CN109363978A - Mild natural plants hair conditioner and preparation method thereof - Google Patents

Mild natural plants hair conditioner and preparation method thereof Download PDF

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CN109363978A
CN109363978A CN201811616989.3A CN201811616989A CN109363978A CN 109363978 A CN109363978 A CN 109363978A CN 201811616989 A CN201811616989 A CN 201811616989A CN 109363978 A CN109363978 A CN 109363978A
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extract
parts
natural plants
hair conditioner
plants hair
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CN109363978B (en
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戴金花
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Shantou Runjing Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • A61K8/416Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The invention discloses a kind of mild natural plants hair conditioner and preparation method thereof, the mild natural plants hair conditioner includes the raw material of following weight parts: hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride, tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant regulation agent, water.The bactericide is Cortex Lycii extract and/or Salix Babylonica L.P.E.The plant regulation agent is trigonella bean gum and/or locust bean gum.Compared with prior art, the mild natural plants hair conditioner of the present invention is rich in a variety of active skull cap components, does not stimulate mildly, health environment-friendly, effectively moist scalp and scared, facilitates the hair of maintenance damage, prevent hair jag, it is withered, have the function of good profit hair, take care of hair.

Description

Mild natural plants hair conditioner and preparation method thereof
Technical field
The present invention relates to daily chemical product technical fields, and in particular to a kind of mild natural plants hair conditioner and its preparation Method.
Background technique
The hair surface layer of health is made of the protective film of hair the grease of one group of complete hair scale piece and naturally secret, excessively The natural protective film of this layer can all be destroyed by washing reason, boiling hot dye, exposure in sunshine, led to cortex water loss, kept hair withered, follow the string And flexibility.
There is no too many requirement when past people select shampoo, only requiring can be the dust and grease on hair It washes away, but with the development of the society, people have been not content with only cleans hair, and is desirable to after hair washes Can it is smooth it is submissive, it is easy combing and health it is glossy.
Hair conditioner is only commonly used, could persistently form the protective film of hair, hair is made to escape injury.Hair conditioner is people Common daily necessities, and almost daily use health skin on, therefore to wash shield product quality requirement it is higher, What is first had to is securely and reliably, must not there is side effect when must not hinder human health, while use.
The present invention provides a kind of mild natural plants hair conditioner, is rich in a variety of active skull cap components, does not stimulate mildly, health Environmental protection, effectively moist scalp and scared facilitate the hair of maintenance damage, prevent hair jag, it is withered, there is good profit The function of hair, hair care.
Summary of the invention
Aiming at the above shortcomings existing in the prior art, technical problem to be solved by the invention is to provide a kind of mild days Right plant hair conditioner and preparation method thereof, obtained mild natural plants hair conditioner is rich in a variety of active skull cap components, mildly not Stimulation, health environment-friendly, effectively moist scalp and scared facilitate the hair of maintenance damage, prevent hair jag, dry up, have The function of good profit hair, hair care.
Object of the present invention is to what is be achieved through the following technical solutions:
A kind of mild natural plants hair conditioner, including following raw material: hexadecyltrimethylammonium chloride, dimethicone, Trialkyl methyl ammonium chloride, tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, Plant regulation agent, water.
Preferably, the mild natural plants hair conditioner, is made of: cetyl three following raw material in percentage terms Ammonio methacrylate 1~6%, dimethicone 1~6%, trialkyl methyl ammonium chloride 1~3%, tricholoma matsutake 10~ 30%, german chamomile extract 0.1~1%, olive extract 0.1~1%, edenweiss flower extract 0.1~1%, bactericide 0.2 ~2%, plant regulation agent 3-6%, surplus are water.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40-60 mesh obtains Trichotoma matsutake crushed material, 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of water is mixed, with 100-300 revs/min Stirring 5-10 minutes obtains suspension, 0.001-0.01 parts of saccharomycete and 0.001-0.01 parts of aspergillus oryzaes is added in suspension, with 100-300 revs/min stirring 5-10 minutes, obtain mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, then be warming up to 95-100 DEG C sterilizing 10-20 minutes, 15-25 parts of ethyl alcohol are added in the mixture after sterilizing, in 60-70 DEG C of refluxing extraction 60-120 Minute, 500-800 mesh filter-cloth filtering is being used, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is become less severe Mushroom extract.
The bactericide is Cortex Lycii extract and/or Salix Babylonica L.P.E;Preferably, the fungicide is ground bone The mass ratio of the mixture of bark extract and Salix Babylonica L.P.E, the Cortex Lycii extract and Salix Babylonica L.P.E is (1-5): (1-5)。
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake 40-60 mesh obtains root bark of Chinese wolf-berry crushed material, and the 1-5 parts and water 20-30 parts mixing of root bark of Chinese wolf-berry crushed material are mentioned in 80-90 DEG C of reflux It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed 40-60 mesh obtains salicis,cortex crushed material, and the 1-5 parts and water 20-30 parts mixing of salicis,cortex crushed material are mentioned in 80-90 DEG C of reflux It takes 40-60 minutes, using 500-800 mesh filter-cloth filtering, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, is obtained To Salix Babylonica L.P.E.
The plant regulation agent is trigonella bean gum and/or locust bean gum;Preferably, the conditioner is trigonella bean gum and thorn The mass ratio of the mixture of locust bean gum, the trigonella bean gum and locust bean gum is 1:(1-5).
A kind of preparation method of mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 30~60min under conditions of 60~80 DEG C, 200~400 revs/min, obtain A phase;
S3 by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride 60~80 DEG C, 300~ It is stirred 30~60min under conditions of 600 revs/min, obtains B phase;
S4 mixes A phase with B, is stirred 4~8h under conditions of 50~70 DEG C, 100~300 revs/min, has stirred At it is rear stand 12~for 24 hours to get the mild natural plants hair conditioner.
The mild natural plants hair conditioner of the present invention is rich in a variety of active skull cap components, does not stimulate mildly, health environment-friendly, effectively Scalp and scared is moistened, the hair of maintenance damage is facilitated, prevents hair jag, withered function with good profit hair, hair care Energy.
Specific embodiment
In the present invention, if not refering in particular to, all devices and raw material is commercially available or the industry is common are following Method in embodiment is unless otherwise instructed conventional method in that art.
German chamomile (Matricariarecutita) also known as chamomile are had using Shaanxi Pa Nier biotechnology in embodiment Flos Chrysanthemi/leaf/stem extraction of limit company production.
Olive (Canariumalbum (Lour.) Raeusch.) uses Olive leaf P.E in embodiment, specific to use The Olive leaf P.E that Shaanxi Sen Fu natural product Co., Ltd provides, specification 10:1.
Edelweiss also known as edelweiss (Leontopodiumalpinum), are composite families, and the plant of Leontopodium is implemented The flower extract of the edelweiss provided in example using Shaanxi Cheng Gan Biotechnology Co., Ltd, specification 10:1.
The root bark of Chinese wolf-berry is matrimony vine of solanaceae plant LyciumchinenseMill.'s or lycium barbarum LyciumbarbarumL. Dry root skin.Bozhou treasured giant Science and Technology Ltd. provides, source area: Gansu.
Salicis,cortex, the drying stem skin of white willow (Salix alba L.), Danfeng County high mountain medicine company Co., Ltd provide, Source area: Shaanxi.
Sponge gourd, using commercially available fresh patola.
Trichotoma matsutake, Classification system: Tricholoma matsutake (lto et lmai) Singer also known as matsutake use The drying matsutake that Yanji sincerity matsutake Trade Co., Ltd. of Jilin Province provides, source area: Changbai mountain, Jilin.
Hexadecyltrimethylammonium chloride: No. CAS: 112-02-7.
Dimethicone: No. CAS: 63148-62-9,350 ± 25mPas of viscosity.
Trialkyl methyl ammonium chloride: No. CAS: 63393-96-4.
Trigonella bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Locust bean gum is bought from Hunan century Hua Xing bioengineering Co., Ltd.
Aspergillus oryzae, purchase is from Chinese industrial Culture Collection, and culture presevation number: CICC2002, viable bacteria are dense Degree is 1 × 1010CFU/g。
Saccharomycete, using purchase from the saccharomyces cerevisiae of Chinese industrial Culture Collection, culture presevation is numbered: CICC1060, viable bacteria concentration are 1 × 1010CFU/g。
Embodiment 1
A kind of mild natural plants hair conditioner (mass percent): hexadecyltrimethylammonium chloride 5%, dimethicone 4%, trialkyl methyl ammonium chloride 3%, tricholoma matsutake 25%, german chamomile extract 1%, olive extract 1%, edelweiss mention Taking object 1%, bactericide 2%, plant regulation agent 5%, surplus is water.
The preparation method of the mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 50min under conditions of 70 DEG C, 300 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride at 70 DEG C, 500 revs/min Under the conditions of be stirred 50min, obtain B phase;
S4 mixes A phase with B, and 6h is stirred under conditions of 50 DEG C, 200 revs/min, stands 20h after the completion of stirring, Up to the mild natural plants hair conditioner.
The conditioner is trigonella bean gum.
The fungicide is Cortex Lycii extract.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, is stirred 8 minutes, is obtained with 200 revs/min To suspension, 20 parts of ethyl alcohol are added in suspension, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate exists 50 DEG C, absolute pressure be that the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtain tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake 40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Cortex Lycii extract.
Embodiment 2
Substantially the same manner as Example 1, difference is only that:
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of water are mixed, is stirred 8 minutes, is obtained with 200 revs/min To suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae are added in suspension, is stirred 8 minutes, is mixed with 200 revs/min Material is closed, mixture 36 hours is kept the temperature at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, is added 20 in the mixture after sterilizing Part ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure 0.03MPa The density for being concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
Embodiment 3
Substantially the same manner as Example 1, difference is only that:
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
Embodiment 4
A kind of mild natural plants hair conditioner (mass percent): hexadecyltrimethylammonium chloride 5%, dimethicone 4%, trialkyl methyl ammonium chloride 3%, tricholoma matsutake 25%, german chamomile extract 1%, olive extract 1%, edelweiss mention Taking object 1%, bactericide 2%, plant regulation agent 5%, surplus is water.
The preparation method of the mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 50min under conditions of 70 DEG C, 300 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride at 70 DEG C, 500 revs/min Under the conditions of be stirred 50min, obtain B phase;
S4 mixes A phase with B, and 6h is stirred under conditions of 50 DEG C, 200 revs/min, stands 20h after the completion of stirring, Up to the mild natural plants hair conditioner.
The conditioner is trigonella bean gum.
The fungicide is Salix Babylonica L.P.E.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed 40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Salix Babylonica L.P.E.
Embodiment 5
A kind of mild natural plants hair conditioner (mass percent): hexadecyltrimethylammonium chloride 5%, dimethicone 4%, trialkyl methyl ammonium chloride 3%, tricholoma matsutake 25%, german chamomile extract 1%, olive extract 1%, edelweiss mention Taking object 1%, bactericide 2%, plant regulation agent 5%, surplus is water.
The preparation method of the mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 50min under conditions of 70 DEG C, 300 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride at 70 DEG C, 500 revs/min Under the conditions of be stirred 50min, obtain B phase;
S4 mixes A phase with B, and 6h is stirred under conditions of 50 DEG C, 200 revs/min, stands 20h after the completion of stirring, Up to the mild natural plants hair conditioner.
The conditioner is trigonella bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake 40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed 40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Salix Babylonica L.P.E.
Embodiment 6
A kind of mild natural plants hair conditioner (mass percent): hexadecyltrimethylammonium chloride 5%, dimethicone 4%, trialkyl methyl ammonium chloride 3%, tricholoma matsutake 25%, german chamomile extract 1%, olive extract 1%, edelweiss mention Taking object 1%, bactericide 2%, plant regulation agent 5%, surplus is water.
The preparation method of the mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 50min under conditions of 70 DEG C, 300 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride at 70 DEG C, 500 revs/min Under the conditions of be stirred 50min, obtain B phase;
S4 mixes A phase with B, and 6h is stirred under conditions of 50 DEG C, 200 revs/min, stands 20h after the completion of stirring, Up to the mild natural plants hair conditioner.
The conditioner is locust bean gum.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake 40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed 40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Salix Babylonica L.P.E.
Embodiment 7
A kind of mild natural plants hair conditioner (mass percent): hexadecyltrimethylammonium chloride 5%, dimethicone 4%, trialkyl methyl ammonium chloride 3%, tricholoma matsutake 25%, german chamomile extract 1%, olive extract 1%, edelweiss mention Taking object 1%, bactericide 2%, plant regulation agent 5%, surplus is water.
The preparation method of the mild natural plants hair conditioner, includes the following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant tune Reason agent, water are stirred 50min under conditions of 70 DEG C, 300 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride at 70 DEG C, 500 revs/min Under the conditions of be stirred 50min, obtain B phase;
S4 mixes A phase with B, and 6h is stirred under conditions of 50 DEG C, 200 revs/min, stands 20h after the completion of stirring, Up to the mild natural plants hair conditioner.
The conditioner is the mixture of trigonella bean gum and locust bean gum, the mass ratio of the trigonella bean gum and locust bean gum For 1:4.
The fungicide is the mixture of Cortex Lycii extract and Salix Babylonica L.P.E, the Cortex Lycii extract and white willow The mass ratio of bark extract is 3:2.
The tricholoma matsutake is prepared using following methods, and described part is parts by weight: Trichotoma matsutake being crushed, mistake 40 meshes obtain Trichotoma matsutake crushed material, 5mm × 5mm × 5mm block will be cut into after fresh loofah peeling, by 5 parts of blocks Mixed with 15 parts of water, 50 DEG C ultrasonic extraction 80 minutes, supersonic frequency 20kHz, ultrasonic power 250W, using 800 mesh filter cloth mistakes Filter, filtrate are sponge gourd extracting solution, and 8 parts of Trichotoma matsutake crushed materials and 20 parts of sponge gourd extracting solutions are mixed, and stir 8 points with 200 revs/min Clock is obtained suspension, 0.005 part of saccharomycete and 0.005 part of aspergillus oryzae is added in suspension, is stirred 8 minutes, is obtained with 200 revs/min To mixture, mixture is kept the temperature 36 hours at 30 DEG C, then be warming up to 100 DEG C and sterilize 15 minutes, added in the mixture after sterilizing Enter 20 parts of ethyl alcohol, 65 DEG C refluxing extraction 90 minutes, using 800 mesh filter-cloth filterings, filtrate is in 50 DEG C, absolute pressure The density that 0.03MPa is concentrated under reduced pressure into 50 DEG C is 1.12g/mL, obtains tricholoma matsutake.
The Cortex Lycii extract is prepared using following methods, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, mistake 40 meshes obtain root bark of Chinese wolf-berry crushed material, by 3 parts of root bark of Chinese wolf-berry crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Cortex Lycii extract.
The Salix Babylonica L.P.E is prepared using following methods, and described part is parts by weight: salicis,cortex crushed 40 meshes obtain salicis,cortex crushed material, by 3 parts of salicis,cortex crushed material and 25 parts of water mixing, 85 DEG C refluxing extraction 50 minutes, adopt With 800 mesh filter-cloth filterings, it is 1.12g/mL that filtrate, which is the density that 0.03MPa is concentrated under reduced pressure into 50 DEG C in 50 DEG C, absolute pressure, is obtained To Salix Babylonica L.P.E.
Test case 1
Fungistatic effect test: by strain inoculated on the nutrient agar panel to have sterilized, being placed in (36 ± 1) DEG C insulating box Bacterial strain for 24 hours, is transferred in the nutrient agar test tube slant to have sterilized with oese, is placed in (36 ± 1) DEG C insulating box by culture Culture is for 24 hours.Sterile saline or sterile water shaken well is added in the strain test tube slant that recovery is completed again, it is outstanding to be made into bacterium Liquid, when testing, by 0.1mL bacteria suspension be made in sterile water concentration be 5 × 104The bacteria suspension dilution of cfu/mL.Using Beating holes method, with aseptic cotton carrier by concentration be 5 × 104The experiment bacteria suspension of cfu/mL, in lecithin, Tween-80 nutrition fine jade Rouge plating medium surface is uniformly smeared 3 times, and drying at room temperature 5min is placed.Then the sterile round punch for being 3cm with diameter Punching takes appropriate mild natural plants hair conditioner, with 100 times of normal saline dilution of its quality, in adding hole, and until filling it up with, It must not overflow, do 3 groups of parallel laboratory tests.Culture dish is placed in (36 ± 1) DEG C insulating box again and cultivates 18h, observation is taken out, uses slide calliper rule The diameter of inhibition zone is measured, boundary is in the antibacterial ring size outer for being born long using integral asepsis.Surveyed bacterial strain is escherichia coli ATCC 25922, Malassezia furfur (Malassezia furfur) CMCC (F) Y17.
The mild natural plants hair conditioner fungistatic effect that embodiment is prepared is tested, specific test result is shown in Table 1。
The mild natural plants hair conditioner antibacterial circle diameter test result table of table 1
Escherichia coli, mm Malassezia furfur, mm
Embodiment 1 17.0 14.9
Embodiment 2 17.3 15.2
Embodiment 3 17.9 15.5
Embodiment 4 17.7 15.4
Embodiment 5 18.7 16.5
Embodiment 6 18.3 16.3
Embodiment 7 19.1 17.1
Test case 2
Hair setting measure of merit: referring to the Master's thesis " modification of hydroxyethyl cellulose and in shampoo of Lv Miao Application study " method in 3.3.2 section, test wet carding property and dry carding property, and combing power is calculated according to combing curve.
The mild natural plants hair conditioner carding property that embodiment is prepared is tested, specific test result is shown in Table 2。
2 carding property test result table of table
Wet combing power Dry combing power
Embodiment 1 8743 5832
Embodiment 2 8667 5748
Embodiment 3 8558 5627
Embodiment 4 8607 5671
Embodiment 5 8462 5499
Embodiment 6 8488 5556
Embodiment 7 8273 5250
Embodiment 3 ferments to Trichotoma matsutake using sponge gourd extracting solution as can be seen from Table 1 and Table 2, then to fermentation material into Row extracts, and the bacteriostasis property and carding property of hair are significantly better than embodiment 1-2.Containing needed for fermenting microbe in sponge gourd extracting solution Nutriment, can promote fermentation and carry out, fermentation process discharges the effective active composition of Trichotoma matsutake sufficiently, make in extract Active component content is promoted, to promote the performance of mild natural plants hair conditioner;Moreover, mild natural plant of the invention Object hair conditioner can significantly inhibit the generation of dandruff.
Test case 3
Sensory evaluation is carried out to mild natural plants hair conditioner of the invention:
140 volunteers, women of the age distribution at 20~40 years old are chosen, hair generally occurs drying up, follow the string And the phenomenon that flexibility.Volunteer is divided into 7 groups, every group of 20 people;
Application method: after hair washing, drying hair, hair conditioner is uniformly applied on hair and hair tail, makes it on hair It stops after five minutes, is rinsed well with clear water.Each sampling January, tester according to oneself feel score.
Standards of grading: taking ten point system, and 1 point worst, and 10 points best, and score more high effect is better, test result such as the following table 3 It is shown.
The mild natural plants hair conditioner sensory evaluation effect of table 3
Embodiment It is smooth It is easy to comb
Embodiment 1 7.8 8.2
Embodiment 2 8.3 8.4
Embodiment 3 8.9 9.0
Embodiment 4 8.7 8.8
Embodiment 5 9.4 9.6
Embodiment 6 9.2 9.4
Embodiment 7 9.7 9.8
The above, only of the invention illustrates embodiment, not to the present invention in any form with substantial limitation, It should be pointed out that for those skilled in the art, under the premise of not departing from the method for the present invention, that makes several changes It also should be regarded as protection scope of the present invention into supplement.All those skilled in the art, do not depart from spirit of that invention and In the case where range, using the equivalent variations of a little change, modification and differentiation that disclosed above technology contents are made, it is Equivalent embodiment of the invention;Meanwhile any equivalent variations that all substantial technologicals according to the present invention do above-described embodiment Change, modification and differentiation, still fall within protection scope of the present invention.

Claims (9)

1. a kind of mild natural plants hair conditioner, which is characterized in that including following raw material: hexadecyltrimethylammonium chloride, two Methyl-silicone oil, tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, is planted at trialkyl methyl ammonium chloride Object fungicide, plant regulation agent, water.
2. mild natural plants hair conditioner as described in claim 1, which is characterized in that by following raw material group in percentage terms At: hexadecyltrimethylammonium chloride 1~6%, dimethicone 1~6%, trialkyl methyl ammonium chloride 1~3%, Trichotoma matsutake Extract 10~30%, olive extract 0.1~1%, edenweiss flower extract 0.1~1%, is planted at german chamomile extract 0.1~1% Object fungicide 0.2~2%, plant regulation agent 3-6%, surplus are water.
3. mild natural plants hair conditioner as claimed in claim 1 or 2, it is characterised in that: the tricholoma matsutake uses Following methods are prepared, and described part is parts by weight: Trichotoma matsutake is crushed, 40-60 mesh is crossed, obtains Trichotoma matsutake crushed material, 5-10 parts of Trichotoma matsutake crushed materials and 15-25 parts of water are mixed, with 100-300 revs/min stirring 5-10 minutes, obtain suspension, it is outstanding 0.001-0.01 parts of saccharomycete and 0.001-0.01 parts of aspergillus oryzaes are added in supernatant liquid, with 100-300 revs/min stirring 5-10 minutes, Obtain mixture, by mixture 25-35 DEG C heat preservation 24-48 hours, then be warming up to 95-100 DEG C of sterilizing 10-20 minutes, sterilize In mixture afterwards be added 15-25 part ethyl alcohol, 60-70 DEG C refluxing extraction 60-120 minutes, use 500-800 mesh filter cloth mistake Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains tricholoma matsutake.
4. mild natural plants hair conditioner as claimed in claim 1 or 2, it is characterised in that: the bactericide is ground bone Bark extract and/or Salix Babylonica L.P.E.
5. mild natural plants hair conditioner as claimed in claim 4, it is characterised in that: the fungicide is Cortex Lycii extract With the mixture of Salix Babylonica L.P.E, the mass ratio of the Cortex Lycii extract and Salix Babylonica L.P.E is (1-5): (1-5).
6. mild natural plants hair conditioner as claimed in claim 5, which is characterized in that the Cortex Lycii extract is using following Method is prepared, and described part is parts by weight: the root bark of Chinese wolf-berry being crushed, 40-60 mesh is crossed, root bark of Chinese wolf-berry crushed material is obtained, by ground 1-5 parts of bone skin crushed material and water 20-30 part mix, 80-90 DEG C refluxing extraction 40-60 minutes, using 500-800 mesh filter cloth mistake Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains Cortex Lycii extract.
7. mild natural plants hair conditioner as claimed in claim 5, which is characterized in that the Salix Babylonica L.P.E is using following Method is prepared, and described part is parts by weight: salicis,cortex crushed 40-60 mesh, obtain salicis,cortex crushed material, by white willow 1-5 parts of skin crushed material and water 20-30 part mix, 80-90 DEG C refluxing extraction 40-60 minutes, using 500-800 mesh filter cloth mistake Filter, the density that filtrate decompression is concentrated into 50 DEG C is 1.10-1.15g/mL, obtains Salix Babylonica L.P.E.
8. mild natural plants hair conditioner as claimed in claim 1 or 2, it is characterised in that: the plant regulation agent is cucurbit Bar glue and/or locust bean gum.
9. the preparation method of mild natural plants hair conditioner as described in any one of claims 1 to 8, which is characterized in that including Following steps:
S1 weighs raw material by mass percentage;
S2 is by tricholoma matsutake, german chamomile extract, olive extract, edenweiss flower extract, bactericide, plant regulation Agent, water are stirred 30~60min under conditions of 60~80 DEG C, 200~400 revs/min, obtain A phase;
S3 is by hexadecyltrimethylammonium chloride, dimethicone, trialkyl methyl ammonium chloride in 60~80 DEG C, 300~600 It is stirred 30~60min under conditions of rev/min, obtains B phase;
S4 mixes A phase with B, 4~8h is stirred under conditions of 50~70 DEG C, 100~300 revs/min, after the completion of stirring Standing 12~for 24 hours to get the mild natural plants hair conditioner.
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