CN109498513A - A kind of natural tricholoma matsutake and its application in mild shampoo - Google Patents
A kind of natural tricholoma matsutake and its application in mild shampoo Download PDFInfo
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- CN109498513A CN109498513A CN201811617026.5A CN201811617026A CN109498513A CN 109498513 A CN109498513 A CN 109498513A CN 201811617026 A CN201811617026 A CN 201811617026A CN 109498513 A CN109498513 A CN 109498513A
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- 241000121220 Tricholoma matsutake Species 0.000 title claims abstract description 96
- 239000002453 shampoo Substances 0.000 title claims abstract description 43
- 239000000284 extract Substances 0.000 claims abstract description 56
- 239000000463 material Substances 0.000 claims abstract description 51
- 241001088563 Trichotoma Species 0.000 claims abstract description 48
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000000706 filtrate Substances 0.000 claims abstract description 33
- 238000001914 filtration Methods 0.000 claims abstract description 31
- 239000000725 suspension Substances 0.000 claims abstract description 31
- 238000000034 method Methods 0.000 claims abstract description 28
- 238000010992 reflux Methods 0.000 claims abstract description 26
- 238000000605 extraction Methods 0.000 claims abstract description 25
- 235000019441 ethanol Nutrition 0.000 claims abstract description 19
- 230000006837 decompression Effects 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims description 33
- 244000302544 Luffa aegyptiaca Species 0.000 claims description 30
- 235000009814 Luffa aegyptiaca Nutrition 0.000 claims description 30
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 29
- 239000004744 fabric Substances 0.000 claims description 26
- 230000000855 fungicidal effect Effects 0.000 claims description 21
- 239000000417 fungicide Substances 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 20
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 19
- 244000020191 Salix babylonica Species 0.000 claims description 18
- 235000002493 Salix babylonica Nutrition 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 17
- 244000042664 Matricaria chamomilla Species 0.000 claims description 16
- 240000007817 Olea europaea Species 0.000 claims description 16
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 15
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 14
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 14
- 235000004429 Matricaria chamomilla var recutita Nutrition 0.000 claims description 14
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 14
- 229960000458 allantoin Drugs 0.000 claims description 14
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 14
- RZRNAYUHWVFMIP-HXUWFJFHSA-N glycerol monolinoleate Natural products CCCCCCCCC=CCCCCCCCC(=O)OC[C@H](O)CO RZRNAYUHWVFMIP-HXUWFJFHSA-N 0.000 claims description 14
- 229940074096 monoolein Drugs 0.000 claims description 14
- 229910052708 sodium Inorganic materials 0.000 claims description 14
- 239000011734 sodium Substances 0.000 claims description 14
- 239000001632 sodium acetate Substances 0.000 claims description 14
- 235000017281 sodium acetate Nutrition 0.000 claims description 14
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims description 14
- 229940119217 chamomile extract Drugs 0.000 claims description 13
- JDRSMPFHFNXQRB-IBEHDNSVSA-N decyl glucoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O JDRSMPFHFNXQRB-IBEHDNSVSA-N 0.000 claims description 13
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims description 13
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 10
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 10
- 241000235342 Saccharomycetes Species 0.000 claims description 10
- 241001312519 Trigonella Species 0.000 claims description 10
- 235000011187 glycerol Nutrition 0.000 claims description 9
- 238000002137 ultrasound extraction Methods 0.000 claims description 9
- 238000010792 warming Methods 0.000 claims description 8
- 229920000161 Locust bean gum Polymers 0.000 claims description 7
- 239000000711 locust bean gum Substances 0.000 claims description 7
- 235000010420 locust bean gum Nutrition 0.000 claims description 7
- 238000004321 preservation Methods 0.000 claims description 4
- 238000007873 sieving Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 2
- 241000228212 Aspergillus Species 0.000 claims 1
- 240000007594 Oryza sativa Species 0.000 claims 1
- 235000007164 Oryza sativa Nutrition 0.000 claims 1
- 150000001335 aliphatic alkanes Chemical group 0.000 claims 1
- 235000009566 rice Nutrition 0.000 claims 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims 1
- 238000009960 carding Methods 0.000 abstract description 9
- 230000003115 biocidal effect Effects 0.000 abstract description 7
- 208000001840 Dandruff Diseases 0.000 abstract description 6
- 230000036541 health Effects 0.000 abstract description 6
- 210000004761 scalp Anatomy 0.000 abstract description 4
- 230000003752 improving hair Effects 0.000 abstract description 3
- 241000050051 Chelone glabra Species 0.000 abstract description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 abstract 1
- 244000241872 Lycium chinense Species 0.000 description 18
- 235000015468 Lycium chinense Nutrition 0.000 description 18
- 239000000243 solution Substances 0.000 description 18
- 238000012360 testing method Methods 0.000 description 11
- 239000008367 deionised water Substances 0.000 description 10
- 229910021641 deionized water Inorganic materials 0.000 description 10
- 240000006439 Aspergillus oryzae Species 0.000 description 9
- 235000002247 Aspergillus oryzae Nutrition 0.000 description 9
- 241000894006 Bacteria Species 0.000 description 8
- 125000005227 alkyl sulfonate group Chemical group 0.000 description 8
- -1 polyoxy Ethylene ether sulfate Polymers 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 241001278097 Salix alba Species 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 238000000855 fermentation Methods 0.000 description 5
- 230000004151 fermentation Effects 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 241000226556 Leontopodium alpinum Species 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 241000555688 Malassezia furfur Species 0.000 description 3
- 244000241838 Lycium barbarum Species 0.000 description 2
- 235000015459 Lycium barbarum Nutrition 0.000 description 2
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 2
- 235000002725 Olea europaea Nutrition 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000006916 nutrient agar Substances 0.000 description 2
- 239000008223 sterile water Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 244000012254 Canarium album Species 0.000 description 1
- 235000009103 Canarium album Nutrition 0.000 description 1
- 240000008886 Ceratonia siliqua Species 0.000 description 1
- 235000013912 Ceratonia siliqua Nutrition 0.000 description 1
- 235000007866 Chamaemelum nobile Nutrition 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000241257 Cucumis melo Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241001360526 Escherichia coli ATCC 25922 Species 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- 241000226555 Leontopodium Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 description 1
- 241000208292 Solanaceae Species 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000004500 asepsis Methods 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920006317 cationic polymer Polymers 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- RJWRQCMERCINIU-UHFFFAOYSA-L disodium 2-(carboxylatomethylamino)tetradecanoate Chemical compound [Na+].C(CCCCCCCCCCC)C(C(=O)[O-])NCC(=O)[O-].[Na+] RJWRQCMERCINIU-UHFFFAOYSA-L 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229960005150 glycerol Drugs 0.000 description 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 description 1
- 239000004247 glycine and its sodium salt Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229940029258 sodium glycinate Drugs 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Botany (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of natural tricholoma matsutake and its applications in mild shampoo.The natural mushroom extract is prepared by the following method: Trichotoma matsutake being crushed, is sieved, obtains Trichotoma matsutake crushed material；Trichotoma matsutake crushed material and water are mixed evenly S2, obtain suspension；Ethyl alcohol is added into suspension by S3,60-70 DEG C refluxing extraction 60-120 minutes, filtering, filtrate decompression concentration to get.Compared with prior art, natural tricholoma matsutake of the invention is applied in mild shampoo, the mild shampoo being prepared is rich in active skull cap components, it does not stimulate mildly, health environment-friendly effectively moistens scared, the carding property and scalp biocidal property for improving hair, reduce the generation of dandruff.
Description
Technical field
The present invention relates to daily chemical product technical fields, and in particular to a kind of natural tricholoma matsutake and its mild
Application in shampoo.
Background technique
There is no too many requirement when past people select shampoo, only requiring can be the dust and grease on hair
It washes away, but with the development of the society, people have been not content with only cleans hair, and is desirable to after hair washes
Can it is smooth it is submissive, it is easy combing and health it is glossy.In order to meet the needs of market, shampoo manufacturers continuously attempt to release new
Product, but for the quality of shampoo, there is no too big breakthroughs, close two until Procter & Gamble is proposed hair-washing hair-care at first
For one conditioner shampoo, market is opened from this Two-in-one shampoo in China, this is the revolution in shampoo history.Conditioning
Shampoo can not only clean hair, and the cardability that can also most importantly improve hair, is repaired at the glossiness for improving hair
Jag sends out tip etc..Since multiple functions can be completed once, it is well received by consumers.Shampoo brand currently on the market
It is numerous, but mostly use and hair washing product is made with industrial chemicals, these raw materials include: cationic polymer, silicone oil, fatty alcohol polyoxy
Ethylene ether sulfate, alkanolamide amine oxide etc., the chemical raw material majority of these chemical industry synthesis is to skin and the irritating work of hair
With the delicate skin of unsuitable baby is used for a long time harmful to the health of skin.
The present invention provides a kind of mild natural tricholoma matsutake, by will extract after Trichotoma matsutake drying and crushing with sponge gourd
Refluxing extraction obtains object after fermentation process together；It mildly has one's hair wash applied to the mild shampoo in mild shampoo, being prepared
Water does not stimulate mildly, health environment-friendly, effectively moistens scared, improves the carding property and scalp biocidal property of hair, reduces dandruff
Generation.
Summary of the invention
Aiming at the above shortcomings existing in the prior art, technical problem to be solved by the invention is to provide a kind of mild
Natural tricholoma matsutake, by by refluxing extraction obtains after fermentation process together with Fructus Luffae extract after Trichotoma matsutake drying and crushing
It arrives；Applied to the mild shampoo of mild shampoo in mild shampoo, being prepared, do not stimulate mildly, health environment-friendly, effectively
It moistens scared, improves the carding property and scalp biocidal property of hair, reduce the generation of dandruff.
Specific technical solution is as follows:
A kind of natural tricholoma matsutake, is prepared using following methods:
S1 crushes Trichotoma matsutake, and sieving obtains Trichotoma matsutake crushed material；
Trichotoma matsutake crushed material and water are mixed evenly S2, obtain suspension；
Ethyl alcohol is added into suspension by S3,60-70 DEG C refluxing extraction 60-120 minutes, filtering, filtrate decompression concentration, i.e.,
?.
In one of embodiment of the present invention, a kind of natural tricholoma matsutake is prepared using following methods:
S1 crushes Trichotoma matsutake, and sieving obtains Trichotoma matsutake crushed material；
Stripping and slicing after fresh loofah peeling is obtained block by S2, and block and water are mixed, at ultrasonic extraction 60-90 points
Clock, filtering, obtained filtrate are sponge gourd extracting solution；
S3 mixes Trichotoma matsutake crushed material and sponge gourd extracting solution, stirs evenly, and obtains suspension, fermentation is added in suspension
Bacterium is stirred, and obtains mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, after sterilizing be added 15-25 parts of ethyl alcohol,
60-70 DEG C refluxing extraction 60-120 minutes, filtering, filtrate decompression concentration to get.
A kind of preferred technical solution, a kind of natural tricholoma matsutake are prepared using following methods, and described part is equal
For parts by weight:
S1 crushes Trichotoma matsutake, crosses 40-60 mesh, obtains Trichotoma matsutake crushed material；
S2 will be cut into (1-10) mm × (1-10) mm × (1-10) mm block after fresh loofah peeling, by 2-8 parts of blocks
Shape object and the mixing of 10-20 parts of water, 40-60 DEG C ultrasonic extraction 60-90 minutes, using 500-800 mesh filter-cloth filtering, filtrate is silk
Melon extracting solution；
S3 mixes 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of sponge gourd extracting solutions, with 100-300 revs/min of stirring 5-10
Minute, obtain suspension, 0.002-0.02 parts of zymophytes be added in suspension, with 100-300 revs/min stirring 5-10 minutes, obtain
To mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, then 95-100 DEG C of sterilizing 10-20 minutes is warming up to, after sterilizing
Mixture in be added 15-25 part ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, use 500-800 mesh filter cloth mistake
Filter, filtrate decompression be concentrated into 50 DEG C density be 1.10-1.15g/mL to get.
The zymophyte is saccharomycete and/or aspergillus oryzae；Preferably, the zymophyte is that saccharomycete and aspergillus oryzae press quality
It is mixed than 1:1.
The invention also discloses application of the above-mentioned natural tricholoma matsutake in mild shampoo.
Concrete application is as follows:
A kind of mild shampoo is made of the raw material of following parts by weight meter: 10-15 parts of lauryl both sexes sodium acetate, decyl
3-8 parts of glucoside, 3-8 parts of sodium secondary alkyl sulfonate, 1-5 parts of sodium cocoyl glycinate, 1-5 parts of glycerine, Monoolein
0.2-2 parts, 0.1-1 parts of german chamomile extract, 0.1-1 parts of olive extract, 0.1-1 parts of edenweiss flower extract, allantoin 0.1-0.3
Part, tricholoma matsutake 1-2 parts natural, 1-2 parts of fungicide, 0.1-1 parts of conditioner, 100-150 parts of water；It weighs by weight each
Raw material heats water to 75-85 DEG C, sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, cocounut oil
Acyl Sodium Glycinate, glycerine, Monoolein, 75-85 DEG C with 100-300 revs/min stirring 20-40 minutes, be cooled to 45-
55 DEG C, german chamomile extract, olive extract, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, tune is added
Manage agent, with 40-100 revs/min of stirring 40-60 minutes to get.
The fungicide is Cortex Lycii extract and/or Salix Babylonica L.P.E；Preferably, the fungicide mentions for the root bark of Chinese wolf-berry
Take the mixture of object and Salix Babylonica L.P.E, the mass ratio of the Cortex Lycii extract and Salix Babylonica L.P.E is (1-5): (1-
5)。
The conditioner is trigonella bean gum and/or locust bean gum；Preferably, the conditioner is trigonella bean gum and locust bean
The mass ratio of the mixture of glue, the trigonella bean gum and locust bean gum is 1:(1-5).
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40-60 mesh obtains root bark of Chinese wolf-berry crushed material, and the 1-5 parts and water 20-30 parts mixing of root bark of Chinese wolf-berry crushed material are mentioned in 80-90 DEG C of reflux
It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40-60 mesh obtains salicis,cortex crushed material, and the 1-5 parts and water 20-30 parts mixing of salicis,cortex crushed material are mentioned in 80-90 DEG C of reflux
It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained
To Salix Babylonica L.P.E.
Natural tricholoma matsutake of the invention is applied in mild shampoo, the mild shampoo being prepared is rich in
Active skull cap components do not stimulate mildly, health environment-friendly, effectively moisten scared, improve the carding property and scalp biocidal property of hair,
Reduce the generation of dandruff.
Specific embodiment
In the present invention, if not refering in particular to, all devices and raw material is commercially available or the industry is common are following
Method in embodiment is unless otherwise instructed conventional method in that art.
Olive (Canariumalbum (Lour.) Raeusch.) uses Olive leaf P.E in embodiment, specific to use
The Olive leaf P.E that Shaanxi Sen Fu natural product Co., Ltd provides, specification 10:1.
German chamomile (Matricariarecutita) also known as chamomile are had using Shaanxi Pa Nier biotechnology in embodiment
Flos Chrysanthemi/leaf/stem extraction of limit company production.
Edelweiss also known as edelweiss (Leontopodiumalpinum), are composite families, and the plant of Leontopodium is implemented
The flower extract of the edelweiss provided in example using Shaanxi Cheng Gan Biotechnology Co., Ltd, specification 10:1.
The root bark of Chinese wolf-berry is matrimony vine of solanaceae plant LyciumchinenseMill.'s or lycium barbarum LyciumbarbarumL.
Dry root skin.Bozhou treasured giant Science and Technology Ltd. provides, source area: Gansu.
Salicis,cortex, the drying stem skin of white willow (Salix alba L.), Danfeng County high mountain medicine company Co., Ltd provide,
Source area: Shaanxi.
Sponge gourd, using commercially available fresh patola.
Lauryl both sexes sodium acetate, chemical name: lauryl Iminodiacetic acid sodium salt is produced using BASF in embodiment
LAD-30.
Sodium secondary alkyl sulfonate, the SAS-60 produced using German Clariant.
Plantacare 818, No. CAS: 68515-73-1, Shanghai Bepharm Science & Technology Co., Ltd.'s production, product number:
BD233981。
Sodium cocoyl glycinate, No. CAS: 90387-74-9, Shouguang City's Coudé chemical industry has new company's offer, model KD-
552。
Glycerine, No. CAS: 56-81-5, it buys from this biochemical technology Co., Ltd of Tianjin Skien.
Monoolein, No. CAS: 111-03-5, it buys from Shanghai Aladdin biochemical technology limited liability company, product
Number: M107454.
Allantoin, No. CAS: 97-59-6, it buys from Shanghai Yuan Ye Biotechnology Co., Ltd.
Trichotoma matsutake, Classification system: Tricholoma matsutake (lto et lmai) Singer also known as matsutake use
The drying matsutake that Yanji sincerity matsutake Trade Co., Ltd., Jilin Province provides, source area: Changbai mountain, Jilin.
Trigonella bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Locust bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Aspergillus oryzae, purchase is from Chinese industrial Culture Collection, and culture presevation number: CICC2002, viable bacteria are dense
Degree is 1 × 1010CFU/g。
Saccharomycete, using purchase from the saccharomyces cerevisiae of Chinese industrial Culture Collection, culture presevation is numbered:
CICC1060, viable bacteria concentration are 1 × 1010CFU/g。
Fungistatic effect test: by strain inoculated on the nutrient agar panel to have sterilized, being placed in (36 ± 1) DEG C insulating box
Bacterial strain for 24 hours, is transferred in the nutrient agar test tube slant to have sterilized with oese, is placed in (36 ± 1) DEG C insulating box by culture
Culture is for 24 hours.Sterile saline or sterile water shaken well is added in the strain test tube slant that recovery is completed again, it is outstanding to be made into bacterium
Liquid, when testing, by 0.1mL bacteria suspension be made in sterile water concentration be 5 × 104The bacteria suspension dilution of cfu/mL.Using
Beating holes method, with aseptic cotton carrier by concentration be 5 × 104The experiment bacteria suspension of cfu/mL, in lecithin, Tween-80 nutrition fine jade
Rouge plating medium surface is uniformly smeared 3 times, and drying at room temperature 5min is placed.Then the sterile round punch for being 3cm with diameter
Punching takes appropriate mild shampoo, with 100 times of normal saline dilution of its quality, in adding hole, until filling it up with, must not overflow,
Do 3 groups of parallel laboratory tests.Culture dish is placed in (36 ± 1) DEG C insulating box again and cultivates 18h, takes out observation, it is antibacterial with calliper to measure
The diameter of circle, boundary is in the antibacterial ring size outer for being born long using integral asepsis.Surveyed bacterial strain is escherichia coli ATCC 25922, chaff
Not plump chlosma (Malassezia furfur) CMCC (F) Y17.
Hair setting measure of merit: referring to the Master's thesis " modification of hydroxyethyl cellulose and in shampoo of Lv Miao
Application study " method in 3.3.2 section, test wet carding property and dry carding property, and combing power is calculated according to combing curve.
Embodiment 1
Mild shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl sulfonic acid
5 parts of sodium, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive extract
0.5 part, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of natural tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is Cortex Lycii extract.
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, stir 8 points with 200 revs/min
Clock, obtains suspension, and 20 parts of ethyl alcohol are added in suspension, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings,
It is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, obtains natural Trichotoma matsutake and extracts
Object.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The preparation method of the mild shampoo, comprising the following steps: weigh each raw material by weight, by deionized water plus
Heat sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, the third three to 80 DEG C
Alcohol, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract are added, olive extracts
Object, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 2
Substantially the same manner as Example 1, difference is only that:
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
Embodiment 3
Substantially the same manner as Example 1, difference is only that:
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts
Block and the mixing of 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh
Filter-cloth filtering, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, are stirred with 200 revs/min
It mixes 8 minutes, obtains suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, stir 8 points with 200 revs/min
Clock obtains mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, the mixture after sterilizing
20 parts of ethyl alcohol of middle addition, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
Embodiment 4
Mild shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl sulfonic acid
5 parts of sodium, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive extract
0.5 part, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of natural tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is Salix Babylonica L.P.E.
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts
Block and the mixing of 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh
Filter-cloth filtering, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, are stirred with 200 revs/min
It mixes 8 minutes, obtains suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, stir 8 points with 200 revs/min
Clock obtains mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, the mixture after sterilizing
20 parts of ethyl alcohol of middle addition, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild shampoo, comprising the following steps: weigh each raw material by weight, by deionized water plus
Heat sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, the third three to 80 DEG C
Alcohol, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract are added, olive extracts
Object, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 5
Mild shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl sulfonic acid
5 parts of sodium, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive extract
0.5 part, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of natural tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts
Block and the mixing of 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh
Filter-cloth filtering, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, are stirred with 200 revs/min
It mixes 8 minutes, obtains suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, stir 8 points with 200 revs/min
Clock obtains mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, the mixture after sterilizing
20 parts of ethyl alcohol of middle addition, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild shampoo, comprising the following steps: weigh each raw material by weight, by deionized water plus
Heat sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, the third three to 80 DEG C
Alcohol, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract are added, olive extracts
Object, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 6
Mild shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl sulfonic acid
5 parts of sodium, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive extract
0.5 part, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of natural tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is locust bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts
Block and the mixing of 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh
Filter-cloth filtering, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, are stirred with 200 revs/min
It mixes 8 minutes, obtains suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, stir 8 points with 200 revs/min
Clock obtains mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, the mixture after sterilizing
20 parts of ethyl alcohol of middle addition, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild shampoo, comprising the following steps: weigh each raw material by weight, by deionized water plus
Heat sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, the third three to 80 DEG C
Alcohol, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract are added, olive extracts
Object, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 7
Mild shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl sulfonic acid
5 parts of sodium, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive extract
0.5 part, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of natural tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is the mixture of trigonella bean gum and locust bean gum, the mass ratio of the trigonella bean gum and locust bean gum
For 1:4.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The natural tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake powder
It is broken, 40 meshes are crossed, Trichotoma matsutake crushed material is obtained, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts
Block and the mixing of 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh
Filter-cloth filtering, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, are stirred with 200 revs/min
It mixes 8 minutes, obtains suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, stir 8 points with 200 revs/min
Clock obtains mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, the mixture after sterilizing
20 parts of ethyl alcohol of middle addition, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains natural tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild shampoo, comprising the following steps: weigh each raw material by weight, by deionized water plus
Heat sequentially adds lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, the third three to 80 DEG C
Alcohol, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract are added, olive extracts
Object, edenweiss flower extract, allantoin, natural tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Test case 1
The mild shampoo fungistatic effect that embodiment is prepared is tested, specific test result is shown in Table 1.
The mild shampoo antibacterial circle diameter test result table of table 1
| Escherichia coli, mm | Malassezia furfur, mm | |
| Embodiment 1 | 16.6 | 17.2 |
| Embodiment 2 | 16.8 | 17.5 |
| Embodiment 3 | 17.4 | 17.9 |
| Embodiment 4 | 17.2 | 17.7 |
| Embodiment 5 | 18.2 | 19.0 |
| Embodiment 6 | 17.8 | 18.8 |
| Embodiment 7 | 18.6 | 19.7 |
From table 1 it follows that antibacterial circle diameter is greater than 15mm, there is good biocidal property.Especially to chaff horse traction
Color bacterium has significant biocidal property, and Malassezia furfur is the main reason for causing dandruff to generate, it is seen then that of the invention is mild
The antibacterial generation that can significantly inhibit dandruff of shampoo.
Test case 2
The mild shampoo carding property that embodiment is prepared is tested, specific test result is shown in Table 2.
2 carding property test result table of table
| Wet combing power | Dry combing power | |
| Embodiment 1 | 9687 | 6431 |
| Embodiment 2 | 9603 | 6338 |
| Embodiment 3 | 9482 | 6205 |
| Embodiment 4 | 9536 | 6253 |
| Embodiment 5 | 9376 | 6064 |
| Embodiment 6 | 9405 | 6125 |
| Embodiment 7 | 9166 | 5789 |
Embodiment 3 ferments to Trichotoma matsutake using sponge gourd extracting solution, then extracts to fermentation material, the biocidal property of hair
Embodiment 1-2 can be significantly better than with carding property.Containing nutriment needed for fermenting microbe in sponge gourd extracting solution, hair can promote
Ferment carries out, and fermentation process discharges the effective active composition of Trichotoma matsutake sufficiently, promotes the active component content in extract, from
And promote the performance of mild shampoo.
Claims (6)
1. a kind of natural tricholoma matsutake, which is characterized in that be prepared using following methods:
S1 crushes Trichotoma matsutake, and sieving obtains Trichotoma matsutake crushed material；
Trichotoma matsutake crushed material and water are mixed evenly S2, obtain suspension；
Ethyl alcohol is added into suspension by S3,60-70 DEG C refluxing extraction 60-120 minutes, filtering, filtrate decompression concentration to get.
2. a kind of natural tricholoma matsutake, which is characterized in that be prepared using following methods:
S1 crushes Trichotoma matsutake, and sieving obtains Trichotoma matsutake crushed material；
Stripping and slicing after fresh loofah peeling is obtained block by S2, and block and water are mixed, at ultrasonic extraction 60-90 minutes, mistake
Filter, obtained filtrate are sponge gourd extracting solution；
S3 mixes Trichotoma matsutake crushed material and sponge gourd extracting solution, stirs evenly, obtains suspension, zymophyte is added in suspension,
Be stirred, obtain mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, after sterilizing be added 15-25 parts of ethyl alcohol,
60-70 DEG C refluxing extraction 60-120 minutes, filtering, filtrate decompression concentration to get.
3. natural tricholoma matsutake as claimed in claim 2, which is characterized in that it is prepared using following methods, it is described
Part is parts by weight:
S1 crushes Trichotoma matsutake, crosses 40-60 mesh, obtains Trichotoma matsutake crushed material；
S2 will be cut into (1-10) mm × (1-10) mm × (1-10) mm block after fresh loofah peeling, by 2-8 parts of blocks
Mixed with 10-20 parts of water, 40-60 DEG C ultrasonic extraction 60-90 minutes, using 500-800 mesh filter-cloth filtering, filtrate mentions for sponge gourd
Take liquid；
S3 mixes 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of sponge gourd extracting solutions, with 100-300 revs/min stirring 5-10 minutes,
Obtain suspension, 0.002-0.02 parts of zymophytes be added in suspension, with 100-300 revs/min stirring 5-10 minutes, mixed
Material, by mixture 25-35 DEG C heat preservation 24-48 hours, then be warming up to 95-100 DEG C of sterilizing 10-20 minutes, the mixing after sterilizing
In material be added 15-25 part ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, use 500-800 mesh filter-cloth filtering, filtrate
Be concentrated under reduced pressure into 50 DEG C density be 1.10-1.15g/mL to get.
4. natural tricholoma matsutake as claimed in claim 3, it is characterised in that: the zymophyte is saccharomycete and/or rice
Aspergillus.
5. such as application of the described in any item natural tricholoma matsutakes of Claims 1 to 4 in mild shampoo.
6. natural application of the tricholoma matsutake in mild shampoo as claimed in claim 5, which is characterized in that the temperature
It is made of with shampoo the raw material of following parts by weight meter: 10-15 parts of lauryl both sexes sodium acetate, 3-8 parts of Plantacare 818, secondary alkane
3-8 parts of base sodium sulfonate, 1-5 parts of sodium cocoyl glycinate, 1-5 parts of glycerine, 0.2-2 parts of Monoolein, german chamomile extract
0.1-1 parts, 0.1-1 parts of olive extract, 0.1-1 parts of edenweiss flower extract, 0.1-0.3 parts of allantoin, such as Claims 1 to 4
Described in any item natural tricholoma matsutake 1-2 parts, 1-2 parts of fungicide, 0.1-1 parts of conditioner, 100-150 parts of water；It is described
Fungicide is Cortex Lycii extract and/or Salix Babylonica L.P.E；The conditioner is trigonella bean gum and/or locust bean gum.
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| CN111481477A (en) * | 2020-05-27 | 2020-08-04 | 融致丰生制药有限公司 | Matsutake extract for repairing damaged hair and delaying scalp aging, composition and application |
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