CN109385139B - 氧化锌基纳米颗粒墨水的提纯方法 - Google Patents
氧化锌基纳米颗粒墨水的提纯方法 Download PDFInfo
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- CN109385139B CN109385139B CN201710656041.XA CN201710656041A CN109385139B CN 109385139 B CN109385139 B CN 109385139B CN 201710656041 A CN201710656041 A CN 201710656041A CN 109385139 B CN109385139 B CN 109385139B
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 title claims abstract description 304
- 239000002105 nanoparticle Substances 0.000 title claims abstract description 164
- 239000011787 zinc oxide Substances 0.000 title claims abstract description 152
- 238000000034 method Methods 0.000 title claims abstract description 53
- 238000000746 purification Methods 0.000 title claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 118
- 238000005194 fractionation Methods 0.000 claims abstract description 66
- 238000000926 separation method Methods 0.000 claims abstract description 31
- 229920006395 saturated elastomer Polymers 0.000 claims description 41
- 230000009467 reduction Effects 0.000 claims description 10
- 238000011946 reduction process Methods 0.000 claims description 9
- 230000006837 decompression Effects 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 150000001298 alcohols Chemical class 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 2
- -1 ether alcohols Chemical class 0.000 claims description 2
- 150000002170 ethers Chemical class 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- 239000012043 crude product Substances 0.000 abstract description 9
- 239000000976 ink Substances 0.000 description 116
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 23
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical group CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 18
- 239000000243 solution Substances 0.000 description 17
- 230000015572 biosynthetic process Effects 0.000 description 9
- 238000007641 inkjet printing Methods 0.000 description 9
- 238000003786 synthesis reaction Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- KBPLFHHGFOOTCA-UHFFFAOYSA-N caprylic alcohol Natural products CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000001308 synthesis method Methods 0.000 description 5
- 229940028356 diethylene glycol monobutyl ether Drugs 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000000593 microemulsion method Methods 0.000 description 4
- JCGNDDUYTRNOFT-UHFFFAOYSA-N oxolane-2,4-dione Chemical compound O=C1COC(=O)C1 JCGNDDUYTRNOFT-UHFFFAOYSA-N 0.000 description 4
- 238000005086 pumping Methods 0.000 description 4
- 238000003980 solgel method Methods 0.000 description 4
- CUVLMZNMSPJDON-UHFFFAOYSA-N 1-(1-butoxypropan-2-yloxy)propan-2-ol Chemical compound CCCCOCC(C)OCC(C)O CUVLMZNMSPJDON-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical group CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 3
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 230000001276 controlling effect Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000703 high-speed centrifugation Methods 0.000 description 3
- TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- OAYXUHPQHDHDDZ-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethanol Chemical group CCCCOCCOCCO OAYXUHPQHDHDDZ-UHFFFAOYSA-N 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000007810 chemical reaction solvent Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000012716 precipitator Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000013557 residual solvent Substances 0.000 description 2
- 238000007740 vapor deposition Methods 0.000 description 2
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000005233 alkylalcohol group Chemical group 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000005291 magnetic effect Effects 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002096 quantum dot Substances 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1388827A (zh) * | 2000-09-08 | 2003-01-01 | 纳米技术有限公司 | 纳米粒子的合成 |
CN101386723A (zh) * | 2008-10-30 | 2009-03-18 | 上海大学 | 纳米铜导电墨水的制备方法 |
CN103395809A (zh) * | 2013-07-23 | 2013-11-20 | 浙江万里学院 | 一种采用溶剂置换/共沸点蒸馏干燥法合成纳米γ-Al2O3的方法及其应用 |
CN106006611A (zh) * | 2016-05-18 | 2016-10-12 | 中国科学院山西煤炭化学研究所 | 一种高效制备氧化石墨烯有机溶液的方法 |
CN106118216A (zh) * | 2016-07-29 | 2016-11-16 | 宁波工程学院 | 一种Ga掺杂ZnO纳米墨水及其制备方法 |
CN106380934A (zh) * | 2016-08-30 | 2017-02-08 | Tcl集团股份有限公司 | 一种氧化锌基纳米颗粒墨水及其制备方法 |
CN106634948A (zh) * | 2016-10-31 | 2017-05-10 | 纳晶科技股份有限公司 | 氧化锌纳米晶、其制备方法、氧化锌纳米晶墨水和电致发光器件 |
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Publication number | Priority date | Publication date | Assignee | Title |
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US8507556B2 (en) * | 2007-09-22 | 2013-08-13 | Boise State University | Fluorescent particles comprising nanoscale ZnO layer and exhibiting cell-specific toxicity |
EP3173246A1 (en) * | 2015-11-30 | 2017-05-31 | Agfa Graphics NV | Inkjet ink set for a method of manufacturing a packaging |
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- 2017-08-03 CN CN201710656041.XA patent/CN109385139B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1388827A (zh) * | 2000-09-08 | 2003-01-01 | 纳米技术有限公司 | 纳米粒子的合成 |
CN101386723A (zh) * | 2008-10-30 | 2009-03-18 | 上海大学 | 纳米铜导电墨水的制备方法 |
CN103395809A (zh) * | 2013-07-23 | 2013-11-20 | 浙江万里学院 | 一种采用溶剂置换/共沸点蒸馏干燥法合成纳米γ-Al2O3的方法及其应用 |
CN106006611A (zh) * | 2016-05-18 | 2016-10-12 | 中国科学院山西煤炭化学研究所 | 一种高效制备氧化石墨烯有机溶液的方法 |
CN106118216A (zh) * | 2016-07-29 | 2016-11-16 | 宁波工程学院 | 一种Ga掺杂ZnO纳米墨水及其制备方法 |
CN106380934A (zh) * | 2016-08-30 | 2017-02-08 | Tcl集团股份有限公司 | 一种氧化锌基纳米颗粒墨水及其制备方法 |
CN106634948A (zh) * | 2016-10-31 | 2017-05-10 | 纳晶科技股份有限公司 | 氧化锌纳米晶、其制备方法、氧化锌纳米晶墨水和电致发光器件 |
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Effective date of registration: 20240513 Address after: Room 802-1, unit B1, building D4, R & D building, TCL Science Park, 1001 Zhongshan Park Road, Xili Liuxian cave, Nanshan District, Shenzhen City, Guangdong Province Patentee after: SHENZHEN TCL HIGH-NEW TECHNOLOGY DEVELOPMENT CO.,LTD. Country or region after: China Address before: 518000 TCL building, Nanyi Road, South District, Shenzhen hi tech park, Guangdong Province Patentee before: Shenzhen TCL Industry Research Institute Co.,Ltd. Country or region before: China |