CN109680524A - A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method - Google Patents
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method Download PDFInfo
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- CN109680524A CN109680524A CN201811435431.5A CN201811435431A CN109680524A CN 109680524 A CN109680524 A CN 109680524A CN 201811435431 A CN201811435431 A CN 201811435431A CN 109680524 A CN109680524 A CN 109680524A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
- D06B3/18—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
- D06B3/185—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines below the bath level
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B7/00—Mercerising, e.g. lustring by mercerising
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C9/00—Singeing
- D06C9/02—Singeing by flame
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/14—De-sizing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0032—Determining dye recipes and dyeing parameters; Colour matching or monitoring
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8238—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye
- D06P3/8252—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye using dispersed and reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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Abstract
The present invention has separated a kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method, includes the following steps: to select fabric, singes, arrangements of desizing, kiering, bleaching, mercerising, pre-setting, dyeing and uvioresistant single bath process, fixation of soaping, is formed.Polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method according to the present invention has used cold dome method to carry out desizing and bleaching, can reduce influence of the temperature for fabric.And use benzyl alcohol that there is plasticising expanded performance to terylene as the carrier of low temperature dyeing, be conducive to the upper dye of neutral fixation reactive dye when a certain amount of, reasonable technique is taken to may be implemented to bathe polyester-cotton fabric one low temperature dyeing technique, and every dyefastness can achieve wearability.
Description
Technical field
The present invention relates to textile fabric dyeing technical field, especially a kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and anti-purple
Outer single bath process processing method.
Background technique
Polyester cotton is the important fabric of summer clothes, and dispersion/direct dyes can be used, dispersion/reducing dye, divide
Scattered/reactive dye are dyed.However, dispersion/direct dyeing fabric color fastness is poor, dispersion/reducing dye is usual
Two bath process need to be used, it is most widely used that Dyeing with Disperse/Reactive contaminates polyester-cotton fabric.
Technology of polyester-cotton fabric disperse/reactive dyeing can be carried out with a bath and two baths.Two bath process stable product quality is right
Without particular/special requirement, single bath process requires to select alkaline-proof disperse dyes and active dyestuff or common disperse dyes and neutrality solid dyestuff
Color reactive dyeing.As to energy-saving and emission-reduction, environmentally protective attention, Dyeing with Disperse/Reactive bathes polyester cotton one
Dyeing becomes the important topic of dyeing and finishing worker research, which breaks through conventional polyester-cotton blend two-bath dyeing method, make to disperse
Dyestuff and the bath of reactive dyeing one are completed, and dyeing cycle is shortened, energy-saving, save water resource, improve equipment benefit
With rate and worker's production efficiency.
When reactive dyeing, for the Covalent bonding together for promoting dyestuff and fiber, need to be added alkaline agent, but due to alkaline agent
Addition higher requirement is proposed to the alkali resistance of disperse dyes, therefore, the research of neutral fixation reactive dye is paid attention to.
When using neutral fixation reactive dyeing, it is not necessary that alkaline agent is added, in neutral conditions, directly promoted by improving dyeing temperature
Into the Covalent bonding together between dyestuff and cotton fiber, the dye-uptake and degree of fixation of dyestuff can be improved.So neutral fixation activity dye
Expect every excellent performance of existing traditional activated dyestuff, and production routine can be simplified, is particularly suitable for the one of the blended fabric such as polyester-cotton blend
Bath method dyeing.
But single bath process dip dyeing and dye gigging dyeing still need to carry out under conditions of high temperature and pressure, in consideration of it, exploring in the present invention
Polyester-cotton fabric realizes that dyeing and ultraviolet protection arrange a bath processing under cryogenic.
Summary of the invention
The object of the present invention is to provide a kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method, can
Low temperature dyeing and uvioresistant processing technology are bathed to polyester-cotton fabric one to realize, and every dyefastness can achieve taking
Energy.
In order to solve the above technical problems, the object of the present invention is achieved like this:
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method according to the present invention, including such as
Lower step:
Step S1, select fabric: the content of cotton is 35-60% in selected polyester-cotton fabric；
Step S2, it singes: respectively burning primary method using natural gas gassing frame front and back sides and selected fabric is burnt
Hair processing, when singing the flow of natural gas be 0.8-1 cubic metre per hour, speed is 100-120 meters per minute；Burner and weaving
Distance be 8-10mm, keep cloth cover temperature to be not higher than 180 DEG C, and cold water roller is installed above burner, dry behind burner,
Cropping temperature is maintained at 50 DEG C hereinafter, the door width of fabric shrinks and is no more than 2%；
Step S3, desizing: cold dome desizing method is used；Fabric Jing Guo previous step is padded into desizing liquid, bath temperature 45-50
DEG C, liquid carrying rate 90-100%, cold dome 16-24 hours, cold dome temperature was 25-30 DEG C；90-95 DEG C of cleaning solution is used after cold dome
Cleaning, and by supersonic oscillations, reuse cold water wash；
Step S4, kiering: padding kiering liquid for the fabric Jing Guo desizing, pick-up 70-80%, and in 95-100 DEG C
Processing processing 1-3min, is washed after kiering；
Step S5, it bleaches: being bleached using cold dome method；By the fabric after kiering, bleaching liquid is padded, liquid carrying rate is
90-100%, clot are simultaneously wrapped up with plastic cloth, and bank up 16-24h in rotation at a slow speed, are then washed again；
Step S6, mercerising: by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are 160- at room temperature
170g/L applies tension, expanding, elution, and the decatize lixiviating at 100-105 DEG C, 70-80 DEG C of washing, addition dosage is 3-6g/L
Acetum neutralize, roll compacting, drying；
Step S7, pre-setting: pre-setting temperature is 110-120 DEG C, and the pre-setting time is 20-30s；
Step S8, dyeing and uvioresistant single bath process arrange: will immerse to the fabric for crossing pre-setting according to the bath raio of 1:15-20
In dye liquor, room temperature enters dye, is warming up to 75-80 DEG C according to the heating rate of 0.7-1 DEG C/min, polyester fiber levelling agent is added
UNIVADINE TOP keeps 15-20min, is warming up to 130 DEG C according still further to the heating rate of 0.7-1 DEG C/min, keeps 30-
40min is cooled to 90-100 DEG C according still further to the rate of temperature fall of 2-3 DEG C/min, keeps 20-30min, then be cooled to 60-65 DEG C, take
Sample is to color；In the dye liquor, including disperse dyes, neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton are used
Levelling agent Goon301；The dosage of the ultraviolet absorbing agent HLF is 10-20% (o.w.f), and the dosage of benzyl alcohol is 20-
40ml/L, cotton are 0.5-2% (o.w.f) with the dosage of levelling agent Goon 301；The polyester fiber levelling agent being added
The amount of UNIVADINE TOP is 1-2g/L；The sodium chloride being added is 20-40g/L；
Step S9, it soaps fixation: will immerse in liquid of soaping and soap through hyperchromatic polyester-cotton fabric, 85-90 DEG C, processing
10-15min；
Step S10, be formed: the fabric that will be cleaned after dyeing is formed by foam in foaming machine and impregnates, passing through
Forming machine sizing；Contain setting agent and softening agent in foam, setting temperature is 120-130 DEG C, setting time 1.5-2min.
As a further illustration of the above scheme, in step S3, in the desizing liquid, efficient cold dome refining agent MCH-
119 content is 9-18g/L, and the content of BF-7658 enzyme is 1-2g/L, and the content of sodium hydroxide is 25-60g/L, and hydrogen peroxide is
12-20g/L；In the cleaning solution, the content for aoxidizing desizing agent is DL3-5g/L, and the content of chelated dispersants AB is 1-2g/
L, the content of liquid alkaline are 5-8g/L.
As a further illustration of the above scheme, in step S4, in the kiering liquid, RUCOGENAIL-S multi-function fine
The content for practicing agent is 1-3g/L, and the content of soda ash is 1-2g/L, and the content of hydrogen peroxide is 2-4g/L.
As a further illustration of the above scheme, in the bleaching liquid, the content of 100% hydrogen peroxide is in step S5
10-17g/L, the content of 35% sodium metasilicate are 40-65g/L, and the content for permeating scouring agent is 3-5g/L, and the content of sodium hydroxide is
8-10g/L。
As a further illustration of the above scheme, in step S9, in the liquid of soaping, the content of DMF-323S soaping agent
For 0.5-1.5g/L, the content of soap flakes is 1-2g/L, and the content of ALBAFIX ECO color fixing agent is 0.25-2g/L.
As a further illustration of the above scheme, used softening agent is Solusoft UP liq in step S10.
The beneficial effects of the present invention are: polyester-cotton blend Dyeing with Disperse/Reactive fixation according to the present invention and uvioresistant single bath process
Processing method has used cold dome method to carry out desizing and bleaching, can reduce influence of the temperature for fabric.And benzyl alcohol is used
Carrier as low temperature dyeing has plasticising expanded performance to terylene, is conducive to the upper of neutral fixation reactive dye when a certain amount of
Dye takes reasonable technique to may be implemented to bathe polyester-cotton fabric one low temperature dyeing technique, and every dyefastness can achieve
Wearability.
Specific embodiment
The present invention is further described combined with specific embodiments below.
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method according to the present invention, including such as
Lower step: selection fabric singes, the arrangement of desizing, kiering, bleaching, mercerising, pre-setting, dyeing and uvioresistant single bath process, soaps admittedly
Color, sizing.
In step S1 selection fabric, the content of cotton is 35-60% in selected polyester-cotton fabric.In selected fabric
Longitude and latitude uses polyester cotton blended yarns, specially polyester-cotton blend 65/35, polyester-cotton blend 55/45, polyester-cotton blend 40/60, used polyester cotton blended yarn
Fineness be 32-45 branch.Terylene can strongly decline, cotton fiber is in heat when meeting the sulfuric acid of concentrated hydrochloric acid and nitric acid and 75%
Diluted acid and cold concentrated acid can decompose, and cold diluted acid influences little.Polyester fiber is when meeting 10% sodium hydroxide and concentrated ammonia liquor under strength meeting
Drop, and cotton fiber is meeting alkali swelling.Terylene and cotton fiber not as do not dissolve in organic solvent.Polyester fiber can use dispersion, restore, no
Soluble azo dyestuff is dyed, and activity, direct, vulcanization, reduction, azoic dyeing can be used in cotton fiber.It washs
Synthetic fibre fiber dyeing needs dyed under the conditions of high temperature and pressure, carrier and thermosol, and cotton fiber can under the normal pressure slipped into
Row dyeing.
In step S2 singes, primary method is respectively burnt using natural gas gassing frame front and back sides, selected fabric is carried out
Singe processing, when singing the flow of natural gas be 0.8-1 cubic metre per hour, speed is 100-120 meters per minute；Burner with knit
The distance made is 8-10mm, and cloth cover temperature is kept to be not higher than 180 DEG C, and cold water roller is installed above burner, is blown behind burner
Wind, cropping temperature are maintained at 50 DEG C hereinafter, the door width of fabric shrinks and is no more than 2%.The purpose singed is defeathering villus and improvement
Pilling effect.The temperature of requirement villus when singing is greater than 485 DEG C, and cloth cover temperature is not higher than 180 DEG C, after otherwise singing
Fabric hand feel is coarse, contraction is excessive, strongly declines or even tendering.Polyester-cotton blend is singed appropriate to the occasion using gas singeing machine, and plate signeing is not
It preferably uses, generates black glue spot because terylene is easy melting and burning.It can be used in the measure for reducing cloth cover temperature
Cold water roller is installed, at least three cold water rollers prevent thin fabric from singing for reducing the temperature of cloth cover above burner
Degree.Another measure for reducing cloth cover temperature is that wind apparatus of cooking a meal is installed behind burner.During singing, strict control is needed
Technique, so that cropping temperature is kept for 50 DEG C or less.The quality requirement singed reaches 3-4 grades of quality standards, and door width, which must not shrink, to be surpassed
2% is crossed, is shunk excessively, the tearing brute force of fabric is decreased obviously.
In step S3 desizing, using cold dome desizing method.Fabric Jing Guo previous step is padded into desizing liquid, bath temperature is
45-50 DEG C, liquid carrying rate 90-100%, cold dome 16-24 hours, cold dome temperature was 25-30 DEG C；90-95 DEG C is used after cold dome
Cleaning solution cleaning, and by supersonic oscillations, reuse cold water wash.In used desizing liquid, efficient cold dome refining agent
The content of MCH-119 is 9-18g/L, and the content of BF-7658 enzyme is 1-2g/L, and the content of sodium hydroxide is 25-60g/L, dioxygen
Water is 12-20g/L.In used cleaning solution, the content for aoxidizing desizing agent is DL3-5g/L, and the content of chelated dispersants AB is
1-2g/L, the content of liquid alkaline are 5-8g/L.
Polyester-cotton fabric generally carries out warp thread using Starch Size to increase strength, if moved back when weaving prepares starching
It starches not clean, will affect later mercerising, dyeing and stamp, it is desirable that leftover slurry of the desizing rate on 80% or more, cloth is in 1% cloth
Weight is following.Using cold dome desizing, energy consumption when desizing in process of production can be reduced.Use efficient cold dome refining agent MCH-
119, have many advantages, such as low bubble, high alkali resistance, good dispersion.There is splendid fabric wetability and concise effect under alkaline condition
Fruit is resistant to the lye of sodium hydroxide 130g/L, can prevent from precipitating and condense.
In step S4 kiering, the fabric Jing Guo desizing is padded into kiering liquid, pick-up 70-80%, and in 95-100
Processing processing 1-3min, is washed after kiering in DEG C.In used kiering liquid, the multi-functional scouring agent of RUCOGEN AIL-S contains
Amount is 1-3g/L, and the content of soda ash is 1-2g/L, and the content of hydrogen peroxide is 2-4g/L.The multi-functional scouring agent of RUCOGEN AIL-S
A kind of scouring agent gone out by Rudoiph company, has splendid permeance property, and brilliant dispersibility can effectively go to decontaminate
Stain.
In step S5 bleaching, bleached using cold dome method.By the fabric after kiering, bleaching liquid, band liquid are padded
Rate is 90-100%, and clot is simultaneously wrapped up with plastic cloth, and banks up 16-24h in rotation at a slow speed, is then washed again.Rotation can at a slow speed
Fabric is avoided not bleach down when standing uneven.In used bleaching liquid, the content of 100% hydrogen peroxide is 10-17g/L,
The content of 35% sodium metasilicate is 40-65g/L, and the content for permeating scouring agent is 3-5g/L, and the content of sodium hydroxide is 8-10g/L.
In step S6 mercerising, by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are at room temperature
160-170g/L applies tension, expanding, elution, and the decatize lixiviating at 100-105 DEG C, 70-80 DEG C of washing, addition dosage is 3-
The acetum of 6g/L neutralizes, roll compacting, drying.
It is that will make a reservation for by the fabric of mercerising under the conditions of pre-setting temperature is 110-120 DEG C in step S7 pre-setting
The type time is 20-30s.
It is the bath by the fabric to pre-setting excessively according to 1:15-20 in step S8 dyeing and uvioresistant single bath process arrange
Than immersing in dye liquor, room temperature enters dye, is warming up to 75-80 DEG C according to the heating rate of 0.7-1 DEG C/min, polyester fiber level dyeing is added
Agent UNIVADINE TOP keeps 15-20min, is warming up to 130 DEG C according still further to the heating rate of 0.7-1 DEG C/min, keeps 30-
40min is cooled to 90-100 DEG C according still further to the rate of temperature fall of 2-3 DEG C/min, keeps 20-30min, then be cooled to 60-65 DEG C, take
Sample is to color；In the dye liquor, including disperse dyes, neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton are used
Levelling agent Goon301；The dosage of the ultraviolet absorbing agent HLF is 10-20% (o.w.f), and the dosage of benzyl alcohol is 20-
40ml/L, cotton are 0.5-2% (o.w.f) with the dosage of levelling agent Goon 301；The polyester fiber levelling agent being added
The amount of UNIVADINE TOP is 1-2g/L；The sodium chloride being added is 20-40g/L.
It soaps in fixation in step S9, is that will immerse in liquid of soaping to soap through hyperchromatic polyester-cotton fabric, 85-90
DEG C, handle 10-15min.In used liquid of soaping, the content of DMF-323S soaping agent is 0.5-1.5g/L, the content of soap flakes
For 1-2g/L, the content of ALBAFIX ECO color fixing agent is 0.25-2g/L.
In step S10 sizing, it is the fabric that will be cleaned after dyeing, is formed by foam and impregnates in foaming machine,
It is formed by forming machine；Contain setting agent and softening agent in foam, setting temperature is 120-130 DEG C, setting time 1.5-
2min.Used softening agent is Solusoft UP liq.After sizing, the fabric after dyeing sizing is subjected to clot and is packaged into
Library.
Embodiment one
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method involved in the present embodiment, including
Following steps: selection fabric singes, the arrangement of desizing, kiering, bleaching, mercerising, pre-setting, dyeing and uvioresistant single bath process, soaps
Fixation, sizing.
In step S1 selection fabric, the content of cotton is 35-60% in selected polyester-cotton fabric.In selected fabric
Longitude and latitude uses polyester cotton blended yarns, specially polyester-cotton blend 65/35, and the fineness of used polyester cotton blended yarn is 32.
In step S2 singes, primary method is respectively burnt using natural gas gassing frame front and back sides, selected fabric is carried out
Singe processing, when singing the flow of natural gas be 1 cubic metre per hour, speed be 120 meters per minute；Burner and woven distance
For 10mm, cloth cover temperature is kept to be not higher than 180 DEG C, and cold water roller is installed above burner, dried behind burner, cropping temperature
50 DEG C are maintained at hereinafter, the door width of fabric shrinks and is no more than 2%.
In step S3 desizing, using cold dome desizing method.Fabric Jing Guo previous step is padded into desizing liquid, bath temperature 50
DEG C, liquid carrying rate 100%, cold dome 24 hours, cooling temperature was 30 DEG C；It is cleaned, and used using 95 DEG C of cleaning solution after cold dome
Supersonic oscillations reuse cold water wash.In used desizing liquid, the content of efficient cold dome refining agent MCH-119 is 18g/
The content of L, BF-7658 enzyme is 2g/L, and the content of sodium hydroxide is 60g/L, hydrogen peroxide 20g/L.In used cleaning solution,
The content for aoxidizing desizing agent is DL5g/L, and the content of chelated dispersants AB is 2g/L, and the content of liquid alkaline is 8g/L.
In step S4 kiering, the fabric Jing Guo desizing is padded into kiering liquid, pick-up 80%, and in 100 DEG C
Reason processing 3min, is washed after kiering.In used kiering liquid, the content of the multi-functional scouring agent of RUCOGENAIL-S is 3g/L,
The content of soda ash is 2g/L, and the content of hydrogen peroxide is 4g/L.
In step S6 mercerising, by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are at room temperature
170g/L, applies tension, expanding, elution, the decatize lixiviating at 105 DEG C, and the acetum that dosage is 6g/L is added in 80 DEG C of washings
It neutralizes, roll compacting, drying.
In step S7 pre-setting, being will be by the fabric of mercerising under the conditions of pre-setting temperature is 120 DEG C, when pre-setting
Between be 30s.
It is that the fabric for crossing pre-setting will be soaked according to the bath raio of 1:20 in step S8 dyeing and uvioresistant single bath process arrange
Enter in dye liquor, room temperature enters dye, is warming up to 80 DEG C according to the heating rate of 1 DEG C/min, polyester fiber levelling agent UNIVADINE is added
TOP keeps 20min, is warming up to 130 DEG C according still further to the heating rate of 1 DEG C/min, 40min is kept, according still further to the drop of 3 DEG C/min
Warm rate is cooled to 100 DEG C, keeps 30min, then be cooled to 65 DEG C, samples to color；In the dye liquor, including disperse dyes,
Neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton levelling agent Goon 301；The ultraviolet absorbing agent
The dosage of HLF is 20% (o.w.f), and the dosage of benzyl alcohol is 40ml/L, and the dosage of cotton levelling agent Goon 301 is 2%
(o.w.f)；The amount for the polyester fiber levelling agent UNIVADINE TOP being added is 2g/L；The sodium chloride being added is 40g/L.
In staining procedure, the dyestuff being added is Disperse Red 3B and active red CN-3B.Wherein the content of Disperse Red 3B is
The content of 3% (o.w.f), active red CN-3B are 1% (o.w.f).
It soaps in fixation in step S9, is that will immerse in liquid of soaping to soap through hyperchromatic polyester-cotton fabric, 90 DEG C, place
Manage 15min.In used liquid of soaping, the content of DMF-323S soaping agent is 1.5g/L, and the content of soap flakes is 2g/L,
The content of ALBAFIX ECO color fixing agent is 2g/L.
In step S10 sizing, it is the fabric that will be cleaned after dyeing, is formed by foam and impregnates in foaming machine,
It is formed by forming machine；Contain setting agent and softening agent in foam, setting temperature is 130 DEG C, setting time 2min.Made
Softening agent is SolusoftUP liq.After sizing, the fabric after dyeing sizing is subjected to clot and is packed and stored.
Embodiment two
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method involved in the present embodiment, including
Following steps: selection fabric singes, the arrangement of desizing, kiering, bleaching, mercerising, pre-setting, dyeing and uvioresistant single bath process, soaps
Fixation, sizing.
In step S1 selection fabric, the content of cotton is 35-60% in selected polyester-cotton fabric.In selected fabric
Longitude and latitude uses polyester cotton blended yarns, specially polyester-cotton blend 55/45, and the fineness of used polyester cotton blended yarn is 40.
In step S2 singes, primary method is respectively burnt using natural gas gassing frame front and back sides, selected fabric is carried out
Singe processing, when singing the flow of natural gas be 1 cubic metre per hour, speed be 110 meters per minute；Burner and woven distance
For 9mm, cloth cover temperature is kept to be not higher than 180 DEG C, and cold water roller is installed above burner, dried behind burner, cropping temperature
50 DEG C are maintained at hereinafter, the door width of fabric shrinks and is no more than 2%.
In step S3 desizing, using cold dome desizing method.Fabric Jing Guo previous step is padded into desizing liquid, bath temperature 50
DEG C, liquid carrying rate 95, cold dome 20 hours, cooling temperature was 28 DEG C；It is cleaned after cold dome using 93 DEG C of cleaning solution, and uses ultrasound
Wave oscillation, reuses cold water wash.In used desizing liquid, the content of efficient cold dome refining agent MCH-119 is 15g/L, BF-
The content of 7658 enzymes is 1.5g/L, and the content of sodium hydroxide is 40g/L, hydrogen peroxide 16g/L.In used cleaning solution, oxygen
The content for changing desizing agent is DL45g/L, and the content of chelated dispersants AB is 1.5/L, and the content of liquid alkaline is 6g/L.
In step S4 kiering, the fabric Jing Guo desizing is padded into kiering liquid, pick-up 75%, and handle in 95 DEG C
1-3min is handled, is washed after kiering.In used kiering liquid, the content of the multi-functional scouring agent of RUCOGENAIL-S is 2g/L,
The content of soda ash is 1.5g/L, and the content of hydrogen peroxide is 3g/L.
In step S6 mercerising, by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are at room temperature
165g/L, applies tension, expanding, elution, the decatize lixiviating at 100 DEG C, and the acetum that dosage is 5g/L is added in 75 DEG C of washings
It neutralizes, roll compacting, drying.
In step S7 pre-setting, being will be by the fabric of mercerising under the conditions of pre-setting temperature is 115 DEG C, when pre-setting
Between be 25s.
It is that the fabric for crossing pre-setting will be soaked according to the bath raio of 1:18 in step S8 dyeing and uvioresistant single bath process arrange
Enter in dye liquor, room temperature enters dye, is warming up to 80 DEG C according to the heating rate of 0.7 DEG C/min, polyester fiber levelling agent is added
UNIVADINE TOP keeps 18min, is warming up to 130 DEG C according still further to the heating rate of 0.7 DEG C/min, keeps 35min, according still further to
The rate of temperature fall of 2.5 DEG C/min is cooled to 95 DEG C, keeps 25min, then be cooled to 63 DEG C, samples to color；In the dye liquor, packet
Include disperse dyes, neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton levelling agent Goon 301；Described
The dosage of ultraviolet absorbing agent HLF is 15% (o.w.f), and the dosage of benzyl alcohol is 30ml/L, and cotton is with levelling agent Goon's 301
Dosage is 1% (o.w.f)；The amount for the polyester fiber levelling agent UNIVADINE TOP being added is 1.5g/L；The chlorination being added
Sodium is 30g/L.
In staining procedure, the dyestuff being added is the golden yellow E-TD and active yellow CN-EX of dispersion.Wherein disperse golden yellow E-TD
Content be 2% (o.w.f), the content of active yellow CN-EX is 2% (o.w.f).
It soaps in fixation in step S9, is that will immerse in liquid of soaping to soap through hyperchromatic polyester-cotton fabric, 85 DEG C, place
Manage 13min.In used liquid of soaping, the content of DMF-323S soaping agent is 1g/L, and the content of soap flakes is 1.5g/L,
The content of ALBAFIX ECO color fixing agent is 1.5g/L.
In step S10 sizing, it is the fabric that will be cleaned after dyeing, is formed by foam and impregnates in foaming machine,
It is formed by forming machine；Contain setting agent and softening agent in foam, setting temperature is 120 DEG C, setting time 1.5min.Institute
The softening agent used is Solusoft UP liq.After sizing, the fabric after dyeing sizing is subjected to clot and is packed and stored.
Embodiment three
A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method involved in the present embodiment, including
Following steps: selection fabric singes, the arrangement of desizing, kiering, bleaching, mercerising, pre-setting, dyeing and uvioresistant single bath process, soaps
Fixation, sizing.
In step S1 selection fabric, the content of cotton is 35-60% in selected polyester-cotton fabric.In selected fabric
Longitude and latitude uses polyester cotton blended yarns, specially polyester-cotton blend 40/60, and the fineness of used polyester cotton blended yarn is 45.
In step S2 singes, primary method is respectively burnt using natural gas gassing frame front and back sides, selected fabric is carried out
Singe processing, when singing the flow of natural gas be 0.8 cubic metre per hour, speed be 100 meters per minute；Burner and it is woven away from
From for 8mm, keeps cloth cover temperature to be not higher than 180 DEG C, and cold water roller is installed above burner, dry behind burner, cropping temperature
Degree is maintained at 50 DEG C hereinafter, the door width of fabric shrinks and is no more than 2%.
In step S3 desizing, using cold dome desizing method.Fabric Jing Guo previous step is padded into desizing liquid, bath temperature 45
DEG C, liquid carrying rate 90%, cold dome 16 hours, cooling temperature was 25 DEG C；It is cleaned, is reused super using 90 DEG C of cleaning solution after cold dome
Sonication reuses cold water wash.In used desizing liquid, the content of efficient cold dome refining agent MCH-119 is 9g/L,
The content of BF-7658 enzyme is 1g/L, and the content of sodium hydroxide is 25g/L, hydrogen peroxide 12g/L.In used cleaning solution, oxygen
The content for changing desizing agent is DL3g/L, and the content of chelated dispersants AB is 1g/L, and the content of liquid alkaline is 5g/L.
In step S4 kiering, the fabric Jing Guo desizing is padded into kiering liquid, pick-up 70%, and handle in 95 DEG C
1min is handled, is washed after kiering.In used kiering liquid, the content of the multi-functional scouring agent of RUCOGENAIL-S is 1g/L, pure
The content of alkali is 1g/L, and the content of hydrogen peroxide is 2g/L.
In step S6 mercerising, by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are at room temperature
160g/L, applies tension, expanding, elution, the decatize lixiviating at 100 DEG C, and the acetum that dosage is 3g/L is added in 70 DEG C of washings
It neutralizes, roll compacting, drying.
In step S7 pre-setting, being will be by the fabric of mercerising under the conditions of pre-setting temperature is 110 DEG C, when pre-setting
Between be 20s.
It is that the fabric for crossing pre-setting will be soaked according to the bath raio of 1:15 in step S8 dyeing and uvioresistant single bath process arrange
Enter in dye liquor, room temperature enters dye, is warming up to 75 DEG C according to the heating rate of 0.7 DEG C/min, polyester fiber levelling agent is added
UNIVADINE TOP keeps 15min, is warming up to 130 DEG C according still further to the heating rate of 0.7 DEG C/min, keeps 30min, according still further to
The rate of temperature fall of 2 DEG C/min is cooled to 90 DEG C, keeps 20-30min, then be cooled to 60 DEG C, samples to color；In the dye liquor,
Including disperse dyes, neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton levelling agent Goon 301；It is described
The dosage of ultraviolet absorbing agent HLF be 10% (o.w.f), the dosage of benzyl alcohol is 20ml/L, cotton levelling agent Goon 301
Dosage be 0.5% (o.w.f)；The amount for the polyester fiber levelling agent UNIVADINE TOP being added is 1g/L；The chlorine being added
Change sodium is 20g/L.
In staining procedure, the dyestuff being added is Disperse Blue 2BLN and reactive blue CNMG.Wherein Disperse Blue 2BLN contains
Amount is 1% (o.w.f), and the content of reactive blue CNMG is 3% (o.w.f).
It soaps in fixation in step S9, is that will immerse in liquid of soaping to soap through hyperchromatic polyester-cotton fabric, 85 DEG C, place
Manage 10min.In used liquid of soaping, the content of DMF-323S soaping agent is 0.5g/L, and the content of soap flakes is 1g/L,
The content of ALBAFIX ECO color fixing agent is 0.25g/L.
In step S10 sizing, it is the fabric that will be cleaned after dyeing, is formed by foam and impregnates in foaming machine,
It is formed by forming machine；Contain setting agent and softening agent in foam, setting temperature is 120 DEG C, setting time 1.5min.Institute
The softening agent used is Solusoft UP liq.After sizing, the fabric after dyeing sizing is subjected to clot and is packed and stored.
Comparative example
Polyester-cotton fabric dispersion/activity the fixation and uvioresistant single bath process processing method that the present embodiment is related to, are before passing through
Polyester-cotton fabric that treated, room temperature enter dye, and bath raio 1:30 is warming up to 80 DEG C with 3 DEG C/min rate, then with 1.5 DEG C/min speed
Rate is warming up to 130 DEG C, keeps the temperature 40min；70 DEG C are cooled to the rate of 3 DEG C/min, washes, soaps after taking out sample, is dried.Dye
The disperse dyes disperse red being added in liquid is 1% (o.w.f), the neutral active fixing dyes active red CN-3BYL being added
3% (o.w.f).Middle bath raio of soaping is 1:30, and the soaping agent of addition is 2g/L, and temperature of soaping is 95 DEG C, and the processing time is
15min。
Embodiment one to three and comparative example test ultraviolet protection performance, apparent shade depth K/S value, color fastness.
Wherein, it ultraviolet protection performance: according to AS/NZS 4399-1996 " testing standard of textile resistance to ultraviolet radiation energy ", adopts
With the ultraviolet ray transmissivity and UPF value of polyamide fibre after the measurement dyeing of UV-2000F ultraviolet protection performance tester, each sample exists
Different position finding 8 times, is averaged.Apparent shade depth K/S value: it is measured on Color-Eye 7000A colour photometer, test light
Source D65, field angle are 10 °, sample testing 4 times, are averaged.Color fastness to washing: by GB/T 3921.1-2008, " textile is resistance to
Wash color fastness test method " measurement.Colour fastness to rubbing: " the textile colour fastness to rubbing test side GB/T 3920-2008 is pressed
Method " measurement.
The dyefastness and UPF index of 1 polyester-cotton fabric of table
As can be seen from the above table, surpass 4 grades in terms of color fastness, meet requirement of the clothes for color fastness.And UPF
Value has been more than 50, meets requirement of the fabric for UV resistance.And two indexs are superior to comparative example.
Each 3 pieces of the dyeing sample of comparative example and embodiment one to three are taken, the dyeing K/S value and standard deviation S of fabric are measured.
K/S the and S value of 2 polyester-cotton fabric of table
As can be seen from the above table, embodiment one to three has good level-dyeing property, is better than comparative example.
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be within the scope of protection determined by the claims.
Claims (6)
1. a kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method, which is characterized in that including walking as follows
It is rapid:
Step S1, select fabric: the content of cotton is 35-60% in selected polyester-cotton fabric；
Step S2, it singes: respectively burning primary method using natural gas gassing frame front and back sides and the place that singes is carried out to selected fabric
Reason, when singing the flow of natural gas be 0.8-1 cubic metre per hour, speed is 100-120 meters per minute；Burner and it is woven away from
From for 8-10mm, keeps cloth cover temperature to be not higher than 180 DEG C, and cold water roller is installed above burner, dry behind burner, cropping
Temperature is maintained at 50 DEG C hereinafter, the door width of fabric shrinks and is no more than 2%；
Step S3, desizing: cold dome desizing method is used；Fabric Jing Guo previous step is padded into desizing liquid, bath temperature is 45-50 DEG C,
Liquid carrying rate is 90-100%, and cold dome 16-24 hours, cold dome temperature was 25-30 DEG C；It is clear using 90-95 DEG C of cleaning solution after cold dome
It washes, and by supersonic oscillations, reuses cold water wash；
Step S4, kiering: the fabric Jing Guo desizing is padded into kiering liquid, pick-up 70-80%, and is handled in 95-100 DEG C
1-3min is handled, is washed after kiering；
Step S5, it bleaches: being bleached using cold dome method；By the fabric after kiering, bleaching liquid, liquid carrying rate 90- are padded
100%, clot is simultaneously wrapped up with plastic cloth, and banks up 16-24h in rotation at a slow speed, is then washed again；
Step S6, mercerising: by the polyester-cotton fabric after bleaching, alkali immerging, the concentration of lye are 160-170g/ at room temperature
L, applies tension, expanding, elution, the decatize lixiviating at 100-105 DEG C, and the acetic acid that dosage is 3-6g/L is added in 70-80 DEG C of washing
Solution neutralizes, roll compacting, drying；
Step S7, pre-setting: pre-setting temperature is 110-120 DEG C, and the pre-setting time is 20-30s；
Step S8, dyeing and uvioresistant single bath process arrange: will immerse dye liquor according to the bath raio of 1:15-20 to the fabric for crossing pre-setting
In, room temperature enters dye, is warming up to 75-80 DEG C according to the heating rate of 0.7-1 DEG C/min, polyester fiber levelling agent is added
UNIVADINE TOP keeps 15-20min, is warming up to 130 DEG C according still further to the heating rate of 0.7-1 DEG C/min, keeps 30-
40min is cooled to 90-100 DEG C according still further to the rate of temperature fall of 2-3 DEG C/min, keeps 20-30min, then be cooled to 60-65 DEG C, take
Sample is to color；In the dye liquor, including disperse dyes, neutral fixation reactive dye, ultraviolet absorbing agent HLF, benzyl alcohol, cotton are used
Levelling agent Goon 301；The dosage of the ultraviolet absorbing agent HLF is 10-20% (o.w.f), and the dosage of benzyl alcohol is 20-
40ml/L, cotton are 0.5-2% (o.w.f) with the dosage of levelling agent Goon 301；The polyester fiber levelling agent being added
The amount of UNIVADINE TOP is 1-2g/L；The sodium chloride being added is 20-40g/L；
Step S9, it soaps fixation: will immerse in liquid of soaping and soap through hyperchromatic polyester-cotton fabric, 85-90 DEG C, handle 10-
15min；
Step S10, be formed: the fabric that will be cleaned after dyeing is formed by foam in foaming machine and impregnates, and is passing through sizing
Machine sizing；Contain setting agent and softening agent in foam, setting temperature is 120-130 DEG C, setting time 1.5-2min.
2. polyester-cotton blend Dyeing with Disperse/Reactive fixation as described in claim 1 and uvioresistant single bath process processing method, feature exist
In in step S3, in the desizing liquid, the content of efficient cold dome refining agent MCH-119 is 9-18g/L, and BF-7658 enzyme contains
Amount is 1-2g/L, and the content of sodium hydroxide is 25-60g/L, hydrogen peroxide 12-20g/L；In the cleaning solution, desizing is aoxidized
The content of agent is DL3-5g/L, and the content of chelated dispersants AB is 1-2g/L, and the content of liquid alkaline is 5-8g/L.
3. polyester-cotton blend Dyeing with Disperse/Reactive fixation as described in claim 1 and uvioresistant single bath process processing method, feature exist
In in step S4, in the kiering liquid, the content of the multi-functional scouring agent of RUCOGENAIL-S is 1-3g/L, the content of soda ash
For 1-2g/L, the content of hydrogen peroxide is 2-4g/L.
4. polyester-cotton blend Dyeing with Disperse/Reactive fixation as described in claim 1 and uvioresistant single bath process processing method, feature exist
In in step S5, in the bleaching liquid, the content of 100% hydrogen peroxide is 10-17g/L, and the content of 35% sodium metasilicate is 40-
65g/L, the content for permeating scouring agent is 3-5g/L, and the content of sodium hydroxide is 8-10g/L.
5. polyester-cotton blend Dyeing with Disperse/Reactive fixation as described in claim 1 and uvioresistant single bath process processing method, feature exist
In in step S9, in the liquid of soaping, the content of DMF-323S soaping agent is 0.5-1.5g/L, and the content of soap flakes is 1-2g/
The content of L, ALBAFIX ECO color fixing agent is 0.25-2g/L.
6. polyester-cotton blend Dyeing with Disperse/Reactive fixation as described in claim 1 and uvioresistant single bath process processing method, feature exist
In in step S10, used softening agent is SolusoftUP liq.
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Application publication date: 20190426 |