CN109646318A - A kind of whitening anti-aging clarifying lotion and preparation method thereof - Google Patents
A kind of whitening anti-aging clarifying lotion and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of whitening anti-aging clarifying lotion and preparation method thereof.The whitening anti-aging clarifying lotion includes following raw material: protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate, water.The protein hydrolysate is rice bran protein, avenin, one or more mixtures in modified oat albumen.The antioxidant is ophiopogonpolysaccharide and/or root bark of white mulberry polysaccharide.Compared with prior art, the whitening anti-aging clarifying lotion that the present invention is prepared has significant anti-oxidation efficacy, can be obviously improved the elasticity of skin, reduce the generation of wrinkle, it can be applied in all kinds of skin care item promote the skin-care effect of skin care item, there is wide application prospect.
Description
Technical field
The present invention relates to daily chemical product technical fields, and in particular to a kind of whitening anti-aging clarifying lotion and its preparation side
Method.
Background technique
Skin can change with advancing age, and skin care is a lifetime homework to be learnt.Skin cell it is old
Change will lead to skin keratin metabolism and be slowed by, and old cutin can block pore at this time, and pore supports greatly gradually, more seem skin not
Smoothly, the colour of skin is uneven.Either due to pressure and environmental factor, the skin of quite a few 25-30 years old women can go out extremely
Oil, pore are coarse etc..For woman, the basis of skin health is exactly moisture, and cell senescence will lead to dry skin water shortage,
It enables epidermis skin lack to moisten, it is no longer full.Human body forms various free radicals in metabolic processes.Wherein,
95% free radical is all to our harmful oxygen radicals.Their attack cells generate oxidation, injure cell function,
Decline human activity, the aging phenomenons such as wrinkle, color spot occurs in face, and skin becomes gloomy.In addition, increasingly due to environmental pollution
Seriously, it can also allow in skin and generate toxin.Most of skin-protection product has skin mostly based on adding chemical substance at present
There is certain nocuity, is suitable for prolonged use.
The present invention provides a kind of whitening anti-aging clarifying lotion, using the protein hydrolysate such as rice bran protein and modified oat albumen with
The antioxidant of ophiopogonpolysaccharide and/or root bark of white mulberry polysaccharide composition, the whitening anti-aging clarifying lotion being prepared have significant antioxygen
Change effect, the elasticity of skin can be obviously improved, reduce the generation of wrinkle, can be applied in all kinds of skin care item promote the shield of skin care item
Skin effect has wide application prospect.
Summary of the invention
The purpose of the present invention is to provide a kind of whitening anti-aging clarifying lotion.
Specific technical solution is as follows:
A kind of whitening anti-aging clarifying lotion, including following raw material: protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water
Dissolubility azone, pyrrolidone sodium carboxylate, water.
Preferred technical solution, a kind of whitening anti-aging clarifying lotion are prepared by following raw material by mass percentage:
Protein hydrolysate 10~20%, antioxidant 1~3%, hyaluronic acid 1~3%, allantoin 0.5~2%, water-solubleazone 0.5~
2%, pyrrolidone sodium carboxylate 0.5~2%, surplus are water.
The protein hydrolysate is rice bran protein, avenin, one or more mixtures in modified oat albumen.
In one embodiment of the invention, the protein hydrolysate is modified oat albumen.
In another embodiment of the present invention, the protein hydrolysate is the mixture of rice bran protein and modified oat albumen, institute
The mass ratio for stating rice bran protein and modified oat albumen is 1:(1-5).
The avenin is prepared using following methods: being weighed oat 8-12g, is impregnated in 100-200mL ethyl alcohol
30-60 minutes, using 300 mesh filter-cloth filterings, filter cake was 30-60 minutes dry at 40-50 DEG C, crushed, and crossed 40-100 mesh,
40-50 DEG C 1-3 hours dry, obtains oatmeal, adds water 80-120mL in oatmeal, with 100-300 revs/min of stirring 5-10 points
Clock, be added mixed enzyme 0.02-0.2 parts, 40-50 DEG C with 100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with
100-300 revs/min stirring 3-6 minutes, with 3000-5000 revs/min centrifugation 10-20 minutes, supernatant is with lemon acid for adjusting pH
4.0-4.5, with 100-300 revs/min stirring 5-10 minutes, 30-40 DEG C standing 40-80 minutes, then it is small in 2-8 DEG C of standing 5-10
When with 3000-5000 revs/min centrifugation 10-20 minutes, lower sediment is dry to constant weight at 40-60 DEG C, obtains avenin；It is described
Mixed enzyme is cellulase, papain, phytase (1-5) in mass ratio: (1-5): 1 mixture.
The modified oat albumen is prepared using following methods: oat 8-12g is weighed, in 100-200mL ethyl alcohol
It impregnates 30-60 minutes, using 300 mesh filter-cloth filterings, filter cake is 30-60 minutes dry at 40-50 DEG C, crushes, 40-100 mesh is crossed,
It is 1-3 hours dry at 40-50 DEG C, oatmeal is obtained, adds water 80-120mL in oatmeal, with 100-300 revs/min of stirring 5-10 points
Clock, be added mixed enzyme 0.02-0.2 parts, 40-50 DEG C with 100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with
100-300 revs/min stirring 3-6 minutes, with 3000-5000 revs/min centrifugation 10-20 minutes, supernatant is with lemon acid for adjusting pH
4.0-4.5, with 100-300 revs/min stirring 5-10 minutes, 30-40 DEG C standing 40-80 minutes, then it is small in 2-8 DEG C of standing 5-10
When with 3000-5000 revs/min centrifugation 10-20 minutes, lower sediment is with water washing 1-3 times of 200-300mL, then at 40-60 DEG C
Drying obtains avenin, by avenin and water 1:(40-60 in mass ratio to constant weight) mixing, it is stirred with 100-300 revs/min
Mix 20-30 minutes, be added tea polyphenols, 20-30 DEG C with 100-300 revs/min stirring 1-3 hours, then in 1-5 DEG C of standing 10-
20 hours, be 4.0-4.5 with lemon acid for adjusting pH, with 100-300 revs/min stirring 5-10 minutes, in 30-40 DEG C of standing 40-80
Minute, then 2-8 DEG C of standing 5-10 hours with 3000-5000 revs/min centrifugation 10-20 minutes, lower sediment is in 40-60 DEG C of drying
To constant weight, modified oat albumen is obtained, the mass ratio of the tea polyphenols and avenin is (1-3): (1-3)；The mixed enzyme
For cellulase, papain, phytase (1-5) in mass ratio: (1-5): 1 mixture.
The rice bran protein is prepared using following methods: being weighed rice bran 8-12g, is impregnated in 100-200mL ethyl alcohol
30-60 minutes, using 300 mesh filter-cloth filterings, filter cake was 30-60 minutes dry at 40-50 DEG C, crushed, and crossed 40-100 mesh,
40-50 DEG C 1-3 hours dry, obtains bran powder, adds water 80-120mL in bran powder, with 100-300 revs/min of stirring 5-10 points
Clock, be added mixed enzyme 0.02-0.2 parts, 40-50 DEG C with 100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with
100-300 revs/min stirring 3-6 minutes, with 3000-5000 revs/min centrifugation 10-20 minutes, supernatant is with lemon acid for adjusting pH
4.0-4.5, with 100-300 revs/min stirring 5-10 minutes, 30-40 DEG C standing 40-80 minutes, then it is small in 2-8 DEG C of standing 5-10
When with 3000-5000 revs/min centrifugation 10-20 minutes, lower sediment is with water washing 1-3 times of 200-300mL, then at 40-60 DEG C
Drying obtains rice bran protein to constant weight；The mixed enzyme is cellulase, papain, phytase (1-5) in mass ratio:
(1-5): 1 mixture.
The antioxidant is ophiopogonpolysaccharide and/or root bark of white mulberry polysaccharide.Preferably, the antioxidant is ophiopogonpolysaccharide and Sang Bai
The mass ratio of the mixture of skin polysaccharide, the ophiopogonpolysaccharide and root bark of white mulberry polysaccharide is (1-3): (1-3).
The ophiopogonpolysaccharide is prepared using following methods: it will crush Radix Ophiopogonis, and cross 40-100 mesh, obtain ophiopogon powder,
By 8-12g ophiopogon powder with 100-200mL ethyl alcohol impregnate 30-60 minute, with 3000-5000 revs/min centrifugation 10-20 minutes, precipitate
Be added 220-320mL water, 40-60 DEG C ultrasonic extraction 30-60 minutes, ultrasonic power 100-200W, supersonic frequency 15-25kHz,
With 3000-5000 revs/min centrifugation 10-20 minutes, supernatant is concentrated under reduced pressure into 80-120mL, and adding ethyl alcohol makes the quality of ethyl alcohol
Score is 75-85%, with 100-300 revs/min stirring 10-20 minutes, 30-40 DEG C standing 40-80 minutes, then it is quiet at 2-8 DEG C
Set 10-20 hours, with 3000-5000 revs/min centrifugation 10-20 minutes, precipitating use 80-120mL ethanol washing 2 times, at 40-60 DEG C
Drying obtains ophiopogonpolysaccharide to constant weight.
The root bark of white mulberry polysaccharide is prepared using following methods: the root bark of white mulberry being crushed, 40-100 mesh is crossed, obtains Sang Bai
Pi Fen impregnates the 8-12g root bark of white mulberry powder 100-200mL ethyl alcohol 30-60 minutes, with 3000-5000 revs/min of centrifugation 10-20 points
Clock, precipitating be added 220-320mL water, 40-60 DEG C ultrasonic extraction 30-60 minutes, ultrasonic power 100-200W, supersonic frequency
15-25kHz, with 3000-5000 revs/min centrifugation 10-20 minutes, supernatant is concentrated under reduced pressure into 80-120mL, and adding ethyl alcohol makes
The mass fraction of ethyl alcohol be 75-85%, with 100-300 revs/min stirring 10-20 minutes, 30-40 DEG C standing 40-80 minutes, then
2-8 DEG C standing 10-20 hours, with 3000-5000 revs/min centrifugation 10-20 minutes, precipitating use 80-120mL ethanol washing 2 times,
It is dry to constant weight at 40-60 DEG C, obtain root bark of white mulberry polysaccharide.
The invention also discloses the preparation methods of above-mentioned whitening anti-aging clarifying lotion, weigh each raw material by weight, by water
Solution albumen, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to the water, at 10~25 DEG C
With 100-300 revs/min of stirring 10-20 minutes to get.
Whitening anti-aging clarifying lotion of the invention has significant anti-oxidation efficacy, can be obviously improved the elasticity of skin, subtract
The generation of few wrinkle can be applied in all kinds of skin care item promote the skin-care effect of skin care item, have wide application prospect.
Specific embodiment
In the present invention, if not refering in particular to, all devices and raw material is commercially available or the industry is common are following
Method in embodiment is unless otherwise instructed conventional method in that art.
Hyaluronic acid, No. CAS: 9004-61-9.
Allantoin, No. CAS: 97-59-6, it buys from Shanghai Mai Ruier chemical technology Co., Ltd, product number:
A90025。
Water-solubleazone, No. CAS: 59227-82-3.
Pyrrolidone sodium carboxylate, No. CAS: 28874-51-3.
Oat buys the naked oats from Shijiazhuang Ling Feng agricultural and sideline product development corporation, Ltd., protein content 16-18%.
Radix Ophiopogonis, from Haozhou city, often rich medicine company sells Co., Ltd, source area: Sichuan for purchase.
The root bark of white mulberry, from Haozhou city, often rich medicine company sells Co., Ltd, source area: Jiangsu for purchase.
Rice bran, The Great Northern Wilderness Rice Co., Ltd,Heilongjiang provide, protein content: 14-16%.
Tea polyphenols, No. CAS: 84650-60-2, it buys from Shanghai Yuan Ye Biotechnology Co., Ltd.
Cellulase is bought from the emerging Biotechnology Co., Ltd in Wuhan one hundred, 100,000 U/g of enzyme activity.
Bromelain is bought from the emerging Biotechnology Co., Ltd in Wuhan one hundred, 100,000 U/g of enzyme activity.
Phytase is bought from Shandong Ke Langqi Biotechnology Co., Ltd, 100,000 U/g of enzyme activity.
Embodiment 1
A kind of whitening anti-aging clarifying lotion, the raw material including following mass percent: protein hydrolysate 20%, antioxidant 3%,
Hyaluronic acid 3%, allantoin 1%, water-solubleazone 0.8%, pyrrolidone sodium carboxylate 0.8%, surplus are water.Claim by weight
Each raw material is taken, protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to water
In, 15 DEG C with 200 revs/min stir 10 minutes to get.
The protein hydrolysate is avenin.
The antioxidant is ophiopogonpolysaccharide.
The avenin is prepared using following methods: oat 10g weighed, is impregnated 50 minutes in 150mL ethyl alcohol,
Using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, 2 hours dry at 45 DEG C, obtains oat
Powder in oatmeal plus water 100mL, is stirred 8 minutes with 200 revs/min, is added 0.05 part of mixed enzyme, is stirred at 45 DEG C with 200 revs/min
It mixes 2 hours, is warming up to 98 DEG C and is stirred 5 minutes with 200 revs/min, is centrifuged 15 minutes with 4000 revs/min, supernatant citric acid tune
Save pH be 4.3, with 200 revs/min stir 8 minutes, 35 DEG C stand 60 minutes, then 5 DEG C stand 6 hours, with 4000 revs/min from
The heart 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained avenin.
The mixed enzyme is cellulase, papain, the phytase mixture of 2:2:1 in mass ratio.
The ophiopogonpolysaccharide is prepared using following methods: will be crushed Radix Ophiopogonis, and be crossed 60 meshes, ophiopogon powder is obtained, by 10g
Ophiopogon powder is impregnated 50 minutes with 150mL ethyl alcohol, is centrifuged 15 minutes with 4000 revs/min, and 300mL water is added in precipitating, in 50 DEG C of ultrasounds
Extract 50 minutes, ultrasonic power 150W, supersonic frequency 20kHz, with 4000 revs/min be centrifuged 15 minutes, supernatant 50 DEG C, absolutely
Pressure is that 0.02MPa is concentrated under reduced pressure into 100mL, and adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, is stirred with 200 revs/min
15 minutes, 60 minutes is stood at 35 DEG C, then stand 15 hours at 5 DEG C, be centrifuged 15 minutes with 4000 revs/min, precipitating 100mL second
Alcohol washs 2 times, dry to constant weight at 50 DEG C, obtains ophiopogonpolysaccharide.
Embodiment 2
Substantially the same manner as Example 1, difference is only that:
The protein hydrolysate is modified oat albumen.
The modified oat albumen is prepared using following methods: being weighed oat 10g, is impregnated 50 in 150mL ethyl alcohol
Minute, using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, and it is 2 hours dry at 45 DEG C, it obtains
To oatmeal, in oatmeal plus water 100mL, is stirred 8 minutes with 200 revs/min, 0.05 part of mixed enzyme is added, at 45 DEG C with 200
Rev/min stirring 2 hours, be warming up to 98 DEG C with 200 revs/min stir 5 minutes, with 4000 revs/min be centrifuged 15 minutes, supernatant lemon
Lemon acid for adjusting pH is 4.3, is stirred 8 minutes with 200 revs/min, 60 minutes is stood at 35 DEG C, then stand 6 hours at 5 DEG C, with 4000
Revs/min centrifugation 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained avenin, in mass ratio by avenin and water
1:50 mixing, is stirred 25 minutes with 200 revs/min, and tea polyphenols are added, and is stirred 2 hours at 25 DEG C with 200 revs/min, then at 3 DEG C
15 hours are stood, is 4.2 with lemon acid for adjusting pH, is stirred 8 minutes with 200 revs/min, stands 60 minutes at 35 DEG C, then quiet at 5 DEG C
It sets 6 hours, is centrifuged 15 minutes with 4000 revs/min, lower sediment obtains modified oat albumen in 50 DEG C of dryings to constant weight, described
The mass ratio of tea polyphenols and avenin is 1:1.
The mixed enzyme is cellulase, papain, the phytase mixture of 2:2:1 in mass ratio.
Embodiment 3
A kind of whitening anti-aging clarifying lotion, the raw material including following mass percent: protein hydrolysate 20%, antioxidant 3%,
Hyaluronic acid 3%, allantoin 1%, water-solubleazone 0.8%, pyrrolidone sodium carboxylate 0.8%, surplus are water.Claim by weight
Each raw material is taken, protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to water
In, 15 DEG C with 200 revs/min stir 10 minutes to get.
The protein hydrolysate is rice bran protein.
The antioxidant is ophiopogonpolysaccharide.
The rice bran protein is prepared using following methods: rice bran 10g weighed, is impregnated 50 minutes in 150mL ethyl alcohol,
Using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, 2 hours dry at 45 DEG C, obtains rice bran
Powder in bran powder plus water 100mL, is stirred 8 minutes with 200 revs/min, is added 0.05 part of mixed enzyme, is stirred at 45 DEG C with 200 revs/min
It mixes 2 hours, is warming up to 98 DEG C and is stirred 5 minutes with 200 revs/min, is centrifuged 15 minutes with 4000 revs/min, supernatant citric acid tune
Save pH be 4.3, with 200 revs/min stir 8 minutes, 35 DEG C stand 60 minutes, then 5 DEG C stand 6 hours, with 4000 revs/min from
The heart 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained rice bran protein.
The ophiopogonpolysaccharide is prepared using following methods: will be crushed Radix Ophiopogonis, and be crossed 60 meshes, ophiopogon powder is obtained, by 10g
Ophiopogon powder is impregnated 50 minutes with 150mL ethyl alcohol, is centrifuged 15 minutes with 4000 revs/min, and 300mL water is added in precipitating, in 50 DEG C of ultrasounds
Extract 50 minutes, ultrasonic power 150W, supersonic frequency 20kHz, with 4000 revs/min be centrifuged 15 minutes, supernatant 50 DEG C, absolutely
Pressure is that 0.02MPa is concentrated under reduced pressure into 100mL, and adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, is stirred with 200 revs/min
15 minutes, 60 minutes is stood at 35 DEG C, then stand 15 hours at 5 DEG C, be centrifuged 15 minutes with 4000 revs/min, precipitating 100mL second
Alcohol washs 2 times, dry to constant weight at 50 DEG C, obtains ophiopogonpolysaccharide.
Embodiment 4
A kind of whitening anti-aging clarifying lotion, the raw material including following mass percent: protein hydrolysate 20%, antioxidant 3%,
Hyaluronic acid 3%, allantoin 1%, water-solubleazone 0.8%, pyrrolidone sodium carboxylate 0.8%, surplus are water.Claim by weight
Each raw material is taken, protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to water
In, 15 DEG C with 200 revs/min stir 10 minutes to get.
The protein hydrolysate is the mixture of rice bran protein and modified oat albumen, the rice bran protein and modified oat egg
White mass ratio is 1:2.
The antioxidant is ophiopogonpolysaccharide.
The modified oat albumen is prepared using following methods: being weighed oat 10g, is impregnated 50 in 150mL ethyl alcohol
Minute, using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, and it is 2 hours dry at 45 DEG C, it obtains
To oatmeal, in oatmeal plus water 100mL, is stirred 8 minutes with 200 revs/min, 0.05 part of mixed enzyme is added, at 45 DEG C with 200
Rev/min stirring 2 hours, be warming up to 98 DEG C with 200 revs/min stir 5 minutes, with 4000 revs/min be centrifuged 15 minutes, supernatant lemon
Lemon acid for adjusting pH is 4.3, is stirred 8 minutes with 200 revs/min, 60 minutes is stood at 35 DEG C, then stand 6 hours at 5 DEG C, with 4000
Revs/min centrifugation 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained avenin, in mass ratio by avenin and water
1:50 mixing, is stirred 25 minutes with 200 revs/min, and tea polyphenols are added, and is stirred 2 hours at 25 DEG C with 200 revs/min, then at 3 DEG C
15 hours are stood, is 4.2 with lemon acid for adjusting pH, is stirred 8 minutes with 200 revs/min, stands 60 minutes at 35 DEG C, then quiet at 5 DEG C
It sets 6 hours, is centrifuged 15 minutes with 4000 revs/min, lower sediment obtains modified oat albumen in 50 DEG C of dryings to constant weight, described
The mass ratio of tea polyphenols and avenin is 1:1.
The rice bran protein is prepared using following methods: rice bran 10g weighed, is impregnated 50 minutes in 150mL ethyl alcohol,
Using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, 2 hours dry at 45 DEG C, obtains rice bran
Powder in bran powder plus water 100mL, is stirred 8 minutes with 200 revs/min, is added 0.05 part of mixed enzyme, is stirred at 45 DEG C with 200 revs/min
It mixes 2 hours, is warming up to 98 DEG C and is stirred 5 minutes with 200 revs/min, is centrifuged 15 minutes with 4000 revs/min, supernatant citric acid tune
Save pH be 4.3, with 200 revs/min stir 8 minutes, 35 DEG C stand 60 minutes, then 5 DEG C stand 6 hours, with 4000 revs/min from
The heart 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained rice bran protein.
The mixed enzyme is cellulase, papain, the phytase mixture of 2:2:1 in mass ratio.The Radix Ophiopogonis
Polysaccharide is prepared using following methods: will be crushed Radix Ophiopogonis, and be crossed 60 meshes, ophiopogon powder is obtained, by 10g ophiopogon powder 150mL second
Alcohol impregnate 50 minutes, with 4000 revs/min be centrifuged 15 minutes, precipitating be added 300mL water, 50 DEG C ultrasonic extraction 50 minutes, ultrasound
Power 150W, supersonic frequency 20kHz are centrifuged 15 minutes with 4000 revs/min, and supernatant subtracts in 50 DEG C, absolute pressure for 0.02MPa
Pressure is concentrated into 100mL, and adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, is stirred 15 minutes with 200 revs/min, quiet at 35 DEG C
It sets 60 minutes, then stands 15 hours at 5 DEG C, be centrifuged 15 minutes with 4000 revs/min, precipitating is used 100mL ethanol washing 2 times, 50
It is DEG C dry to constant weight, obtain ophiopogonpolysaccharide.
Embodiment 5
A kind of whitening anti-aging clarifying lotion, the raw material including following mass percent: protein hydrolysate 20%, antioxidant 3%,
Hyaluronic acid 3%, allantoin 1%, water-solubleazone 0.8%, pyrrolidone sodium carboxylate 0.8%, surplus are water.Claim by weight
Each raw material is taken, protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to water
In, 15 DEG C with 200 revs/min stir 10 minutes to get.
The protein hydrolysate is the mixture of rice bran protein and modified oat albumen, the rice bran protein and modified oat egg
White mass ratio is 1:2.
The antioxidant is root bark of white mulberry polysaccharide.
The modified oat albumen is prepared using following methods: being weighed oat 10g, is impregnated 50 in 150mL ethyl alcohol
Minute, using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, and it is 2 hours dry at 45 DEG C, it obtains
To oatmeal, in oatmeal plus water 100mL, is stirred 8 minutes with 200 revs/min, 0.05 part of mixed enzyme is added, at 45 DEG C with 200
Rev/min stirring 2 hours, be warming up to 98 DEG C with 200 revs/min stir 5 minutes, with 4000 revs/min be centrifuged 15 minutes, supernatant lemon
Lemon acid for adjusting pH is 4.3, is stirred 8 minutes with 200 revs/min, 60 minutes is stood at 35 DEG C, then stand 6 hours at 5 DEG C, with 4000
Revs/min centrifugation 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained avenin, in mass ratio by avenin and water
1:50 mixing, is stirred 25 minutes with 200 revs/min, and tea polyphenols are added, and is stirred 2 hours at 25 DEG C with 200 revs/min, then at 3 DEG C
15 hours are stood, is 4.2 with lemon acid for adjusting pH, is stirred 8 minutes with 200 revs/min, stands 60 minutes at 35 DEG C, then quiet at 5 DEG C
It sets 6 hours, is centrifuged 15 minutes with 4000 revs/min, lower sediment obtains modified oat albumen in 50 DEG C of dryings to constant weight, described
The mass ratio of tea polyphenols and avenin is 1:1.
The rice bran protein is prepared using following methods: rice bran 10g weighed, is impregnated 50 minutes in 150mL ethyl alcohol,
Using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, 2 hours dry at 45 DEG C, obtains rice bran
Powder in bran powder plus water 100mL, is stirred 8 minutes with 200 revs/min, is added 0.05 part of mixed enzyme, is stirred at 45 DEG C with 200 revs/min
It mixes 2 hours, is warming up to 98 DEG C and is stirred 5 minutes with 200 revs/min, is centrifuged 15 minutes with 4000 revs/min, supernatant citric acid tune
Save pH be 4.3, with 200 revs/min stir 8 minutes, 35 DEG C stand 60 minutes, then 5 DEG C stand 6 hours, with 4000 revs/min from
The heart 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained rice bran protein.
The mixed enzyme is cellulase, papain, the phytase mixture of 2:2:1 in mass ratio.
The root bark of white mulberry polysaccharide is prepared using following methods: the root bark of white mulberry being crushed, 60 meshes is crossed, obtains the root bark of white mulberry
10g root bark of white mulberry powder 150mL ethyl alcohol is impregnated 50 minutes, is centrifuged 15 minutes with 4000 revs/min by powder, and 300mL water is added in precipitating,
50 DEG C ultrasonic extraction 50 minutes, ultrasonic power 150W, supersonic frequency 20kHz, with 4000 revs/min be centrifuged 15 minutes, supernatant
It is that 0.02MPa is concentrated under reduced pressure into 100mL in 50 DEG C, absolute pressure, adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, with
200 revs/min are stirred 15 minutes, are stood 60 minutes at 35 DEG C, then stand 15 hours at 5 DEG C, are centrifuged 15 minutes with 4000 revs/min,
Precipitating is used 100mL ethanol washing 2 times, dry to constant weight at 50 DEG C, obtains root bark of white mulberry polysaccharide.
Embodiment 6
A kind of whitening anti-aging clarifying lotion, the raw material including following mass percent: protein hydrolysate 20%, antioxidant 3%,
Hyaluronic acid 3%, allantoin 1%, water-solubleazone 0.8%, pyrrolidone sodium carboxylate 0.8%, surplus are water.Claim by weight
Each raw material is taken, protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added to water
In, 15 DEG C with 200 revs/min stir 10 minutes to get.
The protein hydrolysate is the mixture of rice bran protein and modified oat albumen, the rice bran protein and modified oat egg
White mass ratio is 1:2.
The antioxidant is the mixture of ophiopogonpolysaccharide and root bark of white mulberry polysaccharide, the matter of the ophiopogonpolysaccharide and root bark of white mulberry polysaccharide
Amount is than being 1:1.
The modified oat albumen is prepared using following methods: being weighed oat 10g, is impregnated 50 in 150mL ethyl alcohol
Minute, using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, and it is 2 hours dry at 45 DEG C, it obtains
To oatmeal, in oatmeal plus water 100mL, is stirred 8 minutes with 200 revs/min, 0.05 part of mixed enzyme is added, at 45 DEG C with 200
Rev/min stirring 2 hours, be warming up to 98 DEG C with 200 revs/min stir 5 minutes, with 4000 revs/min be centrifuged 15 minutes, supernatant lemon
Lemon acid for adjusting pH is 4.3, is stirred 8 minutes with 200 revs/min, 60 minutes is stood at 35 DEG C, then stand 6 hours at 5 DEG C, with 4000
Revs/min centrifugation 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained avenin, in mass ratio by avenin and water
1:50 mixing, is stirred 25 minutes with 200 revs/min, and tea polyphenols are added, and is stirred 2 hours at 25 DEG C with 200 revs/min, then at 3 DEG C
15 hours are stood, is 4.2 with lemon acid for adjusting pH, is stirred 8 minutes with 200 revs/min, stands 60 minutes at 35 DEG C, then quiet at 5 DEG C
It sets 6 hours, is centrifuged 15 minutes with 4000 revs/min, lower sediment obtains modified oat albumen in 50 DEG C of dryings to constant weight, described
The mass ratio of tea polyphenols and avenin is 1:1.
The rice bran protein is prepared using following methods: rice bran 10g weighed, is impregnated 50 minutes in 150mL ethyl alcohol,
Using 300 mesh filter-cloth filterings, filter cake is 40 minutes dry at 45 DEG C, crushes, and crosses 60 meshes, 2 hours dry at 45 DEG C, obtains rice bran
Powder in bran powder plus water 100mL, is stirred 8 minutes with 200 revs/min, is added 0.05 part of mixed enzyme, is stirred at 45 DEG C with 200 revs/min
It mixes 2 hours, is warming up to 98 DEG C and is stirred 5 minutes with 200 revs/min, is centrifuged 15 minutes with 4000 revs/min, supernatant citric acid tune
Save pH be 4.3, with 200 revs/min stir 8 minutes, 35 DEG C stand 60 minutes, then 5 DEG C stand 6 hours, with 4000 revs/min from
The heart 15 minutes, lower sediment was dry to constant weight at 50 DEG C, obtained rice bran protein.
The mixed enzyme is cellulase, papain, the phytase mixture of 2:2:1 in mass ratio.
The ophiopogonpolysaccharide is prepared using following methods: will be crushed Radix Ophiopogonis, and be crossed 60 meshes, ophiopogon powder is obtained, by 10g
Ophiopogon powder is impregnated 50 minutes with 150mL ethyl alcohol, is centrifuged 15 minutes with 4000 revs/min, and 300mL water is added in precipitating, in 50 DEG C of ultrasounds
Extract 50 minutes, ultrasonic power 150W, supersonic frequency 20kHz, with 4000 revs/min be centrifuged 15 minutes, supernatant 50 DEG C, absolutely
Pressure is that 0.02MPa is concentrated under reduced pressure into 100mL, and adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, is stirred with 200 revs/min
15 minutes, 60 minutes is stood at 35 DEG C, then stand 15 hours at 5 DEG C, be centrifuged 15 minutes with 4000 revs/min, precipitating 100mL second
Alcohol washs 2 times, dry to constant weight at 50 DEG C, obtains ophiopogonpolysaccharide.
The root bark of white mulberry polysaccharide is prepared using following methods: the root bark of white mulberry being crushed, 60 meshes is crossed, obtains the root bark of white mulberry
10g root bark of white mulberry powder 150mL ethyl alcohol is impregnated 50 minutes, is centrifuged 15 minutes with 4000 revs/min by powder, and 300mL water is added in precipitating,
50 DEG C ultrasonic extraction 50 minutes, ultrasonic power 150W, supersonic frequency 20kHz, with 4000 revs/min be centrifuged 15 minutes, supernatant
It is that 0.02MPa is concentrated under reduced pressure into 100mL in 50 DEG C, absolute pressure, adding ethyl alcohol makes the mass fraction 80% of ethyl alcohol, with
200 revs/min are stirred 15 minutes, are stood 60 minutes at 35 DEG C, then stand 15 hours at 5 DEG C, are centrifuged 15 minutes with 4000 revs/min,
Precipitating is used 100mL ethanol washing 2 times, dry to constant weight at 50 DEG C, obtains root bark of white mulberry polysaccharide.
Test case 1
It removes DPPH ability to the whitening anti-aging clarifying lotion that embodiment is prepared to test, specific test result is shown in
Table 1.
The measurement of whitening anti-aging clarifying lotion removing DPPH ability: taking 1g whitening anti-aging clarifying lotion, 9g water be added, with
200 revs/min are stirred 20 minutes, as sample to be tested, take 2mL sample to be tested in test tube, and adding 2mL concentration is 0.04g/mL
DPPH ethanol solution, be uniformly mixed, react 20min, 3500 revs/min of centrifuge separation 10min take supernatant in 517nm
It is A that place, which surveys its light absorption value,i, it separately takes sample to be tested 2mL in test tube, dehydrated alcohol 2mL is added, be uniformly mixed, react 20min,
3500 revs/min of centrifuge separation 10min, taking supernatant to survey its light absorption value at 517nm is Aj, 2mL concentration is 0.04g/mL's
DPPH ethanol solution and the reaction of 2mL dehydrated alcohol are used as reference, and light absorption value is denoted as A0.Sample to be tested is calculated according to the following formula
To the clearance rate K=[1- (A of DPPH free radicali-Aj)/A0] × 100%；
In formula, K is the clearance rate to DPPH free radical；A0Add 2mL for the DPPH ethanol solution of 2mL, 0.04g/mL
Dehydrated alcohol light absorption value；AiAdd the light absorption value of 2mL sample to be tested for the DPPH ethanol solution of 2mL, 0.04g/mL；AjFor 2mL
Dehydrated alcohol adds the light absorption value of 2mL sample to be tested.
1 whitening anti-aging clarifying lotion of table removes DPPH aptitude tests result table
| The clearance rate of DPPH free radical, % | |
| Embodiment 1 | 43.6 |
| Embodiment 2 | 47.4 |
| Embodiment 3 | 42.5 |
| Embodiment 4 | 52.0 |
| Embodiment 5 | 50.8 |
| Embodiment 6 | 56.3 |
Test case 2
Improve skin elasticity effect to the whitening anti-aging clarifying lotion that embodiment is prepared to test, specific test knot
Fruit is shown in Table 2.
Test method: subject is 140 35-45 years old healthy womens, and skin is stemness, is randomly divided into 7 groups, every group
20 people.It is carried out improving skin elasticity measure of merit with deionized water and embodiment 1-6 whitening anti-aging clarifying lotion respectively.Test department
Position be inboard arm, test before skinanalysis apparatus (German CK company, model: Derma-Expert MC760) test subject by
Try area skin elasticity number A0, smearing counter sample 2 times sooner or later at ranging palm base portion 8cm in left and right arm daily, every time
0.5mg/cm is pressed respectively2Dosage uniformly smear, continuous use 6 weeks after, the smearing position of subject is cleaned, test it is tested
Person's recipient site skin elasticity value A1, and everyone skin elasticity incrementss are calculated, calculation method is as follows: (A1-A0)/A0×
100%, every group is averaged, the mean skin elasticity incrementss as the group.
2 skin elasticity incrementss test result table of table
| Mean skin elasticity incrementss, % | |
| Deionized water | -0.41 |
| Embodiment 1 | 28.63 |
| Embodiment 2 | 31.52 |
| Embodiment 3 | 28.12 |
| Embodiment 4 | 35.72 |
| Embodiment 5 | 35.04 |
| Embodiment 6 | 40.38 |
Test case 3
Improve dermatoglyph effect to the whitening anti-aging clarifying lotion that embodiment is prepared to test, specific test knot
Fruit is shown in Table 3.
Test method: subject is 140 40-50 years old healthy womens, is mainly shown as skin of face aging, wrinkles
Line.7 groups are randomly divided into, every group of 20 people.Improvement skin is carried out with deionized water and embodiment 1-6 whitening anti-aging clarifying lotion respectively
Grain effect test.Test position is face, and face is smeared counter sample 2 times sooner or later daily, presses 0.5mg/cm respectively every time2's
Dosage is uniformly smeared, and after continuous use 6 weeks, the face of subject is cleaned, using U.S. VISIA face-image analyzer,
Dermatoglyph change rate is tested and calculates, every group is averaged, the mean skin texture variations rate as the group.
3 dermatoglyph change rate test result table of table
Avenin is modified using tea polyphenols in embodiment 2, whitening anti-aging clarifying lotion can be obviously improved
Properties.The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be within the scope of protection determined by the claims.
Claims (10)
1. a kind of whitening anti-aging clarifying lotion, which is characterized in that including following raw material: protein hydrolysate, antioxidant, hyaluronic acid,
Allantoin, water-solubleazone, pyrrolidone sodium carboxylate, water.
2. whitening anti-aging clarifying lotion as described in claim 1, which is characterized in that by following raw material system by mass percentage
It is standby to form: protein hydrolysate 10~20%, antioxidant 1~3%, hyaluronic acid 1~3%, allantoin 0.5~2%, water-solubleazone
0.5~2%, pyrrolidone sodium carboxylate 0.5~2%, surplus are water.
3. whitening anti-aging clarifying lotion as claimed in claim 1 or 2, it is characterised in that: the protein hydrolysate be rice bran protein,
One or more mixtures in avenin, modified oat albumen.
4. whitening anti-aging clarifying lotion as claimed in claim 3, it is characterised in that: the protein hydrolysate is modified oat egg
It is white.
5. whitening anti-aging clarifying lotion as claimed in claim 3, it is characterised in that: the protein hydrolysate is rice bran protein and changes
Property avenin mixture, the mass ratio of the rice bran protein and modified oat albumen is 1:(1-5).
6. whitening anti-aging clarifying lotion as claimed in claim 3, it is characterised in that: the avenin uses following methods system
It is standby to obtain: to weigh oat 8-12g, impregnated 30-60 minutes in 100-200mL ethyl alcohol, using 300 mesh filter-cloth filterings, filter cake exists
40-50 DEG C 30-60 minutes dry, crushes, and crosses 40-100 mesh, 1-3 hours dry at 40-50 DEG C, obtains oatmeal, oatmeal
In plus water 80-120mL, with 100-300 revs/min stirring 5-10 minutes, addition mixed enzyme 0.02-0.2 parts, 40-50 DEG C with
100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with 100-300 revs/min stirring 3-6 minutes, with 3000-5000
Rev/min centrifugation 10-20 minutes, supernatant is 4.0-4.5 with lemon acid for adjusting pH, with 100-300 revs/min stirring 5-10 minutes,
30-40 DEG C standing 40-80 minutes, then 2-8 DEG C of standing 5-10 hours with 3000-5000 revs/min centrifugation 10-20 minutes, under
Layer is deposited in 40-60 DEG C of drying to constant weight, obtains avenin.
7. such as the described in any item whitening anti-aging clarifying lotion of claim 3~5, it is characterised in that: the modified oat albumen
It is prepared using following methods: weighing oat 8-12g, impregnated 30-60 minutes in 100-200mL ethyl alcohol, filtered using 300 mesh
Cloth filtering, filter cake is 30-60 minutes dry at 40-50 DEG C, crushes, and crosses 40-100 mesh, 1-3 hours dry at 40-50 DEG C, obtains
Oatmeal, in oatmeal plus water 80-120mL, with 100-300 revs/min stirring 5-10 minutes, mixed enzyme 0.02-0.2 parts of addition,
40-50 DEG C with 100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with 100-300 revs/min stirring 3-6 minutes, with
3000-5000 revs/min centrifugation 10-20 minutes, supernatant is 4.0-4.5 with lemon acid for adjusting pH, with 100-300 revs/min stir
5-10 minutes, 30-40 DEG C standing 40-80 minutes, then 2-8 DEG C standing 5-10 hours with 3000-5000 revs/min of centrifugation 10-
20 minutes, lower sediment was dry to constant weight with water washing 1-3 times of 200-300mL, then at 40-60 DEG C, obtains avenin, will
Avenin and water 1:(40-60 in mass ratio) mixing, with 100-300 revs/min stirring 20-30 minutes, addition tea polyphenols,
20-30 DEG C with 100-300 revs/min stirring 1-3 hours, then 1-5 DEG C standing 10-20 hours, be with lemon acid for adjusting pH
4.0-4.5, with 100-300 revs/min stirring 5-10 minutes, 30-40 DEG C standing 40-80 minutes, then it is small in 2-8 DEG C of standing 5-10
When with 3000-5000 revs/min centrifugation 10-20 minutes, lower sediment is dry to constant weight at 40-60 DEG C, obtain modified oat albumen,
The mass ratio of the tea polyphenols and avenin is (1-3): (1-3).
8. whitening anti-aging clarifying lotion as claimed in claim 3 or 5, it is characterised in that: the rice bran protein uses following sides
Method is prepared: weighing rice bran 8-12g, impregnates 30-60 minutes in 100-200mL ethyl alcohol, using 300 mesh filter-cloth filterings, filter
Cake is 30-60 minutes dry at 40-50 DEG C, crushes, and crosses 40-100 mesh, 1-3 hours dry at 40-50 DEG C, obtains bran powder, rice
In chaff powder plus water 80-120mL, with 100-300 revs/min stirring 5-10 minutes, mixed enzyme 0.02-0.2 parts of addition, at 40-50 DEG C
With 100-300 revs/min stirring 1-3 hours, be warming up to 90-100 DEG C with 100-300 revs/min stirring 3-6 minutes, with 3000-5000
Rev/min centrifugation 10-20 minutes, supernatant is 4.0-4.5 with lemon acid for adjusting pH, with 100-300 revs/min stirring 5-10 minutes,
30-40 DEG C standing 40-80 minutes, then 2-8 DEG C of standing 5-10 hours with 3000-5000 revs/min centrifugation 10-20 minutes, under
Water washing 1-3 times of 200-300mL of layer precipitating, then it is dry to constant weight at 40-60 DEG C, obtain rice bran protein.
9. whitening anti-aging clarifying lotion as claimed in claim 1 or 2, it is characterised in that: the antioxidant be ophiopogonpolysaccharide and/
Or root bark of white mulberry polysaccharide.
10. such as the preparation method of the described in any item whitening anti-aging clarifying lotion of claim 1-9, it is characterised in that: by weight
Part weighs each raw material, and protein hydrolysate, antioxidant, hyaluronic acid, allantoin, water-solubleazone, pyrrolidone sodium carboxylate are added
Into water, 10~25 DEG C with 100-300 revs/min of stirring 10-20 minutes to get.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111544333A (en) * | 2020-05-18 | 2020-08-18 | 广州卡迪莲化妆品科技有限公司 | Polypeptide composition, moisturizing and anti-aging composition and cosmetic |
| WO2022218174A1 (en) * | 2021-04-16 | 2022-10-20 | 云南白药集团健康产品有限公司 | Preparation method for facial mask liquid, facial mask product, and application |
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2019
- 2019-01-29 CN CN201910084737.9A patent/CN109646318A/en not_active Withdrawn
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111544333A (en) * | 2020-05-18 | 2020-08-18 | 广州卡迪莲化妆品科技有限公司 | Polypeptide composition, moisturizing and anti-aging composition and cosmetic |
| CN111544333B (en) * | 2020-05-18 | 2021-09-14 | 广州卡迪莲化妆品科技有限公司 | Polypeptide composition, moisturizing and anti-aging composition and cosmetic |
| WO2022218174A1 (en) * | 2021-04-16 | 2022-10-20 | 云南白药集团健康产品有限公司 | Preparation method for facial mask liquid, facial mask product, and application |
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