CN109730956A - Ginger shampoo and preparation method thereof - Google Patents
Ginger shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN109730956A CN109730956A CN201910189705.5A CN201910189705A CN109730956A CN 109730956 A CN109730956 A CN 109730956A CN 201910189705 A CN201910189705 A CN 201910189705A CN 109730956 A CN109730956 A CN 109730956A
- Authority
- CN
- China
- Prior art keywords
- ginger
- shampoo
- polyquaternium
- laureth
- mesh
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention belongs to daily chemical products technical fields, it is related to a kind of ginger shampoo, it is prepared from the following raw materials by weight percentage: ginger 20%-50%, laureth sodium sulfovinate 10%-15%, Polyquaternium-10 0.2%-0.5%, acrylic acid esters co-polymer 2%-6%, Merquat 280 1%-4%, -47 1%-4% of polyquaternium, coconut oleoyl amine DEA 1%-3%, Cocoamidopropyl betaine 6%-10%, -23 1%-2% of laureth, the dry tree benevolence oil 2%-3% of Ci A, DMDM hydantoin 0.3%-1%, flavouring agent 0.2%-1%, pure water surplus；The ginger is fresh ginger particle, and mesh number is 40~60 mesh.The present invention also provides the preparation methods of above-mentioned ginger shampoo.Ginger shampoo of the present invention can produce scalp fever sense by improving content of the fresh ginger in integral formula, ginger shampoo in use；By reasonably controlling ginger size, well ensures fresh ginger and be distributed evenly in shampoo.Rationally, compatibility is good between component, and overall stability is high for component formula collocation disclosed in this invention.
Description
Technical field
The invention belongs to daily chemical products technical field, it is related to a kind of ginger shampoo and preparation method thereof.
Background technique
Ginger (Zingiber officinale Roscoe) also known as ginger belong to Zingiber (Zingiberaceae) perennial grass
This perennial plant, rhizome are plump, have fragrance and acid, complex chemical composition, it has been found that have more than 100 kinds, can return
Are as follows: 3 major class of volatile oil, gingerol (Gingerol) and hexichol ring group heptane.Wherein, volatile oil is a kind of transparent, pale yellow to withered
Yellow flowable liquid, main chemical compositions are terpene substances, have strong aromatic odor；Gingerol is in yellow oily, is
The mixture of many kinds of substance composition, gingerol is main active in gingerol；Hexichol ring group heptane is a kind of with 1,7- bis-
Substituted-phenyl and using heptane skeleton as the general designation of the compound of precursor structure.
Studies have shown that ginger not only has anti-inflammatory, antifungic action, it may also be used for treatment trichophyton, pityrosporum furfur etc.
Caused infection, it can also be used to which seborrhagia disease and dandruff effectively prevent alopecia, inhibit scalp pruritus.In order to allow consumer to make
With obtaining most intuitive experience and impression in the process, when use, is felt with the presence of ginger true, there is hair washing in the prior art
Water directlys adopt ginger as raw material, and but there are the following problems:
(1) gingerol and other effective substances in ginger can not be made to dissolve out to greatest extent, cannot be uniform and stable deposit
It is in system；
(2) ginger is easy sedimentation, and effect cannot be fully utilized, and Anti-hair loss effect is unobvious and cleans antibacterial effect
Fruit is undesirable；
(3) in order to generate fever sense in use, heat sensitizer is added in shampoo, thus skin tape is hurt
Evil.
Patent CN105687048A discloses a kind of shampoo containing fresh ginger particle, includes following weight percent
Each raw material component: fresh ginger particle 0.1%-60%, surfactant 8-55%, fresh ginger juice 0.1-60%, thickener 0.01-
7%, conditioner 0.01-10%, nutritional agents 0.01-10%, preservative 0.01-2%, pH adjusting agent 0.01-2%, chelating agent
0.01-2%, aromatic 0.01-2%, colorant 0.01-2%, surplus are water；Wherein the diameter of fresh ginger particle is less than 3mm.
But in the actual production process, the size of fresh ginger particle will affect the stability of whole system, only be ground into fresh ginger
Fresh ginger particle of the diameter less than 3mm is put into system, which does not illustrate how subsequent process is prepared yet,
The shampoo being so prepared is easy to appear layering, unstable disadvantage.
Summary of the invention
The purpose of the present invention is to provide a kind of ginger shampoo and preparation method thereof, with one in solving the above problems
Or it is several.
According to an aspect of the invention, there is provided a kind of ginger shampoo, by weight percentage by the following raw material system
It is standby to form: ginger 20%-50%, laureth sodium sulfovinate 10%-15%, Polyquaternium-10 0.2%-0.5%, propylene
Acid esters analog copolymer 2%-6%, Merquat 280 1%-4%, polyquaternium -47 1%-4%, coconut oleoyl amine DEA 1%-
3%, Cocoamidopropyl betaine 6%-10%, -23 1%-2% of laureth pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 2%-3%, DMDM hydantoin 0.3%-1%, flavouring agent 0.2%-1%, pure water surplus.
Wherein, ginger is fresh ginger particle, and mesh number is 40~60 mesh.Due to reasonable formula of taking of the invention, especially
It is thickener and suspending agent cooperation, it is thus possible to so that the particle of ginger is in reasonable particle size, both be unlikely to meticulous and nothing
Granular sensation, and it was unlikely to the disadvantages of being slightly easily delaminated.If grain diameter is too big, it is easy sedimentation and showing for interface debonding occurs
As leading to the reduction of ginger utilization rate；If partial size is too small, without granular sensation in shampoo, consumption experience can then decline.
In some embodiments, fresh ginger preparation method of granules are as follows: first cleaned up with tap water, then cleaned with pure water
Once, it is then cut into the little particle that fritter is ground into 40-60 mesh with pulverizer.
In some embodiments, flavouring agent is edible essence.
Wherein ginger, Polyquaternium-10, Merquat 280, polyquaternium -47 are conditioner；Laureth sulfuric ester
Sodium is foaming agent；Acrylic acid esters co-polymer is suspending agent；Coconut oleoyl amine DEA, Cocoamidopropyl betaine are thickener；Month
Laureth -23, thorn A Ganshu (ARGANIA SPINOSA) benevolence oil are softener；DMDM hydantoin is preservative.
The entire formula system of the present invention increases viscosity and the consistency of formula by the allotment of thickener to improve whole body
It is internal suspending power, while increases the viscosity and density of water liquid of having one's hair wash with suspending agent auxiliary, ensures that ginger particle exists
Suspension stable for a long time in formula system.Wherein, ginger is fresh ginger particle, and mesh number is 40~60 mesh.It is wanted before regrinding ginger
First ginger is cut into along the lines of shredded ginger the segment of 2-4 centimeter length, the purpose for first cutting segment is that ginger there are many shredded gingers, purely
It is mostly and long that there are shredded gingers if grinding ginger with machine, to influence the uniformity of particle, and be first cut into segment regrind ginger can be effective
Solve the problems, such as shredded ginger mostly with it is long, segment is cut in the uniformity of ginger grain to improve 20-30% than the uniformity do not cut；In addition,
If fresh ginger grain diameter is too big, it is easy sedimentation and the phenomenon that interface debonding occurs, leads to the reduction of ginger utilization rate；If partial size is too
Small, then without granular sensation in shampoo, consumption experience can then decline；If shredded ginger is too much and length be easy to cause knotting and discharge port stifled
Plug.
Wherein, suspending agent is the lightly crosslinked acrylic acid esters co-polymer of anion, it is a kind of outstanding rheology improvement
Agent has superior suspending stabilized ability, can thicken and change product rheology.Thickener cost performance is high, easy to use, can be with
Conditioner is used in compounding well.
According to another aspect of the present invention, the preparation method of above-mentioned ginger shampoo is provided, the specific steps are as follows:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
The fresh ginger particle crushed in advance is added, when being heated with stirring to 60 DEG C -65 DEG C, acrylic acid esters co-polymer is added, continues
It is heated with stirring to 95-105 DEG C, and keeps the temperature and boils 40~50min, 15~20rpm of mixing speed between 95-105 DEG C；
(3) 60 DEG C -65 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, 45 DEG C -50 DEG C is cooled to and successively adds
Enter Merquat 280, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIA SPINOSA) benevolence oil, cocounut oil acyl
Amine propyl betaine, DMDM hydantoin, flavouring agent stir 20~30min, 15~20rpm of mixing speed, until being cooled to often
Temperature is to get ginger shampoo.
The application method of ginger shampoo disclosed in this invention are as follows: after wet process, contain fresh ginger with the appropriate present invention
Grain shampoo is rubbed to spume and covers hair, and 3~5min of scalp is gently rubbed, with warm water cleaning, 3~4 times weekly.
Ginger shampoo of the present invention is by improving content and reasonable compatibility of the fresh ginger in integral formula, ginger
Shampoo is not necessarily to add other additives such as heat sensitizer and can generate scalp and generate heat to feel in use, while using fresh ginger
Replace ginger extract, ginger juice as hair washing water constituent, can utmostly retain effective active composition in ginger, play ginger
Optimal effect；The present invention reasonably controls in conjunction with to ginger size particularly by reasonable formula, ginger is avoided to wash
It is settled in shampoo, fresh ginger can be well ensured and be distributed evenly in shampoo, when ensuring that shampoo uses
Grain sense, consumption experience are good.Rationally, compatibility is good between component, overall stability for component formula collocation disclosed in this invention
It is high.
Detailed description of the invention
Fig. 1 is the ginger shampoo outside drawing of the embodiment of the present invention 1；
Fig. 2 is ginger shampoo coating condition shown in Fig. 1；
Fig. 3 is ginger shampoo unstable stratification phenomenon in comparative example 2.
Specific embodiment
The invention will now be described in further detail with reference to the accompanying drawings；Pulverizer therein is full of machine purchased from Guangzhou nine
Tool equipment Co., Ltd's large size ginger mud machine (model TJ-307A) guarantees well-balanced degree and the mesh number accuracy of fresh ginger particle.
Embodiment 1
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 50%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.2%, acrylic acid esters co-polymer 3%, Merquat 280 1%, polyquaternium -47
2%, coconut oleoyl amine DEA 1%, Cocoamidopropyl betaine 8%, laureth -23 1% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 2%, DMDM hydantoin 0.3%, flavouring agent 0.2%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 100-200 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
It adds the fresh ginger particle crushed in advance, at 60 DEG C of agitating and heating, acrylic acid esters co-polymer is added, continues agitating and heating
To 100 DEG C, and keeps the temperature and boil 45min, mixing speed 20rpm between 95 DEG C -105 DEG C；
(3) 55 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 45 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIASPINOSA) benevolence oil, Cocoamidopropyl betaine,
DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until being cooled to room temperature to get ginger shampoo.
Ginger shampoo outside drawing prepared by embodiment 1 is as shown in Figure 1, it can be seen from the figure that shampoo is at golden yellow
It is translucent, it can be seen that fresh ginger little particle.
Embodiment 2
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 30%, laureth sulphur
Acid esters sodium 12%, Polyquaternium-10 0.2%, acrylic acid esters co-polymer 4%, Merquat 280 1%, polyquaternium -47
3%, coconut oleoyl amine DEA 1%, Cocoamidopropyl betaine 6%, laureth -23 1% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 3%, DMDM hydantoin 0.5%, flavouring agent 0.2%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 20-40 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
The fresh ginger particle crushed in advance is added, when being heated with stirring to 65 DEG C, acrylic acid esters co-polymer is added, continues stirring and adds
Heat keeps the temperature to 95 DEG C and boils 50min, mixing speed 15rpm between 95-105 DEG C；
(3) 60 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 50 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIA SPINOSA) benevolence oil, cocamidopropyl propyl amide beet
Alkali, DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until being cooled to room temperature to get ginger shampoo.
The appearance of ginger shampoo prepared by embodiment 2 is similar to Example 1, and details are not described herein again.
Embodiment 3
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 35%, laureth sulphur
Acid esters sodium 15%, Polyquaternium-10 0.3%, acrylic acid esters co-polymer 3%, Merquat 280 2%, polyquaternium -47
1%, coconut oleoyl amine DEA 1%, Cocoamidopropyl betaine 10%, laureth -23 2% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 3%, DMDM hydantoin 0.5%, flavouring agent 0.3%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
The fresh ginger particle crushed in advance is added, when being heated with stirring to 65 DEG C, acrylic acid esters co-polymer is added, continues stirring and adds
Heat keeps the temperature to 105 DEG C and boils 45min, mixing speed 20rpm between 95-105 DEG C；
(3) 60 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 50 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIASPINOSA) benevolence oil, Cocoamidopropyl betaine,
DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until being cooled to room temperature to get ginger shampoo.
The appearance of ginger shampoo prepared by embodiment 3 is similar to Example 1, and details are not described herein again.
Embodiment 4
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 40%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.5%, acrylic acid esters co-polymer 3%, Merquat 280 3%, polyquaternium -47
4%, coconut oleoyl amine DEA2%, Cocoamidopropyl betaine 6%, laureth -23 2% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 3%, DMDM hydantoin 1%, flavouring agent 0.5%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
The fresh ginger particle crushed in advance is added, when being heated with stirring to 60 DEG C, acrylic acid esters co-polymer is added, continues stirring and adds
Heat keeps the temperature to 100 DEG C and boils 40min, mixing speed 15rpm between 95-105 DEG C；
(3) 55 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 50 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIASPINOSA) benevolence oil, Cocoamidopropyl betaine,
DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until being cooled to room temperature to get ginger shampoo.
The appearance of ginger shampoo prepared by embodiment 4 is similar to Example 1, and details are not described herein again.
Embodiment 5
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 20%, laureth sulphur
Acid esters sodium 15%, Polyquaternium-10 0.3%, acrylic acid esters co-polymer 6%, Merquat 280 4%, polyquaternium -47
2%, coconut oleoyl amine DEA 3%, Cocoamidopropyl betaine 6%, laureth -23 2% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 2%, DMDM hydantoin 1%, flavouring agent 1%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
The fresh ginger particle crushed in advance is added, when being heated with stirring to 65 DEG C, acrylic acid esters co-polymer is added, continues stirring and adds
Heat is kept the temperature to 95 DEG C in 95-105 DEG C of tanning 45min, mixing speed 20rpm；
(3) 60 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 50 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIA SPINOSA) benevolence oil, cocamidopropyl propyl amide beet
Alkali, DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until being cooled to room temperature to get ginger shampoo.
The appearance of ginger shampoo prepared by embodiment 5 is similar to Example 1, and details are not described herein again.
The physicochemical property of ginger shampoo prepared by 1~embodiment of embodiment 5 is tested, examination criteria reference
GB/T29679-2013 " shampoo, hair cream ", specifically:
1, pH: according to GB/T13531.1-2008 " measurement of cosmetics generic inspection method pH value ".
2, low temperature resistant test method
Instrument: refrigerator (temperature accuracy ± 2 DEG C), test tube
Method: sample is poured into 2 respectivelyTest tube in, making liquid level is about 80mm, plug
Upper clean plug.One test tube to be tested is placed in and is pre-adjusted to -8 DEG C of refrigerator, is taken out after for 24 hours, is restored to room
The style of another test tube of Wen Houyu carries out range estimation comparison.
3, heat-resistant experiment method:
Instrument: constant incubator: accuracy of temperature control ± 1 DEG C, test tube
Method: style is poured into 2 respectivelyTest tube in, making liquid level is about 80mm, plug
Upper clean plug.One test tube to be tested is placed in and is pre-adjusted to 40 DEG C of constant incubator, is taken out after for 24 hours, it is extensive
After answering to room temperature compared with the style of another test tube carries out range estimation.4, microorganism detection
It provides to detect by " cosmetics health specification " (version in 2015), the specific method is as follows:
It measures 10mL sample to be added in 90mL sterile saline, after mixing, 1:10 inspection liquid is made.
The diluted inspection liquid 2mL of 1:10 is drawn with sterilized straw, is injected separately into two sterilizing plates, every ware 1mL.Separately take
1mL is injected into 9mL sterile saline test tube, replaces a branched pipette, and mix well, and 1:100 inspection liquid is made.2mL is drawn,
It is injected separately into two sterilizing plates, every ware 1mL.It will melt and be cooled to 45 DEG C~50 DEG C of lecithin Tween-80 nutrition fine jade
Rouge culture medium is poured into plate, and every ware about 15mL rotates plate immediately, is sufficiently mixed sample and culture medium uniformly, to fine jade
After rouge solidification, plate is overturn, sets and cultivates 48h ± 2h in 36 DEG C of ± 1 DEG C of incubators.Separately take the sterilizing sky that sample is not added flat
About 15mL lecithin Tween-80 nutrient agar is added in ware, after agar solidification, overturns plate, sets 36 DEG C of ± 1 DEG C of trainings
It supports and cultivates 48h ± 2h in case, be blank control.
5, testing result
Testing result is as shown in Table 1 and Table 2.
1 Examples 1 to 5 ginger shampoo physicochemical property list of table
2 ginger shampoo microorganism detection result of table
| Try example | Bacterium | Mould |
| Embodiment 1 | It is qualified | It is qualified |
| Embodiment 2 | It is qualified | It is qualified |
| Embodiment 3 | It is qualified | It is qualified |
| Embodiment 4 | It is qualified | It is qualified |
| Embodiment 5 | It is qualified | It is qualified |
Comparative example 1Ginger grain mesh number is 100~200 mesh
The formula composition and preparation method of 1 ginger shampoo of comparative example are same as Example 1, the difference is that, it is right
Fresh ginger mesh number is 100~200 mesh in ratio 1.
Ginger shampoo prepared by comparative example 1 has light Jiang Xiang in golden yellow translucent, but without ginger grain in shampoo
There are senses.
Comparative example 2Ginger grain mesh number is 20~40 mesh
The formula composition and preparation method of 1 ginger shampoo of comparative example are same as Example 1, the difference is that, it is right
Fresh ginger mesh number is 20-40 mesh in ratio 1.
Ginger shampoo prepared by comparative example 2 has light Jiang Xiang in golden yellow translucent, and ginger particle is larger, and 25
There is lamination in it or so, as shown in Figure 3.
Comparative example 3Ginger grain mesh number be40-60 mesh, arrange in pairs or groups different suspending agent and/or thickener
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 50%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.2%, acrylic acid (esters)/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.3%,
Merquat 280 1%, polyquaternium -47 2%, coconut oleoyl amine MEA 2%, Cocoamidopropyl betaine 5%, laruyl alcohol
Polyethers -23 1%, thorn A Ganshu (ARGANIA SPINOSA) benevolence oil 2%, DMDM hydantoin 0.3%, flavouring agent 0.2% are pure
Water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) sequentially added in surplus pure water laureth sodium sulfovinate, Polyquaternium-10, acrylic acid (ester) class/
Simultaneously homogenous disperse is uniform for C10-30 alkylol acrylamide acid esters cross-linked polymer, adds the fresh ginger particle crushed in advance, stirs
When heating 60 DEG C, coconut oleoyl amine MEA is added, continues to be heated with stirring to 100 DEG C, and keep the temperature and boil between 95 DEG C -105 DEG C
45min, mixing speed 20rpm；
(3) 45 DEG C are cooled to and sequentially adds Merquat 280, polyquaternium -47, laureth -23, thorn A Ganshu
(ARGANIA SPINOSA) benevolence oil, Cocoamidopropyl betaine, DMDM hydantoin, flavouring agent stir 30min, stirring speed
Spend 20rpm, until be cooled to room temperature to get.
Comparative example 4Ginger grain mesh number be40-60 mesh, arrange in pairs or groups different suspending agent and/or thickener
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 50%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.2%, acrylic acid esters co-polymer 3%, Merquat 280 1%, polyquaternium -47
2%, coconut oleoyl amine MEA 2%, Cocoamidopropyl betaine 5%, laureth -23 1% pierce A Ganshu (ARGANIA
SPINOSA) benevolence oil 2%, DMDM hydantoin 0.3%, flavouring agent 0.2%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) laureth sodium sulfovinate, Polyquaternium-10 are sequentially added in surplus pure water and homogenous disperse is uniform,
It adds the fresh ginger particle crushed in advance, at 60 DEG C of agitating and heating, acrylic acid esters co-polymer, coconut oleoyl amine MEA is added,
Continue to be heated with stirring to 100 DEG C, and keeps the temperature and boil 45min, mixing speed 20rpm between 95 DEG C -105 DEG C；
(3), 45 DEG C are cooled to and sequentially adds Merquat 280, polyquaternium -47, laureth -23, thorn A Ganshu
(ARGANIA SPINOSA) benevolence oil, Cocoamidopropyl betaine, DMDM hydantoin, flavouring agent stir 30min, stirring speed
Spend 20rpm, until be cooled to room temperature to get.
Comparative example 5Ginger grain mesh number be40-60 mesh, arrange in pairs or groups different suspending agent and/or thickener
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 50%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.2%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.5%,
Merquat 280 1%, the 2% coconut oleoyl amine DEA 3% of polyquaternium -47, Cocoamidopropyl betaine 4%, laruyl alcohol are poly-
Ether -23 1% pierces A Ganshu (ARGANIA SPINOSA) benevolence oil 2%, DMDM hydantoin 0.3%, flavouring agent 0.2%, pure water
Surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) sequentially added in surplus pure water laureth sodium sulfovinate, Polyquaternium-10, acrylic acid (ester) class/
Simultaneously homogenous disperse is uniform for C10-30 alkylol acrylamide acid esters cross-linked polymer, adds the fresh ginger particle crushed in advance, continues
100 DEG C are heated with stirring to, and keeps the temperature and boils 45min, mixing speed 20rpm between 95 DEG C -105 DEG C；
(3) 55 DEG C are cooled to, coconut oleoyl amine DEA is added and is dispersed with stirring uniformly, is cooled to 45 DEG C and sequentially adds polyquaternium-
22, polyquaternium -47, laureth -23, thorn A Ganshu (ARGANIASPINOSA) benevolence oil, Cocoamidopropyl betaine,
DMDM hydantoin, flavouring agent stir 30min, mixing speed 20rpm, until be cooled to room temperature to get.
Comparative example 6Ginger grain mesh number be40-60 mesh, arrange in pairs or groups different suspending agent and/or thickener
A kind of ginger shampoo, is prepared from the following raw materials by weight percentage: ginger 50%, laureth sulphur
Acid esters sodium 10%, Polyquaternium-10 0.2%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.5%,
Merquat 280 1%, polyquaternium -47 2%, PEG-150 distearate 2%, Cocoamidopropyl betaine 4%, the moon
Laureth -23 1% pierces A Ganshu (ARGANIA SPINOSA) benevolence oil 2%, DMDM hydantoin 0.3%, flavouring agent
0.2%, pure water surplus.
Wherein, ginger is the fresh ginger particle of 40-60 mesh.
Above-mentioned ginger shampoo is prepared via a method which:
(1) various raw materials are got ready according to the ratio, fresh ginger is first cleaned up with tap water and is cleaned once, so with pure water again
It is cut into small pieces afterwards and is ground into the little particle of 40-60 mesh with pulverizer；
(2) sequentially added in surplus pure water laureth sodium sulfovinate, Polyquaternium-10, acrylic acid (ester) class/
Simultaneously homogenous disperse is uniform for C10-30 alkylol acrylamide acid esters cross-linked polymer, adds the fresh ginger particle crushed in advance, stirs
When heating 60 DEG C, PEG-150 distearate is added, continues to be heated with stirring to 100 DEG C, and keep the temperature and endure between 95 DEG C -105 DEG C
45min processed, mixing speed 20rpm；
(3) 45 DEG C are cooled to and sequentially adds Merquat 280, polyquaternium -47, laureth -23, thorn A Ganshu
(ARGANIA SPINOSA) benevolence oil, Cocoamidopropyl betaine, DMDM hydantoin, flavouring agent stir 30min, stirring speed
Spend 20rpm, until be cooled to room temperature to get.
By Examples 1 to 5 and the comparison of comparative example 3~6 it is found that thickener used by comparative example 3~6 and suspending agent make
For system that really cannot be stable in system, illustrate acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer and
Other material combinations are poor, do not form mutual supplement with each other's advantages with coconut oleoyl amine DEA, Cocoamidopropyl betaine thickener,
Being influenced instead by it over time can reduction viscosity slowly；And the suspending agent acrylate in Examples 1 to 5
It is even more to form excellent take that analog copolymer, which has excellent compatibility and thickener coconut oleoyl amine DEA, Cocoamidopropyl betaine,
Match, it is ensured that formulation consistencies and suspending power realize the stabilization of system.
The stability of ginger shampoo prepared by 1~embodiment of embodiment 5,1~comparative example of comparative example 6 is carried out pair
Than the results are shown in Table 3:
3 ginger shampoo stability list of table
| Test example | After standing 1 day | After standing 7 days | After standing 14 days | After standing 30 days |
| Embodiment 1 | Stablize | Stablize | Stablize | Stablize |
| Embodiment 2 | Stablize | Stablize | Stablize | Stablize |
| Embodiment 3 | Stablize | Stablize | Stablize | Stablize |
| Embodiment 4 | Stablize | Stablize | Stablize | Stablize |
| Embodiment 5 | Stablize | Stablize | Stablize | Stablize |
| Comparative example 1 | Stablize | Stablize | Stablize | Stablize |
| Comparative example 2 | Stablize | Stablize | It is layered | It is layered, there is obvious interface |
| Comparative example 3 | Stablize | Stablize | It is layered | It is layered, there is obvious interface |
| Comparative example 4 | Stablize | Stablize | It is layered | It is layered, there is obvious interface |
| Comparative example 5 | Stablize | Stablize | It is layered | It is layered, there is obvious interface |
| Comparative example 6 | Stablize | Stablize | Stablize | It is layered, there is obvious interface |
Every part of Examples 1 to 5, comparative example 1~6 example prepare 10 parts of samples respectively, choose 25 years old~55 years old volunteer 110
Name, is randomly divided into experimental group (50 people) and contrast groups (60 people), everyone correspondingly gets one bottle of sample, hair washing one in every two days
It is secondary, it is used continuously one month, and fill in using table and evaluate the synthesis of ginger shampoo prepared by embodiment and comparative example and make
With effect, comparing result is as shown in table 4:
4 shampoo of table uses resultant effect rating sheet
For shampoo is using feeling, to experimental group, 50 volunteers carry out random access, indicate ginger of the present invention
When in use, scalp has obvious fever sense to shampoo, and has no that ginger grain remains on hair after having one's hair wash, wherein enumerating five
The name specifically used effect of volunteer:
Mr. Yang, 41 years old, alopecia was serious, and the greasy humidity of scalp is swollen, and does not wash hair within two days and occurs as soon as greasy heavy feeling.It uses
Behind of the invention ginger shampoo one month, alopecia, hair oil situation are obviously improved.
Ms Zhang, 52 years old, frequent itching of the scalp, dandruff were more, and scalp is dry, used of the invention ginger shampoo one month
Afterwards, itching of the scalp, dandruff situation are obviously improved.
Mrs Li, 28 years old, itching of the scalp, hair were easily broken, and alopecia amount is larger, and hair washing, comb hair have many hairs de- every time
It falls, after of the invention ginger shampoo one month, alopecia amount is significantly reduced, the enhancing of hair toughness, and itching of the scalp situation is bright
It is aobvious to improve.
Mrs Guo, 31 years old, itching of the scalp, dandruff was serious, and alopecia amount is larger, used of the invention ginger shampoo one month
Afterwards, situation is clearly better.
Mr. Wang, 45 years old, hair was greasy, and scalp uses of the invention ginger shampoo one month with red and swollen, itch
Afterwards, situation is obviously improved.
Above-described is only some embodiments of the present invention.For those of ordinary skill in the art, not
Under the premise of being detached from the invention design, various modifications and improvements can be made, these belong to protection model of the invention
It encloses.
Claims (6)
1. ginger shampoo, which is characterized in that be prepared from the following raw materials by weight percentage: ginger 20%-50%, the moon
Laureth sodium sulfovinate 10%-15%, Polyquaternium-10 0.2%-0.5%, acrylic acid esters co-polymer 2%-6% gather
- 22 1%-4% of quaternary ammonium salt, -47 1%-4% of polyquaternium, coconut oleoyl amine DEA 1%-3%, Cocoamidopropyl betaine
6%-10%, -23 1%-2% of laureth pierce A Ganshu benevolence oil 2%-3%, DMDM hydantoin 0.3%-1%, fragrance
Agent 0.2%-1%, pure water surplus；
The ginger is fresh ginger particle, and mesh number is 40~60 mesh.
2. ginger shampoo according to claim 1, which is characterized in that the fresh ginger particle obtains by the following method
It takes: fresh ginger being cleaned up with tap water, then is cleaned with pure water, is then ground into the little particle of 40-60 mesh i.e. with pulverizer
It can.
3. ginger shampoo according to claim 2, which is characterized in that the flavouring agent is essence.
4. the preparation method of the described in any item ginger shampoos of claims 1 to 3, which is characterized in that specific step is as follows:
(1) various raw materials are got ready according to the ratio, the particle of 40-60 mesh is ground into after fresh ginger is cleaned；
(2) laureth sodium sulfovinate, Polyquaternium-10 and homogenous disperse are sequentially added in surplus pure water, add step
Suddenly the fresh ginger particle in (1) when being heated to 60 DEG C -65 DEG C, is added acrylic acid esters co-polymer, is then heated to 95-105
DEG C, and keep the temperature and boiled between 95-105 DEG C；
(3) material of step (2) is cooled to 60 DEG C -65 DEG C, coconut oleoyl amine DEA dispersion is added, is cooled to 45 DEG C -50 DEG C successively
Be added Merquat 280, polyquaternium -47, laureth -23, thorn A Ganshu benevolence oil, Cocoamidopropyl betaine,
DMDM hydantoin, flavouring agent to get.
5. the preparation method according to claim 4, which is characterized in that 40~50min of duration is boiled in step (2), while enduring
Side stirring processed, 15~20rpm of mixing speed.
6. preparation method according to claim 5, which is characterized in that Merquat 280, polyquaternary amine are added in step (3)
It is stirred after salt -47, laureth -23, thorn A Ganshu benevolence oil, Cocoamidopropyl betaine, DMDM hydantoin, flavouring agent
20~30min, 15~20rpm of mixing speed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910189705.5A CN109730956B (en) | 2019-03-13 | 2019-03-13 | Ginger shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910189705.5A CN109730956B (en) | 2019-03-13 | 2019-03-13 | Ginger shampoo and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109730956A true CN109730956A (en) | 2019-05-10 |
| CN109730956B CN109730956B (en) | 2021-12-07 |
Family
ID=66370406
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910189705.5A Active CN109730956B (en) | 2019-03-13 | 2019-03-13 | Ginger shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109730956B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111329825A (en) * | 2020-04-15 | 2020-06-26 | 广州聚泽生物科技有限公司 | Ginger mild anti-dandruff shampoo and preparation method thereof |
| CN112675111A (en) * | 2021-01-28 | 2021-04-20 | 广州碧思特生物科技有限公司 | Ginger shampoo formula and preparation process thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140242020A1 (en) * | 2013-02-27 | 2014-08-28 | Symrise Ag | Ginger Extract for the Protection of Stem Cells |
| JP2016056175A (en) * | 2014-09-10 | 2016-04-21 | 株式会社東洋新薬 | KAEMPFERIA PARVIFLORA-CONTAINING PPARγ EXPRESSION PROMOTING COMPOSITIONS |
| CN105687048A (en) * | 2016-03-16 | 2016-06-22 | 新疆中草堂医药科技有限公司 | Liquid shampoo with fresh ginger granules |
| CN106333911A (en) * | 2016-10-17 | 2017-01-18 | 广州亿达化妆品有限公司 | Plant ginger (fresh ginger paste) hair loss-preventing hair-generating shampoo |
| CN107737068A (en) * | 2017-11-08 | 2018-02-27 | 熊雄 | Ginger shampoo and preparation method thereof |
| CN108524393A (en) * | 2018-06-11 | 2018-09-14 | 广西科技大学 | A kind of ginger shampoo and preparation method thereof |
| CN109652233A (en) * | 2019-01-25 | 2019-04-19 | 广州二广生物科技有限公司 | Cosmetic applicators detergent and preparation method thereof |
-
2019
- 2019-03-13 CN CN201910189705.5A patent/CN109730956B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140242020A1 (en) * | 2013-02-27 | 2014-08-28 | Symrise Ag | Ginger Extract for the Protection of Stem Cells |
| JP2016056175A (en) * | 2014-09-10 | 2016-04-21 | 株式会社東洋新薬 | KAEMPFERIA PARVIFLORA-CONTAINING PPARγ EXPRESSION PROMOTING COMPOSITIONS |
| CN105687048A (en) * | 2016-03-16 | 2016-06-22 | 新疆中草堂医药科技有限公司 | Liquid shampoo with fresh ginger granules |
| CN106333911A (en) * | 2016-10-17 | 2017-01-18 | 广州亿达化妆品有限公司 | Plant ginger (fresh ginger paste) hair loss-preventing hair-generating shampoo |
| CN107737068A (en) * | 2017-11-08 | 2018-02-27 | 熊雄 | Ginger shampoo and preparation method thereof |
| CN108524393A (en) * | 2018-06-11 | 2018-09-14 | 广西科技大学 | A kind of ginger shampoo and preparation method thereof |
| CN109652233A (en) * | 2019-01-25 | 2019-04-19 | 广州二广生物科技有限公司 | Cosmetic applicators detergent and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| I. RAHATH KUBRA等: "An Impression on Current Developments in the Technology, Chemistry, and Biological Activities of Ginger (Zingiber officinale Roscoe)", 《CRITICAL REVIEWS IN FOOD SCIENCE AND NUTRITION》 * |
| 严子军，等: "生姜在洗发水中的应用", 《应用化工》 * |
| 广州二广生物科技有限公司: "网址：http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=201810151751393fp91&nid=201810151751393fp91", 《乐草之源生姜精华洗发乳》 * |
| 王建新: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111329825A (en) * | 2020-04-15 | 2020-06-26 | 广州聚泽生物科技有限公司 | Ginger mild anti-dandruff shampoo and preparation method thereof |
| CN112675111A (en) * | 2021-01-28 | 2021-04-20 | 广州碧思特生物科技有限公司 | Ginger shampoo formula and preparation process thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109730956B (en) | 2021-12-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106591013A (en) | Biological detergent composition | |
| CN114028292B (en) | Shampoo containing plant composite anti-dandruff agent and preparation method thereof | |
| CN108186385A (en) | A kind of hair scalp cleaning compositions | |
| CN100536825C (en) | Hair washing shampoo containing snake bile and Chinese herbal medicine | |
| CN103784365B (en) | Skin whitener and preparation method thereof | |
| CN111265439A (en) | Oil-control, dandruff-removing and itching-relieving shampoo and preparation method thereof | |
| CN108785198A (en) | Strengthen the hair composition, leaves shampoo and preparation method thereof | |
| CN105476950B (en) | Moisturizing foam mildy wash and preparation method thereof | |
| CN107375066A (en) | A kind of anti-dandruff no silicone oil shampoo of ginseng oil-control and preparation method thereof | |
| CN107550795A (en) | Nourish reparation, black hair anticreep camellia oleifera fruit shampoo and preparation method thereof | |
| CN109730956A (en) | Ginger shampoo and preparation method thereof | |
| CN108451858A (en) | A kind of shampoo powder and its preparation method and application | |
| CN101732224A (en) | Shampoo containing snake gall, olive oil and Chinese herbs | |
| CN106214566A (en) | One is good for the sliding shampoo of hair without silicone oil Rhizoma Zingiberis Recens | |
| CN108295010A (en) | A kind of yellow ginger oil-control hair-loss preventing and hair-restoring shampoo and preparation method thereof | |
| CN107669541A (en) | A kind of net profit anti-dandruff shampoo | |
| CN106619273A (en) | Sweet-scented osmanthus oil-removing liquid soap | |
| CN101467955B (en) | Depilating agent | |
| CN105748358B (en) | A kind of agalloch eaglewood essence assigns running water and preparation method thereof | |
| CN106236656B (en) | A kind of compact eye cream of rosemary | |
| CN107811884A (en) | It is a kind of to nourish submissive shampoo without silicone oil | |
| CN106420406A (en) | Velvet smoothening liquid shampoo | |
| CN106566683A (en) | Cleaning liquid as well as preparation method and application thereof | |
| CN107550796B (en) | Desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo and preparation method thereof | |
| CN107737069A (en) | Plant shampoo water without emulsifying agent and oil phase |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |