CN111481477A

CN111481477A - Matsutake extract for repairing damaged hair and delaying scalp aging, composition and application

Info

Publication number: CN111481477A
Application number: CN202010463017.6A
Authority: CN
Inventors: 郭智华; 徐双华; 田冉
Original assignee: Rongzhi Fengsheng Pharmaceutical Co ltd
Current assignee: Rongzhi Fengsheng Pharmaceutical Co ltd
Priority date: 2020-05-27
Filing date: 2020-05-27
Publication date: 2020-08-04

Abstract

The invention relates to the technical field of daily cosmetics, in particular to a tricholoma matsutake extract, a tricholoma matsutake composition and application thereof for repairing damaged hair and delaying scalp aging. The invention provides a novel compound with a preservation number of CCTCC NO: matsutake Mushroom (Tricholoma matsutake) T35 (M2014671) is extracted by a specific method. The composition of the present invention comprises matsutake mushroom extract, malachite extract, and spilanthol extract. The combination of the spilanthol camomile extract and the tricholoma matsutake extract obviously improves the absorption efficiency of the functional components in the tricholoma matsutake extract through the scalp, and the combination of the spilanthol camomile extract and the tricholoma matsutake extract can effectively play the functions of nourishing, moistening, caring the scalp and the hair and repairing the hair damaged by permanent dyeing; the components in the composition can be well coordinated and matched, so that the scalp and hair can be effectively nourished, the hair can be strengthened, the damaged hair can be repaired, the scalp aging can be delayed, and the composition has important significance for solving the health problems of the scalp and the hair.

Description

Matsutake extract for repairing damaged hair and delaying scalp aging, composition and application

Technical Field

The invention relates to the technical field of daily cosmetics, in particular to a tricholoma matsutake extract, a composition containing the tricholoma matsutake extract and application of the tricholoma matsutake extract.

Background

With the development of society and the acceleration of life rhythm, people's life, working pressure are bigger and bigger, produce serious influence to the health of scalp and hair, and the crowd of hair dyeing and permanent wave is more and more simultaneously, can cause the damage to hair in the hair dyeing and permanent wave process, reduces hair intensity, and more people begin to regard for the hair problem, and the development has important meaning to the hair washing and protecting articles that have the function of nourishing nursing to hair and scalp.

Matsutake is one of the most famous and precious wild edible mushrooms in the world, is regarded as a treasure in mushrooms and is entitled "king of mushrooms" and "diamond in mountains". However, the growth environment is harsh, complete artificial cultivation cannot be realized at present, the market demand mainly depends on wild resources, the ecological environment, the change of climatic conditions and an unreasonable harvesting mode are added, the yield of the tricholoma matsutake is reduced, the contradiction between supply and demand of the market is increasingly prominent, the price of the tricholoma matsutake is increased day by day, and the utilization and sustainable development of the tricholoma matsutake resources are greatly limited. Therefore, the cost of the tricholoma matsutake is reduced, and the searching of the utilization mode of tricholoma matsutake resources is of great significance.

Disclosure of Invention

In order to solve the technical problems in the prior art, the invention aims to provide a tricholoma matsutake extract, a composition containing the tricholoma matsutake extract and application of the tricholoma matsutake extract.

The matsutake extract is mainly from wild matsutake and is high in price, at present, the matsutake and the extract thereof are mostly used in products such as food, health care products and the like, and the matsutake is rarely applied to products such as hair washing and protecting products. According to the invention, the tricholoma matsutake extract is prepared by using the tricholoma matsutake strain through a biological technology, so that the cost is greatly reduced, and the utilization field and sustainable development of tricholoma matsutake resources are expanded. According to the research of the tricholoma matsutake extract used for the hair washing and protecting product, experiments show that on one hand, the tricholoma matsutake extract has low percutaneous absorbability, so that the absorption efficiency of active ingredients of the tricholoma matsutake extract through scalp and hair follicles is not high actually when the tricholoma matsutake extract is used for the hair washing and protecting product, and the function exertion of the tricholoma matsutake extract in the hair washing and protecting product is limited to a certain extent, and on the other hand, the nutrition and health care effects of the tricholoma matsutake extract on the hair and the scalp still need to be improved due to the limitation of the. Through a large amount of research and practice, the invention discovers that the tricholoma matsutake extract prepared by adopting a specific extraction method not only has excellent absorption efficiency through scalp and hair follicles, but also better retains active ingredients with the effects of nourishing and caring hair and scalp and repairing dyed and scalded damaged hair; furthermore, the tricholoma matsutake extract and the spilanthol flos chrysanthemi extract are compounded, the spilanthol flos chrysanthemi extract can effectively promote the tricholoma matsutake extract to be absorbed by the scalp and hair follicles, and active ingredients in the tricholoma matsutake extract and the spilanthol flos chrysanthemi extract can also play a synergistic effect, so that the tricholoma matsutake extract and the spilanthol flos chrysanthemi extract can effectively nourish and care the scalp and the hair, repair the hair damaged by dyeing and scalding, recover the elasticity.

In order to realize the purpose of the invention, the following technical scheme is specifically provided:

the invention provides a tricholoma matsutake extract which is prepared from matsutake with a preservation number of CCTCC NO: m2014671 Tricholoma matsutake (Tricholoma matsutake) T35, and the extraction method comprises the following steps: the preparation method comprises the steps of putting Tricholoma matsutake T35 into water, leaching at 20-60 ℃, precipitating supernatant obtained by leaching with ethanol at 10-30 ℃, and separating the supernatant.

According to the invention, when the tricholoma matsutake extract is prepared, the temperature of the first-step water extraction is controlled to be 20-60 ℃, so that the tricholoma matsutake extract can be more beneficial to extracting and obtaining effective components which have the functions of nourishing and caring scalp and repairing dyed and ironed damaged hair in the tricholoma matsutake, and the obtained extract has better absorption efficiency through the scalp and the hair.

The preservation number is CCTCC NO: tricholoma matsutake (Tricholoma matsutake) T35 strain of M2014671 has been disclosed in Chinese patent CN 105039170A, and it is capable of obtaining a large amount of mycelia by a biofermentation method.

Before the extraction of the tricholoma matsutake, the method also comprises a step of crushing tricholoma matsutake mycelium. Preferably, the powder is passed through a 60 mesh screen after pulverization.

In the extraction method, the leaching time is preferably 4-12 hours, and the precipitation time is preferably 10-30 hours.

In the leaching step, the leaching time in the leaching time range is longer in the low-temperature extraction.

In the preparation method of the tricholoma matsutake extract, the mass ratio of the tricholoma matsutake to water in an extraction system is 1 (5-16). In a precipitation system, the mass ratio of the supernatant obtained by leaching to the ethanol is 1 (1-3).

As a preferred embodiment of the present invention, the preparation method of the matsutake mushroom extract of the present invention is as follows:

(1) taking a tricholoma matsutake strain CCTCC NO: crushing the mycelium of M2014671, adding 5-16 times of deionized water, and placing at 20-60 ℃ for extraction for 4-12 h;

(2) filtering the water extract in the step (1) to obtain supernatant, adding 1-3 times of ethanol by mass, standing at 10-30 ℃ for precipitation for 10-30 h, centrifuging at 5000r/min for 30min, and taking the supernatant to obtain the tricholoma matsutake extract.

In the invention, the mycelium of the matsutake strain CCTCC NO: M2014671 is preferably obtained by culturing the mycelium of the matsutake strain by a culture method comprising the following culture media of 18-28 g/L of glucose, 5-15 g/L of yeast extract powder, 5-15 g/L of soybean peptone and KH₂PO₄0.3～0.7g/L、MgSO₄·7H₂O0.3-0.7 g/L and VB 10.1-0.4 g/L, and culturing at 26 ℃.

The invention provides application of the tricholoma matsutake extract in preparing scalp and hair care products.

The present invention provides a composition for scalp and hair care comprising matsutake mushroom extract and spicebush flower extract.

The spilanthol can be matched with the tricholoma matsutake extract to act, so that active ingredients in the composition are promoted to be better absorbed by the scalp, and the functions of relieving, resisting oxidation, resisting radiation, repairing dyed and scalded damaged hair and the like are effectively exerted while sufficient nutritional moisture-preserving ingredients are provided for the scalp and the hair.

In the composition of the present invention, the matsutake mushroom extract is preferably prepared from matsutake mushroom extract having a preservation number of CCTCC NO: m2014671 is extracted from Tricholoma matsutake (Tricholoma matsutake) T35. The mass ratio of the tricholoma matsutake extract to the spicebush flower extract is preferably 1 (0.5-5). The tricholoma matsutake extract and the spicebush flower extract are compounded and used according to a proper proportion, so that the spicebush flower extract can effectively promote the tricholoma matsutake extract to be absorbed by scalp, simultaneously better promotes the synergistic effect of the tricholoma matsutake extract and the spicebush flower extract, and more reasonably provides nutrition and functional components for hair and scalp.

In order to increase the scalp and hair nourishing, nursing and repairing efficacy of the composition, the invention further adds the malachite extract into the composition, and the malachite extract has the effect of scavenging free radicals and can delay skin aging.

After the malachite extract is added into the composition, the mass ratio of the tricholoma matsutake extract to the spicebush flower extract is preferably 1 (0.5-4). Malachite extract can interact with matsutake extract and spilanthol extract to provide the composition with superior scalp and hair care benefits.

Preferably, the composition comprises the following components in parts by weight: 1-10 parts of matsutake extract, 2-7 parts of malachite extract and 2-7 parts of spilanthol herb extract.

As a preferable scheme of the invention, the composition comprises the following components in parts by weight: 1-5 parts of tricholoma matsutake extract, 2-5 parts of malachite extract and 2-5 parts of spicebush flower extract.

In the present invention, the malachite extract and the spilanthol extract may be prepared by a conventional method in the art or may be commercially available.

In order to enable the components in the composition to better cooperate, the spilanthol herb extract is an aqueous extract, and the malachite extract is a concentrated sulfuric acid extract.

The spilanthol extract and the malachite extract are preferably prepared by the following extraction methods:

crushing malachite, adding 25-40% concentrated sulfuric acid aqueous solution, leaching for 10-16 h, adding water with the mass being 2-3 times of that of the malachite, performing suction filtration, adding concentrated ammonia water into filtrate, adjusting the pH of the solution to 8.5-9.0, performing suction filtration for 1-2 times, adding 25-40% concentrated sulfuric acid aqueous solution into the filtrate, adjusting the pH of the solution to 5.5-6.0, standing for 10-16 h, and performing suction filtration to obtain filtrate.

Soaking the spilanthol herb in water for 1-2 hours, heating and decocting for 2 times, wherein the water adding amount is 10-20 times of the mass of the spilanthol herb for 1-2 hours each time, combining extracting solutions obtained in the two times, centrifuging, and performing suction filtration on a centrifugate for 1-2 times to obtain a filtrate.

Further, the invention also provides the use of said composition in the preparation of scalp and hair care products.

The product of the invention is preferably a cosmetic product, including but not limited to shampoo, hair tonic, hair dye, hair conditioner, hair treatment agent, hair cream, hair nourishing lotion.

The invention provides a shampoo product, which comprises the composition.

Preferably, the composition accounts for 2-15% of the shampoo product by mass. More preferably 10 to 15%.

The shampoo product also comprises art-approved shampoo product bases.

As an embodiment of the invention, the shampoo product matrix can adopt a formula (in parts by weight) comprising 10-20 parts of anionic surfactant, 1-10 parts of zwitterionic surfactant, 0.5-5 parts of cocamide MEA, 0.1-3 parts of sodium dilinomidopropyl PG-dimethyl ammonium chloride phosphate, 0.1-2 parts of kelp (L AMINARIA JAPONICA) extract, 0.1-2 parts of guar hydroxypropyl trimonium chloride, 0.1-2 parts of stearamidopropyl dimethylamine, 1-6 parts of polyquaternary ammonium salt, 0.1-0.5 part of cocoyl hydrolyzed soybean protein, 0.05-0.5 part of essence, 0.01-0.2 part of preservative and 40-80 parts of deionized water, wherein the anionic surfactant is one or more of laureth ammonium sulfate, methyl myricyl sodium taurate and laureth ammonium sulfate, the zwitterionic surfactant is one or more of lauramidopropyl betaine, lauryl dimethyl betaine and imidazoline, and the polyquaternary ammonium salt is 53-47 parts of polyquaternary ammonium salt.

The present invention provides a hair care product comprising the composition.

Preferably, the composition accounts for 2-15% of the hair care product by mass. More preferably 10 to 15%.

The invention has the beneficial effects that:

1. the tricholoma matsutake extract is prepared by the tricholoma matsutake strains through a biological technology, so that the cost is greatly reduced, the utilization field of tricholoma matsutake resources is expanded, and the sustainable development of tricholoma matsutake products is facilitated.

2. The invention aims at the preservation number of CCTCC NO: the Tricholoma matsutake (Tricholoma matsutake) T35 strain of M2014671 optimizes the extraction method, and the Tricholoma matsutake extract prepared by the specific extraction method provided by the invention not only has excellent absorption efficiency through scalp and hair follicles, but also has better nourishing, nursing and repairing effects on hair and scalp.

3. According to the invention, the spilanthol herb extract and the tricholoma matsutake extract are compounded for use, so that the absorption efficiency of functional components of the tricholoma matsutake extract through scalp is obviously improved.

4. The components in the scalp and hair care composition can be well coordinated and matched, so that sufficient nutrient substances are provided for the metabolism of the scalp and hair follicles, the scalp and the hair are effectively nourished, the hair is strengthened, the damaged hair is repaired, and the scalp aging is delayed.

5. The scalp and hair care composition provided by the invention is composed of extracts of plant sources and mineral sources, is high in safety, has a high application value in hair washing and caring products, and has important significance for solving the health problems of the scalp and the hair.

Detailed Description

Preferred embodiments of the present invention will be described in detail with reference to the following examples. It is to be understood that the following examples are given for illustrative purposes only and are not intended to limit the scope of the present invention. Various modifications and alterations of this invention will become apparent to those skilled in the art without departing from the spirit and scope of this invention.

The experimental procedures used in the following examples are all conventional procedures unless otherwise specified.

The materials, reagents and the like used in the following examples are commercially available, unless otherwise specified, wherein ammonium laureth sulfate is available from KAO (270S-A1), lauramidopropyl betaine is available from KAO (AMPHITO L20 AB), and the extract of Tricholoma matsutake described in the following examples is DOMANT.

The preparation of malachite extract and spilanthol extract used in the following examples was as follows:

malachite extract: taking malachite, crushing, adding a sulfuric acid solution (concentrated sulfuric acid is diluted by 2 times of water) to immerse the malachite, standing for 12 hours, adding water with the mass being 2 times of that of the malachite, carrying out suction filtration, adding concentrated ammonia water into filtrate, adjusting the pH of the solution to be 9.0, carrying out suction filtration on the solution for 2 times, adding the sulfuric acid solution into the filtrate (concentrated sulfuric acid is diluted by 2 times of water), adjusting the pH of the solution to be 6.0, standing the solution for 12 hours, carrying out suction filtration, and filling the filtrate into a 250ml infusion bottle to obtain the malachite.

The extraction of the spilanthol: soaking flos Stephaniae Japonicae in water for 1 hr, decocting for 2 times (each time for 2 hr) with water amount 20 times of the mass of flos Stephaniae Japonicae, mixing the extractive solutions, centrifuging at 4000r/min for 30min, vacuum filtering the centrifugate with Buchner funnel for 2 times (two pieces of filter paper, paper pulp, diatomaceous earth No. 300, and diatomaceous earth No. 700 are sequentially filled in Buchner funnel), adding 2 times of purified water into the filtrate, pouring into 250ml infusion bottle, capping, sterilizing, controlling sterilization temperature at 121 deg.C, and sterilizing for 20 min.

In the following examples, the tricholoma matsutake strain CCTCC NO: the culture method of M2014671 is as follows:

culture medium including glucose 25.62 g/L, yeast extract powder 10.74 g/L, soybean peptone 10 g/L, KH₂PO₄0.57g/L、MgSO₄·7H₂O0.5 g/L and VB10.25g/L, and the culture conditions are 26 ℃ and shaking culture is carried out.

Example 1 composition for scalp and hair treatment (1)

This example provides a composition for scalp and hair care consisting of (parts by weight): 5 parts of matsutake extract, 2.5 parts of malachite extract and 2.5 parts of spilanthol herb extract.

The preparation method of the tricholoma matsutake extract comprises the following steps:

(1) taking a tricholoma matsutake strain CCTCC NO: pulverizing M2014671 mycelium, sieving with 60 mesh sieve, adding 12 times of deionized water, and leaching at 28 deg.C for 10 hr;

(2) filtering the water extract in the step (1) to obtain supernatant, adding 2 times of ethanol, standing at 20 deg.C for precipitation for 24 hr, centrifuging at 5000r/min for 30min, and collecting supernatant to obtain Tricholoma matsutake extract.

Example 2 composition for scalp and hair treatment (2)

This example provides a composition for scalp and hair care consisting of (parts by weight): 2.5 parts of tricholoma matsutake extract, 5 parts of malachite extract and 2.5 parts of spicebush flower extract.

The preparation method of Tricholoma matsutake extract is the same as that of example 1.

Example 3 composition for scalp and hair treatment (3)

This example provides a composition for scalp and hair care consisting of (parts by weight): 1.5 parts of tricholoma matsutake extract, 3.5 parts of malachite extract and 5 parts of spicebush flower extract.

Example 4 composition for scalp and hair treatment (4)

This example provides a composition for scalp and hair care consisting of (parts by weight): 3 parts of matsutake extract, 3.5 parts of malachite extract and 3.5 parts of spilanthol herb extract.

Example 5 composition for scalp and hair treatment (5)

(1) taking a tricholoma matsutake strain CCTCC NO: pulverizing M2014671 mycelium, sieving with 60 mesh sieve, adding 12 times of deionized water, and leaching at 58 deg.C for 5 hr;

(2) filtering the water extract in the step (1) to obtain supernatant, adding 2 times of ethanol, standing at 20 deg.C for precipitation for 24h, centrifuging at 5000r/min for 30min, and collecting supernatant to obtain Tricholoma matsutake extract.

EXAMPLE 6 shampoo (1)

The embodiment provides shampoo, which comprises the following components (by mass): 10% of the composition of example 1 and 90% of shampoo base.

Wherein, the shampoo matrix comprises the following components (by mass percent):

15% of ammonium laureth sulfate, 3% of sodium methyl myristoyl taurate, 6% of lauramidopropyl betaine, 0.2% of stearamidopropyl dimethylamine, 0.5% of cocamide MEA, 472% of polyquaternium-quaternary ammonium salt, 1% of kelp (L AMINARIPAPONICA) extract, 0.1% of cocoyl hydrolyzed soybean protein, 0.2% of sodium dilinoamidopropyl PG-dimethyl ammonium chloride phosphate, 0.2% of guar hydroxypropyl trimethyl ammonium chloride, 0.1% of essence, 0.1% of iodopropynyl butyl carbamate and 72% of deionized water.

The embodiment also provides a preparation method of the shampoo, which comprises the following steps: mixing Tricholoma matsutake extract, Malachite extract and flos Chrysanthemi Indici extract, adding into shampoo matrix, and stirring.

EXAMPLE 7 shampoo (2)

The embodiment provides shampoo, which comprises the following components (by mass): 10% of the composition of example 2 and 90% of shampoo base.

The shampoo base formulation and shampoo were prepared as in example 6.

EXAMPLE 8 shampoo (3)

The embodiment provides shampoo, which comprises the following components (by mass): 10% of the composition of example 3 and 90% of shampoo base.

The shampoo base formulation and shampoo were prepared as in example 6.

EXAMPLE 9 shampoo (4)

The embodiment provides shampoo, which comprises the following components (by mass): 10% of the composition of example 4 and 90% of shampoo base.

The shampoo base formulation and shampoo were prepared as in example 6.

Example 10 shampoo (5)

The embodiment provides shampoo, which comprises the following components (by mass): 10% of the composition of example 5 and 90% of shampoo base.

The shampoo base formulation and shampoo were prepared as in example 6.

Comparative example 1

This comparative example provides a composition (in parts by weight) containing only the extract of matsutake mushroom prepared in the same manner as in example 1.

Comparative example 2

The present comparative example provides a composition consisting of (parts by weight): 7.5 parts of matsutake extract and 2.5 parts of malachite extract.

Comparative example 3

The present comparative example provides a composition consisting of (parts by weight): 5 parts of matsutake extract, 2.5 parts of malachite extract and 2.5 parts of chamomile extract.

Comparative example 4

The present comparative example provides a composition consisting of (parts by weight): 5 parts of matsutake extract, 2.5 parts of malachite extract and 2.5 parts of spilanthol herb extract.

The preparation method of Tricholoma matsutake extract comprises:

(1) taking a tricholoma matsutake strain CCTCC NO: pulverizing M2014671 mycelium, sieving with 60 mesh sieve, adding 12 times of deionized water, and leaching at 80 deg.C for 5 hr;

Comparative example 5

The comparative example provides shampoo which comprises the following components in percentage by mass: composition 10% of comparative example 1, shampoo base 90%.

The formulation of the shampoo base and the preparation of the shampoo were the same as in example 6.

Comparative example 6

The comparative example provides shampoo which comprises the following components in percentage by mass: composition of comparative example 2 10%, shampoo base 90%.

Comparative example 7

The comparative example provides shampoo which comprises the following components in percentage by mass: composition of comparative example 3 10%, shampoo base 90%.

Comparative example 8

The comparative example provides shampoo which comprises the following components in percentage by mass: composition of comparative example 4 10%, shampoo base 90%.

Comparative example 9

This comparative example provides a shampoo consisting only of shampoo base, formulated as in example 6.

Experimental example 1 skin absorption Effect of the composition

In this experimental example, the skin absorption effect of the compositions of examples 1 to 5 and comparative examples 1 to 4 was analyzed by the following specific method:

experimental animals C57B L/6 mice weighing 18-22g, 80 animals in total, were randomly divided into 8 groups of 10 animals each.

A mouse is unhaired for 30 seconds by 8% sodium sulfide, washed clean by normal saline, peeled off, subcutaneous adipose tissues are removed, the skin of the mouse is cleaned by normal saline, the skin of the mouse which is pretreated is fixed between a diffusion chamber and a receiving chamber of a permeation diffusion device, normal saline 17m L is injected into the receiving chamber through a sampling tube to serve as receiving liquid, the liquid level is in full contact with the inner layer of the skin, the compositions in examples 1-5 and comparative examples 1-4 (the extracts of the tricholoma matsutake in examples 1-5 and comparative examples 1-4 are 3.6g respectively) are added into the diffusion chamber, the top of the diffusion chamber and the sampling port of the receiving chamber are covered by a preservative film, the stirring is continued, the sampling is carried out after 1 hour, the content of the polypeptide in the diffusion chamber before and after the stirring is detected by using a Coomassie brilliant blue kit, the detection results of each group of mice are averaged, and the results are shown in Table 1, and the results show that the effect of the permeation absorption of the compositions in examples 1-5 through the skin is obviously better than that in the comparative examples.

TABLE 1 detection of polypeptide content in solution

Experimental example 2 trial effect experiment of shampoo

In order to verify the hair scalp nourishing effect of the shampoos of the examples and comparative examples, 100 volunteers aged 25-60 years were selected and divided into 10 groups of 10 persons, and one shampoo of examples 6-10 and comparative examples 5-9 was provided for each group of 10 persons, the use time was 2 months, the use frequency was once every two days, and the combing property, softness, moisture retention, itching relieving and stain removing effects of the shampoo were examined. The test performance was set to 6 levels, as follows: 6 represents excellent; 5 stands for good; 4 represents preferably; 3 represents general; 2 represents poor; 1 represents the difference. The test results of each group of volunteers were averaged and the test indices and results are shown in table 2.

TABLE 2 trial effect of shampoo

The results show that: the trial effect of the shampoos in examples 6-10 on combing property, softness, moisture retention, itching relieving and decontamination effect is obviously better than that of comparative examples 5-9, which shows that the compositions in examples 1-5 can significantly improve the shampoo effect of the shampoo, exert effective nourishing, moisture retention, antibacterial and other care effects on scalp and hair, and significantly improve hair quality and health state.

Experimental example 3 shampoo restoration hair dyeing and ironing effect experiment

In order to verify the effect of the shampoos of the examples and the comparative examples on repairing damaged hair by dyeing and perming, 100 volunteers who dyed and permed hair within the last year between the ages of 25 and 60 are selected, the hair is damaged to a certain extent in the dyeing and perming process, the volunteers are divided into 10 groups, 10 people are selected in each group, one shampoo of the examples 6 to 10 and the comparative examples 5 to 9 is provided respectively, the using time is 2 months, the using frequency is once every two days, and the hair strengthening effect of the shampoo is examined. The volunteers measured the breaking strength of hair before the start of the experiment, and the breaking strength of hair 2 months after using shampoo, and compared the change in the strength of hair. The hair strength was tested using INSTRON 5565 universal material testing equipment. The specific test method comprises the following steps: taking a hair sample to be tested, balancing for 24 hours in an atmospheric environment with the temperature of 20 +/-2 ℃ and the relative humidity of 65 +/-3%, then testing under the atmospheric condition, wherein the hair clamping length is 150mm, the stretching speed is 500mm/min, 20 hair samples are respectively tested by each volunteer, the average value of each group of volunteers is obtained, and the result is shown in table 3.

TABLE 3 Hair breaking Strength

The results show that: the shampoo of examples 6-10 has significantly better effects on repairing dyed and ironed damaged hair than comparative examples 5-9, which shows that the compositions of examples 1-5 can significantly improve the hair strength, wherein the composition of example 1 has the best effect.

Although the invention has been described in detail hereinabove by way of general description, specific embodiments and experiments, it will be apparent to those skilled in the art that many modifications and improvements can be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.

Claims

1. A matsutake mushroom extract is characterized by being prepared from matsutake mushroom with a preservation number of CCTCC NO: m2014671 Tricholoma matsutake (Tricholoma matsutake) T35, and the extraction method comprises the following steps: the preparation method comprises the steps of putting Tricholoma matsutake T35 into water, leaching at 20-60 ℃, precipitating supernatant obtained by leaching with ethanol at 10-30 ℃, and separating the supernatant.

2. The tricholoma matsutake extract according to claim 1, wherein the leaching time is 4-12 hours, and the precipitation time is 10-30 hours;

preferably, in the leaching system, the mass ratio of the tricholoma matsutake to the water is 1 (5-16); and/or in the system of the precipitate, the mass ratio of the supernatant obtained by leaching to the ethanol is 1 (1-3).

3. Use of the matsutake mushroom extract according to claim 1 or 2 for the preparation of scalp and hair care products.

4. A composition for scalp and hair care comprising matsutake mushroom extract and spicebush flower extract.

5. The composition according to claim 4, wherein the tricholoma matsutake extract is the tricholoma matsutake extract of claim 1 or 2; the mass ratio of the tricholoma matsutake extract to the spicebush flower extract is 1 (0.5-5).

6. The composition of claim 4 or 5, wherein the composition further comprises malachite extract; the mass ratio of the tricholoma matsutake extract to the spicebush flower extract is 1 (0.5-4);

preferably, the composition comprises the following components in parts by weight: 1-10 parts of tricholoma matsutake extract, 2-7 parts of spilanthol flower extract and 2-7 parts of malachite extract.

7. The composition according to any one of claims 4 to 6, wherein the spilanthol extract is an aqueous extract and the malachite extract is a concentrated sulfuric acid extract.

8. Use of a composition according to any one of claims 4 to 7 for the preparation of scalp and hair care products.

9. A shampoo product comprising a composition according to any of claims 4 to 7;

preferably, the composition accounts for 2-15% of the shampoo product by mass.

10. A hair care product comprising the composition of any one of claims 4 to 7;

preferably, the composition accounts for 2-15% of the hair care product by mass.