CN109431916A - Mild baby shampoo and preparation method thereof - Google Patents
Mild baby shampoo and preparation method thereof Download PDFInfo
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- CN109431916A CN109431916A CN201811617034.XA CN201811617034A CN109431916A CN 109431916 A CN109431916 A CN 109431916A CN 201811617034 A CN201811617034 A CN 201811617034A CN 109431916 A CN109431916 A CN 109431916A
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- extract
- matsutake
- crushed
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- 239000002453 shampoo Substances 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 241000121220 Tricholoma matsutake Species 0.000 claims abstract description 85
- 239000000284 extract Substances 0.000 claims abstract description 59
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 34
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims abstract description 33
- 230000000855 fungicidal effect Effects 0.000 claims abstract description 24
- 239000000417 fungicide Substances 0.000 claims abstract description 24
- 244000042664 Matricaria chamomilla Species 0.000 claims abstract description 18
- 240000007817 Olea europaea Species 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 17
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims abstract description 17
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 claims abstract description 16
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims abstract description 16
- 235000004429 Matricaria chamomilla var recutita Nutrition 0.000 claims abstract description 16
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims abstract description 16
- 229960000458 allantoin Drugs 0.000 claims abstract description 16
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims abstract description 16
- 235000011187 glycerol Nutrition 0.000 claims abstract description 16
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 16
- 239000011734 sodium Substances 0.000 claims abstract description 16
- 239000001632 sodium acetate Substances 0.000 claims abstract description 16
- 235000017281 sodium acetate Nutrition 0.000 claims abstract description 16
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims abstract description 16
- RZRNAYUHWVFMIP-HXUWFJFHSA-N glycerol monolinoleate Natural products CCCCCCCCC=CCCCCCCCC(=O)OC[C@H](O)CO RZRNAYUHWVFMIP-HXUWFJFHSA-N 0.000 claims abstract description 15
- 229940074096 monoolein Drugs 0.000 claims abstract description 15
- 229940119217 chamomile extract Drugs 0.000 claims abstract description 14
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 11
- 125000005227 alkyl sulfonate group Chemical group 0.000 claims abstract description 11
- 239000000463 material Substances 0.000 claims description 54
- 241001088563 Trichotoma Species 0.000 claims description 42
- 239000000203 mixture Substances 0.000 claims description 37
- 239000004744 fabric Substances 0.000 claims description 32
- 239000000706 filtrate Substances 0.000 claims description 32
- 238000000034 method Methods 0.000 claims description 30
- 239000000725 suspension Substances 0.000 claims description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 26
- 238000010992 reflux Methods 0.000 claims description 25
- 238000001914 filtration Methods 0.000 claims description 24
- 244000302544 Luffa aegyptiaca Species 0.000 claims description 23
- 235000009814 Luffa aegyptiaca Nutrition 0.000 claims description 23
- 238000000605 extraction Methods 0.000 claims description 23
- 238000003756 stirring Methods 0.000 claims description 23
- 244000020191 Salix babylonica Species 0.000 claims description 21
- 235000002493 Salix babylonica Nutrition 0.000 claims description 21
- 244000241872 Lycium chinense Species 0.000 claims description 20
- 235000015468 Lycium chinense Nutrition 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 14
- 235000019441 ethanol Nutrition 0.000 claims description 13
- 230000001954 sterilising effect Effects 0.000 claims description 13
- 240000006439 Aspergillus oryzae Species 0.000 claims description 11
- 235000002247 Aspergillus oryzae Nutrition 0.000 claims description 11
- 241000235342 Saccharomycetes Species 0.000 claims description 11
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 10
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 10
- 241001312519 Trigonella Species 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 230000006837 decompression Effects 0.000 claims description 9
- 229920000161 Locust bean gum Polymers 0.000 claims description 8
- 239000000711 locust bean gum Substances 0.000 claims description 8
- 235000010420 locust bean gum Nutrition 0.000 claims description 8
- 238000002137 ultrasound extraction Methods 0.000 claims description 7
- 229960005150 glycerol Drugs 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 3
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 2
- -1 decyl glucose Glycosides Chemical class 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 244000241257 Cucumis melo Species 0.000 claims 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims 1
- 241000124033 Salix Species 0.000 claims 1
- 241000899950 Salix glauca Species 0.000 claims 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims 1
- 210000000988 bone and bone Anatomy 0.000 claims 1
- 229930182470 glycoside Natural products 0.000 claims 1
- 229940049964 oleate Drugs 0.000 claims 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims 1
- 239000006228 supernatant Substances 0.000 claims 1
- 238000005303 weighing Methods 0.000 claims 1
- 238000009960 carding Methods 0.000 abstract description 8
- 230000003115 biocidal effect Effects 0.000 abstract description 6
- 208000001840 Dandruff Diseases 0.000 abstract description 5
- 230000036541 health Effects 0.000 abstract description 4
- 210000004761 scalp Anatomy 0.000 abstract description 3
- 241000050051 Chelone glabra Species 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 15
- JDRSMPFHFNXQRB-IBEHDNSVSA-N decyl glucoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O JDRSMPFHFNXQRB-IBEHDNSVSA-N 0.000 description 12
- 238000012360 testing method Methods 0.000 description 11
- 241000894006 Bacteria Species 0.000 description 7
- 241001278097 Salix alba Species 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 5
- 238000002242 deionisation method Methods 0.000 description 5
- 239000008367 deionised water Substances 0.000 description 5
- 229910021641 deionized water Inorganic materials 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 241000226556 Leontopodium alpinum Species 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 241000555688 Malassezia furfur Species 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 244000241838 Lycium barbarum Species 0.000 description 2
- 235000015459 Lycium barbarum Nutrition 0.000 description 2
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 2
- 235000002725 Olea europaea Nutrition 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- 230000003752 improving hair Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000006916 nutrient agar Substances 0.000 description 2
- 239000008223 sterile water Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 244000012254 Canarium album Species 0.000 description 1
- 235000009103 Canarium album Nutrition 0.000 description 1
- 235000007866 Chamaemelum nobile Nutrition 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001360526 Escherichia coli ATCC 25922 Species 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- 241000226555 Leontopodium Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 description 1
- 241000208292 Solanaceae Species 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000004500 asepsis Methods 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920006317 cationic polymer Polymers 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- RJWRQCMERCINIU-UHFFFAOYSA-L disodium 2-(carboxylatomethylamino)tetradecanoate Chemical compound [Na+].C(CCCCCCCCCCC)C(C(=O)[O-])NCC(=O)[O-].[Na+] RJWRQCMERCINIU-UHFFFAOYSA-L 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of mild baby shampoo and preparation method thereof, the mild baby shampoo includes the raw material of following weight parts: 10-15 parts of lauryl both sexes sodium acetate, 3-8 parts of Plantacare 818,3-8 parts of sodium secondary alkyl sulfonate, 1-5 parts of sodium cocoyl glycinate, 1-5 parts of glycerine, 0.2-2 parts of Monoolein, 0.1-1 parts of german chamomile extract, 0.1-1 parts of olive extract, 0.1-1 parts of edenweiss flower extract, 0.1-0.3 parts of allantoin, 1-2 parts of tricholoma matsutake, 1-2 parts of fungicide, 0.1-1 parts of conditioner, 100-150 parts of water.The mild baby shampoo that the present invention is prepared is rich in natural active skull cap components, does not stimulate mildly, health environment-friendly, effectively moistens scared, improves the carding property and scalp biocidal property of hair, reduces the generation of dandruff.
Description
Technical field
The present invention relates to daily chemical product technical fields, and in particular to a kind of mild baby shampoo and its preparation side
Method.
Background technique
There is no too many requirement when past people select shampoo, only requiring can be the dust and grease on hair
It washes away, but with the development of the society, people have been not content with only cleans hair, and is desirable to after hair washes
Can it is smooth it is submissive, it is easy combing and health it is glossy.In order to meet the needs of market, shampoo manufacturers continuously attempt to release new
Product, but for the quality of shampoo, there is no too big breakthroughs, close two until Procter & Gamble is proposed hair-washing hair-care at first
For one conditioner shampoo, market is opened from this Two-in-one shampoo in China, this is the revolution in shampoo history.Conditioning
Shampoo can not only clean hair, and the cardability that can also most importantly improve hair, is repaired at the glossiness for improving hair
Jag sends out tip etc..Since multiple functions can be completed once, it is well received by consumers.Shampoo brand currently on the market
It is numerous, but mostly use and hair washing product is made with industrial chemicals, these raw materials include: cationic polymer, silicone oil, fatty alcohol polyoxy
Ethylene ether sulfate, alkanolamide amine oxide etc., the chemical raw material majority of these chemical industry synthesis is to skin and the irritating work of hair
With the delicate skin of unsuitable baby is used for a long time harmful to the health of skin.
Summary of the invention
Aiming at the above shortcomings existing in the prior art, technical problem to be solved by the invention is to provide a kind of mild babies
Youngster's shampoo and preparation method thereof, obtained mild baby shampoo are rich in active skull cap components, do not stimulate mildly, healthy ring
It protects, effectively moistens scared, improve the carding property and scalp biocidal property of hair, reduce the generation of dandruff.
Object of the present invention is to what is be achieved through the following technical solutions:
A kind of mild baby shampoo, the raw material including following weight parts: 10-15 parts of lauryl both sexes sodium acetate, decyl
3-8 parts of glucoside, 3-8 parts of sodium secondary alkyl sulfonate, 1-5 parts of sodium cocoyl glycinate, 1-5 parts of glycerine, Monoolein
0.2-2 parts, 0.1-1 parts of german chamomile extract, 0.1-1 parts of olive extract, 0.1-1 parts of edenweiss flower extract, allantoin 0.1-0.3
Part, 1-2 parts of tricholoma matsutake, 1-2 parts of fungicide, 0.1-1 parts of conditioner, 100-150 parts of water.
The conditioner is trigonella bean gum and/or locust bean gum.
Preferably, the conditioner is the mixture of trigonella bean gum and locust bean gum, the trigonella bean gum and locust bean gum
Mass ratio be 1:(1-5).
The fungicide is Cortex Lycii extract and/or Salix Babylonica L.P.E.
Preferably, the fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, and the root bark of Chinese wolf-berry extracts
The mass ratio of object and Salix Babylonica L.P.E is (1-5): (1-5).
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40-60 mesh obtains Trichotoma matsutake crushed material, 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of water is mixed, with 100-300 revs/min
Stirring 5-10 minute, obtains suspension, 15-25 parts of ethyl alcohol of addition in suspension, 60-70 DEG C refluxing extraction 60-120 minutes,
500-800 mesh filter-cloth filtering is being used, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains Trichotoma matsutake and mentions
Take object.
Preferably, the tricholoma matsutake is prepared using following methods, and described part is parts by weight: by Trichotoma matsutake
It crushes, crosses 40-60 mesh, obtain Trichotoma matsutake crushed material, 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of water are mixed, with 100-
300 revs/min stirring 5-10 minutes, obtain suspension, 0.001-0.01 parts of saccharomycete and 0.001-0.01 parts be added in suspension
Aspergillus oryzae, with 100-300 revs/min stirring 5-10 minutes, obtain mixture, by mixture 25-35 DEG C heat preservation 24-48 hours,
It is warming up to 95-100 DEG C of sterilizing 10-20 minutes again, 15-25 parts of ethyl alcohol are added in the mixture after sterilizing, are mentioned in 60-70 DEG C of reflux
It taking 60-120 minutes, is using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL,
Obtain tricholoma matsutake.
It is highly preferred that the tricholoma matsutake is prepared using following methods, described part is parts by weight: will be become less severe
Mushroom crush, cross 40-60 mesh, obtain Trichotoma matsutake crushed material, will be cut into after fresh loofah peeling (1-10) mm × (1-10) mm ×
The block of (1-10) mm mixes 2-8 parts of blocks and 10-20 parts of water, 40-60 DEG C ultrasonic extraction 60-90 minute, use
500-800 mesh filter-cloth filtering, filtrate are sponge gourd extracting solution, and 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of sponge gourd extracting solutions are mixed
Close, with 100-300 revs/min stirring 5-10 minute, obtain suspension, in suspension 0.001-0.01 parts of saccharomycete of addition with
0.001-0.01 parts of aspergillus oryzaes, with 100-300 revs/min stirring 5-10 minutes, obtain mixture, by mixture 25-35 DEG C protect
It is 24-48 hours warm, then it is warming up to 95-100 DEG C of sterilizing 10-20 minutes, 15-25 parts of ethyl alcohol are added in the mixture after sterilizing,
60-70 DEG C refluxing extraction 60-120 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is
1.10-1.15g/mL obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40-60 mesh obtains root bark of Chinese wolf-berry crushed material, and the 1-5 parts and water 20-30 parts mixing of root bark of Chinese wolf-berry crushed material are mentioned in 80-90 DEG C of reflux
It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40-60 mesh obtains salicis,cortex crushed material, and the 1-5 parts and water 20-30 parts mixing of salicis,cortex crushed material are mentioned in 80-90 DEG C of reflux
It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild baby shampoo, comprising the following steps: weigh each raw material by weight, water is heated
To 75-85 DEG C, lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, third are sequentially added
Triol, Monoolein, 75-85 DEG C with 100-300 revs/min stirring 20-40 minutes, be cooled to 45-55 DEG C, german chamomile be added
Extract, olive extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 40-100 turn/
Point stirring 40-60 minutes to get.
Mild baby shampoo of the present invention and preparation method thereof, obtained mild baby shampoo rich in natural activity at
Point, it does not stimulate mildly, health environment-friendly, effectively moistens scared, improve the carding property and scalp biocidal property of hair, reduce dandruff
Generation.
Specific embodiment
In the present invention, if not refering in particular to, all devices and raw material is commercially available or the industry is common are following
Method in embodiment is unless otherwise instructed conventional method in that art.
Olive (Canariumalbum (Lour.) Raeusch.) uses Olive leaf P.E in embodiment, specific to use
The Olive leaf P.E that Shaanxi Sen Fu natural product Co., Ltd provides, specification 10:1.
German chamomile (Matricariarecutita) also known as chamomile are had using Shaanxi Pa Nier biotechnology in embodiment
Flos Chrysanthemi/leaf/stem extraction of limit company production.
Edelweiss also known as edelweiss (Leontopodiumalpinum), are composite families, and the plant of Leontopodium is implemented
The flower extract of the edelweiss provided in example using Shaanxi Cheng Gan Biotechnology Co., Ltd, specification 10:1.
The root bark of Chinese wolf-berry is matrimony vine of solanaceae plant LyciumchinenseMill.'s or lycium barbarum LyciumbarbarumL.
Dry root skin.Bozhou treasured giant Science and Technology Ltd. provides, source area: Gansu.
Salicis,cortex, the drying stem skin of white willow (Salix alba L.), Danfeng County high mountain medicine company Co., Ltd provide,
Source area: Shaanxi.
Sponge gourd, using commercially available fresh patola.
Lauryl both sexes sodium acetate, chemical name: lauryl Iminodiacetic acid sodium salt is produced using BASF in embodiment
LAD-30.
Sodium secondary alkyl sulfonate, the SAS-60 produced using German Clariant.
Plantacare 818, No. CAS: 68515-73-1, Shanghai Bepharm Science & Technology Co., Ltd.'s production, product number:
BD233981。
Sodium cocoyl glycinate, No. CAS: 90387-74-9, Shouguang City's Coudé chemical industry has new company's offer, model KD-
552。
Glycerine, No. CAS: 56-81-5, it buys from this biochemical technology Co., Ltd of Tianjin Skien.
Monoolein, No. CAS: 111-03-5, it buys from Shanghai Aladdin biochemical technology limited liability company, product
Number: M107454.
Allantoin, No. CAS: 97-59-6, it buys from Shanghai Yuan Ye Biotechnology Co., Ltd.
Trichotoma matsutake, Classification system: Tricholoma matsutake (lto et lmai) Singer also known as matsutake use
The drying matsutake that Yanji sincerity matsutake Trade Co., Ltd., Jilin Province provides, source area: Changbai mountain, Jilin.
Trigonella bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Locust bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Aspergillus oryzae, purchase is from Chinese industrial Culture Collection, and culture presevation number: CICC2002, viable bacteria are dense
Degree is 1 × 1010CFU/g。
Saccharomycete, using purchase from the saccharomyces cerevisiae of Chinese industrial Culture Collection, culture presevation is numbered:
CICC1060, viable bacteria concentration are 1 × 1010CFU/g。
Fungistatic effect test: by strain inoculated on the nutrient agar panel to have sterilized, being placed in (36 ± 1) DEG C insulating box
Bacterial strain for 24 hours, is transferred in the nutrient agar test tube slant to have sterilized with oese, is placed in (36 ± 1) DEG C insulating box by culture
Culture is for 24 hours.Sterile saline or sterile water shaken well is added in the strain test tube slant that recovery is completed again, it is outstanding to be made into bacterium
Liquid, when testing, by 0.1mL bacteria suspension be made in sterile water concentration be 5 × 104The bacteria suspension dilution of cfu/mL.Using
Beating holes method, with aseptic cotton carrier by concentration be 5 × 104The experiment bacteria suspension of cfu/mL, in lecithin, Tween-80 nutrition fine jade
Rouge plating medium surface is uniformly smeared 3 times, and drying at room temperature 5min is placed.Then the sterile round punch for being 3cm with diameter
Punching takes appropriate mild baby shampoo,, must not until filling it up in adding hole with 100 times of normal saline dilution of its quality
It overflows, does 3 groups of parallel laboratory tests.Culture dish is placed in (36 ± 1) DEG C insulating box again and cultivates 18h, observation is taken out, uses calliper to measure
The diameter of inhibition zone, boundary is in the antibacterial ring size outer for being born long using integral asepsis.Surveyed bacterial strain is escherichia coli ATCC
25922, Malassezia furfur (Malassezia furfur) CMCC (F) Y17.
Hair setting measure of merit: referring to the Master's thesis " modification of hydroxyethyl cellulose and in shampoo of Lv Miao
Application study " method in 3.3.2 section, test wet carding property and dry carding property, and combing power is calculated according to combing curve.
Embodiment 1
Mild baby shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl
5 parts of sodium sulfonate, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive mention
Take 0.5 part of object, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is Cortex Lycii extract.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, is stirred 8 minutes, is obtained with 200 revs/min
To suspension, 20 parts of ethyl alcohol are added in suspension, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate exists
50 DEG C, absolute pressure be that the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtain tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The preparation method of the mild baby shampoo, comprising the following steps: each raw material is weighed by weight, by deionization
Water is heated to 80 DEG C, sequentially add lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate,
Glycerine, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract, olive is added
Extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 2
Substantially the same manner as Example 1, difference is only that:
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, is stirred 8 minutes, is obtained with 200 revs/min
To suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae are added in suspension, is stirred 8 minutes, is mixed with 200 revs/min
Material is closed, mixture 36 hours is kept the temperature at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, is added 20 in the mixture after sterilizing
Part ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure 0.03MPa
The density for being concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
Embodiment 3
Substantially the same manner as Example 1, difference is only that:
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks
Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes
Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
Embodiment 4
Mild baby shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl
5 parts of sodium sulfonate, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive mention
Take 0.5 part of object, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is Salix Babylonica L.P.E.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks
Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes
Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild baby shampoo, comprising the following steps: each raw material is weighed by weight, by deionization
Water is heated to 80 DEG C, sequentially add lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate,
Glycerine, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract, olive is added
Extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 5
Mild baby shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl
5 parts of sodium sulfonate, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive mention
Take 0.5 part of object, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is trigonella bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks
Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes
Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild baby shampoo, comprising the following steps: each raw material is weighed by weight, by deionization
Water is heated to 80 DEG C, sequentially add lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate,
Glycerine, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract, olive is added
Extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 6
Mild baby shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl
5 parts of sodium sulfonate, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive mention
Take 0.5 part of object, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is locust bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks
Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes
Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild baby shampoo, comprising the following steps: each raw material is weighed by weight, by deionization
Water is heated to 80 DEG C, sequentially add lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate,
Glycerine, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract, olive is added
Extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Embodiment 7
Mild baby shampoo raw material (parts by weight): 12 parts of lauryl both sexes sodium acetate, 5 parts of Plantacare 818, secondary alkyl
5 parts of sodium sulfonate, 3 parts of sodium cocoyl glycinate, 3 parts of glycerine, 1 part of Monoolein, 0.5 part of german chamomile extract, olive mention
Take 0.5 part of object, 0.5 part of edenweiss flower extract, 0.2 part of allantoin, 1.5 parts of tricholoma matsutake, 1.5 parts of fungicide, conditioner
0.5 part, 120 parts of deionized water.
The conditioner is the mixture of trigonella bean gum and locust bean gum, the mass ratio of the trigonella bean gum and locust bean gum
For 1:4.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow
The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake
40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks
Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes
Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min
Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min
To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing
Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure
The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake
40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed
40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt
With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained
To Salix Babylonica L.P.E.
The preparation method of the mild baby shampoo, comprising the following steps: each raw material is weighed by weight, by deionization
Water is heated to 80 DEG C, sequentially add lauryl both sexes sodium acetate, Plantacare 818, sodium secondary alkyl sulfonate, sodium cocoyl glycinate,
Glycerine, Monoolein are stirred 30 minutes with 200 revs/min at 80 DEG C, are cooled to 50 DEG C, german chamomile extract, olive is added
Extract, edenweiss flower extract, allantoin, tricholoma matsutake, fungicide, conditioner, with 60 revs/min stir 50 minutes, i.e.,
?.
Test case 1
The mild baby shampoo fungistatic effect that embodiment is prepared is tested, specific test result is shown in Table 1.
The mild baby shampoo antibacterial circle diameter test result table of table 1
From table 1 it follows that antibacterial circle diameter is greater than 15mm, there is good biocidal property.Especially to chaff horse traction
Color bacterium has significant biocidal property, and Malassezia furfur is the main reason for causing dandruff to generate, it is seen then that of the invention is mild
The antibacterial generation that can significantly inhibit dandruff of baby shampoo.
Test case 2
The mild baby shampoo carding property that embodiment is prepared is tested, specific test result is shown in Table 2.
2 carding property test result table of table
| Wet combing power | Dry combing power | |
| Embodiment 1 | 9687 | 6431 |
| Embodiment 2 | 9603 | 6338 |
| Embodiment 3 | 9482 | 6205 |
| Embodiment 4 | 9536 | 6253 |
| Embodiment 5 | 9376 | 6064 |
| Embodiment 6 | 9405 | 6125 |
| Embodiment 7 | 9166 | 5789 |
Embodiment 3 ferments to Trichotoma matsutake using sponge gourd extracting solution, then extracts to fermentation material, the biocidal property of hair
Embodiment 1-2 can be significantly better than with carding property.Containing nutriment needed for fermenting microbe in sponge gourd extracting solution, hair can promote
Ferment carries out, and fermentation process discharges the effective active composition of Trichotoma matsutake sufficiently, promotes the active component content in extract, from
And promote the performance of mild baby shampoo.
Claims (10)
1. a kind of mild baby shampoo, which is characterized in that the raw material including following weight parts: lauryl both sexes sodium acetate 10-
15 parts, 3-8 parts of Plantacare 818,3-8 parts of sodium secondary alkyl sulfonate, 1-5 parts of sodium cocoyl glycinate, 1-5 parts of glycerine, glycerol list
0.2-2 parts of oleate, 0.1-1 parts of german chamomile extract, 0.1-1 parts of olive extract, 0.1-1 parts of edenweiss flower extract, allantoin
0.1-0.3 parts, 1-2 parts of tricholoma matsutake, 1-2 parts of fungicide, 0.1-1 parts of conditioner, 100-150 parts of water.
2. mild baby shampoo as described in claim 1, which is characterized in that the tricholoma matsutake uses following methods
It is prepared, described part is parts by weight: Trichotoma matsutake is crushed, cross 40-60 mesh, Trichotoma matsutake crushed material is obtained, by 5-10 parts
Trichotoma matsutake crushed material and the mixing of 15-25 parts of water, with 100-300 revs/min stirring 5-10 minutes, obtain suspension, add in suspension
Enter 15-25 parts of ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, using 500-800 mesh filter-cloth filtering, filtrate decompression is dense
The density for being reduced to 50 DEG C is 1.10-1.15g/mL, obtains tricholoma matsutake.
3. mild baby shampoo as described in claim 1, which is characterized in that the tricholoma matsutake uses following methods
It is prepared, described part is parts by weight: Trichotoma matsutake is crushed, cross 40-60 mesh, Trichotoma matsutake crushed material is obtained, by fresh silk
It is cut into (1-10) mm × (1-10) mm × (1-10) mm block after melon peeling, 2-8 parts of blocks and 10-20 parts of water are mixed
Close, 40-60 DEG C ultrasonic extraction 60-90 minute, using 500-800 mesh filter-cloth filtering, filtrate is sponge gourd extracting solution, by 5-10 parts
Trichotoma matsutake crushed material and the mixing of 15-25 parts of sponge gourd extracting solutions, with 100-300 revs/min stirring 5-10 minutes, obtain suspension, it is outstanding
0.001-0.01 parts of saccharomycete and 0.001-0.01 parts of aspergillus oryzaes are added in supernatant liquid, with 100-300 revs/min stirring 5-10 minutes,
Obtain mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, then be warming up to 95-100 DEG C of sterilizing 10-20 minutes, sterilize
In mixture afterwards be added 15-25 part ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, use 500-800 mesh filter cloth mistake
Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains tricholoma matsutake.
4. mild baby shampoo as described in claim 1, which is characterized in that the tricholoma matsutake uses following methods
It is prepared, described part is parts by weight: Trichotoma matsutake is crushed, cross 40-60 mesh, Trichotoma matsutake crushed material is obtained, by 5-10 parts
Trichotoma matsutake crushed material and the mixing of 15-25 parts of water, with 100-300 revs/min stirring 5-10 minutes, obtain suspension, add in suspension
Enter 0.001-0.01 parts of saccharomycete and 0.001-0.01 parts of aspergillus oryzaes, with 100-300 revs/min stirring 5-10 minutes, mixed
Material, by mixture 25-35 DEG C heat preservation 24-48 hours, then be warming up to 95-100 DEG C of sterilizing 10-20 minutes, the mixing after sterilizing
In material be added 15-25 part ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, use 500-800 mesh filter-cloth filtering, filtrate
The density for being concentrated under reduced pressure into 50 DEG C is 1.10-1.15g/mL, obtains tricholoma matsutake.
5. mild baby shampoo as described in claim 1, which is characterized in that the fungicide be Cortex Lycii extract and/
Or Salix Babylonica L.P.E.
6. mild baby shampoo as claimed in claim 5, which is characterized in that the fungicide is Cortex Lycii extract and white
The mass ratio of the mixture of willow bark extract, the Cortex Lycii extract and Salix Babylonica L.P.E is (1-5): (1-5).
7. such as mild baby shampoo described in claim 5 or 6, which is characterized in that the Cortex Lycii extract is using following
Method is prepared, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, 40-60 mesh is crossed, root bark of Chinese wolf-berry crushed material is obtained, by ground
1-5 parts of bone skin crushed material and water 20-30 part mix, 80-90 DEG C refluxing extraction 40-60 minutes, using 500-800 mesh filter cloth mistake
Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains Cortex Lycii extract.
8. such as mild baby shampoo described in claim 5 or 6, which is characterized in that the Salix Babylonica L.P.E is using following
Method is prepared, and described part is parts by weight: salicis,cortex crushed 40-60 mesh, obtain salicis,cortex crushed material, by white willow
1-5 parts of skin crushed material and water 20-30 part mix, 80-90 DEG C refluxing extraction 40-60 minutes, using 500-800 mesh filter cloth mistake
Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains Salix Babylonica L.P.E.
9. mild baby shampoo as described in claim 1, which is characterized in that the conditioner is trigonella bean gum and/or thorn
Locust bean gum.
10. such as the preparation method of the described in any item mild baby shampoos of claim 1-9, which is characterized in that including following
Step: weighing each raw material by weight, heat water to 75-85 DEG C, sequentially adds lauryl both sexes sodium acetate, decyl glucose
Glycosides, sodium secondary alkyl sulfonate, sodium cocoyl glycinate, glycerine, Monoolein are stirred at 75-85 DEG C with 100-300 revs/min
It mixes 20-40 minutes, is cooled to 45-55 DEG C, german chamomile extract is added, olive extract, edenweiss flower extract, allantoin, becomes less severe
Mushroom extract, fungicide, conditioner, with 40-100 revs/min of stirring 40-60 minutes to get.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111481477A (en) * | 2020-05-27 | 2020-08-04 | 融致丰生制药有限公司 | Matsutake extract for repairing damaged hair and delaying scalp aging, composition and application |
| CN114948798A (en) * | 2022-05-30 | 2022-08-30 | 两面针（江苏）实业有限公司 | Traditional Chinese medicine hair conditioner and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004224702A (en) * | 2003-01-20 | 2004-08-12 | Ichimaru Pharcos Co Ltd | External preparation for skin containing mushroom extract |
| CN1545840A (en) * | 2003-12-16 | 2004-11-17 | 敖宗华 | Technique for production of Tricholoma matsutake and polysaccharide thereof by large scale liquid submerged fermentation |
| US20090070945A1 (en) * | 2007-09-14 | 2009-03-19 | L'oreal | Method of coloring hair |
| US20130287708A1 (en) * | 2010-12-09 | 2013-10-31 | Yissum Research Development Company Of The Hebrew University Of Jerusalem Ltd. | Natural formulations |
| CN105102070A (en) * | 2013-04-12 | 2015-11-25 | 化工产品开发公司Seppic | Novel oil-in-water emulsions with high aqueous phase content, liquid consistencies and that are stable in storage |
| CN105534816A (en) * | 2016-01-21 | 2016-05-04 | 苏州派腾生物医药科技有限公司 | Natural pet shampoo |
| CN107669552A (en) * | 2017-10-31 | 2018-02-09 | 思拓科（上海）生物科技股份有限公司 | Organic baby's shampoo |
-
2018
- 2018-12-28 CN CN201811617034.XA patent/CN109431916B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004224702A (en) * | 2003-01-20 | 2004-08-12 | Ichimaru Pharcos Co Ltd | External preparation for skin containing mushroom extract |
| CN1545840A (en) * | 2003-12-16 | 2004-11-17 | 敖宗华 | Technique for production of Tricholoma matsutake and polysaccharide thereof by large scale liquid submerged fermentation |
| US20090070945A1 (en) * | 2007-09-14 | 2009-03-19 | L'oreal | Method of coloring hair |
| US20130287708A1 (en) * | 2010-12-09 | 2013-10-31 | Yissum Research Development Company Of The Hebrew University Of Jerusalem Ltd. | Natural formulations |
| CN105102070A (en) * | 2013-04-12 | 2015-11-25 | 化工产品开发公司Seppic | Novel oil-in-water emulsions with high aqueous phase content, liquid consistencies and that are stable in storage |
| CN105534816A (en) * | 2016-01-21 | 2016-05-04 | 苏州派腾生物医药科技有限公司 | Natural pet shampoo |
| CN107669552A (en) * | 2017-10-31 | 2018-02-09 | 思拓科（上海）生物科技股份有限公司 | Organic baby's shampoo |
Non-Patent Citations (4)
| Title |
|---|
| SEUNG-YOON OH 等: ""Diversity and effect of Trichoderma isolated from the roots of Pinus densiflora within the fairy ring of pine mushroom (Tricholoma matsutake)"", 《PLOS ONE》 * |
| 刘吉华: "《中药生物技术》", 31 October 2015, 中国医药科技出版社 * |
| 王建新: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
| 邓影妹 等: ""松口蘑活性物提取工艺研究及其安全功效评价"", 《日用化学工业》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111481477A (en) * | 2020-05-27 | 2020-08-04 | 融致丰生制药有限公司 | Matsutake extract for repairing damaged hair and delaying scalp aging, composition and application |
| CN114948798A (en) * | 2022-05-30 | 2022-08-30 | 两面针（江苏）实业有限公司 | Traditional Chinese medicine hair conditioner and preparation method thereof |
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| CN109431916B (en) | 2021-06-01 |
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