause the great interest of scientific circles, by the extensive attention of international the world of medicine and cosmetic field, turn into The hot issue researched and developed now.However, application of the white fungus in hair products are washed not yet has been reported.
The content of the invention
Technical problem solved by the invention is to overcome existing hair products excitant of washing larger, and head can be made after use Skin is itched, hair follicle necrosis, be not easy to rinse defect there is provided the application of a kind of white fungus heteropolysaccharideand and its extract, wash hair care Product and preparation method.According to the present invention, white fungus heteropolysaccharideand and its extract are applied to wash in hair products, have been not only able to To abundant foam, deep clean scalp and hair-care, it is easy to rinsing, improves hair smoothness, increase damaged hair with respect to gloss, make quiet The effect of electric charge reduction, can also be repaired impaired cuticula, and then effectively protect damaged hair.
In the present invention, described " white fungus heteropolysaccharideand and its extract " is used as an entirety, it should be understood that " the white fungus Heteroglycan " and/or " the white fungus heteropolysaccharideand extract ".
The present inventor is after numerous studies it has surprisingly been found that will use special disclosed in Chinese patent literature CN1807463A The white fungus heteropolysaccharideand and its extract that different separation purifying technique is obtained are applied to hair care product, can improve damaged hair Hydrophobicity, helps damaged hair reparation, makes hair more compliant and smooth after washing shield, and will not accumulate or cause hair to glue Knot, the formula that helps to take care of hair provide needed for conditioning effect, with overcome it is growing day by day bleaching and dyeing, Exposure to Sunlight and air pollution be to hair quality Harmful effect, makes bright, submissive hair, high resilience, is easy to comb, and white fungus heteropolysaccharideand can improve bubble applied to shampoo The quality of foam.The principle for improving foam quality using white fungus heteropolysaccharideand and its extract is as follows:The process of foam destruction, mainly The liquid film for separating gas is thinning by thickness, until the process of rupture, therefore, the stability of foam depends primarily on discharge opeing speed and liquid Film-strength, influences the principal element that is, influence liquid film of foam stability to keep the factor of thickness and surface film-strength, relatively more multiple It is miscellaneous, and white fungus heteropolysaccharideand and its extract enter to subtract mainly by increasing the viscosity of moisture film and slowing down liquid flow velocity The drain age velocity of slow foam.
The final present invention solves above-mentioned technical problem by the following technical programs.
The invention provides a kind of application of white fungus heteropolysaccharideand and its extract in hair products are washed;
Wherein, the structure of the white fungus heteropolysaccharideand be using α-(1-3) mannose as main chain, the white fungus heteropolysaccharideand mainly by The associated proteins group of neutral total reducing sugar, 6%-28% glucuronic acid and 0.1%-3% that percentage by weight is 70%-93% Into;The mean molecule quantity of the white fungus heteropolysaccharideand is the dalton of 85-160 ten thousand, and its middle-molecular-weihydroxyethyl is more than accounting for for 6000 dalton More than 90wt%;
White fungus heteropolysaccharideand extract includes the described white fungus heteropolysaccharideand that percentage by weight is 80-98%, 0.1%-3.3% Floating preteins and 0.5%-8% ash content;The mean molecule quantity of the white fungus heteropolysaccharideand extract is the dalton of 75-140 ten thousand, its Middle-molecular-weihydroxyethyl accounts for 75wt%-98wt% more than 6000 dalton.
Wherein, the white fungus heteropolysaccharideand and its extract are the conventional white fungus heteropolysaccharideand and its extract in this area, as long as It meets foregoing structure, composition and molecular weight.In CN1807463A, it has been disclosed that the present invention in white fungus heteropolysaccharideand and Its extract.When using white fungus heteropolysaccharideand and its extract, the consumption of the white fungus heteropolysaccharideand and its extract is preferably White fungus heteropolysaccharideand and its extract and wash the 0.03%~0.3% of hair products gross weight.In the preferable embodiment party of the present invention In formula, the white fungus heteropolysaccharideand and its extract be Shanghai Hui Wen Biotechnology Ltd. produce white fungus heteropolysaccharideand and Its extract WSK.
Wherein, the definition for washing hair products is that this area is conventional with concept, generally comprises shampoo, hair conditioner and hair The products such as film.
Hair products are washed present invention also offers one kind, it contains described white fungus heteropolysaccharideand and its extract.
Wherein, described to wash in hair products, the consumption of the white fungus heteropolysaccharideand and its extract is preferably described wash The 0.03%~0.3% of hair products gross weight.
Wherein, the other components washed in hair products can be the conventional component in this area.In general, it is described other Component generally comprises surfactant, silicone emulsion, pearling agent, thickening suspending agent, conditioner, chelating agent and grease etc., and its is equal Belong to convenient source.
In the better embodiment of the present invention, the hair products of washing is shampoos, and the shampoo includes following The component of parts by weight:
Wherein, the surfactant can be surfactant commonly used in the art, and preferably composite surface is lived Property agent, the complexed surfactant is made up of following components in parts by weight:
20~35 parts of laureth sodium sulfovinate (AES);
5.0~10.0 parts of Cocoamidopropyl betaine (CAB);
0.5~2.5 part of coconut oleoyl amine MEA.
The laureth sodium sulfovinate is anion surfactant, and it is the interface shape for changing solution system that it, which is acted on, State, while can also play the effect of foaming agent and detergent.The Cocoamidopropyl betaine is amphoteric surfactant, its Effect is the interface state for changing solution system, while can also play the effect of foaming agent and foam stabilizer.The coconut oleoyl amine is Nonionic surfactant, it is the interface state for changing solution system that it, which is acted on, while can also play foam stabilizer and thickener Effect.By the coordinated of above-mentioned three kinds of surfactants, moderate cleaning force, foam type and comfortableness can be achieved.
Wherein, the conditioner can be conditioner commonly used in the art, preferably composite conditioner, described compound Conditioner is made up of following components in parts by weight:
Acting as the Polyquaternium-10 is antistatic, submissive.The effect of the guar hydroxypropyltrimonium ammonium chloride Predominantly cardability is adjusted.The main function of the vegetable fat is regulation hair light.The cetostearyl alcohol is act as Improve hair gloss.The effect of the silicone emulsion is mainly integrally-regulated hair feel.Pass through above-mentioned five kinds of conditioners Coordinated, achievable hair is bright, submissive, be easy to comb.
Wherein, the pearling agent can be pearling agent commonly used in the art, preferably glycol distearate, use In the good outward appearance of acquisition.
Wherein, the chelating agent can be chelating agent commonly used in the art, preferably EDETATE SODIUM.
Wherein, the thickener can be thickener commonly used in the art, preferably carbomer.
Wherein, the preservative can be preservative commonly used in the art, preferably hydantoins.
Wherein, the need for the shampoo can also be according to consumer, different types of essence is added.The content of the essence Generally 0.05~0.5 part.
Wherein, in the shampoo white fungus heteropolysaccharideand and its extract main function horn of plenty foam, increase foam Sophistication, it is easy to rinse, reduce product excitant, it is antistatic after washing, make bright, submissive hair, high resilience, dry and wet comb property Good, long-term use can repair damaged hair.
In another better embodiment of the present invention, the hair products of washing is shampoos, and the shampoo is by following The component composition of parts by weight:
In another better embodiment of the present invention, the hair products of washing is hair conditioner, under the hair conditioner includes State the component of parts by weight:
Wherein, the conditioner can be conditioner commonly used in the art, preferably composite conditioner, described compound Conditioner is made up of following components in parts by weight:
0.5~6.0 part of glycerine;
0.5~4.0 part of hexadecyltrimethylammonium chloride.
The main function of the glycerine is the moisturizing sense of increase hair.The hexadecyltrimethylammonium chloride is a kind of sun Ionic surface active agent, its main function is regulation Hair setting.
Wherein, the thickener can be thickener commonly used in the art, preferably hydroxyethyl cellulose.
Wherein, the preservative can be preservative commonly used in the art, preferably compound preservative, described compound Preservative is made up of following components in parts by weight:
0.05~0.2 part of methyl hydroxybenzoate;
0.03~0.10 part of Nipasol;
0.05~0.3 part of hydantoins.
Wherein, the emulsifying agent can be thickener commonly used in the art, preferably stearine and/or PEG-100 stearates.
Wherein, the grease is preferably grease commonly used in the art, is preferably combined grease, the compound oil Fat is made up of following components in parts by weight:
0.3~1.5 part of Dormant oils;
3.0~6.0 parts of cetostearyl alcohol;
0.3~2.0 part of Nexbase 2004.
Wherein, the need for the hair conditioner can also be according to consumer, different types of essence is added.The content of the essence Generally 0.03~0.5 part.
Wherein, the main function of white fungus heteropolysaccharideand and its extract is hair moisturizing, combed, Yi Chong in the hair conditioner Wash, provide nutrition to hair, repair damaged hair.
In the another better embodiment of the present invention, the hair products of washing is hair conditioner, and the hair conditioner is by following The component composition of parts by weight:
In the present invention, the preparation method for washing hair products is this area conventional method, and each component is well mixed i.e. Can.It is preferred that prepare when the white fungus heteropolysaccharideand and its extract be first configured to solution with part water, then again with other components It is well mixed.The technological parameter being related in preparation process can refer to this area routine, such as mixing temperature.
In a preferred embodiment of the present invention, the hair products of washing is shampoos, and the shampoo is by following weight parts Component composition:0.03~0.3 part of white fungus heteropolysaccharideand and its extract, 20~35 parts of laureth sodium sulfovinate (AES), coconut palm 5.0~10.0 parts of oleamide CAB (CAB), 0.5~2.5 part of coconut oleoyl amine MEA, glycol distearate 1.0~ 3.0 parts, 0.05~0.2 part of EDETATE SODIUM, 0.1~0.8 part of carbomer, 0.05~0.5 part of hydantoins, Polyquaternium-10 0.05~0.5 part, 0.05~0.5 part of guar hydroxypropyltrimonium ammonium chloride, 3.0~6.0 parts of silicone emulsion, vegetable fat 0.1~1.0 part, 0.1~3.0 part of cetostearyl alcohol and complements to 100 parts of water at 0.05~0.5 part of essence;
The shampoo is prepared by following methods, and step is as follows:
(1) by the EDETATE SODIUM, carbomer, white fungus heteropolysaccharideand and its extract and 48.42~57.97 parts of water in 85~ Mixed at 80 DEG C, obtain compound A, by the compound A and the laureth sodium sulfovinate, ethylene glycol distearyl acid Ester, cetostearyl alcohol, vegetable fat, coconut oleoyl amine MEA and Cocoamidopropyl betaine mixing, obtain compound B, will be described Compound B is mixed with the guar hydroxypropyltrimonium ammonium chloride and Polyquaternium-10, is incubated 20~30 minutes, is mixed Close material C;
(2) 50 DEG C are cooled to, the compound C is mixed with the silicone emulsion, compound D is obtained;
(3) 45 DEG C are continued cool to, the compound D is mixed with the hydantoins, essence and remaining water;
(4) room temperature is subsequently cooled to, is produced.
In another preferred embodiment of the invention, the hair products of washing is hair conditioner, and the hair conditioner is by following weight The component composition of part:0.03~0.3 part of white fungus heteropolysaccharideand and its extract, 0.5~6.0 part of glycerine, cetyl trimethyl chlorine 0.5~4.0 part of ammonium of change, 0.05~0.60 part of hydroxyethyl cellulose, 0.05~0.2 part of methyl hydroxybenzoate, Nipasol 0.03~ 0.10 part, 0.05~0.3 part of hydantoins, 0.5~2.5 part of stearine and/or PEG-100 stearates, Dormant oils 0.3 ~1.5 parts, 3.0~6.0 parts of cetostearyl alcohol, 0.3~2.0 part of Nexbase 2004 and complements to 100 at 0.03~0.5 part of essence The water of part;
The hair conditioner is prepared by following methods, and step is as follows:
(1) by the glycerine, white fungus heteropolysaccharideand and its extract, hydroxyethyl cellulose, methyl hydroxybenzoate, cetyl front three Ammonium chloride and 84.87~87.9 parts of water obtain compound A in being mixed at 80~85 DEG C;
(2) by the Nexbase 2004, Dormant oils, cetostearyl alcohol, stearine/PEG-100 stearates and hydroxyl Phenylpropyl alcohol ester obtains compound B in being mixed at 75~80 DEG C;
(3) the compound B is mixed with the compound A, is incubated 30~45 minutes, obtains compound C;
(4) 45 DEG C are cooled to, the compound C is mixed with the hydantoins, essence and remaining water, mixed Expect D;
(5) room temperature is subsequently cooled to, is produced.
On the basis of common sense in the field is met, above-mentioned each optimum condition can be combined, and produce each preferable reality of the present invention Example.
Agents useful for same and raw material of the present invention are commercially available.
The positive effect of the present invention is:
White fungus heteropolysaccharideand and its extract are applied to hair care product, can improve the hydrophobicity of damaged hair, help Damaged hair is repaired, and makes hair more compliant and smooth after washing shield, and will not be accumulated or be caused hair to bond, and help, which is taken care of hair, matches somebody with somebody Side provide needed for conditioning effect, with overcome it is growing day by day bleaching and dyeing, the harmful effect of Exposure to Sunlight and air pollution to hair quality, make head Luminance, submissive, high resilience, be easy to comb.And white fungus heteropolysaccharideand and its extract can make product more applied to shampoo Easy to foaming, foam is more rich, and stable foam, using the teaching of the invention it is possible to provide more smooth flushing is felt.
Brief description of the drawings
Fig. 1 is that the foam height and foam of embodiment 1~3 and the sample of comparative example 1 are held time figure.
Fig. 2 is the microscope figure of the hair washing water bubble of embodiment 1~3 and comparative example 1, and wherein a is comparative example 1, b is embodiment 1, and c is embodiment 2, and d is embodiment 3.
Embodiment
The present invention is further illustrated below by the mode of embodiment, but does not therefore limit the present invention to described reality Apply among a scope.The experimental method of unreceipted actual conditions in the following example, conventionally and condition, or according to business Product specification is selected.
In following embodiments, white fungus heteropolysaccharideand used and its extract are Shanghai Hui Wen Biotechnology Ltd. It is disclosed in the white fungus heteropolysaccharideand and its extract WSK of offer, the white fungus heteropolysaccharideand and its extract WSK that is, CN1807463A White fungus heteropolysaccharideand and its extract:The structure of white fungus heteropolysaccharideand is using α-(1-3) mannose as main chain, mainly by weight percent Associated proteins than neutral total reducing sugar, 6%-28% glucuronic acid, 0.1%-3% for 70%-93% are constituted, mean molecule Measure as the dalton of 85-160 ten thousand, what its middle-molecular-weihydroxyethyl was more than 6000 dalton accounts for more than 90wt%;White fungus heteropolysaccharideand extract bag Include the above-mentioned white fungus heteropolysaccharideand that percentage by weight is 80%-98%, 0.1%-3.3% floating preteins and 0.5%-8% ash Point, mean molecule quantity is the dalton of 75-140 ten thousand, and its middle-molecular-weihydroxyethyl accounts for 75wt%-98wt% more than 6000 dalton.
Embodiment 1~5 and comparative example 1
The formula of shampoo is (percentage by weight) as shown in table 1 below.
Table 1
Preparation method is as follows:
(1) each raw material components for preparing shampoo are weighed according to table 1, A phases material is added into reactor and is completely dispersed, is stirred Mix and be heated to 85~80 DEG C, B phase materials are added while stirring, treat that material is completely dissolved uniformly, add C phases, be incubated 20~30 points Clock, stirring and dissolving substantially uniformity.
(2) cooling water cooling is opened, treats that temperature is down to 50 DEG C, adds D phase materials, stir.
(3) 45 DEG C are continued cool to, E phase materials is added, stirs.
(4) to be mixed to be cooled to room temperature, it is qualified to examine, discharging.
Embodiment 6~10 and comparative example 2
The formula of hair conditioner is (percentage by weight) as shown in table 2 below.
Table 2
Preparation method is as follows:
(1) each raw material components for preparing hair conditioner are weighed according to table 2, A phases material is added into reactor and is completely dispersed, is stirred Mix and be heated to 80~85 DEG C.
(2) B phases material is added in oil cauldron, is stirred and heated to 75~80 DEG C, treats that material is completely dissolved uniformly.
(3) B stirred is added in A phases, stirring insulation 30~45 minutes.
(4) cooling water cooling is opened, 45 DEG C are cooled to, C phase materials is added, stirs.
(5) to be mixed to be cooled to room temperature, it is qualified to examine, discharging.
Effect example 1
Shampoo brbble test method:
Super thermostat is preheating to (40 ± 1) DEG C, makes Roche foam meter constant temperature in (40 ± 1) DEG C.Sample 2.5g is weighed, 1500mg/kg hard water 100mL are added, distilled water 900mL is added, is heated to (40 ± 1) DEG C.Stirring makes sample uniform dissolution, Part test solution is drawn with the quantitative funnels of 200mL, is rinsed along foam meter tube wall.Then test solution is taken to be put into foam meter bottom alignment Master scale draws test solution to 50mL, then with the quantitative funnels of 200mL, and fixed funnel center puts down test solution, bubble is write down immediately Foam height, examines product foam moisture preserving time.As a result whole digit is retained.According to said method it is repeated 3 times.
Test sample of the formula used using comparative example 1 and embodiment 1~5 below, the white fungus heteropolysaccharideand of addition and Its extract WSK percentage by weight is 0.0%, 0.03%, 0.10%, 0.30%, 0.03%, 0.03% respectively.Experiment knot Fruit is as shown in Figure 1.
It will be seen from figure 1 that embodiment 1~3 with the addition of white fungus heteropolysaccharideand and its extract WSK formula in foam volume and There is positive effect in terms of the foam retention time, and with the increase of white fungus heteropolysaccharideand and its extract WSK additions, generation Foam volume also increases, but the foam retention time in 0.03% white fungus heteropolysaccharideand of addition and its extract WSK formula is slightly higher In 0.1% formula.The foam height and foam for adding 0.30% white fungus heteropolysaccharideand and its extract WSK are held time all most It is good.Effect of the embodiment 4~5 on foam volume and foam retention time is suitable with embodiment 1.
Effect example 1 shows that white fungus heteropolysaccharideand and its extract can increase table work foam.Table work foam is in the present invention Refer to the foam of surfactant.
Effect example 2
Observe the fine and smooth degree of the hair washing water bubble of embodiment 1~5 and comparative example 1.Specific test method is as follows:
A) operating process, configuration comparative example 1, embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5 are pressed Money shampoo product;
B) shampoo configured is made to 15% aqueous solution, is fills up in compressing pump type foaming agent container;
C) amount (1g) for pressing 5 times is placed in shallow bottom dish, with (50 times) observations of microscope.
Result of the test is shown in that a is comparative example 1 in Fig. 2, Fig. 2, and b is embodiment 1, and c is embodiment 2, and d is embodiment 3.Knot Fruit shows that the foam exquisiteness sense of the shampoo of comparative example 1 is poor, and foam is uneven, and the hair washing bubble of embodiment 1~3 Foam is fine and smooth uniform.The fine and smooth effect of the foam of embodiment 4~5 is suitable with embodiment 1~3.It can be seen that, add white fungus heteropolysaccharideand and its carry Thing is taken to improve the foam quality of shampoo.
Effect example 3
Test sample of the formula used using comparative example 1 and embodiment 1~5 below, the white fungus heteropolysaccharideand of addition and Its extract WSK percentage by weight is 0.0%, 0.03%, 0.10%, 0.30%, 0.03%, 0.03% respectively.
It is tested to use crowd:The people of healthy volunteer 40, at 25~50 years old age, tries out 15 days, according to evaluation table, can summarize Table 3 below conclusion.
Table 3
It is the optimal basic components selected that embodiment 1, which can be drawn, and it is also best, and white fungus to wash the effect that reaches Heteroglycan and its extract WSK are made an addition in shampoo, with obvious improvement.Because foam is big, uniform and abundant is A shampoo big major criterion popular with consumers, and white fungus heteropolysaccharideand and its extract addition are more than 0.1%, shampoo Although foam it is fine and smooth, it is smaller and airtight, thus 0.03% white fungus heteropolysaccharideand of addition and its extract WSK formula more It is welcome.In addition, test result indicates that, white fungus heteropolysaccharideand and its extract can improve the cardability of the hair after shampoo use And smoothness.

Claims (10)

1. a kind of application of white fungus heteropolysaccharideand and its extract in hair products are washed, it is characterised in that
The structure of the white fungus heteropolysaccharideand is that, using α-(1-3) mannose as main chain, the white fungus heteropolysaccharideand is main by weight percent Associated proteins than neutral total reducing sugar, 6%-28% glucuronic acid and 0.1%-3% for 70%-93% are constituted;The silver The mean molecule quantity of ear heteroglycan is the dalton of 85-160 ten thousand, and its middle-molecular-weihydroxyethyl accounts for more than 90wt% more than 6000 dalton;
The extract include percentage by weight be 80-98% the white fungus heteropolysaccharideand, 0.1%-3.3% floating preteins and 0.5%-8% ash content;The mean molecule quantity of the extract is the dalton of 75-140 ten thousand, and its middle-molecular-weihydroxyethyl is more than 6000 dongles That pauses accounts for 75wt%-98wt%.
2. application as claimed in claim 1, it is characterised in that described when using the white fungus heteropolysaccharideand and its extract The consumption of white fungus heteropolysaccharideand and its extract be white fungus heteropolysaccharideand and its extract and wash hair products gross weight 0.03%~ 0.3%.
3. one kind washes hair products, it is characterised in that described to wash hair products to contain white fungus as described in claim 1 miscellaneous more Sugar and its extract.
4. wash hair products as claimed in claim 3, it is characterised in that the consumption of the white fungus heteropolysaccharideand and its extract is Wash the 0.03%~0.3% of hair products gross weight.
5. wash hair products as claimed in claim 3, it is characterised in that the hair products of washing is shampoos, the hair washing Water includes following components in parts by weight:0.03~0.3 part of white fungus heteropolysaccharideand and its extract, surfactant 25.5~47.5 Part, 1.0~3.0 parts of pearling agent, 0.05~0.2 part of chelating agent, 0.1~0.8 part of thickener, 0.05~0.5 part of preservative, conditioning 0.5~10.0 part of agent and complement to 100 parts of water.
6. wash hair products as claimed in claim 5, it is characterised in that the surfactant is complexed surfactant, The complexed surfactant is made up of following components in parts by weight:20~35 parts of laureth sodium sulfovinate, coconut oleoyl amine 5.0~10.0 parts of CAB and coconut oleoyl amine MEA0.5~2.5 part;
And/or, the conditioner is composite conditioner, and the composite conditioner is made up of following components in parts by weight:Polyquaternary amine 0.05~0.5 part of salt -10,0.05~0.5 part of guar hydroxypropyltrimonium ammonium chloride, 3.0~6.0 parts of silicone emulsion, plant 0.1~3.0 part of 0.1~1.0 part of grease and cetostearyl alcohol;
And/or, the pearling agent is glycol distearate;
And/or, the chelating agent is EDETATE SODIUM;
And/or, the thickener is carbomer;
And/or, the preservative is hydantoins;
And/or, the shampoo also includes essence, and the consumption of the essence is 0.05~0.5 part.
7. wash hair products as claimed in claim 3, it is characterised in that the hair products of washing is hair conditioner, the hair care Element includes following components in parts by weight:0.03~0.3 part of white fungus heteropolysaccharideand and its extract, 1.0~10.0 parts of conditioner, thickening 0.05~0.60 part of agent, 0.1~0.65 part of preservative, 0.5~2.5 part of emulsifying agent and complements to 100 at 1.0~10.0 parts of grease The water of part.
8. wash hair products as claimed in claim 7, it is characterised in that the conditioner is composite conditioner, it is described compound Conditioner is made up of following components in parts by weight:0.5~4.0 part of 0.5~6.0 part of glycerine and hexadecyltrimethylammonium chloride;
And/or, the thickener is hydroxyethyl cellulose;
And/or, the preservative is compound preservative, and the compound preservative is made up of following components in parts by weight:Oxybenzene first 0.05~0.3 part of 0.05~0.2 part of ester, 0.03~0.10 part of Nipasol and hydantoins;
And/or, the emulsifying agent is stearine and/or PEG-100 stearates;
And/or, the grease is compound grease, and the compound grease is made up of following components in parts by weight:Dormant oils 0.3~1.5 Part, 0.3~2.0 part of 3.0~6.0 parts of cetostearyl alcohol and Nexbase 2004;
And/or, the hair conditioner also includes essence, and the consumption of the essence is 0.03~0.5 part.
9. a kind of preparation method for washing hair products as described in any one of claim 3~8, it is characterised in that the preparation Method is to mix each component.
10. preparation method as claimed in claim 9, it is characterised in that the white fungus heteropolysaccharideand and its extract are first during mixing Solution is configured to part water, is then mixed again with other components.
CN201611103396.8A 2016-12-05 2016-12-05 The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method Pending CN107007484A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611103396.8A CN107007484A (en) 2016-12-05 2016-12-05 The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611103396.8A CN107007484A (en) 2016-12-05 2016-12-05 The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method

Publications (1)

Publication Number Publication Date
CN107007484A true CN107007484A (en) 2017-08-04

Family

ID=59439134

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611103396.8A Pending CN107007484A (en) 2016-12-05 2016-12-05 The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method

Country Status (1)

Country Link
CN (1) CN107007484A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107822947A (en) * 2017-11-10 2018-03-23 丁玉琴 A kind of preparation method of conditioner
CN107982110A (en) * 2017-12-21 2018-05-04 广州神采化妆品有限公司 One kind is without silicone oil shampoo
CN110042005A (en) * 2019-05-08 2019-07-23 山东大学 A kind of rush foam system and preparation method thereof for improving alkyl glycosides foaming properties based on the different poly- polysaccharide of tremella
WO2024088060A1 (en) * 2022-10-28 2024-05-02 上海家化联合股份有限公司 Composition for regulating and controlling skin micro-ecological diversity

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1807463A (en) * 2005-01-18 2006-07-26 上海辉文生物技术有限公司 White fungus heteropolysaccharide and its extract, preparation method and uses

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1807463A (en) * 2005-01-18 2006-07-26 上海辉文生物技术有限公司 White fungus heteropolysaccharide and its extract, preparation method and uses

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
裘炳毅等编著: "《现代化妆品科学与技术 中册》", 31 March 2016, 中国轻工业出版社 *
钱辉华等: "高效保湿因子WSK的功能及其在化妆品中应用", 《香料香精化妆品》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107822947A (en) * 2017-11-10 2018-03-23 丁玉琴 A kind of preparation method of conditioner
CN107982110A (en) * 2017-12-21 2018-05-04 广州神采化妆品有限公司 One kind is without silicone oil shampoo
CN110042005A (en) * 2019-05-08 2019-07-23 山东大学 A kind of rush foam system and preparation method thereof for improving alkyl glycosides foaming properties based on the different poly- polysaccharide of tremella
WO2024088060A1 (en) * 2022-10-28 2024-05-02 上海家化联合股份有限公司 Composition for regulating and controlling skin micro-ecological diversity

Similar Documents

Publication Publication Date Title
CN107007484A (en) The application of white fungus heteropolysaccharideand and its extract, wash hair products and preparation method
CN108186385A (en) A kind of hair scalp cleaning compositions
CN110123721B (en) Shampoo composition for improving oily scalp
CN105878128B (en) It is a kind of containing moisturizer without silicon transparent shampoo and preparation method thereof
CN108785198A (en) Strengthen the hair composition, leaves shampoo and preparation method thereof
WO2018118160A1 (en) Cosmetic compositions for treating keratinous substrates
CN105147538A (en) Transparent bathing mousse free of silicone oil and preparation method thereof
CN108125870B (en) Scalp nourishing composition, preparation method and application thereof, and scalp nourishing shampoo
CN103550072B (en) A kind of Application way of aqueous extraction Oleum Camelliae technique waste water and shampoo prescription
CN107438425A (en) A kind of hair care and nourishing composition of the complexing agent containing moisturizing
CN106176337A (en) A kind of shampoo and preparation technology thereof
CN103893050A (en) Anti-hair loss shampoo
CN109464314A (en) Gold bullet moistens Face-protecting mask and preparation method thereof
CN107184406A (en) One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof
CN110638717A (en) Softening composition and shampoo thereof
CN103330650B (en) Composition with characteristics of moisturizing, scurf removing and itching alleviating
CN113599335B (en) Bubble mousse type shampoo and preparation method thereof
CN108553334A (en) A kind of hair care composition of the smooth not silicate-containing oil of maintenance and its application
CN106109275A (en) A kind of foaming bath oil rich in vegetable oil and preparation method thereof
CN109172494A (en) A kind of aloe shampoo and its preparation process of sterilizing and itch-relieving
CN106798656A (en) A kind of depth hair conditioner comprising Yak Bone small-molecular peptides and preparation method thereof
CN111759752A (en) Water-soluble hair washing cream and preparation method thereof
JP5900956B2 (en) Method for producing gel-like cleaning material
CN107375062B (en) Silicone-oil-free shampoo containing persimmon extract and preparation method thereof
CN110368329B (en) Silicone oil-free homogeneous phase nursing composition

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170804

RJ01 Rejection of invention patent application after publication