CN110055143A - A kind of composition of the component containing natural activity and its preparation method and application - Google Patents

A kind of composition of the component containing natural activity and its preparation method and application Download PDF

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Publication number
CN110055143A
CN110055143A CN201910468597.5A CN201910468597A CN110055143A CN 110055143 A CN110055143 A CN 110055143A CN 201910468597 A CN201910468597 A CN 201910468597A CN 110055143 A CN110055143 A CN 110055143A
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Prior art keywords
extract
natural activity
composition
parts
chain alkane
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Granted
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CN201910468597.5A
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CN110055143B (en
Inventor
何玉东
张建喜
贺春良
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Xi'an Youluqing Technology Co Ltd
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Xi'an Youluqing Technology Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38618Protease or amylase in liquid compositions only
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38627Preparations containing enzymes, e.g. protease or amylase containing lipase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38636Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/26Organic compounds containing oxygen
    • C11D7/261Alcohols; Phenols
    • C11D7/262Alcohols; Phenols fatty or with at least 8 carbon atoms in the alkyl or alkenyl chain
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/40Products in which the composition is not well defined
    • C11D7/44Vegetable products

Abstract

The present invention relates to detergent applications, provide a kind of composition of component containing natural activity, and by weight, raw material includes at least, 50-100 parts of natural activity components, 0.5-5 parts of polyhydroxy long-chain alkane, 1-5 parts of biological enzyme.Additionally provide the preparation method and application of the composition of the component containing natural activity.

Description

A kind of composition of the component containing natural activity and its preparation method and application
Technical field
The present invention relates to detergent applications, specifically further relate to composition and its preparation side of a kind of component containing natural activity Method and application.
Background technique
Fruit and vegetable residual pesticide refers to that vegetables remain in the pesticide and toxic metabolite, Degradation and Transformation on its surface after spraying pesticide The general name of product and reaction impurities.Today's society, people lead to the use lack of standardization of pesticide, agriculture to the excessive pursuit of economic benefit Although a large amount of uses of medicine improve fruit, the yield of vegetables, remaining pesticide has seriously endangered human health.With people People's improvement of living standard and the food-safe reinforcement with environmental protection consciousness of people, surface of agricultural products Pesticide Residue It is increasingly subject to public concerns.Currently, develop can effectively remove surface of agricultural products agriculture is residual, microorganism and dirt mud Sand, and can be free from environmental pollution, and the hot spot that fast and easily strong detergent is paid close attention at the whole world is cleaned, it is most at present to wash Fruit surface pesticide residue, dirt and various pathogenic bacteria can effectively be cleaned by washing agent, but some cleaning agents in the prior art, clear Net agent product finds that chemically surfactant component can be added in product component, so causing chemistry in the process of washing Component also has residual, and veterinary antibiotics is not made to reach real cleaning, and people can be damaged by eating chemically surfactant for a long time Body health, causes edible safety hidden danger, in addition, it is single for the component effect in fruits and vegetables cleaning product in the prior art, mainly To remove pesticide.Therefore it needs to research and develop that there is the cleaning combination of high security can be applied to various cleaning agents or peace and quiet Agent, and there is multi-functional effect.
Summary of the invention
In order to solve the above technical problems, the first aspect of the invention provides a kind of group of component containing natural activity Object is closed, by weight, raw material includes at least, 50-100 parts of natural activity components, 0.5-5 parts of polyhydroxy long-chain alkane, and 1-5 parts Biological enzyme.
As a kind of perferred technical scheme, heretofore described natural activity component includes plant extracts;The plant Object extract in Flos Lonicerae extractive solution, Cassia Nomame P.E, Folium Artemisiae Argyi extract, Maca extract, lemon extract one Kind or a variety of combinations.
As a kind of perferred technical scheme, there is 2-6 hydroxyl in heretofore described polyhydroxy long-chain alkane;It is described more There is 5-12 methylene in hydroxyl long chain alkane.
As a kind of perferred technical scheme, heretofore described biological enzyme be selected from zytase, lipase, phytase, Amylase, protease, cutinase, cellulase, pectase, mannonase arabinase, Galactanase, oxide One of enzyme or a variety of combinations.
As a kind of perferred technical scheme, heretofore described raw material further includes 5-20 parts of water soluble chitosans.
As a kind of perferred technical scheme, heretofore described plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract;The Folium Artemisiae Argyi extract, Maca extract, lemon extract weight ratio be 1:(1-5): (0.1- 1)。
As a kind of perferred technical scheme, heretofore described biological enzyme is the group of lipase, phytase, zytase It closes;The phytase, lipase, zytase weight ratio be 1:(0.05-0.5): (0.5-1.5).
As a kind of perferred technical scheme, heretofore described natural activity component further includes butter berry extract, reed Luxuriant growth extract, citrus berry extract, bermuda lily flower extract, rose extract, purslane extract, dried tremella extract, tea One of leaf extract, Gotu Kola P.E, german chamomile flower extract, rosemary leaf extract or a variety of combinations.
The second aspect of the invention provides the preparation method of the composition of the component containing natural activity described in one kind, step It includes at least, (1) weighs each raw material in composition, spare;(2) first natural activity component, polyhydroxy long-chain alkane are stirred equal It is even;It adds biological enzyme and continues to stir evenly and poured into clean container to obtain the final product, sealed.
The third aspect of the invention provides the application of the composition of the component containing natural activity described in one kind, is applied to clear Wash water fruits and vegetables.
The utility model has the advantages that
The present invention is to provide a kind of composition of component containing natural activity, the present invention has and reduces pesticide, microorganism, thin The remarkable result of bacterium residual volume on fruit and vegetable food, and have that pesticides removal is high-efficient, the fast excellent characteristics of removal rate;Due to Main component of the present invention is containing natural active component, safety and environmental protection, and long-time service not only will not cause skin to human body Injury, can be with the state of conditioning skin.
Specific embodiment
Unless otherwise indicated, from context cues or belong to the convention of the prior art, otherwise number all in the application It is all based on weight with percentage, and test and characterizing method used is all synchronous with the submission date of the application.If existing There is defining for the concrete term disclosed in technology inconsistent with any definition provided herein, then with provided herein Subject to term definition.
It is further clear, complete that the technical characteristic work in technical solution is provided to the present invention With reference to embodiment Description, not to the limitation of its protection scope.
Word " preferred ", " preferably ", " preferred " in the present invention etc. refer to, can provide certain in some cases The embodiment of the present invention of a little beneficial effects.However, other embodiments may also under identical circumstances or in the case of other It is preferred.In addition, not implying that other embodiments are unavailable to the statement of one or more preferred embodiments, it is not yet It is intended to exclude other embodiments except the scope of the present invention.The source of unmentioned component is commercially available in the present invention.
The first aspect of the invention provides a kind of composition of component containing natural activity, and by weight, raw material is extremely It less include 50-100 parts of natural activity components, 0.5-5 parts of polyhydroxy long-chain alkane, 1-5 parts of biological enzyme.
In some preferred embodiments, the composition of the component containing natural activity, by weight, raw material is at least It include 60-90 parts of natural activity components, 1-4 parts of polyhydroxy long-chain alkane, 2-4 parts of biological enzyme.
In some preferred embodiments, the composition of the component containing natural activity, by weight, raw material is at least It include 80 parts of natural activity components, 2.5 parts of polyhydroxy long-chain alkane, 3 parts of biological enzyme.
In some embodiments, the natural activity component includes plant extracts;The plant extracts is selected from gold One of honeysuckle flower extracting solution, Cassia Nomame P.E, Folium Artemisiae Argyi extract, Maca extract, lemon extract or a variety of combinations; Preferably, the plant extracts in Cassia Nomame P.E, Folium Artemisiae Argyi extract, Maca extract, lemon extract one Kind or a variety of combinations;It is furthermore preferred that the plant extracts is in Folium Artemisiae Argyi extract, Maca extract, lemon extract One or more combinations.
In some embodiments, the plant extracts is the group of Folium Artemisiae Argyi extract, Maca extract, lemon extract It closes;The Folium Artemisiae Argyi extract, Maca extract, lemon extract weight ratio be 1:(1-5): (0.1-1);Preferably, described Folium Artemisiae Argyi extract, Maca extract, lemon extract weight ratio be 1:(2-3): (0.3-0.7);It is furthermore preferred that the folium artemisiae argyi Extract, Maca extract, lemon extract weight ratio be 1:2.5:0.5.
No. CAS of the Folium Artemisiae Argyi extract is 94-24-6;No. CAS of the Maca extract is 138-59-0;The lemon No. CAS of lemon extract is 84929-31-7.
In some embodiments, there is 2-6 hydroxyl in the polyhydroxy long-chain alkane;In the polyhydroxy long-chain alkane There is 5-12 methylene;Preferably, there is 3-5 hydroxyl in the polyhydroxy long-chain alkane;Have in the polyhydroxy long-chain alkane 7-10 methylene;It is furthermore preferred that there is 4 hydroxyls in the polyhydroxy long-chain alkane;There are 9 in the polyhydroxy long-chain alkane Methylene.
In some embodiments, the polyhydroxy long-chain alkane is alkyl glycosides.
In some embodiments, the polyhydroxy long-chain alkane is selected from lauryl glucoside, undecyl glucoside, just One of decyl glucoside, butyl glucoside or a variety of combinations;Preferably, the polyhydroxy long-chain alkane is selected from laurel One of base glucoside, undecyl glucoside, positive decyl glucoside or a variety of combinations;It is furthermore preferred that the polyhydroxy Base long chain alkane is positive decyl glucoside.
In some embodiments, the biological enzyme be selected from zytase, lipase, phytase, amylase, protease, One of cutinase, cellulase, pectase, mannonase arabinase, Galactanase, oxide enzyme are more The combination of kind;Preferably, the biological enzyme be selected from one of zytase, lipase, phytase, amylase, protease or A variety of combinations;It is furthermore preferred that the biological enzyme is selected from one of zytase, lipase, phytase or a variety of combinations.
The CAS 9025-57-4 of the zytase;No. CAS of the lipase is 9001-62-1;The phytase No. CAS be 37288-11-2.
In some embodiments, the biological enzyme is the combination of lipase, phytase, zytase;The phytase, Lipase, zytase weight ratio be 1:(0.05-0.5): (0.5-1.5);Preferably, the phytase, lipase, wood are poly- The weight ratio of carbohydrase is 1:(0.1-0.3): (0.8-1.2);It is furthermore preferred that the weight of the phytase, lipase, zytase Than for 1:0.2:1.
It is found by the applicant that chitosan of the present invention, natural plant extracts, alkyl glycosides, phytase, protease are multiple With the removal rate that can be improved to pesticide is used, the residual quantity of pesticide and microorganism and bacterium on fruits and vegetables is significantly reduced, Realization thoroughly removes fruit-vegetable pesticide residues;Speculate possible cause, alkyl glycosides can reduce the surface tension of solution, increase Contact area between natural plant extracts and chitosan and phytase facilitates the natural activity group in plant extracts Divide and promotes biological enzyme to the degradation reaction of pesticide, and the Folium Artemisiae Argyi extract, Maca extract and lemon in plant extracts extract Active component in object can play excellent concertedness, further promote the removal to pesticide and microorganism and bacterium, can Can the reason is that due to having a large amount of a variety of amino acid in the extract of Maca simultaneously and rich in glucosinolate and taurine component, And it can be with chitosan jointly to the pesticide composition after degradation under the collaboration of active component of the glucosinolate in lemon extract Complexing is generated, the forward reaction direction for further promoting degradation reaction carries out, and taurine is active in Folium Artemisiae Argyi extract Under the collaboration of component, the osmotic pressure of the cell peripheral of microorganism and bacterium is adjusted, so that phosphatide of the bioactive enzyme to cell membrane Damage, to kill the microorganisms such as bacterium.
In some embodiments, the raw material further includes 5-20 parts of water soluble chitosans;Preferably, the raw material also wraps Include 10-18 parts of water soluble chitosans;It is furthermore preferred that the raw material further includes 16 parts of water soluble chitosans.
Can have when it has been found that being used in conjunction in the present invention using plant extracts and biological enzyme and very excellent go agriculture The effect of medicine and microorganism, be added a certain amount of zytase and chitosan can be further improved improve biological enzyme to pesticide and The degrading activities such as microorganism, removal efficiency significantly improve, and the purpose of Rapid Cleaning may be implemented, and avoid present people allegro Life style and lead to the halfway situation of cleaning that will cause pesticide etc., and hardly have catabolite and detersive Component is remained in the contact site of fruit and vegetable surfaces and human body, realizes noresidue truly, safety and environmental protection;Speculating may It is that chitosan can not only adsorb metal ion and other particles in fruits and vegetables, but also have in chitosan macromolecular active Hydroxyl and amino, absorption can also be generated to the residue after degradation, the residue of fruit and vegetable surfaces can taken away, due to shell Complex reaction occurs for the electropositive of glycan and the mustard seed glycerol in the extract of Maca, to greatly improve in whole process to pesticide Degradation rate.Fruits and vegetables are produced further, since zytase reduces detersive component by the cell wall generation effect to plant The active force of product reduces the tension force effect of plant surface, conducive to flowing away for chitosan macromolecular and biological enzyme, further increases Except the speed of pesticide, and it can accomplish noresidue.
Particular determination does not do in water soluble chitosan purchase producer, and general commercially available water soluble chitosan can be applicable in In the present invention;Preferably, it buys from Xiang Tan source Jia Ye Biotechnology Co., Ltd, model 2277-92-1.
In some embodiments, the natural activity component further includes butter berry extract, aloe extract, citrus fruit Extract, bermuda lily flower extract, rose extract, purslane extract, dried tremella extract, tea extract, centella One of extract, german chamomile flower extract, rosemary leaf extract or a variety of combinations;Preferably, the natural activity group Dividing further includes one of butter berry extract, aloe extract, rose extract, purslane extract, Gotu Kola P.E Or a variety of combination;It is furthermore preferred that the natural activity component further include one of butter berry extract, aloe extract or A variety of combinations.
In some embodiments, the natural activity component further includes the combination of butter berry extract, aloe extract; Preferably, the butter berry extract, Maca extract, aloe extract weight ratio be 1:(1-5): (0.5-2);More preferably , the butter berry extract, Maca extract, aloe extract weight ratio be 1:(2-4): (1-1.6);Further preferably , the butter berry extract, Maca extract, aloe extract weight ratio be 1:3:1.4.
It has been found that the effect that can have conditioning skin state is used for a long time in fruits and vegetables cleaning agent of the present invention, The possible reason is what the present invention used is all natural active component and biological enzyme, any damage not will cause to skin;Especially It is that a small amount of butter berry extract and aloe extract is added, and is used in compounding with Maca extract, alkyl glycosides, can be with Generate concertedness, thus it is speculated that possible cause is, has moisturizing factor in butter berry extract and aloe extract, and alkyl glycosides can be with The surface tension of skin is reduced, and Maca extract can promote skin to the knot of the absorption of moisturizing factor by adjusting osmotic pressure Fruit.
No. CAS of the butter berry extract is 84695-98-7.
No. CAS of the aloe extract is 85507-69-3.
No. CAS of the citrus berry extract is 94266-47-4.
No. CAS of the bermuda lily flower extract is 84776-67-0.
No. CAS of the rose extract is 90106-38-0.
No. CAS of the purslane extract is 90083-07-1.
No. CAS of the dried tremella extract is 778577-37-0.
No. CAS of the tea extract is 84650-60-2.
No. CAS of the Gotu Kola P.E is 84696-21-9.
No. CAS of the german chamomile flower extract is 84082-60-0.
No. CAS of the rosemary leaf extract is 84604-14-8.
The second aspect of the invention provides the preparation method of the composition of the component containing natural activity described in one kind, step It includes at least, (1) weighs each raw material in composition, spare;(2) first natural activity component, polyhydroxy long-chain alkane are stirred equal It is even;It adds biological enzyme and continues to stir evenly and poured into clean container to obtain the final product, sealed.
In some preferred embodiments, the preparation method of the composition of the component containing natural activity, step is at least Including,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
The third aspect of the invention provides the application of the composition of the component containing natural activity described in one kind, is applied to clear Wash water fruits and vegetables.
In some embodiments, the application of the composition of the heretofore described component containing natural activity, can be used for making Standby fruits and vegetables cleaning agent.
In some embodiments, the fruits and vegetables cleaning agent, by weight, raw material include 20-40 parts and contain natural activity The composition of component, 0.1-0.5 dispersing agent, 0.1-0.5 parts of pH adjusting agents, 5-10 parts of sodium chloride, 0.1-1 parts of light stabilizers, 5- 15 parts of ethyl alcohol, 80-100 parts of deionized waters.
In some preferred embodiments, the fruits and vegetables cleaning agent, by weight, raw material include 30 parts containing natural living The composition of property component, 0.25 dispersing agent, 0.3 part of pH adjusting agent, 8 parts of sodium chloride, 0.5 part of light stabilizer, 10 parts of ethyl alcohol, 90 parts Deionized water.
In some embodiments, the preparation method of the fruits and vegetables cleaning agent does not do particular determination, it is preferred that according to this hair The preparation method of fruits and vegetables cleaning agent described in bright is prepared.
The preparation method of heretofore described fruits and vegetables cleaning agent, includes the following steps:
S1: each raw material prepared in fruits and vegetables cleaning agent is weighed;
S2: composition, the water of sodium chloride, ethyl alcohol, the component containing natural activity are added in blender, are 30- in temperature It is stirred 10-30 minutes at 60 DEG C, speed of agitator is that 200-400r/min obtains mixed solution A;
S3: dispersing agent, pH adjusting agent being added into mixed solution A, stir 5-20 minutes, speed of agitator 100-300r/ Min is warming up to 40-60 DEG C later, then light stabilizer is added in the mixed liquor after stirring, continues to stir 10-30min, stir Revolving speed 300-600r/min is mixed to get fruits and vegetables cleaning agent.
Preferably, the preparation method of the fruits and vegetables cleaning agent, includes the following steps:
S1: each raw material prepared in fruits and vegetables cleaning agent is weighed:
S2: composition, the water of sodium chloride, ethyl alcohol, the component containing natural activity are added in blender, are 40 DEG C in temperature Lower stirring 15 minutes, speed of agitator are that 300r/min obtains mixed solution A;
S3: being added dispersing agent into mixed solution A, pH adjusting agent, stirs 10 minutes, speed of agitator 200r/min, later 50 DEG C are warming up to, then light stabilizer is added in the mixed liquor after stirring, continues to stir 15min, speed of agitator 500r/min, Up to fruits and vegetables cleaning agent.
The present invention is specifically described below by embodiment, following embodiment is only used for the present invention and does further Illustrate, can not be interpreted as the limitation that the present invention protects, professional and technical personnel in the field makes according to the content of foregoing invention Nonessential correction and adjustment, still fall within the range of protection of the invention.
Fruits and vegetables cleaning agent method described in following example 1-16 is as follows:
S1: each raw material prepared in fruits and vegetables cleaning agent is weighed;
S2: 8 parts of sodium chloride, 10 parts of ethyl alcohol, the composition of 30 components containing natural activity, 90 water are added in blender, It is stirred 15 minutes at being 40 DEG C in temperature, speed of agitator is that 300r/min obtains mixed solution A;
S3: 0.25 dispersing agent being added into mixed solution A, and 0.3pH regulator stirs 10 minutes, speed of agitator 200r/ Min is warming up to 50 DEG C later, then 0.5 light stabilizer is added in the mixed liquor after stirring, continues to stir 15min, stirring turns Fast 500r/min is to get fruits and vegetables cleaning agent.
Embodiment 1
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 2
A kind of composition of the component containing natural activity, by weight, raw material include 50 parts of natural activity components, and 0.5 part Polyhydroxy long-chain alkane, 1 part of biological enzyme, 5 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:1:0.1;The polyhydroxy long-chain alkane is undecyl glucoside;The biology Enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.05:0.5;The natural activity component further includes ox The combination of oily berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:1:0.5;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
Embodiment 3
A kind of composition of the component containing natural activity, by weight, raw material include 100 parts of natural activity components, and 5 parts Polyhydroxy long-chain alkane, 5 parts of biological enzyme, 20 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:5:1;The polyhydroxy long-chain alkane is undecyl glucoside;The biological enzyme For the combination of phytase, lipase, zytase, weight ratio 1:0.5:1.5;The natural activity component further includes butter fruit The combination of extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:5: 2;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
Embodiment 4
A kind of composition of the component containing natural activity, by weight, raw material include 60 parts of natural activity components, more than 1 part Hydroxyl long chain alkane, 2 parts of biological enzyme, 10 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2:0.3;The polyhydroxy long-chain alkane is undecyl glucoside;The biology Enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.1:0.8;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 2:1;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
Embodiment 5
A kind of composition of the component containing natural activity, by weight, raw material include 90 parts of natural activity components, more than 4 parts Hydroxyl long chain alkane, 4 parts of biological enzyme, 18 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:3:0.7;The polyhydroxy long-chain alkane is undecyl glucoside;The biology Enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.3:1.2;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 4:1.6;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
Embodiment 6
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component includes plant extracts, and the plant extracts is Folium Artemisiae Argyi extract, lemon extract Combination, weight ratio 1:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The biological enzyme is phytase, rouge The combination of fat enzyme, zytase, weight ratio 1:0.2:1;The natural activity component further includes that butter berry extract, aloe mention Take the combination of object, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 7
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component includes plant extracts, and the plant extracts is Maca extract, lemon extract Combination, weight ratio 5:1;The polyhydroxy long-chain alkane is positive decyl glucoside;The biological enzyme is phytase, fat The combination of enzyme, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter berry extract, aloe extraction The combination of object, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 8
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:0.5:1;The polyhydroxy long-chain alkane is positive decyl glucoside;The biology Enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter fruit The combination of extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3: 1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 9
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:10:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The biology Enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter fruit The combination of extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3: 1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 10
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 11
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 1 part of water soluble chitosan;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 12
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, weight ratio 1:0.2;The natural activity component further includes butter berry extract, reed The combination of luxuriant growth extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 13
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of protease, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1: 3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 14
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 0.5:3:1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 15
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is positive decyl glucoside;The life Object enzyme is the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes butter The combination of berry extract, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 0.5:3:0.1;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Embodiment 16
A kind of composition of the component containing natural activity, by weight, raw material include 80 parts of natural activity components, and 2.5 parts Polyhydroxy long-chain alkane, 3 parts of biological enzyme, 16 parts of water soluble chitosans;
The natural activity component include plant extracts, the plant extracts be Folium Artemisiae Argyi extract, Maca extract, The combination of lemon extract, weight ratio 1:2.5:0.5;The polyhydroxy long-chain alkane is butyl glucoside;The biological enzyme For the combination of phytase, lipase, zytase, weight ratio 1:0.2:1;The natural activity component further includes that butter fruit mentions Take the combination of object, aloe extract, the butter berry extract, Maca extract, aloe extract weight ratio be 1:3: 1.4;
The preparation method of the composition of the component containing natural activity, step include,
(1) each raw material in composition is weighed, it is spare;
(2) it is first stirred evenly in natural activity component, polyhydroxy long-chain alkane investment blender;Add biological enzyme Continue to stir evenly, is eventually adding surplus stock and continues to stir evenly;
(3) it pours into clean container, seals.
A kind of fruits and vegetables cleaning agent of the composition preparation of the component containing natural activity as described in the present embodiment.
Performance test
1. in the present invention embodiment 1-13 prepare fruits and vegetables cleaning agent performance test it is as follows, select two kinds of different brands A, B commercially available fruits and vegetables cleaning agent is control group;Fruits and vegetables cleaning agent removes effect to remains of pesticide and adopts national standard GB/T-24691 fruit-vegetable clear Remains of pesticide in lotion in appendix A removes Efficacy Method and is measured;It is divided into three groups to be cleaned, three groups of scavenging period point The residual rate (%) of cypermethrin, arprocarb after Wei not only washed once for 30 seconds, 1 minute, 3 minutes.
The test result of 1 fruits and vegetables cleaning agent pesticides removal of table
2. greater skin conditioning efficacy is tested:
300 people of random selection number, is randomly divided into 10 groups, and every group of 30 people do not use any hand care during test Product, daily using fruits and vegetables cleaning agent prepared by embodiment 1-6, embodiment 14-16 in the present invention to the vegetable and fruit of household It is hand-washed, selecting commercially available A brand fruits and vegetables cleaning agent is control group.Continuous use 2 months calculates hand dorsal area and is used in conjunction 1 It with the difference of initial basis value is that keratoderma moisture content is rised in value after a month and after being used in conjunction 2 months, wherein keratoderma Moisture content increment is bigger, and the effect for indicating that hand is improved is better.Keratoderma water content is by skin moisture tester Corneometer CM825 is measured, and the test environment of this test is 20.0 DEG C~21.5 DEG C of temperature, and relative humidity 48.0%~ 56.0%, meet the requirement of conceptual design.
2 greater skin conditioning efficacy test result of table
Example above-mentioned is merely illustrative, some features of the feature for explaining the disclosure.The attached claims It is intended to the range as wide as possible for requiring to be contemplated that, and embodiments as presented herein is only according to all possible embodiment Combined selection embodiment explanation.Therefore, the purpose of applicant is that the attached claims are not illustrated the present invention Feature exemplary selectional restriction.And the progress in science and technology will be formed language express it is inaccurate due to and not The possible equivalent being presently considered or son replacement, and these variations should also be interpreted in the conceived case by appended Claim covering.

Claims (10)

1. a kind of composition of component containing natural activity, which is characterized in that by weight, raw material includes at least, and 50-100 parts Natural activity component, 0.5-5 parts of polyhydroxy long-chain alkane, 1-5 parts of biological enzyme.
2. composition as described in claim 1, which is characterized in that the natural activity component includes plant extracts;It is described Plant extracts is in Flos Lonicerae extractive solution, Cassia Nomame P.E, Folium Artemisiae Argyi extract, Maca extract, lemon extract One or more combinations.
3. composition as described in claim 1, which is characterized in that have 2-6 hydroxyl in the polyhydroxy long-chain alkane;It is described There is 5-12 methylene in polyhydroxy long-chain alkane.
4. composition as described in claim 1, which is characterized in that the biological enzyme is selected from zytase, lipase, phytic acid Enzyme, amylase, protease, cutinase, cellulase, pectase, mannonase arabinase, Galactanase, oxidation One of object enzyme or a variety of combinations.
5. composition as described in claim 1, which is characterized in that the raw material further includes 5-20 parts of water soluble chitosans.
6. composition as claimed in claim 2, which is characterized in that the plant extracts is Folium Artemisiae Argyi extract, Maca extraction The combination of object, lemon extract;The Folium Artemisiae Argyi extract, Maca extract, lemon extract weight ratio be 1:(1-5): (0.1-1)。
7. composition as claimed in claim 4, which is characterized in that the biological enzyme is lipase, phytase, zytase Combination;The phytase, lipase, zytase weight ratio be 1:(0.05-0.5): (0.5-1.5).
8. such as the described in any item compositions of claim 1-7, which is characterized in that the natural activity component further includes butter fruit Extract, aloe extract, citrus berry extract, bermuda lily flower extract, rose extract, purslane extract, tremella One of extract, tea extract, Gotu Kola P.E, german chamomile flower extract, rosemary leaf extract or a variety of groups It closes.
9. a kind of preparation method of the composition of the component containing natural activity as described in claim any one of 1-8, which is characterized in that Step includes at least, and (1) weighs each raw material in composition, spare;(2) first natural activity component, polyhydroxy long-chain alkane are stirred It mixes uniformly;It adds biological enzyme and continues to stir evenly and poured into clean container to obtain the final product, sealed.
10. a kind of application of the composition of the component containing natural activity as described in claim any one of 1-8, which is characterized in that answer For ejected wash water fruits and vegetables.
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