CN109897394A - A method of degradable package material is prepared using Schizophyllum commune for Mycelium - Google Patents

A method of degradable package material is prepared using Schizophyllum commune for Mycelium Download PDF

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Publication number
CN109897394A
CN109897394A CN201910058513.0A CN201910058513A CN109897394A CN 109897394 A CN109897394 A CN 109897394A CN 201910058513 A CN201910058513 A CN 201910058513A CN 109897394 A CN109897394 A CN 109897394A
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mycelium
schizophyllum commune
parts
wheat
package material
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CN201910058513.0A
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董洪新
杨树德
刘佳琳
胡永强
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Ludong University
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Ludong University
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Abstract

The present invention relates to a kind of methods for preparing degradable package material using Schizophyllum commune for Mycelium, comprising steps of S101: compost prepares: by corn stover, wheat stalk, apple sawdust, wheat shell, cotton seed hulls, lime, gypsum is uniformly mixed;It adds water into compost to mix, sterilizing;S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, and covers lid culture;S103: mold filling culture: in the packaged die for aseptically having sterilized the material for covering with Schizophyllum commune for Mycelium filling, continue to cultivate after being pressed and sealed;S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, sample is taken out out of mold and is dried to obtain product.For the present invention using crop material as primary raw material, apple sawdust, wheat shell is auxiliary material, using Schizophyllum commune for Mycelium as the environment-friendly package material of binder, the problem of existing packaging non-degradable can be solved, can also preferably handle crop material and fruit tree.

Description

A method of degradable package material is prepared using Schizophyllum commune for Mycelium
Technical field
The invention belongs to field of packaging material more particularly to a kind of utilization Schizophyllum commune for Mycelium to prepare degradable package The method of material.
Background technique
With white pollution increasingly aggravate and natural resources it is increasingly in short supply, degradable, green, environment-friendly package material is got over To get over the attention by the majority of consumers.Currently, the correlative study of biomass full degradable product has become the heat studied both at home and abroad Point.
China is large agricultural country, and corn actual production in 2016 is 2.2463 hundred million tons.It is changed according to corn yield and stalk amount Calculation relationship: stalk amount=1.2 × corn yield.China's stalk in 2016 is about 2.6955 hundred million tons.China's corn stover is handled at present Biogas is mainly made, domestic animal foodstuff, production plant ash returning to the field etc. are done.But it is incinerated using small scale and there are also a large amount of stalks, Pollution is generated, the wasting of resources is also resulted in.The annual output of China's wheat stalk is about 1.8 hundred million tons or so, is gone out in some areas The phenomenon that now huddling, disorderly abandon, or even burning, wheat stalk is treated as problem.In fact, wheat stalk is not waste, But a kind of renewable resource of preciousness.
Apple is the big kind of yield first in all kinds of fruit in China, and China is maximum apple production state in the world. In these years, China's apple production stablize increase, the whole city's cultivated area of the apple of Yantai in 2015 up to 2,720,000 mu, fruit-bearing forest branch Pruning rate also year by year it is whole plus, discarded fruit-bearing forest branch should what course to follow become a Xiang Wenti.
There are many macro fungis in nature, using in extensive range.Many has been exploited for industrial fermentation and agriculture Industry production.Schizophyllum commune (Schizophyllum commune Fr.) is a kind of edible medicinal macro fungi, is widely distributed in all over the world, Food industry, medical and health, in terms of be widely used.Schizophyllum commune includes mycelium and fructification two parts group At, fructification edible value is high, and matter is tender delicious, has special strong fragrance, and it is mild-natured, there is strengthening by means of tonics, sedation, be High-grade edible and medical fungi.The bacterium mycelium contains more strongly active cellulase, and can generate malic acid, and when mycelia submerged fermentation can Generate a large amount of organic acids, also can produce regulator heteroauxin, using its mycelium production packaging material there is not yet.
At present patent of invention (CN106633990A) using corn stover as the fungi based biomass packaging material of major ingredient and its Preparation method, patent of invention (CN106633989A) are using bagasse as the fungi based biomass packaging material of major ingredient and its preparation side Method, patent of invention (CN106633990A) are by fungi based biomass packaging material of major ingredient and preparation method thereof of corn stover Column patent is all solely using a kind of material as major ingredient, and base-material requires relatively complicated, and not to be related to fire-resistance resistance to for only excellent mechanical property It is aqueous;Patent of invention (CN104025909A) it is a kind of be inoculated with edible fungus species culture degradable package material method, have compared with Good fire line, but without the advantage in weight.
Summary of the invention
Degradable package material is prepared using Schizophyllum commune for Mycelium in order to solve the above technical problem, the present invention provides a kind of Method, the present invention is one kind based on agricultural crop straw, and apple sawdust, the Schizophyllum commune for Mycelium supplemented by wheat shell prepares packaging The technology of material.
The present invention is achieved through the following technical solutions, and the present invention, which provides a kind of prepare using Schizophyllum commune for Mycelium, to drop The method for solving packaging material, comprising the following steps:
S101: compost prepares: by corn stover, wheat stalk, apple sawdust, wheat shell, cotton seed hulls, lime, gypsum mixing Uniformly;1.25 ~ 1.50 times of water of the dry weight that adds materials into compost mix, the water content in regulation culture raw material to 55%- 60%, it is then charged into sterilizing bag sterilizing;
S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, and covers lid culture;
S103: mold filling culture: the spectacle case for aseptically having sterilized the material for covering with Schizophyllum commune for Mycelium filling is die-filling In tool, continue to cultivate after being pressed and sealed;
S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, sample is taken out of mold It is dried out to the water content of sample and is lower than 20%, degradable package material can be obtained.
The present invention, for primary raw material, is made with plant fiber (wheat shell, wheat stalk, corn stover etc.) and apple branch It is standby a kind of novel based on the mycelial degradable package material of macro fungi;Raw material extensive, preparation process with raw material sources Simply, low in cost, the advantages that Life cycle is pollution-free, belong to environmental type packaging material, and can make full use of Agricultural straw resource has wide promotion prospect.
Schizophyllum commune is a kind of edible medicinal macro fungi, is widely distributed in all over the world, in food industry, medical and health, bioid Learn etc. is widely used.Schizophyllum commune includes mycelium and fructification two parts composition, and fructification edible value is high, the tender taste of matter Beauty has special strong fragrance, mild-natured, has strengthening by means of tonics, sedation, for high-grade edible and medical fungi.The bacterium mycelium contains More strongly active cellulase, and can generate malic acid, when mycelia submerged fermentation, can produce a large amount of organic acids, also can produce growth-promoting Plain heteroauxin, using its mycelium production packaging material there is not yet.
Preferably, material is added and is calculated by weight as: 20~25 parts of corn stovers, 20~25 portions of wheats in S101 Stalk, 10~15 parts of apple sawdusts, 5~10 parts of wheat shells, 5~10 parts of cotton seed hulls, 1~3 part of lime, 1~2 part of gypsum.
Preferably, material is added and is calculated by weight as 25 parts of corn stovers, 25 parts of wheat stalks, 15 parts in S101 Apple sawdust, 10 parts of wheat shells, 10 parts of cotton seed hulls, 3 parts of lime, 2 parts of gypsum.
Preferably, in S101, sterilizing bag in autoclaving equipment in sterilizing 2 hours.
Preferably, in S102, condition of culture are as follows: 20 DEG C -25 DEG C of temperature, envionmental humidity 60%, draughty It is cultivated -15 days 10 days in dark constant incubator, until covering with mycelium on material.
Preferably, in S103, condition of culture are as follows: 20 DEG C of temperature, humidity 60% cultivates 5 in dark constant incubator It.
Preferably, S104: sample takes out dry under the conditions of 60 DEG C out of mold.
The invention has the benefit that
1) present invention produces one kind using crop material as primary raw material, and apple sawdust, wheat shell is auxiliary material, with schizophyllum commune bacterium The problem of filament is the environment-friendly package material of binder, and existing packaging non-degradable can be solved, can also preferably handle work Object stalk and fruit tree.
2) raw material of the invention is with raw material sources are extensive, preparation process is simple, low in cost, Life cycle is pollution-free The advantages that, belong to environmental type packaging material, and agricultural straw resource can be made full use of, before there is wide popularization Scape.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
Application principle of the invention is further described combined with specific embodiments below.
Embodiment 1, a method of degradable package material is prepared using Schizophyllum commune for Mycelium, comprising the following steps:
S101: compost prepares: by 25 parts of corn stovers, 25 parts of wheat stalks, 15 parts of apple sawdusts, 10 parts of wheat shells, and 10 parts Cotton seed hulls, 3 parts of lime, 2 parts of gypsum are uniformly mixed;1.25 times of the dry weight that adds materials into compost ~ 1.50 times of water mix, Water content in regulation culture raw material is then charged into sterilizing bag to 55%-60%, in sterilizing 2 hours in autoclaving equipment.
S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, lid is covered, is put It is placed in 20 DEG C -25 DEG C of temperature, envionmental humidity 60% or so, cultivates 10 days -15 in draughty dark constant incubator It, until covering with mycelium on material.
S103: the material for covering with Schizophyllum commune for Mycelium aseptically mold filling culture: is inserted to the spectacle case sterilized In die-filling tool, it is placed in 20 DEG C of temperature after being pressed and sealed, humidity 60% is cultivated 5 days in dark constant incubator.
S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, by sample from mold Interior taking-up, which is dried under the conditions of 60 DEG C to the water content of sample, is lower than 20%, can be obtained with plant fiber (wheat shell, Wheat Straw Stalk, corn stover etc.) and apple branch be primary raw material fungi based biomass packaging material.
Embodiment 2, a method of degradable package material is prepared using Schizophyllum commune for Mycelium, comprising the following steps:
S101: compost prepares: by 20 parts of corn stovers, 20 parts of wheat stalks, 10 parts of apple sawdusts, 5 parts of wheat shells, 5 portions of cottons Seed shell, 1 part of lime, 1 part of gypsum are uniformly mixed;1.25 times of the dry weight that adds materials into compost ~ 1.50 times of water mix, and adjust Water content in control culture raw material is then charged into sterilizing bag to 55%-60%, in sterilizing 2 hours in autoclaving equipment.
S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, lid is covered, is put It is placed in 20 DEG C -25 DEG C of temperature, envionmental humidity 60% or so, cultivates 10 days -15 in draughty dark constant incubator It, until covering with mycelium on material.
S103: the material for covering with Schizophyllum commune for Mycelium aseptically mold filling culture: is inserted to the spectacle case sterilized In die-filling tool, it is placed in 20 DEG C of temperature after being pressed and sealed, humidity 60% is cultivated 5 days in dark constant incubator.
S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, by sample from mold Interior taking-up, which is dried under the conditions of 60 DEG C to the water content of sample, is lower than 20%, can be obtained with plant fiber (wheat shell, Wheat Straw Stalk, corn stover etc.) and apple branch be primary raw material fungi based biomass packaging material.
Embodiment 3, a method of degradable package material is prepared using Schizophyllum commune for Mycelium, comprising the following steps:
S101: compost prepares: by 22 parts of corn stovers, 22 parts of wheat stalks, 12 parts of apple sawdusts, 8 parts of wheat shells, 8 portions of cottons Seed shell, 2 parts of lime, 2 parts of gypsum are uniformly mixed;1.25 times of the dry weight that adds materials into compost ~ 1.50 times of water mix, and adjust Water content in control culture raw material is then charged into sterilizing bag to 55%-60%, in sterilizing 2 hours in autoclaving equipment.
S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, lid is covered, is put It is placed in 20 DEG C -25 DEG C of temperature, envionmental humidity 60% or so, cultivates 10 days -15 in draughty dark constant incubator It, until covering with mycelium on material.
S103: the material for covering with Schizophyllum commune for Mycelium aseptically mold filling culture: is inserted to the spectacle case sterilized In die-filling tool, it is placed in 20 DEG C of temperature after being pressed and sealed, humidity 60% is cultivated 5 days in dark constant incubator.
S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, by sample from mold Interior taking-up, which is dried under the conditions of 60 DEG C to the water content of sample, is lower than 20%, can be obtained with plant fiber (wheat shell, Wheat Straw Stalk, corn stover etc.) and apple branch be primary raw material fungi based biomass packaging material.
Certainly, above description is also not limited to the example above, technical characteristic of the present invention without description can by or It is realized using the prior art, details are not described herein;It is not to this that the above examples are only used to illustrate the technical scheme of the present invention The limitation of invention, describes the invention in detail referring to preferred embodiment, and those skilled in the art should Understand, the variations, modifications, additions or substitutions that those skilled in the art are made within the essential scope of the present invention Without departure from spirit of the invention, it also should belong to claims of the invention.

Claims (7)

1. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium, it is characterised in that: the following steps are included:
S101: compost prepares: by corn stover, wheat stalk, apple sawdust, wheat shell, cotton seed hulls, lime, gypsum mixing Uniformly;1.25 ~ 1.50 times of water of the dry weight that adds materials into compost mix, the water content in regulation culture raw material to 55%- 60%, it is then charged into sterilizing bag sterilizing;
S102: strain preculture: schizophyllum commune liquid spawn is inoculated in the bacterium bag being cooled to room temperature, and covers lid culture;
S103: mold filling culture: the spectacle case for aseptically having sterilized the material for covering with Schizophyllum commune for Mycelium filling is die-filling In tool, continue to cultivate after being pressed and sealed;
S104: sample drying: after Schizophyllum commune for Mycelium is tied again in the material in mold, sample is taken out of mold It is dried out to the water content of sample and is lower than 20%, degradable package material can be obtained.
2. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 1, feature It is: in S101, material is added and is calculated by weight as: 20~25 parts of corn stovers, 20~25 parts of wheat stalks, 10~15 parts Apple sawdust, 5~10 parts of wheat shells, 5~10 parts of cotton seed hulls, 1~3 part of lime, 1~2 part of gypsum.
3. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 2, feature It is: in S101, material is added and is calculated by weight as 25 parts of corn stovers, 25 parts of wheat stalks, 15 parts of apple sawdusts, 10 parts Wheat shell, 10 parts of cotton seed hulls, 3 parts of lime, 2 parts of gypsum.
4. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 1, feature Be: in S101, sterilizing bag in autoclaving equipment in sterilizing 2 hours.
5. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 1, feature It is: in S102, condition of culture are as follows: 20 DEG C -25 DEG C of temperature, envionmental humidity 60%, draughty dark constant temperature incubation It is cultivated -15 days 10 days in case, until covering with mycelium on material.
6. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 1, feature It is: in S103, condition of culture are as follows: 20 DEG C of temperature, humidity 60% is cultivated 5 days in dark constant incubator.
7. a kind of method for preparing degradable package material using Schizophyllum commune for Mycelium according to claim 1, feature Be: S104: sample takes out dry under the conditions of 60 DEG C out of mold.
CN201910058513.0A 2019-01-22 2019-01-22 A method of degradable package material is prepared using Schizophyllum commune for Mycelium Pending CN109897394A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110655801A (en) * 2019-11-18 2020-01-07 常熟理工学院 Bio-based composite material and preparation method thereof
CN113692913A (en) * 2021-09-15 2021-11-26 吉林大学 Method for preparing biological fiber buffer packaging material by utilizing oyster mushroom hypha
CN113930080A (en) * 2021-10-18 2022-01-14 吉林工程技术师范学院 Fireproof material with corn straw as base material and preparation method thereof
US11920126B2 (en) 2018-03-28 2024-03-05 Ecovative Design Llc Bio-manufacturing process
US11932584B2 (en) 2006-12-15 2024-03-19 Ecovative Design Llc Method of forming a mycological product

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CN1263129A (en) * 2000-03-01 2000-08-16 李克升 Degradable disposable tabreware and its production method
JP2009234266A (en) * 2003-06-03 2009-10-15 Biotec Biologische Naturverpackungen Gmbh & Co Kg Fiber sheet coated or impregnated by biodegradable polymer or polymer blend
CN108753624A (en) * 2018-04-19 2018-11-06 鲁东大学 A method of preparing degradable package material using Schizophyllum commune for Mycelium
CN108934760A (en) * 2018-07-11 2018-12-07 鲁东大学 A method of degradable package material is prepared using Schizophyllum commune for Mycelium

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1263129A (en) * 2000-03-01 2000-08-16 李克升 Degradable disposable tabreware and its production method
JP2009234266A (en) * 2003-06-03 2009-10-15 Biotec Biologische Naturverpackungen Gmbh & Co Kg Fiber sheet coated or impregnated by biodegradable polymer or polymer blend
CN108753624A (en) * 2018-04-19 2018-11-06 鲁东大学 A method of preparing degradable package material using Schizophyllum commune for Mycelium
CN108934760A (en) * 2018-07-11 2018-12-07 鲁东大学 A method of degradable package material is prepared using Schizophyllum commune for Mycelium

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11932584B2 (en) 2006-12-15 2024-03-19 Ecovative Design Llc Method of forming a mycological product
US11920126B2 (en) 2018-03-28 2024-03-05 Ecovative Design Llc Bio-manufacturing process
CN110655801A (en) * 2019-11-18 2020-01-07 常熟理工学院 Bio-based composite material and preparation method thereof
CN113692913A (en) * 2021-09-15 2021-11-26 吉林大学 Method for preparing biological fiber buffer packaging material by utilizing oyster mushroom hypha
CN113930080A (en) * 2021-10-18 2022-01-14 吉林工程技术师范学院 Fireproof material with corn straw as base material and preparation method thereof

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Application publication date: 20190618