CN109695150A - 一种亲肤型抗紫外线真丝面料的制备方法 - Google Patents
一种亲肤型抗紫外线真丝面料的制备方法 Download PDFInfo
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Abstract
本发明公开了一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于硝酸锌水溶液中，过滤，洗涤，再浸泡于氨水中，调节温度，保温得到预覆盖蚕丝纤维；向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干得到氧化锌亲和抗紫外线抗菌蚕丝纤维。本发明所得蚕丝纤维具有优异的抗紫外性能，抑菌抗菌除臭，具有一定的保健功效。加入珍珠粉，进行微波处理后，真丝面料的表面更佳光滑，恢复了真丝纤维的良好的亲肤性能。
Description
技术领域
本发明涉及纺织技术领域，特别地，涉及一种亲肤型抗紫外线真丝面料的制备方法。
背景技术
随着生活水平的提高，人们越来越追求天然材料制品，如蚕丝，蚕丝是熟蚕结茧时分泌丝液凝固而成的连续长纤维，也称“天然丝”。它与羊毛一样，是人类最早利用的动物纤维之一，蚕丝纤维由两根呈三角形或半椭圆形的丝素外包丝胶组成，横截面呈椭圆形。蚕丝纤维为蛋白质纤维，丝胶和丝素是其主要组成部分，其中丝素约占3/4，丝胶约占1/4，蚕丝与人体的角质和胶原同为蛋白质，结构十分相近，因此，具有极好的人体生物相容性。蚕丝纤维材料由于出色的生物亲和性，成为人们的首选。但是蚕丝纤维的抗菌抗紫外线性较差；在中国专利CN104594025B（公开日2015.05.06）公开了一种氧化锌改性的抗紫外蚕丝的制备方法，将蚕丝去除杂脱胶后表面活化处理，浸渍于锌的前驱体溶液中，再浸泡于反应溶剂中反应，得到氢氧化锌覆盖的蚕丝，置于加热加湿的蒸汽中静置，取出水洗烘干，得到氧化锌改性的蚕丝，但亲和力差，经过浸泡洗涤后易流失，亟待解决。
发明内容
基于背景技术存在的技术问题，本发明提出了一种亲肤型抗紫外线真丝面料的制备方法。
本发明的技术方案如下：
一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于硝酸锌水溶液中，过滤，洗涤，再浸泡于氨水中，调节温度，保温得到预覆盖蚕丝纤维；
C、向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。
本发明将脱胶蚕丝经活化处理后，在蚕丝的表面生成一层氧化锌薄膜，将表面覆盖氧化锌薄膜的蚕丝浸入乙酸乙酯中，加入桑叶提取物与藏红花提取物，在甘草提取物的催化下，所形成共聚物具有疏水嵌段末端胆酸基团，可提高氧化锌在蚕丝表面的亲和力，稳定性好，经过浸泡洗涤后不易流失，另外共聚物的亲水嵌段包绕在外形成保护性外壳，不仅对蚕丝表面无损伤，吸湿性极好，穿着舒适，而且制备方法简便，成本低廉，适用于大规模生产。
优选的，C中，预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为5-10：25-40：0.3-0.5：0.05-0.1：1-3。
优选的，珍珠粉的加入量为预覆盖蚕丝纤维加入量的6-10%（重量比）。
优选的，C中，微波处理的时间为15-25min，微波处理的功率为600-800W。
优选的，B中，硫酸锌水溶液的质量分数为10-15%。
优选的，B中，浸渍时间为10-20min。
优选的，B中，调节温度至30-40℃，保温25-30min。
本发明的有益之处在于：
通过对B中相关工艺进行调整，使蚕丝表面生成的氧化锌薄膜更加均匀，而且不会对蚕丝产生伤害。
加入珍珠粉，进行微波处理后，真丝面料的表面更佳光滑，恢复了真丝纤维的良好的亲肤性能。
本发明所得的亲肤型真丝面料，不但具有良好的抗菌效果，而且长期穿着还具有一定的保健功效。
具体实施方式
实施例1
一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：
A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于质量分数为12%的硫酸锌水溶液中20min，过滤，洗涤，再浸泡于质量分数为 40%的氨水中，调节温度至35℃，保温30min，得到预覆盖蚕丝纤维；
C、按重量份向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理15min，微波处理的功率为800W，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。
预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为6：35：0.35：0.08：2。珍珠粉的加入量为预覆盖蚕丝纤维加入量的8%（重量比）。
实施例2
一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：
A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于质量分数为15%的硫酸锌水溶液中10min，过滤，洗涤，再浸泡于质量分数为 50%的氨水中，调节温度至40℃，保温25min，得到预覆盖蚕丝纤维；
C、按重量份向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理25min，微波处理的功率为750W，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。
预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为5：40：0.3：0.1：1。珍珠粉的加入量为预覆盖蚕丝纤维加入量的6%（重量比）。
实施例3
一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：
A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于质量分数为10%的硫酸锌水溶液中18min，过滤，洗涤，再浸泡于质量分数为 40%的氨水中，调节温度至38℃，保温28min，得到预覆盖蚕丝纤维；
C、按重量份向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理18min，微波处理的功率为720W，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。
预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为8：25：0.35：0.08：3。珍珠粉的加入量为预覆盖蚕丝纤维加入量的10%（重量比）。
实施例4
一种亲肤型抗紫外线真丝面料的制备方法，包括以下步骤：
A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于质量分数为13%的硫酸锌水溶液中12min，过滤，洗涤，再浸泡于质量分数为50%的氨水中，调节温度至38℃，保温18min，得到预覆盖蚕丝纤维；
C、按重量份向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理22min，微波处理的功率为780W，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。、
预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为10：25：0.5：0.05：3。珍珠粉的加入量为预覆盖蚕丝纤维加入量的7.5%（重量比）。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。
Claims (6)
1.一种亲肤型抗紫外线真丝面料的制备方法，其特征在于，包括以下步骤：
A、将蚕丝去除杂质后，脱胶，用去离子水洗涤，干燥得到脱胶蚕丝；
B、将脱胶蚕丝采用强氧化剂活化处理，然后浸渍于硝酸锌水溶液中，过滤，洗涤，再浸泡于氨水中，调节温度，保温得到预覆盖蚕丝纤维；
C、向预覆盖蚕丝纤维中加入乙酸乙酯混合均匀，加入桑叶提取物、藏红花提取物、甘草提取物混合，并加入珍珠粉，微波处理，过滤，洗涤，置于加热加湿的蒸汽中静置，水洗，烘干，并按照常规方法纺织得到亲肤型真丝纤维。
2.根据权利要求1所述亲肤型抗紫外线真丝面料的制备方法，其特征在于，C中，预覆盖蚕丝纤维、乙酸乙酯、桑叶提取物、藏红花提取物、甘草提取物的质量比为5-10：25-40：0.3-0.5：0.05-0.1：1-3；珍珠粉的加入量为预覆盖蚕丝纤维加入量的6-10%。
3.根据权利要求1所述亲肤型抗紫外线真丝面料的制备方法，其特征在于，C中，微波处理的时间为15-25min，微波处理的功率为600-800W。
4.根据权利要求1-3任一项所述亲肤型抗紫外线真丝面料的制备方法，其特征在于，B中，硫酸锌水溶液的质量分数为10-15%。
5.根据权利要求1-3任一项所述亲肤型抗紫外线真丝面料的制备方法，其特征在于，B中，浸渍时间为10-20min。
6.根据权利要求1-3任一项所述亲肤型抗紫外线真丝面料的制备方法，其特征在于，B中，调节温度至30-40℃，保温25-30min。
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