CN109793680B - Skin-care composite fruit and plant anti-allergy extracting solution and preparation method and application thereof - Google Patents
Skin-care composite fruit and plant anti-allergy extracting solution and preparation method and application thereof Download PDFInfo
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- CN109793680B CN109793680B CN201811593435.6A CN201811593435A CN109793680B CN 109793680 B CN109793680 B CN 109793680B CN 201811593435 A CN201811593435 A CN 201811593435A CN 109793680 B CN109793680 B CN 109793680B
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Abstract
The invention relates to a skin-care composite fruit and plant anti-allergy extracting solution as well as a preparation method and application thereof, wherein the extracting solution comprises the following raw materials: radix Isatidis, radix Stephaniae Tetrandrae, Poria, radix Sophorae Flavescentis, herba Taraxaci, and fructus Actinidiae chinensis; the mass ratio of the isatis root to the tetrandra root to the poria cocos to the radix sophorae flavescentis to the dandelion to the Chinese kiwi fruit is (1-5): (5-10): (2-5): (1-5): (1-3): (0.1-0.5). The compound extract is extracted from various plant traditional Chinese medicinal materials and fruits, is safe and non-irritant, and has the functions of moisturizing, preventing and relieving sensitive skin allergy and inflammation. The components have synergistic effect, active ingredients in the extracting solution are fully utilized, so that the moisturizing, repairing and anti-allergy effects are fully exerted, and the application range is wide.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a skin-care composite fruit and plant anti-allergy extracting solution and a preparation method and application thereof.
Background
With age, metabolism of the human body begins to slow, moisture and subcutaneous fat are reduced, and the skin loses elastic luster. In addition, the continuous popularization of computers and the gradual change of the environment lead people to be suffered from various radiation and ultraviolet rays, and the skin is seriously injured due to the fact that inferior and overproof cosmetics are applied by mistake, and a plurality of skin allergy and inflammation phenomena occur.
At present, anti-allergic products are various, most of which are chemical synthesis agents, and although the anti-allergic products can play a certain treatment effect in a short period, the anti-allergic products can also damage the skin in a long period, so that a skin care product which has an anti-allergic effect and does not cause any damage to the skin is needed, and the fundamental problem of the skin of people can be really solved.
Disclosure of Invention
The invention aims to provide a skin-care composite fruit and plant anti-allergy extracting solution as well as a preparation method and application thereof, so as to solve the technical problems.
The technical purpose of the invention is realized by the following technical scheme:
in a first aspect, the invention provides a skin-care compound fruit and plant anti-allergy extracting solution, which comprises the following raw materials: radix Isatidis, radix Stephaniae Tetrandrae, Poria, radix Sophorae Flavescentis, herba Taraxaci, and fructus Actinidiae chinensis; the radix isatidis, the radix stephaniae tetrandrae, the poria cocos, the radix sophorae flavescentis, the dandelion and the Chinese kiwi fruit are prepared from the following components in a mass ratio of (1-5): (5-10): (2-5): (1-5): (1-3): (0.1-0.5).
In a second aspect, the invention provides a preparation method of a skin-care compound fruit and plant anti-allergy extracting solution, wherein the preparation method is based on the skin-care compound fruit and plant anti-allergy extracting solution, and the preparation method comprises the following steps:
s1: mixing the five components of the isatis root, the tetrandra root, the poria cocos, the sophora flavescens root and the dandelion according to the proportion and the dosage, putting the mixture into a vacuum emulsifying pot, adding a solvent to soak the mixture for 1 to 1.5 hours, stirring the mixture at a speed of 15 revolutions per minute, and heating the mixture simultaneously, wherein the Chinese kiwi fruit is prefabricated separately;
s2: peeling the Chinese gooseberry in advance, putting the Chinese gooseberry into a wall breaking machine with the power of 1200W, adding a proper amount of pure water, stirring at a high speed for 3 minutes, stopping a motor, and then stirring at a high speed for 3 minutes to obtain Chinese gooseberry juice;
s3: when the temperature of the materials in the vacuum emulsifying pot is reduced to 40-45 ℃, adding the Chinese gooseberry juice, scouring the inner wall of the wall breaking machine cup with a proper amount of pure water, and pouring into the vacuum emulsifying pot;
s4: continuously stirring the materials in the vacuum emulsifying pot for 20 minutes at the rotating speed of 20 revolutions per minute;
s5: discharging, filtering with 150 mesh filter screen, and storing the decocted plant composite extract in a sealed container for use.
According to a further development of the invention, the solvent is selected from pure water, hexanediol, propylene glycol.
The invention is further provided with that the mass ratio of the water, the hexanediol and the propylene glycol is (82-88): (0.5-1.0): (3-5).
In a third aspect, the invention provides an application of a skin-care compound fruit and plant anti-allergy extracting solution in preparation of cosmetics.
In conclusion, the invention has the following beneficial effects:
1. the compound extract is extracted from various plant traditional Chinese medicinal materials and fruits, is safe and non-irritant, and has the functions of moisturizing, preventing and relieving sensitive skin allergy and inflammation. The components have synergistic effect, and active ingredients in the extracting solution are fully utilized, so that the moisturizing, repairing and anti-allergy effects are fully exerted.
2. The skin-care composite fruit and plant anti-allergy extracting solution has wide application range, and is suitable for skin-care washing products in various dosage forms such as cream, emulsion, facial mask solution, skin lotion, essence, shampoo, shower gel, bath lotion and the like.
Drawings
FIG. 1 is a graph showing the inhibition effect of each group of extracts on hyaluronidase activity in this example;
FIG. 2 is a graph showing the results of measurement in effect example 4;
FIG. 3 is a graph showing the results of measurement in effect example 4;
FIG. 4 is a graph showing the results of measurement in effect example 4.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.
It is to be understood that the terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. Further, for numerical ranges in this disclosure, it is understood that the upper and lower limits of the range, and each intervening value therebetween, is specifically disclosed. Every smaller range between any stated value or intervening value in a stated range and any other stated or intervening value in a stated range is encompassed within the invention. The upper and lower limits of these smaller ranges may independently be included or excluded in the range.
The invention provides a skin-care composite fruit and plant anti-allergy extracting solution, which comprises the following components: radix isatidis, radix stephaniae tetrandrae, poria cocos, radix sophorae flavescentis, dandelion and Chinese gooseberry; the mass ratio of the isatis root to the tetrandra root to the poria cocos to the radix sophorae flavescentis to the dandelion to the Chinese kiwi fruit is (1-5): (5-10): (2-5): (1-5): (1-3): (0.1-0.5).
Example 1:
the preparation method of the skin-care composite fruit and plant anti-allergy extracting solution provided by the embodiment comprises the following steps of:
s1: taking the following raw materials by weight: putting the five raw materials of 1 part of isatis root, 5 parts of tetrandra root, 2 parts of poria cocos, 1 part of sophora flavescens root and 1 part of dandelion into a vacuum emulsifying pot, preparing a solvent from 82 parts of pure water, 0.5 part of hexanediol and 3 parts of propylene glycol, adding the solvent into the vacuum emulsifying pot, soaking the raw materials for 1-1.5 hours, starting heating, and stirring at 15 revolutions per minute;
s2: on the other hand, 0.1 part of Chinese gooseberry is taken to be peeled, put into a wall breaking machine with the power of 1200W, added with a proper amount of pure water, stirred at high speed for 3 minutes, and stirred at high speed for 3 minutes after the motor is stopped, so as to obtain the Chinese gooseberry juice;
s3: when the temperature of the materials in the vacuum emulsifying pot is reduced to 40-45 ℃, adding the prepared Chinese gooseberry juice into the vacuum emulsifying pot, scouring the inner wall of the wall breaking machine cup with a proper amount of pure water, and pouring into the vacuum emulsifying pot;
s4: then the materials in the vacuum emulsifying pot are continuously stirred for 20 minutes at the rotating speed of 20 revolutions per minute;
s5: and finally, filtering the mixture by a filter screen of 150 meshes to obtain the decocted skin-care composite fruit and plant anti-allergy extracting solution, and storing the skin-care composite fruit and plant anti-allergy extracting solution in a closed container for later use.
Example 2:
the preparation method of the skin-care composite fruit and plant anti-allergy extracting solution provided by the embodiment comprises the following steps of:
s1: taking the following raw materials by weight: putting the five raw materials of 3 parts of isatis root, 8 parts of tetrandra root, 3 parts of poria cocos, 3 parts of sophora flavescens root and 2 parts of dandelion into a vacuum emulsifying pot, preparing a solvent from 85 parts of pure water, 0.8 part of hexanediol and 4 parts of propylene glycol, adding the solvent into the vacuum emulsifying pot, soaking the raw materials for 1-1.5 hours, starting heating, and stirring at 15 revolutions per minute;
s2: on the other hand, 0.4 part of Chinese gooseberry is taken to be peeled, put into a wall breaking machine with the power of 1200W, added with a proper amount of pure water, stirred at high speed for 3 minutes, and stirred at high speed for 3 minutes after the motor is stopped, so as to obtain the Chinese gooseberry juice;
s3: when the temperature of the materials in the vacuum emulsifying pot is reduced to 40-45 ℃, adding the prepared Chinese gooseberry juice into the vacuum emulsifying pot, scouring the inner wall of the wall breaking machine cup with a proper amount of pure water, and pouring into the vacuum emulsifying pot;
s4: then the materials in the vacuum emulsifying pot are continuously stirred for 20 minutes at the rotating speed of 20 revolutions per minute;
s5: and finally, filtering the mixture by a filter screen of 150 meshes to obtain the decocted skin-care composite fruit and plant anti-allergy extracting solution, and storing the skin-care composite fruit and plant anti-allergy extracting solution in a closed container for later use.
Comparative example 1:
to further illustrate the beneficial effects of the present invention, the same preparation method as that used in example 2 of the present invention is used to prepare the skin-care compound fruit and plant anti-allergy extract, and the difference between this comparative example and example 2 is only that: the raw materials used in this comparative example only included: 3 parts of isatis root and 2 parts of dandelion.
Comparative example 2:
to further illustrate the beneficial effects of the present invention, the same preparation method as that used in example 2 of the present invention is used to prepare the skin-care compound fruit and plant anti-allergy extract, and the difference between this comparative example and example 2 is only that: the raw materials used in this comparative example only included: 3 parts of isatis root, 2 parts of dandelion, 8 parts of tetrandra root and 3 parts of sophora flavescens root.
Comparative example 3:
to further illustrate the beneficial effects of the present invention, the comparative example employs glycyrrhizic acid dimethyl ester.
Effect example 1:
when an organism receives certain stimulation to trigger antigen-antibody reaction, the cell membrane permeability of mast cells is changed, histamine is released, and the cell membrane permeability and the histamine receptor react to generate pathophysiological reaction, so that skin itch, pain, red swelling and other abnormalities are caused. Substances that affect histamine release from mast cells can modulate hyaluronidase activity. There is a good correlation between inhibition of hyaluronidase activity and inhibition of histamine release from mast cells.
The greater the hyaluronidase inhibition rate, the less histamine released and the greater the anti-allergic activity.
Determination of the inhibitory effect on hyaluronidase: the inhibitory rates of hyaluronidase activity at 0.5h and 1h were recorded at 5% concentrations of the compositions obtained in example 2 and comparative examples 1, 2 and 3, respectively, as shown in FIG. 1.
In the above experimental data, the anti-allergic activity intensity is: the skin-care compound fruit and plant anti-allergy extract is the extract of isatis root, dandelion, tetrandra root and kushen root, and the extract of isatis root and dandelion is the single glycyrrhizic acid dimethyl.
Effect example 2:
measurement of lactic acid stimulation:
20 healthy subjects, 10 men and 10 women, are selected by screening, and can cause skin irritation and burning pain to 10% lactic acid. There is no history of skin or systemic diseases, and no drug or cosmetic is applied during the test period.
Testing temperature (25+ to 1 ℃) and relative humidity of 40 to 45 percent, keeping the tested person in a stable state before testing, wiping the face with clear water at about 35 ℃, and then testing after sitting still for 30 min.
Respectively causing lactic acid stimulation on two sides of a cheek of a subject, respectively smearing distilled water and a skin-care composite fruit and plant anti-allergy extracting solution on the two sides of the cheek for comparison, and confirming that the side smeared with the skin-care composite fruit and plant anti-allergy extracting solution has relieved symptoms according to a comparison result.
Lactic acid stimulation is respectively caused on two sides of a cheek of a subject, single glycyrrhizic acid dimethyl and the skin-care fruit composite plant anti-allergy extracting solution are respectively coated on the two sides of the cheek for comparison, and according to a comparison result, the symptom relieving degree of the side coated with the skin-care composite fruit plant anti-allergy extracting solution is higher.
Effect example 3:
human body test effect:
20 healthy subjects, 10 men and women, were selected, each group contained 7 people with sensitive skin, had no history of skin or systemic diseases, and were not smeared with any drugs or cosmetics unrelated to the experiment during the period of the test.
Testing temperature (25+ to 1 ℃) and relative humidity of 40 to 45 percent, keeping the tested person in a stable state before testing, wiping the two arms with clear water at about 35 ℃, and then testing after sitting still for 30 min.
In the marked area (4 cm and 4cm) of the inner side of the arms of the two hands of the subject 5cm away from the base of the palm, through the standard area stimulated by the hot pepper, the skin in the standard area becomes red, 5ml of the single glycyrrhizic acid dimethyl in the comparative example 3 is smeared on the left arm, and the skin-care compound fruit and plant anti-allergy extracting solution is smeared on the right arm, so that the red phenomenon of the right arm is found to be short in eliminating time and high in relieving degree.
In combination with the test results of examples 1 to 3, the following conclusions can be drawn:
1. all tested groups can distinguish the effect difference of the distilled water and the skin-care composite fruit and plant anti-allergy extracting solution.
2. 73% of tested population can distinguish single prescription and skin-care composite fruit and plant anti-allergy extract product, and the skin-care composite fruit and plant anti-allergy extract product is considered to have obviously better effect than the single prescription.
3. The skin-care composite fruit and plant anti-allergy extract provided by the embodiment of the invention can effectively relieve the stimulation effect of the outside on the skin.
Effect example 4:
moisture retention effect fruit determination:
mmv (moisture measurement value) measurement reflects the hydration state of the skin, and the larger the value, the stronger the water-holding function of the skin stratum corneum.
The experimental method comprises the following steps: and analyzing and testing the hydration state and the percutaneous water loss condition of the skin by adopting an intelligent skin analyzer all-in-one machine.
1. 30 healthy subjects, 15 men and women, each with no history of skin or systemic diseases, were selected, and no drug or cosmetic was applied during the period of the test.
Testing temperature (25+ to 1 ℃) and relative humidity of 40 to 45 percent, keeping the tested person in a stable state before testing, wiping the two arms with clear water at about 35 ℃, and then testing after sitting still for 30 min.
The MMV value of the test area was measured at 0.5, 1 and 2 hours, respectively, by marking the area (4. 4cm) on the inner side of the arm of the subject at a distance of 5cm from the base of the palm, applying 1ml of the skin-care composite fruit-plant anti-allergy extract solution of example 2 to the left arm, and applying nothing to the right front arm as a blank control, and the results are shown in FIG. 2.
2. 30 healthy subjects, 15 men and women, each with no history of skin or systemic diseases, were selected, and no drug or cosmetic was applied during the period of the test.
Testing temperature (25+ to 1 ℃) and relative humidity of 40 to 45 percent, keeping the tested person in a stable state before testing, wiping the two arms with clear water at about 35 ℃, and then testing after sitting still for 30 min.
The MMV value of the test area was measured at 0.5, 1 and 2 hours, respectively, by marking an area (4. about.4 cm) on the inner side of the arm of the subject at a distance of 5cm from the base of the palm, applying 1ml of the extract solution of comparative example 1 to the left arm, and applying nothing to the right front arm as a blank, and the results are shown in FIG. 3.
3. 30 healthy subjects, 15 men and women, each with no history of skin or systemic diseases, were selected, and no drug or cosmetic was applied during the period of the test.
Testing temperature (25+ to 1 ℃) and relative humidity of 40 to 45 percent, keeping the tested person in a stable state before testing, wiping the two arms with clear water at about 35 ℃, and then testing after sitting still for 30 min.
The test area was marked at 5cm (4. multidot.4 cm) from the base of the palm on the inner side of the arm of the subject, 1ml of the extract solution of comparative example 2 was applied to the left arm, nothing was applied to the right front arm as a blank, and the MMV value of the test area was measured at 0.5, 1 and 2 hours, respectively, and the measurement results are shown in FIG. 4.
The above experimental results show that: the skin-care composite fruit and plant anti-allergy extracting solution disclosed by the embodiment of the invention has a good instant moisturizing effect, is remarkable in moisturizing effect, can reduce the loss of moisture content, and enhances the function of skin water.
The compound extract is extracted from various plant traditional Chinese medicinal materials and fruits, is safe and non-irritant, and has the functions of moisturizing, preventing and relieving sensitive skin allergy and inflammation. The components have synergistic effect, active ingredients in the extracting solution are fully utilized, so that the moisturizing, repairing and anti-allergy effects are fully exerted, and the skin-care washing liquid has wide application range and is suitable for skin-care washing products in various dosage forms such as cream, emulsion, facial mask liquid, skin-care water, essence, shampoo, shower gel, bath lotion and the like.
The embodiments of the present invention have been described in detail with reference to the accompanying drawings, but the present invention is not limited to the embodiments described above, and it will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the spirit and scope of the principles of the present invention.
Claims (5)
1. The skin-care composite fruit and plant anti-allergy extracting solution is characterized by comprising the following raw materials: radix Isatidis, radix Stephaniae Tetrandrae, Poria, radix Sophorae Flavescentis, herba Taraxaci, and fructus Actinidiae chinensis;
the mass ratio of the isatis root to the tetrandra root to the poria cocos to the radix sophorae flavescentis to the dandelion to the Chinese kiwi fruit is (1-5): (5-10): (2-5): (1-5): (1-3): (0.1-0.5).
2. A preparation method of a skin-care compound fruit and plant anti-allergy extracting solution, which is characterized in that the preparation method is based on the skin-care compound fruit and plant anti-allergy extracting solution of claim 1, and the preparation method comprises the following steps:
s1: mixing the five components of the isatis root, the tetrandra root, the poria cocos, the sophora flavescens root and the dandelion according to the proportion and the dosage, putting the mixture into a vacuum emulsifying pot, adding a solvent to soak the mixture for 1 to 1.5 hours, stirring the mixture at a speed of 15 revolutions per minute, and heating the mixture simultaneously, wherein the Chinese kiwi fruit is prefabricated separately;
s2: peeling the Chinese gooseberry in advance, putting the Chinese gooseberry into a wall breaking machine with the power of 1200W, adding a proper amount of pure water, stirring at a high speed for 3 minutes, stopping a motor, and then stirring at a high speed for 3 minutes to obtain Chinese gooseberry juice;
s3: when the temperature of the materials in the vacuum emulsifying pot is reduced to 40-45 ℃, adding the Chinese gooseberry juice, scouring the inner wall of the wall breaking machine cup with a proper amount of pure water, and pouring into the vacuum emulsifying pot;
s4: continuously stirring the materials in the vacuum emulsifying pot for 20 minutes at the rotating speed of 20 revolutions per minute;
s5: discharging, filtering with 150 mesh filter screen, and storing the decocted plant composite extract in a sealed container for use.
3. The method for preparing the skin-care composite fruit and plant anti-allergy extracting solution according to claim 2, wherein the solvent is selected from pure water, hexylene glycol and propylene glycol.
4. The preparation method of the skin-care composite fruit and plant anti-allergy extracting solution according to claim 3, wherein the mass ratio of the water, the hexanediol and the propylene glycol is (82-88): (0.5-1.0): (3-5).
5. The use of the skin care composite fruit and plant anti-allergy extract solution according to claim 1 in the preparation of cosmetics.
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