CN109498526A - A kind of neck nursing composition and its preparation method and application - Google Patents
A kind of neck nursing composition and its preparation method and application Download PDFInfo
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- CN109498526A CN109498526A CN201811652646.2A CN201811652646A CN109498526A CN 109498526 A CN109498526 A CN 109498526A CN 201811652646 A CN201811652646 A CN 201811652646A CN 109498526 A CN109498526 A CN 109498526A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Abstract
The invention discloses a kind of neck nursing compositions and its preparation method and application.Composition of the present invention includes each component of following parts by weight: 0.1 ~ 3 part of Chinese gooseberry seed powder, 0.01 ~ 1 part of camellia seed oil, 0.01 ~ 1 part of peony seed oil, print plus 0.01 ~ 1 part of fruit seed oil, 0.001 ~ 1 part of bitter orange flower oil, 0.1 ~ 3 part of walnut parting.The present invention provides mild formula for neck skin feature, can effective cutin-softening unclogging, promote percutaneous absorption nutrition while removing neck skin surface rubbish, nourishing, whitening skin of neck, desalinate melanin deposition, plays moisturizing, moisturizing effects, skin quality applicability is fine.
Description
Technical field
Shield product technical field is washed the present invention relates to daily, more particularly, to a kind of neck nursing composition and its system
Preparation Method and application.
Background technique
The metabolism of human skin cell in cycles, has the cell largely die, while also can with the period
There is new cytothesis, the forming process of skin keratin mainly regenerates neoblast by base low layer cell division, about 28 days can be more
It is new primary, if be not added to clear up in time, the cutin membrane of accumulation will be formed in skin surface, it will cutaneous maintenance, resistance
Keep off the absorption to skincare product.
Neck is the position that aging occurs at first in women, and general women just will appear neck line to neck after 30 years old.With
The increase of life stress, more and more women will not merely shoulder the responsibility for having looked after family, while also throw oneself into workplace,
And with popularizing for electronic product, modern female is bowed increasingly to be grown using the time of electronic product, and neck line is caused to occur
Time is more and more early, " cyclic annular wrinkle " easy to form, will appear wrinkle as long as slightly careless, in addition, the collagen of neck skin
Protein content is fewer than face, thickness only has the 2/3 of facial skin, along with neck be responsible for supporting head part weight and human body rotation
Mechanism, the movement of the fierceness such as regular torsion can all allow the destruction of elastomer to accelerate, it is easy to which elastic force is tired.
The skin that often many women focus on face's nursing and have ignored neck is also required to nurse, and is on the one hand due to neck
Care product class is few, has a single function, and specific aim is poor, is on the other hand then that neck nursing is so convenient unlike washing one's face, causes very
More women do not know how nursing neck.In fact, neck is obligingly maintained with greater need for as facial skin.
Often absorbability is very poor for many neck nursing nourishing foods, has gone out product itself ingredient and has been difficult to absorb, and also one important
Reason is exactly that neck cuticula is blocked up, blocks neck percutaneous absorption nutrition.Existing market is directed to the skin care kind of neck nursing
Class is few, has a single function, and comfort level is low, even more fewer and fewer for the product of neck exfoliating, often produces with face's exfoliating
Product are general, and remove the product of neck cutin mostly on the market, and exfoliating intensity is big, meta-alkalescence, to neck surface skin sparing
Film is destroyed, degree of injury is big, is easy to damage neonatal cell structure, is kept skin fat secretion unbalance, skin of neck
Thinning, natural containment is destroyed, and skin is caused the more to wash the more dry, and causes skin of neck redness, shouting pain, drying, microgroove, mistake
The a series of neck skin problem such as quick.
Summary of the invention
The present invention is big for neck nursing product exfoliating intensity in the prior art, destruction skin of neck surface layer protective film,
The defects of easy allergy, neck cuticula can be effectively removed by providing a kind of neck nursing composition, while take good care of neck skin.
The present invention is another will to be solved the problems, such as to be to provide neck nursing composition and especially grinds preparing neck nursing product
Application in sand cream.
A present invention also technical problems to be solved are to provide the preparation method of neck nursing product.
A kind of neck nursing composition, each component including following parts by weight: 0.1~3 part of Chinese gooseberry seed powder, mountain
0.01~1 part of tea-seed oil, 0.01~1 part of peony seed oil, print plus 0.01~1 part of fruit seed oil, 0.001~1 part of bitter orange flower oil, English walnut
0.1~3 part of shell powder.
Preferably, each component including following parts by weight: 0.5 part of Chinese gooseberry seed powder, 0.1 part of camellia seed oil, male
Red 0.1 part of seed oil, print plus fruit seed oily 0.1 part, 0.01 part of bitter orange flower oil, 0.5 part of walnut parting.
Preferably, for the walnut parting by pretreatment, the preprocess method is to impregnate walnut parting by boiling water
Processing.
Preferably, the 3~8min of soaking time.
Further, the Chinese gooseberry seed powder and walnut parting partial size are 20~80 mesh.
Preferably, the Chinese gooseberry seed powder and walnut parting partial size are 30~50 mesh.
The present invention applies with providing neck nursing composition, applied to neck nursing product is prepared, is preferably applied to prepare
Neck nursing scrub cream.
The neck nursing scrub cream includes each component of following parts by weight: 80~100 parts of A phase raw material and B phase raw material 1
~10 parts；Wherein A phase raw material includes each component of following parts by weight: 78~90 parts of solvent, 5~15 parts of moisturizer, additive 1
~8 parts, 1~8 part of skin conditioning agent；B phase raw material includes each component of following parts by weight: neck nursing composition 0.5~5
Part, 0.1~5 part of solvent, 0.1~5 part of skin conditioning agent and 0.1~3 part of moisturizer.
Preferably, the neck nursing scrub cream includes following parts by weight component: 90~98 parts of A phase raw material former with B phase
2~6 parts of material；Wherein A phase raw material include 80~86 parts of solvent, 8~12 parts of moisturizer, 2~5 parts of additive, skin conditioning agent 2~
4 parts；B phase raw material includes: 1~3 part of neck nursing composition, 0.5~1 part of solvent, 0.5~3 part of skin conditioning agent and moisturizer
0.5~1.5 part.
It is further preferred that the neck nursing product includes following parts by weight component: 97.75 parts of A phase raw material and B phase
3.58 parts of raw material；Wherein A phase raw material includes following parts by weight component: 84.4 parts of solvent, 9.15 parts of moisturizer, additive 2.1
Part, 2.1 parts of skin conditioning agent；B phase raw material includes following parts by weight component: 1.31 parts of neck nursing composition, solvent 0.57
Part, 1 part of skin conditioning agent and 0.7 part of moisturizer.
Chinese gooseberry seed is abundant in Chinese gooseberry, protein, fat and minerals rich in, in addition Flavonoid substances
It is all most important presence in Chinese gooseberry seed with polyphenols and trace elements of selenium isoreactivity ingredient, they can not only be improved
Cell activity, moreover it is possible to inhibit cell carcinogenesis, there is good cancer-resisting effect.Contain a large amount of oil in Chinese gooseberry seed
Rouge contains some unsaturated fatty acids in these greases, can promote the metabolism of body fat mass in human body acid, and body can also be inhibited to consolidate gallbladder
The absorption of alcohol, and the Flavonoid substances that it contains can also soften blood vessel, avoid vascular sclerosis, prevent coagulating platelets, have
Reducing blood pressure and blood fat, hypoglycemic effect can be avoided blood lipid raising, the aging of delaying skin and blood vessel, and can delay
The aging of brain.Chinese gooseberry seed as scrub cream primary raw material in massage with the continuous frictional impact of neck skin, broken, more have
The nutritional ingredient in Chinese gooseberry seed is absorbed conducive to skin.
The unsaponifiable matter content of camellia seed oil is seldom, and containing substances such as camellianin, tsubakisaponin, tea polyphenols, camellianin has
Heart tonifying, thrombus dissolving effect, and tea polyphenols have a variety of effects such as reduction cholesterol, pre- preventing tumor.Camellia seed oil contains vitamin E
And antioxidant content, therefore it can protect skin, can especially prevent skin injury and aging, and skin is made to have gloss, allow skin
Moisturizing, lubrication prevent the appearance of dry line, so that skin is become delicate careful smooth flexible, wrinkle is reduced.
In peony seed oil, VA, VE, niacin, carrotene, unsaturated fatty acid content are abundant, have to skin fabulous
Nutritional Nursing Care effect, can obviously improve skin epidermal cells circulatory function, promote the microcirculation of capillary of skin, press down
The progress of lipid peroxidation processed improves metabolism, and delay skin aging process has crease-resistant, moisturizing whitening effect, uses
Skin smooth is light afterwards, has centainly to chloasma, skin aging wrinkle, skin keratin hardening decortication, wrinkled skin, dry skin
Therapeutic effect；The fine and smooth sense and elasticity of skin not only can be enhanced, while delaying senility can also be played, wrinkle resistant, removing calmness
Pigment and other effects.
Print plus fruit seed oil are rich in alpha-linolenic acid, are known as the title of long life oil king from print plus fruit seed.It can effective protection skin
Skin, keeps grease balance, and softening skin improves skin pattern.The loss for facilitating lasting control moisture of skin, keeps skin
More water is tender.Phenolic compound there are many containing in print plus fruit, equally has good free radical ability, and phenolic compound passes through blocking
The biography chain process of free radical chain, to block free radical chain and by acting on the relevant enzyme of free radical such as xanthine oxidase
(XOD), myeloperoxidase (MPO), lipoxidase and epoxidase etc. and prevent from aoxidizing.
Bitter orange flower oil can reduce the yield and mild and effective fungicide of sebum, and therefore, it is highly suitable for
In terms of skin care.There are clean and deodorization functions simultaneously, happy intense strain can be helped, especially felt down in spirits for a long time
Melancholia.Adjustable skin, removes acne and whelk of skin etc..
Dipotassium glycyrrhizinate can go deep into inside skin and keep high activity, whitening and high-efficiency antioxidant.Effectively inhibit melanin
The activity of a variety of enzymes in generating process, especially inhibition Tyrosine enzyme activity；Simultaneously also have prevent pachylosis and it is anti-inflammatory,
The effect of antibacterial.Dipotassium glycyrrhizinate is current good effect, full-featured whitening composition.It releives antiallergic, prevents exfoliating from causing
Discomfort.
Allantoin can promote the growth of cell tissue, can influence the quick spheroidizing of epidermis, and renewal process is accelerated.Work as allantois
When element is applied to ulcer and the skin of suppuration, these performances are particularly evident, so it, which has, accelerates speed of wound healing.Thus may be used
See, allantoin is a kind of activating agent of skin injury for the treatment of well.It is used in cosmetics, allantoin is good in addition to having
Outside repair function, it or a kind of good moisturizer and anti-sensitizer, holding moisture of skin maintain the physiology of skin moisture flat
Weighing apparatus；And alleviate stimulation of the active matter to skin.It or a kind of good cutin inorganic agent, it is same removing metabolism cutin
When, assign space between cells abundance moisture content, to it is coarse and cracking skin have good effect so that skin smooth and carefully
It is greasy.
Further, the solvent be water, PPG-26- butylol polyether -26, Cremophor RH40, Phenoxyethanol or
One of Sensiva SC50 is a variety of；Wherein, the water includes pure water, deionized water, drinking water, mineral water or note
It penetrates and uses one of water or a variety of；The moisturizer include one of glycerol, lactic acid, panthenol, Sodium Hyaluronate, allantoin or
It is a variety of；
Preferably, solvent described in A phase raw material is deionized water；
Preferably, solvent described in B phase raw material is that water, PPG-26- butylol polyether -26, Phenoxyethanol, ethylhexyl are sweet
Oil.
Further, the moisturizer is one or more of glycerol, lactic acid, panthenol, Sodium Hyaluronate or allantoin；
Preferably, moisturizer described in A phase raw material is glycerol, allantoin or Sodium Hyaluronate；
Preferably, moisturizer is lactic acid or panthenol in B phase raw material.
Further, the additive is dodecane hexadecyltrimethylammonium chloride or methyl hydroxybenzoate.
Further, the skin conditioning agent is water, lauroyl dilactic acid sodium, Cer NP, Cer AP II, plants
Object sphingol, cholesterine, carbomer, xanthan gum, Cer EOS, tocopherol acetate, Cremophor RH40, PEG-50
Rilanit special, nonyl phenol polyethers -20, propylene glycol, butanediol, 1,2- pentanediol, hydroxy phenylpropionyl amine benzoic acid, glycyrrhizic acid two
One of potassium or ascorbyl palmitate are a variety of；
Preferably, the skin conditioning agent in the A phase raw material is carbomer or dipotassium glycyrrhizinate；
Preferably, the skin conditioning agent in the B phase raw material is lauroyl dilactic acid sodium, Cer NP, ceramide
6II, phytosphingosine, cholesterine, carbomer, xanthan gum, Cer EOS, tocopherol acetate, Cremophor RH40,
PEG-50 rilanit special, nonyl phenol polyethers -20, propylene glycol, butanediol, 1,2- pentanediol, hydroxy phenylpropionyl amine benzoic acid or
Ascorbyl palmitate.
Preferably, the preparation method of neck nursing product includes following preparation step:
S1. A phase raw material is mixed in proportion, heats and stirs, it is to be mixed uniformly to obtain A phase raw mixture, it is spare；
S2. it by A phase raw mixture emulsifying obtained by step S1, vacuumizes, constant temperature；
S3. the material after emulsification obtained by step S2 is cooled down, B phase raw material is added, stirs；
S4. A, B phase raw mixture material obtained by step S3 are cooled down, discharging stands to get neck nursing scrub cream.
Further, heating described in step S1 is to carry out anti-penetration wastewater disposal by water phase pot, wherein heating temperature to 80
~90 DEG C, 15~60min of heating time；1~6min of emulsification times described in step S2, thermostat temperature are 40~60 DEG C, when constant temperature
Between 5~16min；Cooling temperature described in step S3 is 38~50 DEG C, stirs 20~40min；Cooling temperature 35 described in step S4~
45 DEG C, the 30~60min of time of repose.
Preferably, heating described in step S1 is to carry out anti-penetration wastewater disposal by water phase pot, and wherein heating temperature is to 85 DEG C,
Heating time 45min；Emulsification times 3min described in step S2, thermostat temperature are 50 DEG C, constant temperature time 10min；Described in step S3
The temperature that cools down is 45 DEG C, stirs 30min；Cool down 38 DEG C of temperature described in step S4, the time of repose 45min.
Neck texture construction, is configured with very big difference with face skin, collagen content is fewer than face, and thickness is only had the face
The quantity of 2/3rds of portion's skin, sebaceous glands and sweat gland only has the one third of skin of face, therefore skin of neck is very crisp
It is weak, ultraviolet light, temperature and humidity variation, or even improperly daily life system can all cause neck microgroove, neck has been responsible for supporting head part weight
Amount and the mechanism of human body rotation allow the destruction of elastomer to accelerate, and easily cause elastic force tired；The present invention is directed to neck feature, preparation
It is formulated the mild scrub cream that goes, cutin-softening unclogging promotes percutaneous absorption battalion while removing neck skin surface rubbish
It supports, melanin deposition is desalinated in nourishing, skin whitening.
The invention has the following advantages:
The present invention is using Chinese gooseberry seed powder combination walnut parting as cutin exfoliant, certainly by Chinese gooseberry seed powder
Body protein rich in and unsaturated fatty acid, it is neither too hard, nor too soft easily broken, it is aided with walnut parting, camellia seed oil, peony seeds
Oil, print plus fruit seed oil and bitter orange flower oil, are rich in multiple mineral element, and when Chinese gooseberry seed and skin massage, rub broken Shi Keqing
The pollution of clean pore inner wall and the rill of neck lines, while skin ph is adjusted, adjusting pore, who has balance；It is sweet by adding
Oxalic acid dipotassium gos deep into inside skin and keeps high activity, whitening and high-efficiency antioxidant, promotes the life of cell tissue using allantoin
It is long, the quick spheroidizing of epidermis is influenced, renewal process is promoted to accelerate；It is obtained with this and gos deep into Peppermint Extract, conditioning water and oil balance, powder
Fine and smooth, skin friendly, mild relax of matter supports, cleans moist neck nursing scrub cream.
The present invention scrub cream mild for the formula of neck feature preparation, effective cutin-softening unclogging remove neck
Promote percutaneous absorption nutrition while portion's skin surface rubbish, melanin deposition is desalinated in nourishing, skin whitening, is encountered newborn thin
Born of the same parents are directly melted into water, play moisturizing, moisturizing effects, and the present invention is suitble to the crowd of all kinds of skin quality to use.
Neck nursing composition exfoliating provided by the present invention is mild, non-stimulated, and gentle water profit has very old cutin
Good removal effect, takees good care of neonatal cell, moisturizing, moisturizing.
Neck nursing frosted paste composition prepared by the present invention is simply mild, and simple process is easily-controllable, is suitable for large-scale industry
Production, preparation section is simply controllable, and links up, and entire production process does not use security risks substance, and process is simple and environmentally-friendly,
It is green safe.
Specific embodiment
It is explained further and illustrates below with reference to embodiment, but specific embodiment does not have any type of limit to the present invention
It is fixed.Unless otherwise specified, method and apparatus used in embodiment is conventional method in that art and equipment, raw materials used is normal
Advise marketable material.
Primary raw material ingredient of the present invention removes specified otherwise, is that regular market purchase obtains, for convenience of description, providing can
The acquiring way of choosing is as follows:
Seed in Chinese gooseberry seed powder, that is, Fruits of Actinidia Chinensis Planch wins He Huagong purchased from Guangzhou, contains a large amount of oil
Rouge contains some unsaturated fatty acids in these greases, can promote the metabolism of body fat mass in human body acid, and delaying skin and blood vessel decline
Always.Chinese gooseberry seed is that the remaining a large amount of seed residues collected pass through or through China during Fruits of Actinidia Chinensis Planch is processed
The a large amount of seeds collected after kiwifruit fruit processing obtain after crushing drying.
Camellia seed oil is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, and camellia seed oil unsaponifiable matter content is seldom, contains
The substances such as camellianin, tsubakisaponin, tea polyphenols, camellianin have heart tonifying, thrombus dissolving effect, and tea polyphenols have reduce cholesterol,
A variety of effects such as pre- preventing tumor.
Print plus fruit seed oil are purchased from Sheng Jiya Co., Ltd, are rich in alpha-linolenic acid, and there are many phenolic compounds, equally have good
Good free radical ability, phenolic compound passes through the biography chain process for blocking free radical chain, to block free radical chain and pass through
Act on relevant enzyme of free radical such as xanthine oxidase (XOD), myeloperoxidase (MPO), lipoxidase and epoxidase etc.
And it prevents from aoxidizing.
Dipotassium glycyrrhizinate, regular market purchase, No. CAS: 68797-35-3, structural formula is as follows:
Dipotassium glycyrrhizinate is the effect of Radix Glycyrrhizae proposes neutralization acquisition through water ingredient, is extensively answered in medicine food and daily chemicals field
With in the present invention, being cooperateed with Purslane extract and play antibacterial removing toxic substances, anti-inflammatory antiallergic and other effects, and corticosteroid can be activated
Compound, promotes the absorption of skin care item at the effect of preventing cosmetic allergic contact dermatitis from reacting, with purslane extract synergy.
Carbomer, regular market purchase, No. CAS: 9007-20-9, carbomer is that acrylic acid is bonded allyl sucrose or Ji Wusi
The high molecular polymer of alcohol allyl ether.It is calculated by dry product, (- COOH) containing carboxylic acid group should be 56.0%~68.0%.Carbomer
Change colour with Resorcino, and with phenol, cationic polymer, the electrolyte of strong acid and high concentration is incompatible.
Allantoin, regular market purchase, CAS 97-59-6, structural formula are as follows:
Allantoin is a kind of hydantoin derivatives as made from glyoxalic acid, urea synthesizing, and allantoin can promote cell raw
Long, quickening wound healing, cutin-softening albumen simultaneously alleviate xerodermia, and in the present invention, it is just right that allantoin can play
Sterilization and anticorrosion, nourish moisturizing, it is anti-oxidant convergence etc. multi-efficiencies.
Embodiment 1 prepares neck nursing composition
0.1 part of walnut parting is put into boiling water and impregnates 5min, is filtered, it is spare, then by 0.1 part of Chinese gooseberry seed powder powder
30 mesh screens are crossed after broken, and soaked walnut parting, 0.01 part of camellia seed oil, 0.01 part of peony seed oil, 0.01 part of print is added and adds
Fruit seed oil and 0.001 part of bitter orange flower oil are uniformly mixed up to neck nursing composition.
Embodiment 2 prepares neck nursing composition
0.5 part of walnut parting is put into boiling water and impregnates 5min, is filtered, it is spare, then 0.5 part of Chinese gooseberry seed powder crushing
30 mesh screens are crossed afterwards, fall into the walnut parting after impregnating, and 0.1 part of camellia seed oil, 0.1 part of peony seed oil, 0.1 part of print plus fruit is added
Seed oil and 0.01 part of bitter orange flower oil are uniformly mixed up to neck nursing composition.
Embodiment 3 prepares neck nursing composition
3 parts of walnut partings are put into boiling water and impregnate 5min, filtering is spare, then 3 parts of Chinese gooseberry seed powder smash it through
30 mesh screens are added 1 part of camellia seed oil, 1 part of peony seed oil, 1 part of print plus fruit seed oil and 1 part of bitter orange flower oil, are uniformly mixed to obtain the final product
Neck nursing composition.
The preparation of 4 neck nursing scrub cream of embodiment
S1. by 78 parts, 3 parts glycerol of deionized water, 1 part of Sodium Hyaluronate, dodecane hexadecyltrimethylammonium chloride 0.5
Part, 0.5 part of methyl hydroxybenzoate, 0.5 part of carbomer, 0.5 part of dipotassium glycyrrhizinate, 1 part of allantoin mix in proportion, heating 15min extremely
It 80 DEG C and stirs, it is to be mixed uniformly to obtain A phase raw mixture, it is spare；
S2. 80 parts of A phase raw mixture emulsifying 3min obtained by step S1 are taken, are vacuumized, in 40 DEG C of constant temperature 5min；
S3. by 2 0.5 part of gained neck nursing composition of embodiment, 0.01 part, 0.005 part PPG-26- butylol polyether of water-
26,0.004 part, 0.004 part 0.005 part of Phenoxyethanol, 0.08 part of Sensiva SC50, tocopherol acetate PEG-40 hydrogenate castor
Sesame oil, 0.004 part of PEG-50 rilanit special, 0.004 part of nonyl phenol polyethers -20,0.004 part of propylene glycol, 0.002 part of lauroyl
Dilactic acid sodium, 0.004 part of Cer NP, 0.004 part of Cer AP II, 0.004 part of phytosphingosine, 0.004 part of cholesteric
Alcohol, 0.004 part of carbomer, 0.004 part of xanthan gum, 0.004 part of Cer EOS, 0.02 part of butanediol, 0.01 part of 1,2- penta 2
Alcohol, 0.01 part of hydroxy phenylpropionyl amine benzoic acid, 0.01 part of ascorbyl palmitate, 0.05 part of lactic acid, 0.05 part of panthenol mixing
Uniformly to get B phase raw material；The material after emulsification obtained by step S2 is cooled to 38 DEG C again, 1 part of B phase raw material is added, is sufficiently stirred
20min is uniform；
S4. A, B phase raw mixture material obtained by step S3 are cooled to 35 DEG C, discharging stands 30min to get neck
Manage scrub cream.
The preparation of 5 neck nursing scrub cream of embodiment
S1. by 84.4 parts, 9 parts glycerol of deionized water, 0.05 part of Sodium Hyaluronate, dodecane cetyl trimethyl chlorination
1.5 parts of ammonium, 0.6 part of methyl hydroxybenzoate, 1.5 parts of carbomer, 0.6 part of dipotassium glycyrrhizinate, 0.1 part of allantoin mix in proportion, heat
It 15min to 80 DEG C and stirs, it is to be mixed uniformly to obtain A phase raw mixture, it is spare；
S2. 97.75 parts of A phase raw mixture emulsifying 3min obtained by step S1 are taken, are vacuumized, in 40 DEG C of constant temperature
5min；
S3. by 2 1.31 parts of gained neck nursing composition of embodiment, 0.27 part, 0.1 part PPG-26- butylol polyether of water-
26,0.1 part of Phenoxyethanol, 0.1 part of Sensiva SC50,0.04 part, 0.04 part Cremophor RH40 of tocopherol acetate,
0.04 part of PEG-50 rilanit special, 0.04 part of nonyl phenol polyethers -20,0.04 part of propylene glycol, 0.02 part of lauroyl dilactic acid
Sodium, 0.04 part of Cer NP, 0.04 part of Cer AP II, 0.04 part of phytosphingosine, 0.04 part of cholesterine, 0.04 part of card wave
Nurse, 0.04 part of xanthan gum, 0.04 part of Cer EOS, 0.2 part of butanediol, 0.19 part of 1,2- pentanediol, 0.01 part of hydroxy phenylpropionyl
Amine benzoic acid, 0.1 part of ascorbyl palmitate, 0.2 part of lactic acid, 0.5 part of panthenol be uniformly mixed to get B phase raw material；It again will step
Material after emulsification obtained by rapid S2 is cooled to 38 DEG C, and 3.58 parts of B phase raw materials are added, it is uniform that 20min is sufficiently stirred；
S4. A, B phase raw mixture material obtained by step S3 are cooled to 38 DEG C, discharging stands 45min to get neck
Manage scrub cream.
The preparation of 6 neck nursing scrub cream of embodiment
S1. by 90 parts, 10 parts glycerol of deionized water, 1 part of Sodium Hyaluronate, dodecane hexadecyltrimethylammonium chloride 4
Part, 4 parts of methyl hydroxybenzoate, 4 parts of carbomer, 4 parts of dipotassium glycyrrhizinate, 4 parts of allantoin mix in proportion, heating 15min to 80 DEG C simultaneously
Stirring, it is to be mixed uniformly to obtain A phase raw mixture, it is spare；
S2. 100 parts of A phase raw mixture emulsifying 3min obtained by step S1 are taken, are vacuumized, in 40 DEG C of constant temperature 5min；
S3. by 25 parts of gained neck nursing composition of embodiment, 2 parts, 1 part PPG-26- butylol polyether -26 of water, benzene oxygen second
1 part of alcohol, 1 part of Sensiva SC50,2.5 parts, 1 part Cremophor RH40 of tocopherol acetate, 0.1 part of PEG-50 hydrogenate castor
Sesame oil, 0.1 part of nonyl phenol polyethers -20,0.1 part of propylene glycol, 0.1 part of lauroyl dilactic acid sodium, 0.1 part of Cer NP, 0.1
Part Cer AP II, 0.1 part of phytosphingosine, 0.1 part of cholesterine, 0.1 part of carbomer, 0.1 part of xanthan gum, 0.1 part of neural acyl
1,0.1 part of butanediol of amine, 0.19 part of 1,2- pentanediol, 0.01 part of hydroxy phenylpropionyl amine benzoic acid, 0.1 part of vitamin-c palmitate
Ester, 2 parts of lactic acid, 1 part of panthenol be uniformly mixed to get B phase raw material；The material after emulsification obtained by step S2 is cooled to 38 DEG C again,
10 parts of B phase raw materials are added, it is uniform that 20min is sufficiently stirred；
S4. A, B phase raw mixture material obtained by step S3 are cooled to 45 DEG C, discharging stands 60min to get neck
Manage scrub cream.
The preparation of 1 neck nursing scrub cream of comparative example
It is same as Example 5, the difference is that the Chinese gooseberry seed powder in B component is substituted for grape pip.
The preparation of 2 neck nursing scrub cream of comparative example
It is same as Example 5, the difference is that neck nursing composition in B component is free of camellia seed oil, peony seeds
Oil, print plus fruit seed oil and bitter orange flower oil.
The preparation of 3 neck nursing scrub cream of comparative example
It is same as Example 5, the difference is that being not added with dipotassium glycyrrhizinate in step S1.
The preparation of 4 neck nursing scrub cream of comparative example
It is same as Example 5, the difference is that being not added with allantoin in step S1.
The preparation of 5 neck nursing scrub cream of comparative example
For commercially available " fragrance Pei " exfoliating Exfoliating Scrub gel scrub cream product.
1. sample bacterium Indexs measure
According to neck nursing composition and scrub cream prepared by the embodiment of the present invention and comparative example, according to " cosmetics are pacified
Full technical specification " (version in 2015) " Micro biological Tests method " to the progress bacterial regrowth detection of neck nursing scrub cream, table 1 is neck
Nurse scrub cream sample bacterium Indexs measure data result in portion:
Table 1
As shown in Table 1, content of microorganisms meets " cosmetics in neck nursing composition and scrub cream prepared by the present invention
Technical specification of security " (version in 2015) " Micro biological Tests method " requirement.
2. chemical index
The neck nursing scrub cream prepared according to the embodiment of the present invention and comparative example is according to " cosmetics safety technical specification "
The inspection of the method for inspection the first method atomic absorption spectrophotometry, arsenic of lead in (version in 2015) " health chemical testing method "
Proved recipe method the first method hydride generation atomic fluorescence photometry, the detection method of mercury the second method hydride generation atomic fluorescence photometry and cadmium
Detection method atomic absorption spectrophotometry carries out lead, arsenic, mercury and cadmium content index to restructuring compound for the neck and detects.As a result such as table
Shown in 2；
Table 2
| Project | Lead (mg/kg) | Arsenic (mg/kg) | Mercury (mg/kg) | Cadmium (mg/kg) |
| Standard index | ≤10 | ≤2 | ≤1 | ≤5 |
| Embodiment 1 | ≤1 | ≤0.2 | ≤0.1 | ≤0.1 |
| Embodiment 2 | ≤1 | ≤0.2 | ≤0.1 | ≤0.1 |
| Embodiment 3 | ≤1 | ≤0.2 | ≤0.1 | ≤0.1 |
| Embodiment 4 | ≤1 | ≤0.5 | ≤0.1 | ≤0.5 |
| Embodiment 5 | ≤1 | ≤0.5 | ≤0.1 | ≤0.5 |
| Embodiment 6 | ≤1 | ≤0.5 | ≤0.1 | ≤0.5 |
| Comparative example 1 | ≤1 | ≤0.5 | ≤0.5 | ≤0.5 |
| Comparative example 2 | ≤1 | ≤0.5 | ≤0.5 | ≤0.5 |
| Comparative example 3 | ≤1 | ≤0.5 | ≤0.5 | ≤0.5 |
| Comparative example 4 | ≤1 | ≤0.5 | ≤0.5 | ≤0.5 |
| Comparative example 5 | ≤5 | ≤0.5 | ≤0.5 | ≤0.5 |
Neck scrub cream heavy metal component content prepared by the present invention meets " cosmetics safety technology rule as shown in Table 2
Model ".
3. materials safety specified risk material is assessed
Each formula material of neck nursing scrub cream of preparation of the embodiment of the present invention carries out the assessment of security risks substance, as a result
It is as shown in table 3:
Table 3
The safe devoid of risk of each material component of scrub cream prepared by the present invention as shown in Table 3, it is environmentally protective.
4. physicochemical property is evaluated and tested
Directly embodiment 4~6 and comparative example finished product are placed in 42 DEG C of constant temperature oven by resistance to Thermal test habit, protected
It holds 12 hours, then takes out placement and be cooled to room temperature, then observe variation before and after product test.Cold-resistant test is that finished product is placed
It in -20 DEG C of refrigerator, is kept for 24 hours, then takes out placement to room temperature, change before and after observing product test；PH value test
According to the measurement of " cosmetics safety technical specification " (version in 2015) " health chemical testing method " pH value.As a result such as table 4:
Table 4
Neck scrub cream prepared by the present invention is cold-resistant as shown in Table 4, anti-corrosion performance is good, and product stability is high, and pH value is moderate.
5. scrub cream effect detection is applied in test
The voluntary female volunteers that participate in try out of 300 ages between 25~50 years old are chosen, are divided into 6 groups, often
50 people of group, the scrub cream prepared respectively using embodiment 3 and comparative example 1~5, weekly using twice, after one month to effect into
Row detection, is tested, while assessing using effect using VISIA face-image analyzer, each 20 points, is averaged,
Standards of grading are as shown in table 5, and appraisal result is as shown in table 6.
Table 5
Table 6
6 result of table it is found that neck scrub cream prepared by the present invention can deep layer cleaning pore, effectively remove skin of neck angle
Matter avoids having dry skin, and keeps skin of neck smooth surface, promotes neck percutaneous absorption skin care item nutritional ingredient, simultaneously, moreover it is possible to
Antiallergic sense prevents part from reddening, and neck scrub cream exfoliating prepared by the present invention, antiallergy prevent dry skin effect obvious
Better than comparative example.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this
Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention
Protection scope within.
Claims (10)
1. a kind of neck nursing composition, which is characterized in that each component including following parts by weight: Chinese gooseberry seed powder
0.1 ~ 3 part, 0.01 ~ 1 part of camellia seed oil, 0.01 ~ 1 part of peony seed oil, print plus 0.01 ~ 1 part of fruit seed oil, bitter orange flower oil 0.001 ~ 1
Part, 0.1 ~ 3 part of walnut parting.
2. neck nursing composition according to claim 1, which is characterized in that including following parts by weight component: China
0.5 part of Chinese gooseberry seed powder, 0.1 part of camellia seed oil, 0.1 part of peony seed oil, print plus 0.1 part of fruit seed oil, 0.01 part of bitter orange flower oil, Hu
0.5 part of peach shell powder.
3. neck nursing composition according to claim 1 or 2, which is characterized in that the walnut parting passes through pretreatment,
The preprocess method is to impregnate walnut parting with boiling water.
4. application of any one of claims 1 to 3 neck nursing composition in neck nursing product；It is preferably applied to make
Standby neck nursing scrub cream.
5. application according to claim 4, which is characterized in that the neck nursing product includes each of following parts by weight
Component: 1 ~ 10 part of 80 ~ 100 parts of A phase raw material and B phase raw material；Wherein A phase raw material includes each component of following parts by weight: solvent
78 ~ 90 parts, 5 ~ 15 parts of moisturizer, 1 ~ 8 part of additive, 1 ~ 8 part of skin conditioning agent；B phase raw material includes each of following parts by weight
Component: 0.5 ~ 5 part of neck nursing composition, 0.1 ~ 5 part of solvent, 0.1 ~ 5 part and 0.1 ~ 3 part of moisturizer of skin conditioning agent.
6. application according to claim 5, which is characterized in that the solvent is water, PPG-26- butylol polyether -26, PEG-
One of 40 rilanit specials, Phenoxyethanol or Sensiva SC50 are a variety of；Wherein, the water is pure water, deionization
One of water, drinking water, mineral water or water for injection are a variety of；
It is preferred that solvent described in A phase raw material is deionized water；
It is preferred that solvent described in B phase raw material is water, PPG-26- butylol polyether -26, Phenoxyethanol, Sensiva SC50.
7. application according to claim 5, which is characterized in that the moisturizer is glycerol, lactic acid, panthenol, hyaluronic acid
One or more of sodium or allantoin；
It is preferred that moisturizer described in A phase raw material is glycerol, allantoin or Sodium Hyaluronate；
It is preferred that moisturizer is lactic acid or panthenol in B phase raw material.
8. application according to claim 5, which is characterized in that the additive is the chlorination of dodecane cetyl trimethyl
Ammonium or methyl hydroxybenzoate.
9. application according to claim 5, which is characterized in that the skin conditioning agent be water, lauroyl dilactic acid sodium,
Cer NP, Cer AP II, phytosphingosine, cholesterine, carbomer, xanthan gum, Cer EOS, tocopherol acetate,
Cremophor RH40, PEG-50 rilanit special, nonyl phenol polyethers -20, propylene glycol, butanediol, 1,2- pentanediol, oxybenzene
One of base propionamide benzoic acid, ascorbyl palmitate or dipotassium glycyrrhizinate are a variety of；
It is preferred that the skin conditioning agent in the A phase raw material is carbomer or dipotassium glycyrrhizinate；
It is preferred that the skin conditioning agent in the B phase raw material is lauroyl dilactic acid sodium, Cer NP, Cer AP II, plants
Object sphingol, cholesterine, carbomer, xanthan gum, Cer EOS, tocopherol acetate, Cremophor RH40, PEG-50
Rilanit special, nonyl phenol polyethers -20, propylene glycol, butanediol, 1,2- pentanediol, hydroxy phenylpropionyl amine benzoic acid or Vitamin C
Sour palmitate.
10. the preparation method of any one of the claim 1 ~ 8 neck nursing product, which is characterized in that walked including following preparation
It is rapid:
S1. A phase raw material is mixed in proportion, heats and stirs, it is to be mixed uniformly to obtain A phase raw mixture, it is spare；
S2. it by A phase raw mixture emulsifying obtained by step S1, vacuumizes, constant temperature；
S3. the material after emulsification obtained by step S2 is cooled down, B phase raw material is added, stirs；
S4. A, B phase raw mixture material obtained by step S3 are cooled down, discharging stands to get neck nursing scrub cream；
Heating described in preferred steps S1 is to carry out anti-penetration wastewater disposal by water phase pot, and wherein heating temperature is to 80 ~ 90 DEG C, heating
15 ~ 60min of time；1 ~ 6min of emulsification times described in preferred steps S2, thermostat temperature are 40 ~ 60 DEG C, 5 ~ 16min of constant temperature time；
Cooling temperature described in preferred steps S3 is 38 ~ 50 DEG C, stirs 20 ~ 40min；Cool down 35 ~ 45 DEG C of temperature described in preferred steps S4, institute
State 30 ~ 60min of time of repose.
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Application publication date: 20190322 |