CN112359463A - Preparation method of ultraviolet-resistant shirt fabric - Google Patents
Preparation method of ultraviolet-resistant shirt fabric Download PDFInfo
- Publication number
- CN112359463A CN112359463A CN202011196283.3A CN202011196283A CN112359463A CN 112359463 A CN112359463 A CN 112359463A CN 202011196283 A CN202011196283 A CN 202011196283A CN 112359463 A CN112359463 A CN 112359463A
- Authority
- CN
- China
- Prior art keywords
- ultraviolet
- resistant
- steps
- following
- agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 46
- 238000004043 dyeing Methods 0.000 claims abstract description 30
- 229920000742 Cotton Polymers 0.000 claims abstract description 24
- 238000009999 singeing Methods 0.000 claims abstract description 17
- 229920004933 Terylene® Polymers 0.000 claims abstract description 16
- 239000005020 polyethylene terephthalate Substances 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 14
- 239000002250 absorbent Substances 0.000 claims abstract description 13
- 230000002745 absorbent Effects 0.000 claims abstract description 13
- 238000010025 steaming Methods 0.000 claims abstract description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 36
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 22
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 16
- 239000002270 dispersing agent Substances 0.000 claims description 12
- 238000007493 shaping process Methods 0.000 claims description 11
- 235000017550 sodium carbonate Nutrition 0.000 claims description 11
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 11
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 10
- 238000007670 refining Methods 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 239000003513 alkali Substances 0.000 claims description 7
- 229920000728 polyester Polymers 0.000 claims description 7
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 6
- 239000004902 Softening Agent Substances 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 238000002203 pretreatment Methods 0.000 claims description 5
- 238000009991 scouring Methods 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 3
- 239000003345 natural gas Substances 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 238000005096 rolling process Methods 0.000 claims description 3
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- 239000013527 degreasing agent Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 8
- 238000002834 transmittance Methods 0.000 abstract description 6
- 206010002198 Anaphylactic reaction Diseases 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract description 4
- 208000003455 anaphylaxis Diseases 0.000 abstract description 4
- 238000004513 sizing Methods 0.000 abstract description 4
- 230000018044 dehydration Effects 0.000 abstract description 2
- 238000006297 dehydration reaction Methods 0.000 abstract description 2
- 238000005517 mercerization Methods 0.000 abstract description 2
- 239000000985 reactive dye Substances 0.000 abstract description 2
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 238000005406 washing Methods 0.000 description 3
- 206010015150 Erythema Diseases 0.000 description 2
- 239000000986 disperse dye Substances 0.000 description 2
- 231100000321 erythema Toxicity 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 206010019345 Heat stroke Diseases 0.000 description 1
- 229920000433 Lyocell Polymers 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 231100000086 high toxicity Toxicity 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000037072 sun protection Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B7/00—Mercerising, e.g. lustring by mercerising
- D06B7/08—Mercerising, e.g. lustring by mercerising of fabrics of indefinite length
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C9/00—Singeing
- D06C9/02—Singeing by flame
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention relates to a preparation method of fabric, in particular to a preparation method of ultraviolet-resistant shirt fabric. The process route is as follows: grey cloth preparation → pretreatment boiling-off → sizing and drying → singeing → mercerization → high temperature dyeing terylene + ultraviolet absorbent for terylene, one-bath finishing → reactive dye dyeing cotton → dehydration scutching → sizing and drying → soft finishing + ultraviolet absorbent for cotton, one-bath finishing → can steaming. The fabric prepared by the method has no toxicity, no stimulation to skin, no anaphylactic reaction of human body, no influence on the performances of the fabric such as color light, color fastness, strong hand feeling and the like, has good absorption effect on ultraviolet rays (especially ultraviolet rays with the wave band of 280 plus 400 nm), has ultraviolet transmittance lower than 4 percent after being washed for 50 times, and can reach the level of 50+ ultraviolet shielding coefficient UPF.
Description
Technical Field
The invention relates to a preparation method of fabric, in particular to a preparation method of ultraviolet-resistant shirt fabric.
Background
The principle of the ultraviolet-resistant fabric is that the ultraviolet absorbent mixed in the fabric absorbs high-energy ultraviolet rays to convert the ultraviolet rays into low energy and changes low-energy heat energy or electromagnetic waves with shorter wavelength, so that the harm of the ultraviolet rays to human bodies and fabrics is eliminated, the reflection and scattering effects of the ultraviolet rays on the fabrics can be increased by using the ultraviolet reflecting agent, the fabrics are prevented from being transmitted, and the fabric has the performances of heatstroke prevention, heat insulation and solar radiation reduction.
The national standard provides that the fabric with UPF less than 30% and UVA transmittance of 75% cannot be called as an ultraviolet-proof fabric product, the ultraviolet sun protection degree unit is an UPF value, and the function of the ultraviolet-proof fabric is calculated by the method that UPF is the minimum irradiation amount of erythema generated under the condition that the skin is not protected/the minimum irradiation amount of erythema generated under the condition that the skin is protected, namely, the fabric can bear several times of sunlight irradiation time when a person wears the piece of clothes.
The currently marketed anti-ultraviolet fabric mainly has the following problems:
1) the finished fabric has high toxicity and irritation to skin, and sensitive physique and human bodies can generate anaphylactic reaction;
2) the performances of the fabric such as color light, color fastness, strong hand feeling and the like are poor;
3) the ultraviolet-resistant effect is weakened or even disappeared after washing for several times without water washing, and the ultraviolet-resistant effect is poor.
Therefore, the process needs to be improved, and the quality of the ultraviolet-resistant fabric is improved.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a preparation method of an anti-ultraviolet shirt fabric, the prepared fabric is non-toxic and non-irritant to skin, does not cause anaphylactic reaction to human bodies, does not influence the color light, color fastness and hand feeling strength performance of the fabric, has good absorption effect on ultraviolet rays, and still has good anti-ultraviolet effect after being washed for many times.
The preparation method of the ultraviolet-resistant shirt fabric comprises the following process routes: grey cloth preparation → pretreatment boiling-off → sizing and drying → singeing → mercerization → high temperature dyeing terylene + ultraviolet absorbent for terylene, one-bath finishing → reactive dye dyeing cotton → dehydration scutching → sizing and drying → soft finishing + ultraviolet absorbent for cotton, one-bath finishing → can steaming.
The method comprises the following specific steps:
(1) preparing a grey fabric: the polyester-cotton interwoven plain cloth is composed of 90% of terylene and 10% of cotton fiber, the gram weight is 210g/m, the width is 165cm, and the cloth is distributed for each cylinder by 800-1000 meters;
(2) pre-treatment scouring: treating the fabric by using a high-temperature high-pressure overflow dyeing machine and using a mixed solution of soda ash, hydrogen peroxide, a refining agent, a deoiling agent and a chelating dispersant;
(3) shaping and drying;
(4) singeing: singeing by adopting a natural gas singeing machine at the speed of 80-100 m/min;
(5) mercerizing;
(6) dyeing:
the polyester dyeing formula comprises: disperse blue: 0.25%, disperse violet: 0.03 percent, 1g/l of acetic acid, 2-4g/l of ultraviolet absorbent for terylene and 2g/l of high-temperature leveling agent;
the dyeing process comprises the following steps: keeping the temperature at 130 ℃ for 30-50 min;
the cotton fiber dyeing formula comprises the following steps: active red: 0.05 percent of anhydrous sodium sulphate, 20g/l of anhydrous sodium sulphate and 10g/l of sodium carbonate;
the dyeing process comprises the following steps: treating at 60 deg.C for 30-50 min;
the soaping process comprises the following steps: treating soaping agent 1g/l at 80 deg.C for 20 min;
(7) dehydrating and scutching;
(8) shaping and drying;
(9) softening and finishing: the temperature is 150 ℃, the vehicle speed is 30-50m/min, the ultraviolet resistant finishing agent for cotton is 5-20g/l, and the hydrophilic softening agent is 10 g/l;
(10) decating;
(11) and (5) inspecting, packaging and rolling.
Wherein:
in the step (2), the pre-treatment scouring specifically comprises the following steps: treating the fabric by using a high-temperature high-pressure overflow dyeing machine and using a mixed solution of soda ash, hydrogen peroxide, a refining agent, a deoiling agent and a chelating dispersant; 2g/l of soda ash, 3g/l of hydrogen peroxide, 1g/l of non-ionic refining agent, 1g/l of alkali-resistant high-temperature-resistant degreaser and 3g/l of chelating dispersant, wherein the treatment temperature is 100 ℃, and the treatment time is 30 min. The non-ionic refining agent is DR-N6, the alkali-resistant and high-temperature-resistant deoiling agent is alkali-resistant and high-temperature-resistant deoiling agent 101, and the chelating dispersant is DR-99.
And (3) shaping and drying at the temperature of 170 ℃ at the speed of 40 m/min.
In the step (4), the singeing adopts a forward singeing method and a reverse singeing method.
In the step (5), the mercerizing is as follows: mercerizing is carried out by adopting caustic soda solution with the concentration of 180 g/l.
In the step (6), the ultraviolet absorbent for terylene is HF-E.
And (8) shaping and drying at the temperature of 170 ℃ at the speed of 50 m/min.
In the step (9), the ultraviolet-resistant finishing agent for cotton is UV-S, and the hydrophilic softening agent is DR-1.
In the step (10), the decating is as follows: treating with Italian KD series pot steaming machine at 160 deg.C under 0.6bar for 90s from inside to outside and 90s from outside to inside, and cooling for 150 s.
Compared with the prior art, the invention has the following beneficial effects:
1. the ultraviolet absorbent for terylene is added when the disperse dye is used for dyeing, and the ultraviolet finishing agent for cotton is added when the disperse dye is used for shaping and soft finishing. The conventional process is that the ultraviolet finishing agent is added during dyeing, so that the dyed color and light can be influenced, the standard sample is not met, and the dyed color is uneven due to improper operation. By improving the process, the traditional ultraviolet resistant surface is solved
2. The ultraviolet-proof fabric finished by the process has good absorption, conversion, reflection and scattering effects on ultraviolet rays (particularly UV-A and UV-B) in the 280-plus-400 nm wave band, is nontoxic and nonirritating to skin, does not cause anaphylactic reaction to human bodies, and does not influence the performances of the fabric such as color light, color fastness, strong hand feeling and the like.
2. The polyester/cotton, polyester/viscose, polyester/tencel fabrics finished by the method have good absorption effect on 280-plus 400nm ultraviolet rays, particularly UV-A and UV-B, the ultraviolet transmittance is still lower than 4% after washing for 50 times, and the ultraviolet shielding coefficient UPF can reach the level of 50 +.
Detailed Description
The present invention is further illustrated by, but is not limited to, the following examples.
All the starting materials used in the examples are commercially available, except where otherwise indicated.
Example 1
The preparation method of the ultraviolet-resistant shirt fabric comprises the following specific steps:
(1) preparing a grey fabric: the polyester-cotton interwoven plain cloth is composed of 90% of terylene and 10% of cotton fibers, the gram weight is 210g/m, the width is 165cm, and the cloth is distributed for each cylinder by 900 meters.
(2) Pre-treatment scouring: and (3) treating the fabric by using a high-temperature high-pressure overflow dyeing machine and using a mixed solution of soda ash, hydrogen peroxide, a refining agent, a deoiling agent and a chelating dispersant. 2g/l of soda ash, 3g/l of hydrogen peroxide, 1g/l of non-ionic refining agent (DR-N6), 1g/l of alkali-resistant high-temperature-resistant deoiling agent (101) and 3g/l of chelating dispersant (DR-99). The treatment temperature is 100 ℃, and the treatment time is 30 min.
(3) Shaping and drying: the temperature is 170 ℃, and the vehicle speed is 40 m/min.
(4) White blank singeing: a natural gas singeing machine-positive-negative singeing method is adopted, and the speed is 100 m/min.
(5) Mercerizing: mercerizing is carried out by adopting caustic soda solution with the concentration of 180 g/l.
(6) Designing a dyeing formula:
the polyester dyeing formula comprises: disperse blue: 0.25%, disperse violet: 0.03 percent, 1g/l of acetic acid, 2g/l of ultraviolet absorbent (HF-E) for terylene and 2g/l of high-temperature leveling agent.
The dyeing process comprises the following steps: keeping the temperature at 130 ℃ for 30 min.
The cotton fiber dyeing formula comprises the following steps: active red: 0.05 percent, 20g/l of anhydrous sodium sulphate and 10g/l of sodium carbonate.
The dyeing process comprises the following steps: treating at 60 deg.C for 30 min.
The soaping process comprises the following steps: soaping agent 1g/l, and treating at 80 deg.C for 20 min.
(7) Dehydrating and scutching;
(8) shaping and drying: the temperature is 170 ℃, and the vehicle speed is 50 m/min.
(9) Softening and finishing: the temperature is 150 ℃, the vehicle speed is 40m/min, the ultraviolet resistant finishing agent (UV-S) for cotton is 10g/l, and the hydrophilic softening agent (DR-1) is 10 g/l.
(10) Decating: treating with Italian KD series pot steaming machine at 160 deg.C under 0.6bar for 90s from inside to outside and 90s from outside to inside, and cooling for 150 s.
(11) And (5) inspecting, packaging and rolling.
Example 2
The preparation method of the ultraviolet-resistant shirt fabric is the same as that in example 1, and is different from the following steps:
in the step (1), 800 meters of cloth is distributed for each cylinder.
In the step (4), the vehicle speed is 80 m/min.
In the step (6), 1g/l of ultraviolet absorbent (HF-E) for terylene; keeping the temperature of the polyester dyeing process for 40 min; and (5) carrying out heat preservation for 40min by using a cotton fiber dyeing process.
In the step (9), the anti-ultraviolet finishing agent (UV-S) for cotton is 5g/l, and the vehicle speed is 30 m/min.
Example 3
The preparation method of the ultraviolet-resistant shirt fabric is the same as that in example 1, and is different from the following steps:
in the step (1), 1000 meters of cloth is distributed for each cylinder.
In the step (4), the vehicle speed is 90 m/min.
In the step (6), 4g/l of ultraviolet absorbent (HF-E) is used for terylene, and the temperature of the terylene dyeing process is kept for 50 min; and (5) carrying out heat preservation for 50min by using a cotton fiber dyeing process.
In the step (9), 20g/l of ultraviolet resistant finishing agent (UV-S) for cotton is adopted, and the vehicle speed is 50 m/min.
The fabrics prepared in examples 1-3 were tested for uv protection, light fastness and breaking strength and the results are shown in table 1.
TABLE 1 test results
| Ultraviolet ray resistance | Colour fastness to light | Breaking strength | |
| Example 1 | Upf50+, T (uva) transmittance 2.4% | 5-6 stages | 786N |
| Example 2 | Upf30-50+, T (uva) transmittance 4.8% | 5-6 stages | 710N |
| Example 3 | Upf50+, T (uva) transmittance 2.6% | Grade 5 | 780N |
Claims (10)
1. A preparation method of an ultraviolet-resistant shirt fabric is characterized by comprising the following steps: the method comprises the following specific steps:
(1) preparing a grey fabric: the polyester-cotton interwoven plain cloth is composed of 90% of terylene and 10% of cotton fiber, the gram weight is 210g/m, the width is 165cm, and the cloth is distributed for each cylinder by 800-1000 meters;
(2) pre-treatment scouring: treating the fabric by using a high-temperature high-pressure overflow dyeing machine and using a mixed solution of soda ash, hydrogen peroxide, a refining agent, a deoiling agent and a chelating dispersant;
(3) shaping and drying;
(4) singeing: singeing by adopting a natural gas singeing machine at the speed of 80-100 m/min;
(5) mercerizing;
(6) dyeing:
the polyester dyeing formula comprises: disperse blue: 0.25%, disperse violet: 0.03 percent, 1g/l of acetic acid, 2-4g/l of ultraviolet absorbent for terylene and 2g/l of high-temperature leveling agent;
the dyeing process comprises the following steps: keeping the temperature at 130 ℃ for 30-50 min;
the cotton fiber dyeing formula comprises the following steps: active red: 0.05 percent of anhydrous sodium sulphate, 20g/l of anhydrous sodium sulphate and 10g/l of sodium carbonate;
the dyeing process comprises the following steps: treating at 60 deg.C for 30-50 min;
the soaping process comprises the following steps: treating soaping agent 1g/l at 80 deg.C for 20 min;
(7) dehydrating and scutching;
(8) shaping and drying;
(9) softening and finishing: the temperature is 150 ℃, the vehicle speed is 30-50m/min, the ultraviolet resistant finishing agent for cotton is 5-20g/l, and the hydrophilic softening agent is 10 g/l;
(10) decating;
(11) and (5) inspecting, packaging and rolling.
2. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (2), the pre-treatment scouring specifically comprises the following steps: treating the fabric by using a high-temperature high-pressure overflow dyeing machine and using a mixed solution of soda ash, hydrogen peroxide, a refining agent, a deoiling agent and a chelating dispersant; 2g/l of soda ash, 3g/l of hydrogen peroxide, 1g/l of non-ionic refining agent, 1g/l of alkali-resistant high-temperature-resistant degreaser and 3g/l of chelating dispersant, wherein the treatment temperature is 100 ℃, and the treatment time is 30 min.
3. The method for preparing an ultraviolet-resistant shirt fabric according to claim 2, characterized in that: the non-ionic refining agent is DR-N6, the alkali-resistant and high-temperature-resistant deoiling agent is alkali-resistant and high-temperature-resistant deoiling agent 101, and the chelating dispersant is DR-99.
4. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: and (3) shaping and drying at the temperature of 170 ℃ at the speed of 40 m/min.
5. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (4), the singeing adopts a forward singeing method and a reverse singeing method.
6. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (5), the mercerizing is as follows: mercerizing is carried out by adopting caustic soda solution with the concentration of 180 g/l.
7. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (6), the ultraviolet absorbent for terylene is HF-E.
8. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: and (8) shaping and drying at the temperature of 170 ℃ at the speed of 50 m/min.
9. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (9), the ultraviolet-resistant finishing agent for cotton is UV-S, and the hydrophilic softening agent is DR-1.
10. The method for preparing an ultraviolet-resistant shirt fabric according to claim 1, wherein the method comprises the following steps: in the step (10), the decating is as follows: treating with Italian KD series pot steaming machine at 160 deg.C under 0.6bar for 90s from inside to outside and 90s from outside to inside, and cooling for 150 s.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011196283.3A CN112359463A (en) | 2020-10-30 | 2020-10-30 | Preparation method of ultraviolet-resistant shirt fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011196283.3A CN112359463A (en) | 2020-10-30 | 2020-10-30 | Preparation method of ultraviolet-resistant shirt fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112359463A true CN112359463A (en) | 2021-02-12 |
Family
ID=74512397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011196283.3A Pending CN112359463A (en) | 2020-10-30 | 2020-10-30 | Preparation method of ultraviolet-resistant shirt fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112359463A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115522311A (en) * | 2022-09-14 | 2022-12-27 | 深圳全棉时代科技有限公司 | Ultraviolet-proof all-cotton fabric manufacturing process |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1928174A (en) * | 2006-09-27 | 2007-03-14 | 浙江华孚色纺有限公司 | Anti-ultraviolet ray mixed color spinning thread and its producing method |
| CN101985812A (en) * | 2009-07-29 | 2011-03-16 | 襄樊新四五印染有限责任公司 | Cotton-polyester blended fabric and dispersive and reactive dye one-bath dyeing process |
| CN102162197A (en) * | 2011-03-07 | 2011-08-24 | 浙江理工大学 | Method for dip-dyeing polyester rayon (cotton) fabrics or yarns with disperse and reactive dyes by one-bath process |
| CN106149425A (en) * | 2016-07-25 | 2016-11-23 | 安徽亚源印染有限公司 | A kind of dyeing and finishing processing method of cotton-polyester blend fabric |
| CN109295760A (en) * | 2018-09-07 | 2019-02-01 | 安徽亚源印染有限公司 | A kind of polyester-cotton blend disperse dyes and the novel two bath process technique of reactive dye |
| CN109680524A (en) * | 2018-11-28 | 2019-04-26 | 桐乡市金达染整有限责任公司 | A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method |
| WO2019203854A1 (en) * | 2018-04-20 | 2019-10-24 | Accel Lifestyle, Llc | Antimicrobial silver fiber products and methods of manufacturing the same |
-
2020
- 2020-10-30 CN CN202011196283.3A patent/CN112359463A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1928174A (en) * | 2006-09-27 | 2007-03-14 | 浙江华孚色纺有限公司 | Anti-ultraviolet ray mixed color spinning thread and its producing method |
| CN101985812A (en) * | 2009-07-29 | 2011-03-16 | 襄樊新四五印染有限责任公司 | Cotton-polyester blended fabric and dispersive and reactive dye one-bath dyeing process |
| CN102162197A (en) * | 2011-03-07 | 2011-08-24 | 浙江理工大学 | Method for dip-dyeing polyester rayon (cotton) fabrics or yarns with disperse and reactive dyes by one-bath process |
| CN106149425A (en) * | 2016-07-25 | 2016-11-23 | 安徽亚源印染有限公司 | A kind of dyeing and finishing processing method of cotton-polyester blend fabric |
| WO2019203854A1 (en) * | 2018-04-20 | 2019-10-24 | Accel Lifestyle, Llc | Antimicrobial silver fiber products and methods of manufacturing the same |
| CN109295760A (en) * | 2018-09-07 | 2019-02-01 | 安徽亚源印染有限公司 | A kind of polyester-cotton blend disperse dyes and the novel two bath process technique of reactive dye |
| CN109680524A (en) * | 2018-11-28 | 2019-04-26 | 桐乡市金达染整有限责任公司 | A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method |
Non-Patent Citations (3)
| Title |
|---|
| 纪惠军等: "《印染技术》", 31 July 2012, 东华大学出版社 * |
| 范雪荣等: "《纺织品染整工艺学》", 30 June 2000, 中国纺织出版社 * |
| 西鹏等: "《高技术纤维》", 30 September 2004, 化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115522311A (en) * | 2022-09-14 | 2022-12-27 | 深圳全棉时代科技有限公司 | Ultraviolet-proof all-cotton fabric manufacturing process |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106149425B (en) | A kind of dyeing and finishing processing method of cotton-polyester blend fabric | |
| CN109680524A (en) | A kind of polyester-cotton blend Dyeing with Disperse/Reactive fixation and uvioresistant single bath process processing method | |
| CN101962854B (en) | Preparation method of UV protection polyester cotton shell fabric | |
| CN102154830A (en) | Method for dyeing wool fabric at low temperature | |
| CN112359463A (en) | Preparation method of ultraviolet-resistant shirt fabric | |
| CN105780545A (en) | Dyeing and finishing process of bamboo-cotton blended fabric | |
| CN108894034A (en) | A kind of wool fabric method of modifying | |
| CN111005239B (en) | Dyeing and finishing process for reducing strength reduction of PLA-PHBV, tencel and cotton interwoven fabric in dyeing | |
| CN110952348A (en) | Processing method for improving dyeing depth of cation modified piece-dyed fabric | |
| CN113062131B (en) | Short-flow processing technology for polyester-cotton knitted fabric | |
| CN113279264B (en) | Ultraviolet-proof stain-resistant fabric and manufacturing method thereof | |
| CN113308916B (en) | Dyeing method of aramid fiber and dyed aramid fiber | |
| CN107740261B (en) | Bleaching method of soybean protein fiber | |
| CN109295769B (en) | Preparation method of silk with ultraviolet radiation prevention function | |
| CN108716107B (en) | Boiling bleaching liquid, pretreatment liquid, fabric, dyeing method of fabric and clothes | |
| CN114657790B (en) | Washing-resistant waterproof and color-fixing one-bath finishing process for cotton fabric | |
| EP0685013B1 (en) | Wool and wool-blend fabric treatment | |
| CN115976783A (en) | Processing technology for improving ultraviolet resistance of fabric | |
| CN112301735B (en) | Processing technology of anti-ultraviolet pure cotton fabric | |
| CN110607704B (en) | Rare earth coordination-based natural dye dyeing method with ultraviolet resistance | |
| CN112359616B (en) | Method for improving light fastness of aramid fiber | |
| CN113430845B (en) | Dyeing and finishing process of high-friction-resistance nylon four-side elastic fabric | |
| CN109537132B (en) | Production process of white nylon uvioresistant fabric | |
| CN114808494B (en) | Dyeing process for improving dyeing fastness of vegetable dye | |
| Malik et al. | Simultaneous dyeing and finishing of cotton fabric using reactive dyes and citric acid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210212 |