CN108852915A - A kind of lasting type is without silicone oil shampoo - Google Patents
A kind of lasting type is without silicone oil shampoo Download PDFInfo
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- CN108852915A CN108852915A CN201811160304.9A CN201811160304A CN108852915A CN 108852915 A CN108852915 A CN 108852915A CN 201811160304 A CN201811160304 A CN 201811160304A CN 108852915 A CN108852915 A CN 108852915A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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Abstract
The invention belongs to daily cosmetics fields, and in particular to a kind of lasting type is without silicone oil shampoo.A kind of lasting type is without silicone oil shampoo, which is characterized in that by mass percentage, raw material composition includes：The Polyquaternium-10 of 0.05-0.2%；The cation flocculation moisture-regulating agent of 2-5%；The disodium ethylene diamine tetraacetate of 0.05-0.2%；0.05-0.1% cithrol；The anionic surfactant of 20%-27%；The cocoanut fatty acid diethanolamide of 2%-3%；The zwitterionic surfactant of 1-9%；The PEG-7 coco glycerides of 2-5%；The gel water-in-oil emulsion composition of 1%-2%；The moisture-regulating agent of 2%-4%；The essence of 0.5-2%；The pure water of 45-65%.Each component in inventive formulation constitutes Recompounded multielement system, and compound system enhances the ability of dissolution essence, improves the lasting ability of shampoo, improve the stability of product entirety, achievees the effect that health washes shield, safety nourishes scalp, hair.
Description
Technical field
The invention belongs to daily cosmetics fields, and in particular to a kind of lasting type is without silicone oil shampoo.
Background technique
Shampoo also known as shampoo, be a kind of collection Surfactants solution, oily matter solubilising, dispersion suspend, high score
The complex system that sub- colloidal solution is integrated.The major function of shampoo is cleaning hair and scalp, and is beaten for the maintenance of hair
Lower basis.With the development of technology, also increasingly increase the effect of shampoo, nowadays have evolved into degreasing, anti-dandruff, taste
The product of the multiple functions such as profit, hair care, anticreep, hair tonic.Now, while people pursue conditioning effect, fragrant, safety are strong
The shampoo of health is increasingly liked by masses.
Shampoo is a complicated system, often will appear unstable situation, main table in storage and use process
Now decline for viscosity, transparent shampoo occurs muddy or generates precipitating；And the addition of essence easily goes out shampoo in shampoo
The problems such as now defoaming, viscosity reduction, muddiness, discoloration.In the prior art, the essence lasting ability of addition is limited, and not destroy system
Viscosity, foaming capacity, the general content of the essence of addition is lower (generally between 0.3-0.8%).
In view of the above problems, each component that the present invention provides a kind of lasting types without silicone oil shampoo, in inventive formulation
Recompounded multielement system is together constituted, compound system enhances the ability of dissolution essence, improves the lasting ability of shampoo.It washes
Gel water-in-oil emulsion composition in shampoo has excellent stability, is conducive to a variety of greases, surfactant exists
It keeps stablizing in the mixed system of shampoo.
Summary of the invention
Above-mentioned technical purpose of the invention technical scheme is that：
A kind of lasting type is without silicone oil shampoo, and by mass percentage, raw material composition includes：
The Polyquaternium-10 of 0.05-0.2%；The cation flocculation moisture-regulating agent of 2-5%；The second two of 0.05-0.2%
Amine tetraacethyl disodium；0.05-0.1% cithrol；The anionic surfactant of 20%-27%；2%-3%'s
Cocoanut fatty acid diethanolamide；The zwitterionic surfactant of 1-9%；The PEG-7 coco glycerides of 2-5%；1%-
2% gel water-in-oil emulsion composition；The moisture-regulating agent of 2%-4%；The essence of 0.5-2%；45-65%'s is pure
Water.
Preferably, a kind of lasting type is without silicone oil shampoo, and by mass percentage, raw material composition includes：
The Polyquaternium-10 of 0.05-0.2%；The cation flocculation moisture-regulating agent of 2-5%；The second two of 0.05-0.2%
Amine tetraacethyl disodium；0.05-0.1%PEG-6000 distearate；The sodium sulfate of polyethenoxy ether of fatty alcohol of 20%-27%；
The cocoanut fatty acid diethanolamide of 2%-3%；The Cocoamidopropyl betaine of 1-9%；The PEG-7 cocounut oil of 2-5% is sweet
Grease；The gel water-in-oil emulsion composition of 1%-2%；The moisture-regulating agent of 2%-4%；The essence of 0.5-2%；45-
65% pure water.
It is further preferred that a kind of lasting type, without silicone oil shampoo, by mass percentage, raw material composition includes：
0.1% Polyquaternium-10；3.2% cation flocculation moisture-regulating agent；0.1% ethylenediamine tetra-acetic acid two
Sodium；0.65%PEG-6000 distearate；22% sodium sulfate of polyethenoxy ether of fatty alcohol；2.6% coco-nut oil fatty acid
Diglycollic amide；9% Cocoamidopropyl betaine；3.2%PEG-7 coco glycerides；1.6% gel water-in-oil type
Emulsion compositions；3% moisture-regulating agent；1.2% essence；Surplus pure water.
Preferably, the gel water-in-oil emulsion composition is trimethylolpropane tris caprylate, saualane, Ci A
The composition of dry tree benevolence oil, three isostearate of polyglycereol -2, water, by mass percentage, raw material composition includes 60-80%
Trimethylolpropane tris caprylate, the saualane of 1-10%, thorn A Gan tree benevolence oil, the 1-10% polyglycereol -2 three of 1-10% it is different
The water of stearate, 1-10%.
It is further preferred that the gel water-in-oil emulsion composition is prepared by following methods：
(1) by the trimethylolpropane tris caprylate of 60-80%, the thorn A Gan tree benevolence of the saualane of 1-10%, 1-10%
Oil is added in oily phase pot, stirs evenly, obtains mixed liquor A；(2) three isostearate of the polyglycereol -2 of 1-10% is added and is mixed
Where liquid A in oily phase pot, stirs evenly, obtain oil-phase solution；(3) water of 1-10% is slowly pumped into above-mentioned oil-phase solution,
It stirs at low speed and the gel water-in-oil emulsion composition is prepared.
Preferably, the essence is one of lily essence, lemon extract or a variety of.
Preferably, the cithrol is PEG-6000 distearate.
Preferably, the anionic surfactant is lauryl sodium sulfate, ammonium lauryl sulfate, fatty alcohol polyoxy
One of ethylene ether sodium sulfate, alpha-olefin sodium sulfonate, fatty alcohol polyoxyethylene ether ammonium sulfate and lauric acid sodium taurocholate are more
Kind.
It is further preferred that the anionic surfactant is sodium sulfate of polyethenoxy ether of fatty alcohol.
Preferably, the zwitterionic surfactant is Cocoamidopropyl betaine, dodecyl dimethyl beet
One of alkali and palmitamide propyl betaine are a variety of.
It is further preferred that the zwitterionic surfactant is Cocoamidopropyl betaine.
The present invention also provides a kind of preparation method of the lasting type without silicone oil shampoo, the preparation method includes following step
Suddenly：
(1) addition Polyquaternium-10, cation flocculation moisture-regulating agent, stirring are transparent to solution in water, are warming up to 70-80
DEG C, obtain mixed solution A；
(2) under 70-80 DEG C and stirring condition, by disodium ethylene diamine tetraacetate, cithrol, anion surface active
Agent, cocoanut fatty acid diethanolamide are added in mixed solution A, obtain mixed solution B；
(3) PEG-7 coco glycerides and gel water-in-oil emulsion composition are mixed evenly, then with amphoteric ion surface
Activating agent is added in mixed solution B, stirs at 70-80 DEG C, keeps the temperature 30min, obtains mixed solution C；
(4) solution C to be mixed is cooled to 30-45 DEG C, will mix in moisture-regulating agent, essence investment mixed solution C, stirring is equal
It is even, a kind of lasting type is made without silicone oil shampoo.
Compared with prior art, the beneficial effects of the present invention are：
Cation flocculation moisture-regulating agent, anionic surfactant, coco-nut oil fatty acid diethyl in inventive formulation
Alkylolamides, zwitterionic surfactant, moisture-regulating agent and gel water-in-oil emulsion composition etc. together constitute more
First compound system, in the case where essence additive amount improves and do not increase the solubilizer such as rilanit special, system enhances after compounding
The ability of dissolution essence, improves the lasting ability of shampoo.And gel water-in-oil emulsion composition has excellent
Stability, be conducive to a variety of greases, surfactant and keep stablizing in the mixed system of shampoo, do not destroy the viscous of system
Degree promotes release of active constituent during hair washing in formula.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with specific embodiment, the embodiment provided is only
Reach illustration purpose, can not be interpreted as limitation of the invention.Constituent content in following embodiments, such as without special theory
It is bright, it is mass percent.
Embodiment 1-7
Embodiment 1-7 is a kind of lasting type prepared by the present invention without silicone oil shampoo, and contained component includes Polyquaternium-10
(JR400), cation flocculation moisture-regulating agent (QZ-1001), disodium ethylene diamine tetraacetate (EDTA-2Na), polyethylene glycol fatty
Acid esters (PEG-6000 distearate (638)), anionic surfactant (sodium sulfate of polyethenoxy ether of fatty alcohol (AES)),
Cocoanut fatty acid diethanolamide (6501), zwitterionic surfactant (Cocoamidopropyl betaine (CAB)), PEG-
7 coco glycerides (HE), gel water-in-oil emulsion composition, moisture-regulating agent (QZ-CY), essence (lily), essence (lemon
Lemon), pure water, alpha-olefin sodium sulfonate (AOS), lauryl sodium sulfate (K12), dodecyldimethylammonium hydroxide inner salt.
Cation flocculation moisture-regulating agent (QZ-1001) is that our company is commercially available by polyquaternium -49, pyrrolidones carboxylic
The compound that sour sodium, sodium lactate, sodium citrate, glutamic acid, water compound.
The moisture-regulating agent (QZ-CY) is the commercially available pyrrolidone sodium carboxylate of our company, sodium lactate, glutamic acid, citric acid
The compound of sodium, water compounding.
Comparative example 8-12
Embodiment 8 the difference is that, changes coconut oil list isopropanol amide into for 6501 with 1-7 of the embodiment of the present invention
(CMIPA)。
Embodiment 9 the difference is that, changes cocounut oil acid methyl monoethanol acyl into for 6501 with 1-7 of the embodiment of the present invention
Amine (CMMEA).
Embodiment 10 the difference is that, changes coconut oil list isopropanol amide into for 6501 with 1-7 of the embodiment of the present invention
(CMIPA), and solubilizer rilanit special (CH40) is added.
Embodiment 11 the difference is that, is added solubilizer rilanit special (CH40) with 1-7 of the embodiment of the present invention.
Embodiment 12 the difference is that, changes coconut oil list isopropanol amide into for 6501 with 1-7 of the embodiment of the present invention
(CMIPA), essence content is reduced.
A kind of preparation of gel water-in-oil emulsion composition
Weigh the thorn A Gan tree benevolence of the trimethylolpropane tris caprylate of 60-80%, the saualane of 1-10%, 1-10%
Oil is put into oily phase pot, stirs evenly, obtain mixed liquor A；Mixing is added in three isostearate of polyglycereol -2 for weighing 1-10%
Where liquid A in oily phase pot, stirs evenly, obtain oil-phase solution；The aqueous phase solution of 1-10% is slowly pumped into above-mentioned oil to mix
It in liquid, stirs at low speed, a kind of gel water-in-oil emulsion composition is prepared.
A kind of preparation of the lasting type without silicone oil shampoo
(1) in water put into Polyquaternium-10, cation flocculation moisture-regulating agent, stir evenly to be formed it is transparent clarification it is molten
Liquid is warming up to 70-80 DEG C, obtains mixed solution A；
(2) by disodium ethylene diamine tetraacetate, PEG-6000 distearate, sodium sulfate of polyethenoxy ether of fatty alcohol, coconut
Fatty acid oil diglycollic amide is put into mixed solution A, and temperature is maintained at 70-80 DEG C, and stirring forms transparent clear solution, is obtained
To mixed solution B；
(3) PEG-7 coco glycerides and gel water-in-oil emulsion composition are mixed evenly, then with coconut oleoyl amine
Propyl betaine is put into mixed solution B, is stirred at 70-80 DEG C, is kept the temperature 30min, is obtained mixed solution C；
(4) solution C to be mixed is cooled to 45 DEG C hereinafter, by mixing in moisture-regulating agent, essence investment mixed solution C, stirs
It mixes uniformly, a kind of lasting type is made without silicone oil shampoo.
Solubilizer rilanit special (CH40) in embodiment 10-11 is cooled to 45 DEG C or less in step (4) mixed solution C
After be added.
Lasting type of the present invention described in embodiment 1-7 is as shown in the following Table 1 without silicone oil shampoo component information.
The lasting type of the present invention of table 1 is without silicone oil shampoo component information table
Comparative example 8-12 shampoo component information is as shown in the following Table 2.
2 comparative example 8-12 shampoo component information table of table
Testing example 1：Stability experiment
The stability test experiment condition of shampoo is respectively：Shampoo is placed at 40 DEG C for 24 hours by heat-resistant stability,
Whether there is or not laminations for observation after restoring room temperature；Shampoo is placed under 5 DEG C of refrigerating chamber for 24 hours, recovery room by cold resistance stability
Phenomenon is observed after temperature.And be placed on shampoo under -10 DEG C of freezing chamber for 24 hours, phenomenon, test result are observed after restoring room temperature
As shown in table 3.
Different types of amide has been used to be compounded in comparative example 8-11, but its stablizing effect is not as good as addition 6501
's
Embodiment 1-7 is good, and comparative example 8-11 stability is poor, occurs substance in stability test experiment and is precipitated, is layered now
As.Comparative example 10 improves the stability of the shampoo containing CMIPA after solubilizer is added to a certain extent, but its
The phenomenon that there are viscosity declines, the long-term preservation being unfavorable in shampoo practical application.Comparative example 11 is implemented in the present invention
On the basis of example 2 be added solubilizer rilanit special (CH40), stability test the result shows that, although joined solubilizer implementation
Still there is the phenomenon that viscosity decline in example 7, does not significantly improve the effect of hair washing water stability.Comparative example 12 can be seen that
Under the premise of keeping shampoo stable system, the essence content that can be added is generally lower, and when essence content increases, shampoo is easily muddy
Turbid, viscosity reduces.Therefore, formula provided by the invention can improve essence and contain in the case where not using high-cost solubilizer
It measures and keeps stable system.
The stability test result table of 3 embodiment 1-12 of table
Testing example 2：Applied experiments
(A is the siliceous shampoo of certain brand of market sale, certain product that B is market sale to the comparison of this product applied experiments
Board without silicone oil shampoo, C be in inventive formulation described in embodiment 2 without silicone oil shampoo).
Test equipment：Comb force tester.
Test sample：Import topknot (30 ± 1cm of length, 10 ± 1g of weight).
Test method：The dry and wet carding force for first surveying blank topknot, after 2g hair washing water process hair, test hair washing water process
The dry and wet carding force of topknot afterwards, the relatively variation of front and back carding force.Flushing period 30s, resistance unit are newton, and test result is such as
Shown in table 4.
The test result contrast table of shampoo described in 4 commercial product of table and embodiment 2
Embodiment 1 and 3-7 retest embodiment 2 obtain contrast effect even more preferably similar with table 4, wherein
The wet carding force of embodiment 1 and 3-6 reduces 78.04% respectively, 77.32%, 80.03%, 79.80%, 78.90%,
77.42%；Dry carding force reduces 53.16%, 52.81%, 55.11%, 50.87%, 55.43%, 52.13% respectively.
In conclusion the present invention carries out compatibility by many experiments and adjusts the ratio of each component, develops one kind and stay
Odor type is without silicone oil shampoo.The Recompounded multielement system that each group is grouped as in shampoo improves in essence additive amount, and does not increase hydrogen
In the case where changing the solubilizer such as castor oil, the ability of compound system dissolution essence is enhanced, and improves the lasting energy of shampoo
Power reduces production cost.Meanwhile the gel water-in-oil emulsion composition in formula can be substituted in shampoo again and be answered extensively
Silicone oil is attached to hair surface layer and repairs the hair scale piece being damaged, scalp is made clearly to breathe freely.Product formation diversification structure,
The stability for improving integral product is conducive to a variety of greases, surfactant and keeps stablizing in the mixed system of shampoo,
The viscosity for not destroying system achievees the effect that health washes shield, safety nourishes scalp, hair.
Claims (10)
1. a kind of lasting type is without silicone oil shampoo, which is characterized in that by mass percentage, raw material composition includes：0.05-
0.2% Polyquaternium-10；The cation flocculation moisture-regulating agent of 2-5%；The disodium ethylene diamine tetraacetate of 0.05-0.2%；
0.05-0.1% cithrol；The anionic surfactant of 20%-27%；The coco-nut oil fatty acid of 2%-3%
Diglycollic amide；The zwitterionic surfactant of 1-9%；The PEG-7 coco glycerides of 2-5%；The gel oil of 1%-2%
Water-in type emulsion compositions；The moisture-regulating agent of 2%-4%；The essence of 0.5-2%；The pure water of 45-65%.
2. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that by mass percentage, former
Material forms：The Polyquaternium-10 of 0.05-0.2%；The cation flocculation moisture-regulating agent of 2-5%；The second of 0.05-0.2%
Edetate disodium；0.05-0.1%PEG-6000 distearate；The fatty alcohol polyoxyethylene ether sulfuric acid of 20%-27%
Sodium；The cocoanut fatty acid diethanolamide of 2%-3%；The Cocoamidopropyl betaine of 1-9%；The PEG-7 cocounut oil of 2-5%
Glyceride；The gel water-in-oil emulsion composition of 1%-2%；The moisture-regulating agent of 2%-4%；The essence of 0.5-2%；
The pure water of 45-65%.
3. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that by mass percentage, former
Material forms：0.1% Polyquaternium-10；3.2% cation flocculation moisture-regulating agent；0.1% ethylenediamine tetra-acetic acid
Disodium；0.65%PEG-6000 distearate；22% sodium sulfate of polyethenoxy ether of fatty alcohol；2.6% coconut oil fat
Sour diglycollic amide；9% Cocoamidopropyl betaine；3.2%PEG-7 coco glycerides；1.6% gel Water-In-Oil
Type emulsion compositions；3% moisture-regulating agent；1.2% essence；Surplus pure water.
4. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that the gel water-in-oil type cream
Liquid composition is trimethylolpropane tris caprylate, saualane, thorn A Gan tree benevolence oil, three isostearate of polyglycereol -2, water
Composition, by weight percentage, raw material group become：The spiny dogfish of the trimethylolpropane tris caprylate of 60-80%, 1-10%
The water for piercing A Gan tree benevolence oil, -2 three isostearate of 1-10% polyglycereol, 1-10% of alkane, 1-10%.
5. a kind of lasting type as claimed in claim 4 is without silicone oil shampoo, which is characterized in that described by trimethylolpropane tris
The gel water-in-oil emulsion group of caprylate, saualane, thorn A Gan tree benevolence oil, three isostearate of polyglycereol -2, water composition
Object is closed, prepares gained with the following method：
Step 1)：By the trimethylolpropane tris caprylate of 60-80%, the thorn A Gan tree benevolence of the saualane of 1-10%, 1-10%
Oil is added in oily phase pot, stirs evenly, obtains mixed liquor A；
Step 2)：Where mixed liquor A is added in three isostearate of polyglycereol -2 of 1-10% in oily phase pot, stirs evenly, obtain
To oil-phase solution；
Step 3)：The water of 1-10% is slowly pumped into above-mentioned oil-phase solution, stirs at low speed and the gel oil packet is prepared
Water emulsion composition.
6. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that the essence be lily essence,
One of lemon extract is a variety of.
7. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that the anionic surfactant
For lauryl sodium sulfate, ammonium lauryl sulfate, sodium sulfate of polyethenoxy ether of fatty alcohol, alpha-olefin sodium sulfonate, poly alkyl alcohol
One of ethylene oxide ether ammonium sulfate and lauric acid sodium taurocholate are a variety of.
8. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that the amphoteric ion surface-active
Agent is one of Cocoamidopropyl betaine, dodecyldimethylammonium hydroxide inner salt and palmitamide propyl betaine or more
Kind.
9. a kind of lasting type as described in claim 1 is without silicone oil shampoo, which is characterized in that the cithrol
For PEG-6000 distearate.
10. a kind of prepare method of the lasting type without silicone oil shampoo using raw material described in claim 1, which is characterized in that described
In preparation method, ratio used in each raw material is as described in claim 1, comprises the steps of：
(1) addition Polyquaternium-10, cation flocculation moisture-regulating agent, stirring are transparent to solution in water, are warming up to 70-80
DEG C, obtain mixed solution A；
(2) under 70-80 DEG C and stirring condition, by disodium ethylene diamine tetraacetate, cithrol, anion surface active
Agent, cocoanut fatty acid diethanolamide are added in mixed solution A, obtain mixed solution B；
(3) PEG-7 coco glycerides and gel water-in-oil emulsion composition are mixed evenly, then with amphoteric ion surface
Activating agent is added in mixed solution B, stirs at 70-80 DEG C, keeps the temperature 30min, obtains mixed solution C；
(4) solution C to be mixed is cooled to 30-45 DEG C, will mix in moisture-regulating agent, essence investment mixed solution C, stirring is equal
It is even, a kind of lasting type is made without silicone oil shampoo.
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| CN201811160304.9A CN108852915A (en) | 2018-09-30 | 2018-09-30 | A kind of lasting type is without silicone oil shampoo |
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| CN201811160304.9A CN108852915A (en) | 2018-09-30 | 2018-09-30 | A kind of lasting type is without silicone oil shampoo |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111000742A (en) * | 2019-12-27 | 2020-04-14 | 湖北省麦诗特生物科技有限公司 | Composite oil ester composition for hair washing and caring products and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003095886A (en) * | 2001-09-26 | 2003-04-03 | Kose Corp | Shampoo composition |
| CN106420407A (en) * | 2016-08-31 | 2017-02-22 | 福建省梦娇兰日用化学品有限公司 | Child silicone-oil-free shampoo with vegetable oil and fat replacing silicone oil |
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| CN111000742A (en) * | 2019-12-27 | 2020-04-14 | 湖北省麦诗特生物科技有限公司 | Composite oil ester composition for hair washing and caring products and preparation method and application thereof |
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