CN109998948A - A kind of preparation method of red ginseng sleep mask - Google Patents
A kind of preparation method of red ginseng sleep mask Download PDFInfo
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- CN109998948A CN109998948A CN201711480225.1A CN201711480225A CN109998948A CN 109998948 A CN109998948 A CN 109998948A CN 201711480225 A CN201711480225 A CN 201711480225A CN 109998948 A CN109998948 A CN 109998948A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The present invention provides a kind of preparation method of ginseng sleep mask, comprising: the preparation of the preparation of ingredient and sleep mask in ginseng sleep mask；The preparation of ingredient includes: the preparation of red ginseng nano dispersion fluid in the ginseng sleep mask；The preparation of the sleep mask includes: that sleep mask is made in the red ginseng nano dispersion fluid, moisturizer, emulsifier II, assistant for emulsifying agent II, and/or nutritional ingredient.Red ginseng is steamed into using fresh ginseng, and collects distilled panax water, volatile oil, is made full use of by ginseng steaming into the by-product and raw material in this technical process of red ginseng.Both the loss that ingredient had greatly reduced, also saves cost.Present invention employs advanced homogenisation equipmen high pressure microjet homogenizers to break into red ginseng nano dispersion fluid for red ginseng slurries, red ginseng volatile oil, is conducive to skin absorption, plays one's part to the full.
Description
Technical field
The invention belongs to cosmetic field, in particular to a kind of preparation method of red ginseng sleep mask.
Background technique
Red ginseng is processed by fresh ginseng by infiltrating, cleaning, sort, steam.Ginseng is red by leucismus after processing,
Endemic element in red ginseng is generated, and there is significant and unique physiological activity.In addition to the soap shared with fresh ginseng, sun-dried ginseng in red ginseng
Glycosides (such as Re, Rg1, Rb1, Rb2, Rc, Rd, RO, Rf) outside, also contains some peculiar saponin(es, such as: Rh1, Rh2, Rg3,20 (R)-
Rg2, Rg5, Rg6, Rh4, F4, F2, Rs4-Rs7, Rk1-Rk3,20 (R)-Rf (2) etc..The saponin(e in red ginseng after processing
Type and content are improved, and have richer bioactivity.In addition to the variation of saponin(e, in addition, 1996, Zheng Yinan from
Discovery and isolated compound are arginine disaccharide glycosides (AFG) in red ginseng.It has been reported that the AFG in red ginseng can resist sugar
Urine disease anti-obesity, enhancing immune function, removes free radical, is anti-oxidant, promoting microcirculation and have skin effect.In order to reduce
The loss of these effective components of red ginseng can be done from the concocting process of red ginseng, make good use of the distilled panax water for steaming red ginseng, and adopt
Red ginseng is extracted with the squeezing of cold chain mashing mode, avoids the destruction of effective component.
In recent years, what facial mask was consumed as other cosmetics pursues, wherein sleep mask, easy to use, beautiful
It is obvious to hold effect, and is used before the sleeping of relatively leisure, therefore is even more to be liked by Ms.With the development of science and technology,
The high speed development of social economy, people increasingly pay attention to self-image especially appearance, in order to keep the appearance in youth, resist
Oxidation, crease-resistant cosmetics are becoming increasingly popular.Sleep mask inherently has the function of nourishing skin, if adding red ginseng again
Deng having effects that anti-oxidant, crease-resistant natural component, it is bound to effectively nourish skin, makes skin gloss without wrinkle.
The report of sleep mask and related sleep mask research on the market, the red ginseng used in them is that the prepared slices of Chinese crude drugs are red
Ginseng is the red ginseng obtained with ginseng steaming, drying, and red ginseng used steams, dries loss in this way, and steams ginseng process
Volatile component also has lost.Document be using distilled panax water substitute red ginseng, can not adequately make good use of ginseng to red ginseng
Effective component.Liu Jiyong " distilled panax water chemical component and bioactivity research " is proposed: during distilled panax water is as red ginseng processing
By-product, there is preferable utility value, can be used as cosmetics, the immune assistant of healthy food additive and animal biological product
Agent exploitation has established theoretical basis for the utilization of red ginseng distilled panax water.
But it is limited to distilled panax water complicated composition, processing, extracts the factors such as difficulty, there is no based on distilled panax water in the prior art
Want the commercially produced product of raw material.
Summary of the invention
In order to overcome above-mentioned deficiency, the present invention provides a kind of preparation method of red ginseng sleep mask.It is steamed using fresh ginseng
At red ginseng, and distilled panax water, volatile oil are collected, made full use of by ginseng steaming into the by-product and original in this technical process of red ginseng
Material.Both the loss for having greatly reduced ingredient, also saves cost.The application breaks conventional heating extraction mode, and use is cold
The squeezing extracting mode of chain, compared to the loss that heating extraction has been greatly reduced red ginseng ingredient, and active principle recovery rate also has
It improves.The application uses advanced homogenisation equipmen high pressure Microfluidizer and red ginseng slurries, red ginseng volatile oil is broken into red ginseng and received
Rice dispersion liquid is conducive to skin absorption, plays one's part to the full.
To achieve the goals above, the present invention adopts the following technical scheme:
A kind of preparation method of sleep mask red ginseng nano dispersion fluid, comprising:
It takes fresh ginseng to carry out steaming and considers and handles reason, obtain red ginseng, and collect volatile component and distilled panax water respectively；
Red ginseng is broken, grinding, separation of solid and liquid together with distilled panax water, collects red ginseng slurries；
Above-mentioned red ginseng slurries are mixed with volatile component, ginseng seed oil, emulsion I, assistant for emulsifying agent I, are uniformly dispersed, is high
Microjet homogeneous is pressed, red ginseng nano dispersion fluid is made.
Fresh ginseng Total saponin ratio is higher than dry ginseng, and moisture content is less, and sugar is also minimum, and itself battalion more easy to maintain
It forms point.Therefore, it is that primary raw material prepares sleep mask, but traditional ginseng extracting method often needs that the application, which selects fresh ginseng,
Heat treatment while obtaining active constituent, and inevitably causes certain destruction to active constituent.For this purpose, the application
It proposes and is handled using cold chain squeezing to avoid the loss of ginseng effective component, while distilled panax water is added as solution, realize people
Join comprehensive utilization of raw material.But find in subsequent experimental: it is water-insoluble that there are still parts in the red ginseng slurries after cold chain squeezing
Active macromolecules, bioavilability are low.For this purpose, the application wishes the balance that grease phase is realized by way of emulsification, but due to
Complicated composition, non-principal component are more in the application red ginseng slurries, and simple emulsification treatment is unable to reach expected effect, therefore,
The application composition of effective component and the regularity of distribution and many kinds of solids dispersion technology pair in each phase of system research red ginseng slurries
On the basis of the treatment effect of red ginseng slurries, grope to find through large scale experiment: high pressure microjet homogeneous can effectively facilitate oily phase
Dispersion of the ingredient in red ginseng slurries, plays the role of hydrotropy, is combining suitable emulsifier, assistant for emulsifying agent, is realizing red ginseng
The balance of grease phase, the higher bioavilability of acquisition in slurries, compared with existing heating extraction method, the ginseng of acquisition is extracted
Liquid more preferably absorption of human body.
Emulsifier can improve the various surface tension constituted between phase in emulsion, be allowed to form uniform and stable dispersion
System or emulsion, but emulsifier is different, and effect often also differs greatly.How emulsifier is selectively used, makes it
Reach ideal in cost input and application effect, is to have to solve the problems, such as in actual production.The application research discovery: just
For the application red ginseng slurries, on the basis of conventional emulsifier, assistant for emulsifying agent is added, then adds a certain amount of ginseng seed oil and make
For emulsifier, the emulsifying effectiveness and thermal stability of slurries can be effectively promoted, meanwhile, ginseng seed oil is alternatively arranged as nutritional ingredient raising
The effect of product.
On the other hand, in order to guarantee the application preparation red ginseng nano dispersion fluid have preferable absorption of human body, this Shen
System research please has been carried out to the dosage of red ginseng slurries and each component, while guaranteeing oil-water balance, has avoided dispersion liquid to human body
Irritation.Therefore, the preferred red ginseng nano dispersion fluid of the application containing red ginseng extract 70%, oily phase 10%, emulsifier 10%,
Assistant for emulsifying agent 10%, every 1 gram of red ginseng nano dispersion fluid 1.42mg containing general ginsenoside, the 0.31mg of volatile oil containing red ginseng.
Preferably, the separation of solid and liquid includes: filtering, centrifugation.
The application further study show that: existing distilled panax water due to containing impurity, filtering, centrifugation after, if directly use
It will lead to the problems such as lotion is unstable, liquid is muddy in preparing facial mask lotion, for this purpose, the present invention passes through to red ginseng slurries after grinding
At be grouped as, concentration, viscosity, dispersibility have carried out network analysis, grope to find by large scale experiment: can add increase part
Oil-phase solution (preferably ginseng seed oil and red ginseng volatile oil), emulsifier simultaneously starch red ginseng in conjunction with high pressure microjet homogeneous technology
Liquid is prepared into nano dispersion fluid, to obtain the red ginseng nano dispersion fluid of uniform, good dispersion degree, to guarantee subsequent sleep mask lotion
There is preferably skin care, health-care effect, absorption of human body.
Preferably, described to steam the condition for considering and handling reason are as follows: 100-110 DEG C steams 1-2h, cooling.
Present invention also provides the red ginseng nano dispersion fluids of any above-mentioned method preparation.
The present invention also provides a kind of preparation methods of red ginseng sleep mask, comprising: the system of ingredient in red ginseng sleep mask
Standby and sleep mask preparation；
The preparation of ingredient includes: the preparation of above-mentioned red ginseng nano dispersion fluid in the red ginseng sleep mask；
The preparation of the sleep mask includes: by the red ginseng nano dispersion fluid, moisturizer, emulsifier II, assistant for emulsifying agent
II, and/or nutritional ingredient sleep mask is made.
Preferably, the specific steps of the preparation of the sleep mask include:
Oil phase substance is uniformly mixed, oil mixture is obtained；
Red ginseng nano dispersion fluid, water and aqueous phase substance are uniformly mixed, is heated to dissolving, obtains aqueous mixture；
Oil mixture, Sodium Hyaluronate and essence are added to mixing in aqueous mixture to be uniformly dispersed, it is micro- to cross high pressure
Jet homogenizer homogeneous obtains red ginseng sleep mask.
Preferably, the moisturizer includes: glycerol, propylene glycol, Sodium Hyaluronate.
Preferably, the emulsifier and/or assistant for emulsifying agent include: butanediol, dimethyl silicone polymer, acrylic acid hydroxyl second
Ester/sodium acryloyldimethyl taurate copolymers, polyvinyl alcohol, xanthan gum etc..
Preferably, the nutritional ingredient includes: Mel extract, Gotu Kola P.E, Pseudoalteromonas tunning
Extract, brown alga extract.
" Mel extract, Gotu Kola P.E, Pseudoalteromonas tunning extract, brown alga are extracted in the application
Object " is all commercial product.
Present invention also provides the red ginseng sleep masks of any above method preparation.
A kind of red ginseng sleep mask, is made of the raw material of following weight percent: red ginseng nano dispersion fluid 10-15%, sweet
Oily 10-15%, butanediol 8-12%, dimethyl silicone polymer 2-5%, polyvinyl alcohol 1-3%, xanthan gum 0.5-2%, hyalomitome
Sour sodium 0.2-0.5%, sodium benzoate 0.1-0.3%, essence 0.05-0.1%, Yu Weishui；
The red ginseng nano dispersion fluid is red ginseng slurries, red ginseng volatile oil, ginseng seed oil, emulsifier I, assistant for emulsifying agent I
Mixed liquor；
The red ginseng volatile oil is that fresh ginseng steams the volatile oil collected in red ginseng process.
Preferably, the red ginseng slurries are specific the preparation method comprises the following steps: the red ginseng steamed is crushed with cutmixer,
3min is added 0.5-1.5 times of distilled panax water and is ground with colloid mill, and polish 20-40min, crosses 200 mesh filter clothes, crosses tube centrifuge, from
The clear red ginseng slurries of gains in depth of comprehension are red ginseng slurries.
Preferably, the red ginseng volatile oil the preparation method comprises the following steps: take fresh ginseng, elute, drain, the fresh parametric amplifier drained is entered
On steamer, add 2-4 times of water, 100-110 DEG C steams 1-2h；The ginseng steamed is taken out, cools as red ginseng, collects volatilization respectively
Oil, distilled panax water.
Preferably, the preparation method of the red ginseng nano dispersion fluid: by oily phase (ginseng seed oil), emulsifier and assistant for emulsifying agent
(glycerol, propylene glycol, polyvinyl alcohol) is gently added in water phase (red ginseng slurries, red ginseng mixture of volatile oil), is stirred at room temperature
It mixes uniformly mixed, pours into dispersion machine, colostric fluid is made；Colostric fluid is crossed into the homogeneous processing of high pressure Microfluidizer, is obtained molten
Good, the nanoscale red ginseng nano dispersion fluid of solution property.
Preferably, it is made of the raw material of following weight percent: red ginseng nano dispersion fluid 10-12.5%, glycerol 10-
12.5%, butanediol 8-10%, dimethyl silicone polymer 2-3.5%, polyvinyl alcohol 1-2%, xanthan gum 0.5-1.2%, transparent
Matter acid 0.2-0.5%, sodium benzoate 0.1-0.2%, essence 0.06-0.1%, Yu Weishui.
Preferably, it is made of the raw material of following weight percent: red ginseng nano dispersion fluid 12.5-15%, glycerol 12.5-
15%, butanediol 10-12%, dimethyl silicone polymer 3.5-5%, polyvinyl alcohol 2-3%, xanthan gum 1.2-2%, hyaluronic acid
0.35-0.5%, sodium benzoate 0.2-0.3%, essence 0.07-0.1%, Yu Weishui.
The present invention also provides a kind of preparation methods of red ginseng sleep mask, comprising:
(1) glycerol 12%, dimethyl silicone polymer 4% are taken, is uniformly mixed；
(2) red ginseng nano dispersion fluid 15%, butanediol 10%, polyvinyl alcohol 2%, xanthan gum 1%, deionized water are taken
55.2%, it is sufficiently stirred, is uniformly mixed at 60 DEG C；
(3) mixed liquor of step (1) is added in the mixed liquor of step (2), homogeneous 10min adds wait drop at 45 DEG C
Enter, Sodium Hyaluronate 0.5%, sodium benzoate 0.2%, essence 0.1%, be sufficiently stirred, is uniformly mixed, as red ginseng sleep mask
Colostrum.
(4) red ginseng sleep mask colostrum is obtained into red ginseng sleep mask through high pressure microjet homogeneous.
The present invention also provides a kind of red ginseng sleep masks, are made of the raw material of following weight percent: red ginseng nanometer point
Dispersion liquid 5-15%, glycerol 8-15%, butanediol 8-15%, dimethyl silicone polymer 2-5%, hydroxy-ethyl acrylate/acryloyl two
N-methyltaurine sodium copolymer 0.5-1%, Sodium Hyaluronate 0.1-0.5%, Mel extract 1-5%, Gotu Kola P.E 1-
5%, Pseudoalteromonas tunning extract 1-5%, brown alga extract 1-5%, triethanolamine 0.1-0.2%, benzene oxygen second
Alcohol 0.1-0.5%, essence 0.05-0.1%, Yu Weishui.
Preferably, it is made of the raw material of following weight percent: red ginseng nano dispersion fluid 5-10%, glycerol 8-12%, fourth
Glycol 8-12%, dimethyl silicone polymer 2-3.5%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers 0.5-
0.8%, Sodium Hyaluronate 0.1-0.3%, Mel extract 1-3%, Gotu Kola P.E 1-3%, Pseudoalteromonas fermentation
Product extract 1-3%, brown alga extract 1-3%, triethanolamine 0.1-0.15%, Phenoxyethanol 0.1-0.3%, essence
0.05-0.1%, Yu Weishui.
Preferably, it is made of the raw material of following weight percent: red ginseng nano dispersion fluid 8-15%, glycerol 12-15%, fourth
Glycol 12-15%, dimethyl silicone polymer 3.5-5%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers 0.8-
1%, Sodium Hyaluronate 0.3-0.5%, Mel extract 3-5%, Gotu Kola P.E 3-5%, Pseudoalteromonas fermentation produce
Object extract 3-5%, brown alga extract 3-5%, triethanolamine 0.15-0.2%, Phenoxyethanol 0.3-0.5%, essence 0.07-
0.1%, Yu Weishui.
The red ginseng nano dispersion fluid is red ginseng slurries, red ginseng volatile oil, ginseng seed oil, emulsifier I, assistant for emulsifying agent I
Mixed liquor；
Preferably, the preparation method of the red ginseng nano dispersion fluid: by oily phase (ginseng seed oil), emulsifier and assistant for emulsifying agent
(glycerol, propylene glycol, polyvinyl alcohol) is gently added in water phase (red ginseng slurries, red ginseng mixture of volatile oil), is stirred at room temperature
It mixes uniformly mixed, pours into dispersion machine, colostric fluid is made；Colostric fluid is crossed into the homogeneous processing of high pressure Microfluidizer, is obtained molten
Good, the nanoscale red ginseng nano dispersion fluid of solution property.
Preferably, the red ginseng slurries are specific the preparation method comprises the following steps: the red ginseng steamed is crushed with cutmixer,
3min is added 0.5-1.5 times of distilled panax water and is ground with colloid mill, and polish 20-40min, crosses 200 mesh filter clothes, crosses tube centrifuge, from
The clear red ginseng slurries of gains in depth of comprehension are red ginseng slurries.
Preferably, the red ginseng volatile oil the preparation method comprises the following steps: take fresh ginseng, elute, drain, the fresh parametric amplifier drained is entered
On steamer, add 2-4 times of water, 100-110 DEG C steams 1-2h；The ginseng steamed is taken out, cools as red ginseng, collects volatilization respectively
Oil, distilled panax water.
The present invention also provides a kind of preparation methods of red ginseng sleep mask, comprising:
(1) glycerol 10%, dimethyl silicone polymer 2%, triethanolamine 0.1% is taken to be uniformly mixed；
(2) red ginseng nano dispersion fluid 10%, butanediol 10%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate are taken
Copolymer 0.5%, Mel extract 5%, Gotu Kola P.E 3%, Pseudoalteromonas tunning extract 3%, brown alga
Extract 3%, Phenoxyethanol 0.1%, deionized water 52.7%, are sufficiently stirred, and are uniformly mixed at 70 DEG C；
(3) (1) mixture is added to (2), essence 0.1%, hyaluronic acid is added wait drop at 45 DEG C in homogeneous 15min
Sodium 0.5%, stirs, and obtains red ginseng sleep mask colostrum.
(4) red ginseng sleep mask colostrum is crossed under high pressure Microfluidizer 800bar, homogeneous 4 times, obtains red ginseng sleep surface
Film.
It is all mass percent if the percentage in the application is not specifically noted.
Beneficial effects of the present invention
(1) 1 Easy dosing is formulated in the application, it is at low cost, have the function of moisture-keeping crease-shedding, moisturizing；Formula 2 has
It is more to imitate ingredient, the opposite formula 1 of cost is high, but its whitening anti-wrinkling, the function and effect for nourishing skin are more preferable.
(2) preparation method of the present invention is simple, skin effect is good, practical, easy to spread.
Specific embodiment
It is noted that following detailed description is all illustrative, it is intended to provide further instruction to the application.Unless another
It indicates, all technical and scientific terms used herein has usual with the application person of an ordinary skill in the technical field
The identical meanings of understanding.
A kind of preparation method of ginseng sleep mask, including the preparation of ingredient in ginseng sleep mask and the system of sleep mask
It is standby.
1. the preparation of most important ingredient red ginseng nano-emulsion dispersion liquid in ginseng sleep mask；
1) red ginseng described in red ginseng nano-emulsion dispersion liquid is that preparation, preparation process are steamed by fresh ginseng are as follows: takes fresh people
Ginseng elution, drains, the fresh parametric amplifier drained is entered on steamer, add 2-4 times of water, 100 DEG C steam 3h；The ginseng steamed is taken out, is cooled
As red ginseng, and volatile oil, distilled panax water are collected respectively.The volatile oil of collection is ginseng essential oil.Entire technique is sufficiently reserved
Red ginseng and by-product (distilled panax water and volatile oil) in red ginseng process is steamed, and without the processing such as drying after steaming, directly
Using greatly reducing the loss of ingredient.
2) technique used in red ginseng nano dispersion fluid is by the way of squeezing grinding by red ginseng and distilled panax water mashing grinding.
Specifically comprises the processes of: the red ginseng steamed is crushed, 3min with cutmixer, 2 times of distilled panax waters are added and are ground with colloid mill, polished
40min crosses 200 mesh filter clothes, crosses tube centrifuge, the red ginseng slurries being centrifuged.
3) red ginseng extract used in red ginseng nano dispersion fluid is by the slurries of the above-mentioned volatile oil for steaming process and mashing
Mixing is handled with dispersion machine up to red ginseng extract.Every 1g red ginseng extract is equivalent to 0.45g fresh ginseng, contains total saposins
2.03mg, 0.45mg containing volatile oil.
4) technique used in red ginseng nano dispersion fluid is to add ginseng seed oil, emulsion, help cream above-mentioned red ginseng extract
Agent is made into red ginseng nano-emulsion dispersion liquid using the processing of dispersion machine, high pressure Microfluidizer.
2. the preparation of red ginseng sleep mask
1) red ginseng described in refers to the red ginseng nano dispersion fluid of above-mentioned preparation；
2) moisturizer used in red ginseng sleep mask can use glycerol, propylene glycol, Sodium Hyaluronate etc.；
3) emulsifier and assistant for emulsifying agent used in red ginseng sleep mask can use butanediol, dimethyl silicone polymer propylene
Sour hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers polyvinyl alcohol, xanthan gum etc.；
4) nutritional ingredient used in red ginseng sleep mask can use Mel extract, Gotu Kola P.E, Pseudoalteromonas
Tunning extract, brown alga extract etc.；
5) the red ginseng sleep mask described in is first to be made into colostrum, after the processing of high pressure Microfluidizer；
6) the problems such as red ginseng sleep mask described in can allow skin to moisten naturally and releive, and effectively solve dry skin, desalination
Microgroove, compact promotion, careful pore are that skin makes water profit protection, promote skin water content, alleviation skin water shortage, drying are tight
The discomforts such as taut, moisturize the full recovery bullet of skin consolidation bright, found the tender skin of water profit light sensation, the pure and fresh water of skin is kept to moisten
Deng.
Embodiment 1
One, the preparation of red ginseng extract
1. the preparation (being steamed by fresh ginseng) of red ginseng
It takes fresh ginseng to elute, drains, the fresh parametric amplifier drained is entered on steamer, adds 2-4 times of water, 80-120 DEG C steams 2-4h；
The ginseng steamed is taken out, cools as red ginseng, collects volatile oil, distilled panax water respectively.The volatile oil of collection is red ginseng volatile oil.
The parameter that 1.1 fresh ginsengs are processed into red ginseng is investigated
To influence two maximum processing temperature, concocted time factors as investigation object, with total saponin content and total saposins
The rate of transform is index, preferably optimal red ginseng processing procedure.As a result such as following table.
Conclusion: using total Ginsenosides Content as index, 5,6,7,8,9 differences of experiment are smaller, but 7,8,9 experiment conditions
It is 120 DEG C, and the content not than 100 DEG C is high, therefore selects to process temperature to be 100 DEG C, 5,6 contents of experiment is similar, take into account production
Cost selects experiment 5, i.e. processing temperature is 100 DEG C, is processed 3 hours, 90% or more the rate of transform.
1.2 best processing procedures
It takes fresh ginseng to elute, drains, the fresh parametric amplifier drained is entered on steamer, add 2-4 times of water, 100 DEG C steam 3h；It takes out and steams
The ginseng of system cools as red ginseng, collects volatile oil, distilled panax water respectively.The volatile oil of collection is ginseng essential oil.
2. red ginseng squeezes grinding technics
1 part of red ginseng just steamed is taken, is crushed with cutmixer, 3min, 1-2 times of distilled panax water is added and is ground with colloid mill,
Polish 20-50min, crosses 200 mesh filter clothes, filters thick slurries, crosses tube centrifuge centrifugation, obtains red ginseng slurries.
2.1 fresh ginseng extract grinding technics are investigated
With the investigation object of red ginseng milling time and distilled panax water amount, using general ginsenoside yield and the rate of transform as index.Knot
Fruit such as following table.
Note: the grinding effect of 1 times of water has equally been investigated in experiment, but its consistency is too high, and colloid mill can barely recycle discharging,
And it is insufficient visually to observe grinding, therefore not to its high spot reviews.
Conclusion: using general ginsenoside yield as index, 6,7 differences of experiment are smaller, take into account production cost and grinding effect,
Plus 2 times of water of material quantity experiment 6 is selected, i.e., (every 1g red ginseng slurries are equivalent to 0.45g fresh ginseng to grinding 40min, contain total saposins
2.03mg)。
The optimised process of 2.2 red ginseng slurries optimization
The red ginseng steamed is crushed, 3min with cutmixer, 2 times of distilled panax waters are added and are ground with colloid mill, polished
40min crosses 200 mesh filter clothes, crosses tube centrifuge, and the red ginseng slurries being centrifuged are red ginseng slurries.
3. the preparation of red ginseng nano dispersion fluid
1) red ginseng slurries are mixed with red ginseng volatile oil, handles 3-5min with dispersion machine, obtains red ginseng extract (every 1g red ginseng
Extract is equivalent to 0.45g fresh ginseng, and 2.03mg containing total saposins contains volatile oil 0.45mg).
2) red ginseng extract of above-mentioned mashing crosses dispersion machine, the processing of high pressure Microfluidizer, is made into red ginseng nano-dispersed
Liquid.Specific processing is as follows:
Oily phase, emulsifier and assistant for emulsifying agent are gently added in water phase, are uniformly mixed at room temperature, dispersion is poured into
In machine, colostric fluid is made；Colostric fluid is crossed into the homogeneous processing of high pressure Microfluidizer, obtains that dissolubility is good, nanoscale red ginseng
Nano dispersion fluid (every 1 gram of red ginseng nano dispersion fluid 1.42mg containing general ginsenoside, the volatile oil 0.31mg containing red ginseng).
3) the homogeneous condition of high pressure microjet is investigated
Using pressure and homogeneous number as investigation object, using partial size as inspection target, preferred optimum condition.As a result such as following table.
Conclusion: using the partial size of red ginseng nano dispersion fluid as index, experiment 5,6,7 differences it is smaller, take into account production cost and
Particle size considers, selects experiment 5 to feed intake that is, after starting high pressure Microfluidizer, 800bar is arranged in pressure, repeats
Homogeneous 4 times it is homogeneous to obtain the final product.
Two, the preparation of red ginseng sleep mask
Formula 1
Red ginseng nano dispersion fluid 5-15%, glycerol 5-15%, butanediol 8-12%, dimethyl silicone polymer 2-5%, poly- second
Enol 1-3%, xanthan gum 0.5-2%, Sodium Hyaluronate 0.2-0.5%, sodium benzoate 0.1-0.3%, essence 0.05-
0.09%, deionized water is to 100%.
Scheme 1:
(1) glycerol 10%, dimethyl silicone polymer 4% are taken, is uniformly mixed；
(2) red ginseng nano dispersion fluid 15%, butanediol 15%, polyvinyl alcohol 2%, xanthan gum 1%, deionized water are taken
55.2%, it is sufficiently stirred, is uniformly mixed at 60 DEG C；
(3) (1) is added in (2), homogeneous 10min, wait drop at 45 DEG C, Sodium Hyaluronate 0.5%, benzoic acid is added
Sodium 0.2%, essence 0.1%, are sufficiently stirred, and are uniformly mixed, and are red ginseng sleep mask colostrum.
(4) red ginseng sleep mask colostrum is crossed high pressure Microfluidizer 800bar homogeneous 4 times, obtains red ginseng sleep mask.
Formula 2:
Red ginseng nano dispersion fluid 5-15%, glycerol 8-15%, butanediol 8-15%, dimethyl silicone polymer 2-5%, propylene
Sour hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers 0.5-1%, Sodium Hyaluronate 0.1-0.5%, Mel extract 1-
5%, Gotu Kola P.E 1-5%, Pseudoalteromonas tunning extract 1-5%, brown alga extract 1-5%, three ethyl alcohol
Amine 0.1-0.2%, Phenoxyethanol 0.1-0.5%, essence 0.05-0.15%, deionized water to 100%.
Scheme 2
(1) glycerol 10%, dimethyl silicone polymer 2%, triethanolamine 0.1% is taken to be uniformly mixed；
(2) red ginseng nano dispersion fluid 10%, butanediol 10%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate are taken
Copolymer 0.5%, Mel extract 5%, Gotu Kola P.E 3%, Pseudoalteromonas tunning extract 3%, brown alga
Extract 3%, Phenoxyethanol 0.1%, deionized water 52.7%, are sufficiently stirred, and are uniformly mixed at 70 DEG C；
(3) (1) mixture is added to (2), essence 0.1%, hyaluronic acid is added wait drop at 45 DEG C in homogeneous 15min
Sodium 0.5%, stirs, and obtains red ginseng sleep mask colostrum.
(4) red ginseng sleep mask colostrum is crossed high pressure Microfluidizer 800bar homogeneous 4 times, obtains red ginseng sleep mask.
Brief summary: being formulated 1 Easy dosing, at low cost, has the function of moisture-keeping crease-shedding, moisturizing；It is formulated 2 effective components
More, the opposite formula 1 of cost is high, but its whitening anti-wrinkling, the function and effect for nourishing skin are more preferable.
Three, the experience effect analysis of red ginseng sleep mask
1. being changed using red ginseng sleep mask moisture of skin
10 female volunteers from 20-50 years old all ages and classes are looked for, clear water washes face, dries, measured with moisture of skin
Instrument tests skin moisture value, and left side of the face is using 1 (scheme 1) of formula, and right side face uses 2 (schemes 2) of formula, and respectively after smearing
0, moisture 2,4,6, is measured after 8h, each measurement result removes a minimum value, removes a maximum value, remaining calculates average
Value, as moisture content index, as a result such as following table.
Conclusion:
(1) experiment 1 is the moisture for not smearing sleep mask, and experiment 2 is the rigid moisture value smeared and patted after absorbing, by testing
1,2 comparison, it can be deduced that can increase moisture of skin using red ginseng sleep mask formula 1, formula 2, and be formulated 2 and increase than formula 1
Add moisture effect more preferable.
(2) using moisture of skin slightly reduces after 2,4,6,8 hours after red ginseng sleep mask, illustrate the two formulas to skin
The effect of skin moisture moistening effect is obvious；And formula 2 is more preferable compared with 1 water tariff collection of formula.
2. using the sensory evaluation of red ginseng sleep mask
10 female volunteers from 20-50 years old all ages and classes are looked for, respectively at left side of the face 1 (scheme 1) of formula, right side face
With 2 (schemes 2) of formula, sleeps preceding use (by sleep mask application method on the market) every night, be used continuously 7 days, give respectively
It is formulated the marking of 1,2 accordings to the form below, each score removes a best result, removes one minimum point, calculates average value, and as each is most
After score.As a result it see the table below.
Note: each project full marks 10 divide, and score is higher to illustrate that effect is better.
Conclusion:
As seen from the above table, absorbability, the comfort level, whitening effect, moisturizing of 2 pairs of red ginseng sleep mask formula 1, formula skin
Property etc. have a good effect, and it is more prominent to be formulated 2 effects；Improving sleep quality, formula 1 and formula 2 have good effect
Fruit illustrates that addition red ginseng nano dispersion fluid plays certain effect in formula.
Finally it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not limited to this hair
It is bright, although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still
It can modify to technical solution documented by previous embodiment, or part is equivalently replaced.It is all in this hair
Within bright spirit and principle, any modification, equivalent replacement, improvement and so on should be included in protection scope of the present invention
Within.Above-mentioned, although specific embodiments of the present invention have been described, and it is not intended to limit the protection scope of the present invention, institute
Category field technical staff should be understood that based on the technical solutions of the present invention those skilled in the art do not need to pay wound
The various modifications or changes that the property made labour can be made are still within protection scope of the present invention.
Claims (10)
1. a kind of sleep mask preparation method of red ginseng nano dispersion fluid characterized by comprising
It takes fresh ginseng to carry out steaming and considers and handles reason, obtain red ginseng, and collect volatile component and distilled panax water respectively；
Red ginseng is broken, grinding, separation of solid and liquid together with distilled panax water, collects red ginseng slurries；
Above-mentioned red ginseng slurries are mixed with volatile component, ginseng seed oil, emulsion I, assistant for emulsifying agent I, are uniformly dispersed, high pressure it is micro-
Red ginseng nano dispersion fluid is made in jet stream homogeneous.
2. the method as described in claim 1, which is characterized in that the red ginseng nano dispersion fluid contains red ginseng extract
70wt%, oily phase 10wt%, emulsifier 10wt%, assistant for emulsifying agent 10wt%, every 1 gram of red ginseng nano dispersion fluid contain general ginsenoside
1.42mg, the 0.31mg of volatile oil containing red ginseng.
3. the method as described in claim 1, which is characterized in that described to steam the condition for considering and handling reason are as follows: 100-110 DEG C steams 1-
2h, it is cooling.
4. the red ginseng nano dispersion fluid of the described in any item method preparations of claim 1-3.
5. a kind of preparation method of red ginseng sleep mask characterized by comprising the preparation of ingredient and slept in red ginseng sleep mask
The preparation of dormancy facial mask；
The preparation of ingredient includes: the preparation of red ginseng nano dispersion fluid as claimed in claim 4 in the red ginseng sleep mask；
The preparation of the sleep mask include: by the red ginseng nano dispersion fluid, moisturizer, emulsifier II, assistant for emulsifying agent II,
And/or sleep mask is made in nutritional ingredient.
6. method as claimed in claim 5, which is characterized in that the specific steps of the preparation of the sleep mask include:
Oil phase substance is uniformly mixed, oil mixture is obtained；
Red ginseng nano dispersion fluid, water and aqueous phase substance are uniformly mixed, is heated to dissolving, obtains aqueous mixture；
Oil mixture is added to homogeneous in aqueous mixture, cools down, add Sodium Hyaluronate and essence, obtains red ginseng sleep
Facial mask colostrum；
Red ginseng sleep mask colostrum is crossed into high pressure microjet homogeneous to get red ginseng sleep mask.
7. method as claimed in claim 6, which is characterized in that the moisturizer includes: glycerol, propylene glycol, Sodium Hyaluronate.
8. method as claimed in claim 6, which is characterized in that the emulsifier and/or assistant for emulsifying agent include: butanediol, gather
Dimethyl siloxane, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, polyvinyl alcohol, xanthan gum etc..
9. method as claimed in claim 6, which is characterized in that the nutritional ingredient includes: Mel extract, centella extraction
Object, Pseudoalteromonas tunning extract, brown alga extract.
10. the ginseng sleep mask of any one of claim 5-9 the method preparation.
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Application publication date: 20190712 |