CN110090176A - A kind of preparation method of the soap kind for shampoo - Google Patents
A kind of preparation method of the soap kind for shampoo Download PDFInfo
- Publication number
- CN110090176A CN110090176A CN201910373637.8A CN201910373637A CN110090176A CN 110090176 A CN110090176 A CN 110090176A CN 201910373637 A CN201910373637 A CN 201910373637A CN 110090176 A CN110090176 A CN 110090176A
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- China
- Prior art keywords
- amino acid
- water
- preparation
- shampoo
- soap
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetics or similar dressing preparation technical fields, disclose a kind of preparation method of soap kind for shampoo；Corresponding ratio coconut oil, lauroyl glutamate, pure water are measured, water is added and mixture is made in amino acid heating；Well upper pot water proof heating, oil temperature and amino acid temperature are added oil mass at 70 DEG C~80 DEG C, then the mixture of water and amino acid, and Hybrid Heating reaction is boiled 4h, poured into model；It is put into 1h in freezer, cooled and solidified molding；It is 2-3 weeks dry.The soap kind preservation quality of preparation of the invention is fine, and cleaning capacity is strong, smaller than general soap kind to skin damage, and preparation flow is relatively easy, and foaming effect, and the careful stabilization of foam can be played in shampoo, as surfactant, cleaning, starting.
Description
Technical field
The invention belongs to cosmetics or similar dressing preparation technical fields more particularly to a kind of for shampoo
The preparation method of soap kind.
Background technique
Currently, the immediate prior art: major part factory production soap kind is using caustic soda saponification at present, i.e.,
Generation saponification, which is heated, with oil after being dissolved in water with caustic soda obtains soap kind.This method is convenient but does not consider mildness, alkalinity
Being irritating to the skin property of product, easily dry using rear skin, moisture retention is poor, can notably aggravate keratoderma aging.Meanwhile
Alkaline environment is unfavorable for the medical fluid that Chinese herbal medicine extracts and plays a role (most herbal liquid medicines are in acidity), and can be because in soda acid
It causes to be lost with reaction.
In conclusion problem of the existing technology is:
(1) caustic soda is replaced with amino acid, ensure that and the irritation of skin is weakened significantly.
(2) lauroyl glutamate is weakly acidic, ensure that the extracted medical fluid of Chinese medicine can reduce be lost and have it is suitable
Reaction environment.
(3) lauroyl glutamate, which is added in washing product, can provide foam abundant, wash that rear skin is not tight, and moisture retention obtains
To improvement.
Solve the difficulty of above-mentioned technical problem:
Repeatedly discovery lauroyl glutamate is best for skin effects after investigation.
Solve the meaning of above-mentioned technical problem:
Washing product, which is applied to, for herbal liquid medicine provides idea and experiment basis.
Summary of the invention
In view of the problems of the existing technology, the present invention provides a kind of preparation methods of soap kind for shampoo.This
Invention is achieved in that a kind of preparation method of soap kind for shampoo, the preparation side of the soap kind for shampoo
Method the following steps are included:
The first step measures corresponding ratio coconut oil, lauroyl glutamate, pure water, and water is added and amino acid heating is made
Mixture；
Second step, oil mass well upper pot water proof heating, oil temperature and amino acid temperature are at 70 DEG C~80 DEG C, then water and amino
The mixture of acid is added, and boils 4h, pours into model, carries out Hybrid Heating reaction；
Third step, is put into 1h in freezer, and cooled and solidified molding forms soap kind model；
4th step, it is 2-3 weeks dry, test soap kind quality integrity.
Further, the first step is according to volume ratio amino acid: water: coconut oil=1:2:1.
Another object of the present invention is to provide a kind of use prepared by the preparation method by the soap kind for shampoo
In the natural traditional Chinese medicine ingredient soap kind of shampoo deoil, clean, conserved, the soap kind for shampoo by amino acid, water and
Coconut composition；According to volume ratio amino acid: water: coconut oil=1:2:1.
The rat acute percutaneous toxicity of Fig. 1 soap kind is tested
Conclusion: being greater than 2180mg/kg weight to the acute oral toxicity LD50 of rat, belongs to micro- malicious grade
Soap kind is used for shampoo, in (inhomogeneous shampoo in addition), as shown above, foaming characteristic is good.
In conclusion advantages of the present invention and good effect are as follows: the soap kind quality of preparation save it is complete, and preparation flow with
Technique is relatively easy, illustrates that it is smaller than general soap kind to skin damage by the dermal toxicity test of small white mouse, passes through comparison
The general soap kind blistering experiment in market illustrates the soap kind of our traditional Chinese medicine ingredients preparations with more cleaning, the effect of oil-control and maintenance, bubble
The continuous close stabilization of foam, activity are stronger.
Detailed description of the invention
Fig. 1 is the preparation method flow chart of the soap kind provided in an embodiment of the present invention for shampoo.
Fig. 2 is the preparation pictorial diagram of lauroyl glutamate natural soap kind provided in an embodiment of the present invention.
The left side solidifies more, and the right belongs to the liquid of thawing, emulsion process, with sodium carbonate and amino acid reaction life
At amino acid sodium, prepare that shampoo is more preferable, cleaning action of the amino acid sodium as shampoo surfactant, and more amino acid
Play the foaming agent in surfactant.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not used to limit
The fixed present invention.
Application principle of the invention is explained in detail with reference to the accompanying drawing.
As shown in Figure 1, the preparation method of the soap kind provided in an embodiment of the present invention for shampoo the following steps are included:
S101: corresponding ratio coconut oil, lauroyl glutamate (rear abbreviation amino acid), pure water are measured, water and ammonia is added
Mixture is made in the heating of base acid；
S102: oil mass well upper pot water proof heating, oil temperature and amino acid temperature are at 70 DEG C~80 DEG C, then water and amino acid
Mixture be added, Hybrid Heating reaction, boil 4h, pour into model；
S103: 1h in freezer, cooled and solidified molding are put into；
S104: 2-3 weeks dry.
Application principle of the invention is further described below with reference to experiment.
1 natural soap kind manufacture craft
1.1 experimental raws and capital equipment
Experimental raw: coconut oil, lauroyl glutamate etc. (hereinafter referred to as amino acid), pure water；It is matched according to volume ratio:
Amino acid: water: coconut oil=1:2:1；
Capital equipment: corrugation blender, food grade plastic bucket, beaker, stainless-steel pan, Roche foam meter.
1.2 experiment process
(1) corresponding ratio coconut oil, amino acid, pure water are measured, water and amino acid heating are mixed.
(2) oil mass well upper pot water proof heating, oil temperature and amino acid temperature are mixed at 70 DEG C~80 DEG C, then the two
Come.
(3) 40 minutes are stood, stirred 2 hours.
1.3 experimental section
(1) foamability of soap kind tests foam height for test solution from high 900mm, internal diameter 2.9mm with Roche foam meter
Pore in flow down, pour in the test solution for filling same temperature and same concentration, write down foam height when just having flowed solution.Note
Foam height when just having flowed solution down and foam height after five minutes.As foaming agent foamability and foam stability
Evaluation.Determination data is shown in Table 1
T=20 DEG C of foaming high (cm) when 1 foaming agent various concentration of table
As it can be seen from table 1 foaming agent of the same race is in the case where concentration difference, foam height increases with concentration and is increased,
After concentration increases to certain value (most of after 0.2%), foam height is remained unchanged.
(2) influence of the pH to foaming properties
Foam height of the 2 soap kind of table in different pH value
For the anti acid alkali performance of soap kind, it is steady that foaming capacity and foam of the natural soap kind in different pH value have been done in experiment
It is qualitative.Data are shown in Table 2, and as known from Table 2, the foaming capacity and foam stability of natural soap kind increase with pH value and increased, in acid
Foaming properties are poor in stronger (pH < 4) solution of property, but can also blister.This may be the day because in the lower medium of value
Right soap kind exists with non-ionic form, mainly exists in higher value solution with anionic form.
Fig. 2 is the preparation pictorial diagram of lauroyl glutamate natural soap kind provided in an embodiment of the present invention.The left side solidifies more
Some, the right belongs to the liquid of thawing, and emulsion process generates amino acid sodium, preparation hair washing with sodium carbonate and amino acid reaction
Water is more preferable, cleaning action of the amino acid sodium as shampoo surfactant, and more amino acid plays rising in surfactant
Infusion effect.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (3)
1. a kind of preparation method of the soap kind for shampoo, which is characterized in that the preparation side of the soap kind for shampoo
Method the following steps are included:
The first step measures corresponding ratio coconut oil, lauroyl glutamate, pure water, and water is added and mixing is made in amino acid heating
Object；
Second step, oil mass well upper pot water proof heating, oil temperature and amino acid temperature are at 70 DEG C~80 DEG C, then water and amino acid
Mixture is added, and Hybrid Heating reaction is boiled 4h, poured into model；
Third step is put into 1h in freezer, cooled and solidified molding；
4th step, it is 2-3 weeks dry.
2. the preparation method for the soap kind of shampoo as described in claim 1, which is characterized in that the first step is according to body
Product is than amino acid: water: coconut oil=1:2:1.
3. a kind of be used to have one's hair wash as described in claim 1~2 any one for the preparation method preparation of the soap kind of shampoo
The soap kind of water, which is characterized in that the soap kind for shampoo is made of amino acid, water and coconut；According to volume ratio amino
Acid: water: coconut oil=1:2:1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910373637.8A CN110090176A (en) | 2019-05-07 | 2019-05-07 | A kind of preparation method of the soap kind for shampoo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910373637.8A CN110090176A (en) | 2019-05-07 | 2019-05-07 | A kind of preparation method of the soap kind for shampoo |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110090176A true CN110090176A (en) | 2019-08-06 |
Family
ID=67447001
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910373637.8A Pending CN110090176A (en) | 2019-05-07 | 2019-05-07 | A kind of preparation method of the soap kind for shampoo |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055285A (en) * | 2015-08-26 | 2015-11-18 | 浙江奥瑞健生物技术有限公司 | Skin nutrition liquid and preparation method thereof |
| CN106344445A (en) * | 2016-08-26 | 2017-01-25 | 广州舒泰生物技术有限公司 | Amino acid shampoo and preparation method thereof |
| CN106434042A (en) * | 2016-08-12 | 2017-02-22 | 古巧渝 | Amino acid soap and production method |
| CN107349119A (en) * | 2017-07-25 | 2017-11-17 | 北京斯利安药业有限公司 | A kind of amino acid soap of stabilization and preparation method thereof |
| CN107384597A (en) * | 2017-07-25 | 2017-11-24 | 北京斯利安药业有限公司 | A kind of amino acid soap and preparation method thereof |
| CN107929106A (en) * | 2018-01-17 | 2018-04-20 | 广州环亚化妆品科技有限公司 | A kind of natural coconut oil mildy wash and preparation method thereof |
| CN108283583A (en) * | 2018-03-27 | 2018-07-17 | 广州禾力生物科技有限公司 | A kind of no silicoamino-acid shampoo and preparation method thereof |
| CN108309886A (en) * | 2018-04-13 | 2018-07-24 | 石梦成 | Potent strong ferment-Chinese medicine shampoo of one kind and preparation method thereof |
-
2019
- 2019-05-07 CN CN201910373637.8A patent/CN110090176A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055285A (en) * | 2015-08-26 | 2015-11-18 | 浙江奥瑞健生物技术有限公司 | Skin nutrition liquid and preparation method thereof |
| CN106434042A (en) * | 2016-08-12 | 2017-02-22 | 古巧渝 | Amino acid soap and production method |
| CN106344445A (en) * | 2016-08-26 | 2017-01-25 | 广州舒泰生物技术有限公司 | Amino acid shampoo and preparation method thereof |
| CN107349119A (en) * | 2017-07-25 | 2017-11-17 | 北京斯利安药业有限公司 | A kind of amino acid soap of stabilization and preparation method thereof |
| CN107384597A (en) * | 2017-07-25 | 2017-11-24 | 北京斯利安药业有限公司 | A kind of amino acid soap and preparation method thereof |
| CN107929106A (en) * | 2018-01-17 | 2018-04-20 | 广州环亚化妆品科技有限公司 | A kind of natural coconut oil mildy wash and preparation method thereof |
| CN108283583A (en) * | 2018-03-27 | 2018-07-17 | 广州禾力生物科技有限公司 | A kind of no silicoamino-acid shampoo and preparation method thereof |
| CN108309886A (en) * | 2018-04-13 | 2018-07-24 | 石梦成 | Potent strong ferment-Chinese medicine shampoo of one kind and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 化学工业出版社: "《中国化工产品大全》", 31 January 2005, 化学工业出版社 * |
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Application publication date: 20190806 |