CN109363996A - A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia and its preparation method and application - Google Patents

A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia and its preparation method and application Download PDF

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Publication number
CN109363996A
CN109363996A CN201811528686.6A CN201811528686A CN109363996A CN 109363996 A CN109363996 A CN 109363996A CN 201811528686 A CN201811528686 A CN 201811528686A CN 109363996 A CN109363996 A CN 109363996A
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China
Prior art keywords
cotton
fiber
camellia
soft towel
skin
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CN201811528686.6A
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Chinese (zh)
Inventor
黄玉琴
刘凯华
刘少峰
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HUNAN QIANJIN SANITARY PRODUCT CO Ltd
Zhuzhou Qianjin Pharmaceutical Co Ltd
Original Assignee
HUNAN QIANJIN SANITARY PRODUCT CO Ltd
Zhuzhou Qianjin Pharmaceutical Co Ltd
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Priority to CN201811528686.6A priority Critical patent/CN109363996A/en
Publication of CN109363996A publication Critical patent/CN109363996A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0208Tissues; Wipes; Patches
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C1/00Treatment of vegetable material
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/425Cellulose series
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4382Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/44Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
    • D04H1/46Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
    • D04H1/492Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/10Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
    • D06L4/13Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Textile Engineering (AREA)
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  • Wood Science & Technology (AREA)
  • Zoology (AREA)
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  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
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Abstract

The present invention provides a kind of soft towel of bacteriostatic skin-care cotton of fiber containing camellia.The present invention is that successful application camellia fiber prepares the soft towel of cotton, and leading portion bleaching is carried out after first pre-processing cotton fiber, then matches with camellia fiber, the soft towel of bacteriostatic skin-care cotton is prepared.Camellia oil is rich in camellia fiber, moisturizing, anti-oxidant, anti-sensitivity, antiultraviolet, antibacterial effect can also eliminate skin fine wrinkles, and effective delay skin aging alleviates part skin disease, has wide practical use in daily life.

Description

A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia and its preparation method and application
Technical field
The present invention relates to amenities technical fields, more particularly, to a kind of bacteriostatic skin-care cotton of fiber containing camellia Soft towel and its preparation method and application.
Background technique
Cotton is annual plant mostly, is one of most important crops in the world, yield is big, production cost is low, makes Cotton products less expensive.The fabric of plurality of specifications can be made in cotton fiber, from slim and graceful transparent organdy to thick and solid canvas With thick velveteen, it is suitable for making all kinds of clothes, furniture stuff and industrial cloth.Cotton fabric is strong wear-resisting, can wash and press at high temperature It scalds, cotton quickly makes to wear comfortable due to moisture absorption and dehumidification.Cotton fiber is derived from cotton, cotton Products moisture absorption and gas permeability It is good, it is soft and keep warm.
Camellia tree is a kind of natural xylophyta of preciousness, and camellia oil is exactly from the red camellia flower seed of camellia tree It refines, is derived from naturally, it is pollution-free, it is most ancient one of the woody edible vegetable oil in China.Camellia oil is full of nutrition, fatty Acid, camellianin, tea polyphenols, saponin, tannin, and rich in antioxidant and with the squalene of anti-inflammatory effect, squalene and flavones Substance plays the role of anticancer splendid.Camellia oil is also rich in the microelements such as vitamin E and calcium, iron, zinc.
Camellia caul-fat is rich in camellia fiber, and camellia oil is that presently found unsaturated fatty acid content is highest Oil, up to 90% or more, the most close with the 70% of human skin fat, wherein oleic acid reaches 80-83%, and is rich in protein It with vitamin A, B, D, E etc., can easily be absorbed by the skin, deep layer is nourished and conditioning skin, plays moisturizing, anti-oxidant, anti-anaphylaxis Sense, antiultraviolet and antibacterial effect.Linolenic acid abundant especially contained by it is needed by human and cannot synthesize.People Fatty acid in the primary structure constituent of body skin, one of be oleic acid, oleic acid has the function of moisturizing, safeguards skin skin Rouge layer.
The soft towel of cotton has the characteristics that soft exquisiteness, water imbibition is good, does not fall to consider to be worth doing, is the products such as paper handkerchief, cotton pads, washcloth New environment-friendly type substitute products.And the soft towel of cotton a large amount of acarids easy to breed, using the soft towel of such cotton can allow skin become it is coarse and And pore can be coarse, and the mostly only wiping, the effect of cleaning skin of the soft towel of existing cotton, can not play further to skin Protective effect.
Summary of the invention
Aiming at the shortcomings in the prior art, the soft towel of bacteriostatic skin-care cotton and its preparation side of a kind of fiber containing camellia are provided Method.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:
A kind of soft towel of bacteriostatic skin-care cotton of fiber containing camellia is provided, the ontology of the soft towel of skin care cotton containing camellia Preparing raw material includes camellia fiber and cotton fiber, and respectively by pretreatment, the cotton is fine for the camellia fiber and cotton fiber Dimension carries out leading portion bleaching after pretreatment;
The preprocessing process of the camellia fiber includes that fiber impurity is picked, shredding, combs step;
The preprocessing process of the cotton fiber include: by raw cotton by opening picking and carding step processing after at item, break Afterwards at packet;Or, raw cotton is broken Hou Chengbao at item after the processing of opening picking, cotton carding and combing process;
The leading portion bleaching are as follows: by the wax or grease removal on cotton fiber, after bleaching agent then is added into cotton fiber Carry out ultrasonication.
Preferably, when the ultrasonication, it is 1:5~10, is warming up to 65~80 DEG C, benefit in bath raio after bleaching agent is added With 50~60min of ultrasonication, ultrasonic frequency is 30~40KHz.
Preferably, the bleaching agent is the hydrogenperoxide steam generator that concentration is 30%.
Preferably, the mixed proportion of the camellia fiber and cotton quality proportion is 1:19~2:18.
Preferably, the soft towel of bacteriostatic skin-care cotton further includes the Essence of the ontology coated on the soft towel of bacteriostatic skin-care cotton.
Preferably, the method for the coating of the Essence is to be atomized the mutual infiltration method of molecule using micro emulsion;It is preferred that the micro emulsion 16~18 DEG C of atomization temperature, 0.2~0.35MPa of atomizing pressure of the atomization mutual infiltration method of molecule, air column jet air pressure 0.4~ 0.7MPa。
It is further preferred that the Essence is made of the active component extract of following parts by weight of component: aloe is extracted 0.01~0.3 part of object, 0.01~0.3 part of mint extract, 0.01~0.2 part of Millettia extract, Salvia root P.E 0.01~ 0.2 part.
The present invention provides the preferred preparation process of the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia, comprising the following steps:
S1. camellia fiber and cotton fiber are pre-processed respectively, carries out leading portion bleaching after cotton fiber pretreatment;
S2. it will be mixed with treated camellia fiber and cotton fiber;
S3., composite fibre is successively passed through to opening picking, cotton carding, combing process a smart post-tensioning is made and be broken into smart net;
S4. smart net by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and is batched;
S5. plant essence liquid is extracted, the Essence is made of the active component extract of following parts by weight of component: aloe 0.01~0.3 part of extract, 0.01~0.3 part of mint extract, 0.01~0.2 part of Millettia extract, Salvia root P.E 0.01~0.2 part;
By plant extraction liquid through handling the soft towel of cotton using the mutual infiltration method of micro emulsion atomization molecule to get the fiber containing camellia The soft towel of bacteriostatic skin-care cotton.
Further, in preparation method step S1, the preprocessing process of the camellia fiber includes: that fiber impurity is chosen It picks, shredding, combing;It is bleached using leading portion;
Preferably, oiling dosage is 0.5% in the step shredding;
The preprocessing process of the cotton fiber include: by raw cotton by opening picking and carding step processing after at item, break Afterwards at packet;Or, raw cotton is broken Hou Chengbao at item after the processing of opening picking, cotton carding and combing process;
The leading portion bleaching are as follows: by the wax or grease removal on cotton fiber, the peroxidating that concentration is 30% is then added Hydrogen solution, bath raio is 1:5~10, after being warming up to 65~80 DEG C, handles 50~60min, ultrasonic wave to cotton fiber using ultrasonic wave Frequency is 30~40KHz.
Further, in preparation method step S2, the camellia fiber and cotton fiber mixing specific steps include: by It is mixed to carry out case by spun requirement for pretreated camellia fiber and cotton fiber.
Further, in preparation method step S2, the mixed proportion of the camellia fiber and cotton fiber is 1:19~2: 18。
Further, in preparation method step S4, the spun lacing process carries out in rotary drum spun-laced machine.
Further, in preparation method step S4, the spun lacing step includes 4 spun lacing steps;
Preferably, in the 4 spun lacing step, the 1st to the 4th spun lacing pressure are as follows: 17~19kg, 15~19kg, 29~ 34kg, 15~18kg.
Further, in step S4, the drying process temperature is 60~65 DEG C, and the drying process time is 10~15s.
Further, in preparation method step S5, the plant extraction liquid, which passes through, is added 4~8 times of organic solvent dilutings, then By high pressure nozzle jet atomization, the plant extraction liquid after atomization is evenly distributed under the high pressure draught effect of upper and lower convection current to be contained On the soft towel of the cotton of camellia fiber.
Further, the organic solvent is one of ethyl alcohol, glycerol, propylene glycol, benzyl alcohol, polyethylene glycol or several Kind.
Further, in preparation method step S5, the micro emulsion is atomized mutual 16~18 DEG C of infiltration method atomization temperature of molecule, mist Change 0.2~0.35MPa of pressure, 0.4~0.7MPa of air column jet air pressure;
Preferably, the Jet Stream is one of nitrogen or carbon dioxide.
The water jet process that the present invention uses keeps fiber entangled to each other one on the fine water flow jet to web of high pressure Rise, thus make web with reinforce have certain mechanical strength.By breaking strength to camellia fiber and cotton fiber, return The factors such as damp rate, oil content, fiber number, length influence the performance of spunlace non-woven cloth, determine that the spun lacing pressure of blended spun lacing is 15 ~34kg, spun lacing pressure is bigger, and water needle energy is higher, and the non-woven fabrics intensity that spun lacing goes out is also higher, but excessively high hydraulic pressure meeting Make fibrous fracture and fiber loss, causes non-woven fabrics intensity to decline or the fiber in web is directly made to generate two influence nothing of displacement The quality of woven fabric;The surface of hypotony, web cannot consolidate well.
The present invention is reinforced according to the performance and content of camellia fiber and cotton fiber using 4 water jet processes, and using from Low to high to be distributed in reduced pressure, pressure is respectively as follows: 17~19kg, 15~19kg, 29~34kg, 15~18kg.First The hypertonia of road spun lacing can reduce non-woven fabrics quality, be lost fibrous fracture, aggravate the burden of water circulation system, cause two, The snagging of three water jet processes is serious.Two spun lacing pressure are too small, and web is reinforced loosely, and loosely organized, camellia is fine Peacekeeping cotton fiber cannot combine closely, and non-woven fabrics is made to form coarse surface, and the uniformity of nonwoven cloth cover is caused to decline, and fluffing is tight Weight, influences the feel of product;Two spun lacing pressure are excessive, make that fiber alignment is mixed and disorderly, the decline of entanglement degree, to make strength ratio in length and breadth To increasing, fibre damage is caused.Three spun lacing high pressures reinforce web, and camellia fiber and cotton fiber is made to reach good Mechanical property.The main function of four spun lacings is the modification that positive and negative are carried out to nonwoven cloth cover, is not up to saturated to entanglement degree Fiber further puncture, so that it is reached saturation as far as possible, this just determines that spun lacing pressure cannot be too low;Meanwhile four spun lacing pair The surface of non-woven fabrics carries out certain reparation, this just determines that spun lacing pressure cannot be excessively high.It is further preferred that the camellia is fine For dimension with cotton fiber by four spun lacing steps, spun lacing pressure is respectively 18kg, 17kg, 32kg, 17kg.
The non-woven fabrics of preparation is applied to the soft towel of cotton, heretofore described micro emulsion is atomized on the air column in the mutual infiltration method of molecule Lower two rows of one-to-one correspondence, are distributed a high pressure nozzle every 1cm.The plant extraction liquid after dilution is uniformly penetrated into using the method In the soft towel of the cotton of the fiber containing camellia, the method can make the plant extraction liquid in the soft towel of the cotton of the fiber containing camellia micro and equal It is even, the effect of existing plant extraction liquid is brought, and can keep fiber in the soft towel of cotton naturally, comfortable, skin affinity.
Compared with prior art, beneficial effect is:
1. the present invention handles cotton fiber using targetedly pretreatment and preceding sectional bleaching process, cotton fiber pretreatment can be gone Except sundries such as cottonseed, unginned cotton, mote, sands, and certain combing is made to cotton fiber, the cotton fiber for being you can be with other Fiber preferably mixes, and is conducive to preparation multiple fiber fabric.Leading portion bleaches the sundries that can be further processed in cotton fiber, and cotton Wax and grease on fiber can be removed further, and the water imbibition of cotton fiber is further improved.By the pre- of cotton fiber Processing is bleached with leading portion, keeps the performance of cotton fiber more excellent, color is more preferable, and the impurity contained in cotton fiber is fewer.Using The own color that the soft towel of cotton prepared after camellia fiber maintains camellia fiber is added in leading portion bleaching, and will not be to mountain The camellia caul-fat effective component being rich in camellia fiber damages.
2. the present invention uses camellia fiber, the effect that camellia fiber is rich in camellia oil is played, camellia fiber is added Cotton soft towel moisturizing, anti-oxidant, anti-sensitivity, antiultraviolet, antibacterial effect can be played to skin, it is thin skin can also to be eliminated Small wrinkle, effective delay skin aging, use in winter have prevention and treatment effect well for chapped skin, scaling bits, dry itch Fruit, summer can effectively inhibit and resist viral bacterium using can prevent red swelling of the skin shouting pain, with beauty and skin care Effect, it helps skin colour can also be improved as a kind of antioxidant by protecting the softness health of skin, alleviate such as ox The partial skins such as psoriasis disease.
3. of the invention is mainly the non-woven fabrics of cotton fiber and camellia fiber, water jet process using water jet process raw materials for production The softness and comfort level of fibrinogen, the original color of fiber can effectively be retained, and can mainly be retained abundant in camellia Camellia oil component.By the setting to technique, by four water jet processes, the non-woven fabrics prepared is in intensity, quality, and relaxes The aspect of performance such as appropriateness are all very excellent.
It, can be with using the method 4. joined the method mutually seeped of micro emulsion atomization molecule in heretofore described preparation process Sprinkling has the liquid of certain effects on the soft towel of cotton, have the soft towel of cotton of preparation can other than the effect of camellia oil more The effect of, and the liquid of sprinkling can be made uniform using the method, it is adhere strongly on the soft towel of cotton, and the soft towel of cotton will not be destroyed The structure and comfort level of script.The effect of amount of flushing liquor can also significantly be saved, and product will not be reduced.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, it is no intended to limit of the invention Protection scope.
Unless otherwise specified, various raw material, reagent, the instrument and equipment etc. used in the present invention can pass through city Field is commercially available or can be prepared by existing method.
The extracting method of 1 plant essence liquid of embodiment
Essence is made of the active component extract of following parts by weight of component: 0.01~0.3 part of aloe extract, peppermint 0.01~0.3 part of extract, 0.01~0.2 part of Millettia extract, 0.01~0.2 part of Salvia root P.E;
Firstly, aloe is smashed it through 30 meshes, according to the solid-liquid ratio (g:ml) of 1:18, with the ethyl alcohol of volume fraction 90% Ultrasonic extraction 85min, concentrated extracting solution are to get, wherein the frequency of ultrasonic extraction at the medicinal extract of relative density 1.1~1.3 40kHz, power 500W;
Secondly, respectively general, Caulis Spatholobi, Radix Salviae Miltiorrhizae boiling, it is extracted, filter de- slag and obtain corresponding filtrate, by Caulis Spatholobi, Radix Salviae Miltiorrhizae It leaves after boiling and is extracted again;The extracting solution is merged with first time extracting solution;
Finally, aloe extract and Radix Angelicae Sinensis, Radix Salviae Miltiorrhizae and the mixed extract of Caulis Spatholobi is added in peppermint, mixing is equal It is even, 90% ethyl alcohol, ultrasonic dissolution is added, until pink colour clear solution is to get wherein the frequency of ultrasonic dissolution is 40kHz, power For 500W.
Although a kind of above-mentioned specific embodiment for being only exemplified by each extract, it will be appreciated by those skilled in the art that Be be not limited to other extracting methods (method especially in the limited range of the present invention) of ad hoc fashion similarly can be with It realizes essentially identical extraction effect, can be used for realizing the present invention, this is no longer particularly limited.
The pretreatment of 2 camellia fiber of embodiment
In the present embodiment camellia fiber preprocessing process include: fiber impurity pick, shredding, combing;In shredding step Oiling dosage is 0.5%.
The leading portion of 3 cotton fiber of embodiment is bleached
Processing of the present embodiment to the leading portion bleaching of cotton fiber are as follows: pretreated cotton fiber is subjected to ultrasonication, When ultrasonication, bleaching agent is that concentration is 30% hydrogenperoxide steam generator, and being added after bleaching agent in bath raio is 1:5~10, heating To 65~80 DEG C, using 50~60min of ultrasonication, ultrasonic frequency is 30~40KHz.
Embodiment 4
A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia, the soft towel of bacteriostatic skin-care cotton containing camellia include material composition Camellia fiber and cotton fiber are prepared through following method:
S1. camellia fiber and cotton fiber are pre-processed respectively, the preprocessing process of camellia includes: fiber impurity It picks, shredding, combing, oiling dosage is 0.5% in step shredding;
Cotton fiber pretreatment for by raw cotton by opening picking and carding step processing after at item, break Hou Chengbao;Using Leading portion bleaching, bleaching process reference implementation example 3;
S2. pretreated camellia fiber and cotton fiber are carried out according to raw material proportioning camellia fiber: cotton fiber 1: It is mixed that 19 proportion carries out case;
S3., composite fibre is successively passed through to opening picking, cotton carding, combing process a smart post-tensioning is made and be broken into smart net;
S4. smart net by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and is batched;Wherein spun lacing work Sequence carries out in rotary drum spun-laced machine, is divided into four spun lacing steps, the 1st to the 4th spun lacing pressure are as follows: 18kg, 17kg, 32kg, 17kg;Being dried temperature is 65 DEG C, and the drying process time is 15s;
S5. plant essence liquid is extracted, the Essence is made of the active component extract of following parts by weight of component: aloe 0.2 part of extract, 0.13 part of mint extract, 0.21 part of Millettia extract, 0.12 part of Salvia root P.E.
By the plant essence liquid of extraction according to plant extraction liquid: ethyl alcohol is the dilution proportion of 1:6 into weak solution, is reused micro- Plant extraction liquid after dilution by high pressure nozzle jet atomization, 17 DEG C of atomization temperature, is atomized by the cream atomization mutual infiltration method of molecule Pressure 0.25MPa, air column jet air pressure 0.55MPa, Jet Stream is nitrogen, and the plant extraction liquid after atomization is in upper and lower convection current The bacteriostatic skin-care nonwoven on the non-woven fabrics of the fiber containing camellia to get the fiber containing camellia is evenly distributed under high pressure draught effect Cloth.
The bacteriostatic skin-care non-woven fabrics of the fiber obtained containing camellia is applied to the soft towel of cotton.
The plant essence liquid activity extracted in the present invention is high, intact extraction and saves effective ingredient in plant, Middle aloe essence has the function of sterilization, anti-inflammatory, anti-aging, and Radix Salviae Miltiorrhizae essence can circumcise relieving restlessness, Caulis Spatholobi can with clearing and activating the channels and collaterals, Regulating lipid metabolism, peppermint essence have it is refrigerant, also there is good effect to pruitus, fash and eczema.Micro plant Object Essence ensure that with enough care effects, will not cause the waste of plant essence liquid.
Embodiment 5
A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia, the soft towel of bacteriostatic skin-care cotton containing camellia include material composition Camellia fiber and cotton fiber are prepared through following method:
S1. camellia fiber and cotton fiber are pre-processed respectively, the preprocessing process of camellia includes: fiber impurity It picks, shredding, combing, oiling dosage is 0.5% in step shredding;
Cotton fiber pretreatment for by raw cotton by opening picking and carding step processing after at item, break Hou Chengbao;Using Leading portion bleaching, bleaching process reference implementation example 3;
S2. pretreated camellia fiber and cotton fiber are carried out according to raw material proportioning camellia fiber: cotton fiber 2: It is mixed that 18 proportion carries out case;
S3., composite fibre is successively passed through to opening picking, cotton carding, combing process a smart post-tensioning is made and be broken into smart net;
S4. smart net by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and is batched;Wherein spun lacing work Sequence carries out in rotary drum spun-laced machine, is divided into four spun lacing steps, the 1st to the 4th spun lacing pressure are as follows: 19kg, 15kg, 29kg, 18kg;Being dried temperature is 60 DEG C, and the drying process time is 10s;
S5. plant essence liquid is extracted, the Essence is made of the active component extract of following parts by weight of component: aloe 0.15 part of extract, 0.09 part of mint extract, 0.16 part of Millettia extract, 0.14 part of Salvia root P.E.
By the plant essence liquid of extraction according to plant extraction liquid: ethyl alcohol is the dilution proportion of 1:6 into weak solution, is reused micro- Plant extraction liquid after dilution by high pressure nozzle jet atomization, 18 DEG C of atomization temperature, is atomized by the cream atomization mutual infiltration method of molecule Pressure 0.2MPa, air column jet air pressure 0.7MPa, Jet Stream is carbon dioxide, and the plant extraction liquid after atomization is in upper and lower convection current High pressure draught effect under be evenly distributed on the non-woven fabrics of the fiber containing camellia to get the bacteriostatic skin-care of the fiber containing camellia without Woven fabric.Micro plant essence liquid ensure that with enough care effects, will not cause the waste of plant essence liquid.
The bacteriostatic skin-care non-woven fabrics of the fiber obtained containing camellia is applied to the soft towel of cotton.
The plant essence liquid activity extracted in the present invention is high, intact extraction and saves effective ingredient in plant, Middle aloe essence has the function of sterilization, anti-inflammatory, anti-aging, and Radix Salviae Miltiorrhizae essence can circumcise relieving restlessness, Caulis Spatholobi can with clearing and activating the channels and collaterals, Regulating lipid metabolism, peppermint essence have it is refrigerant, also there is good effect to pruitus, fash and eczema.
Embodiment 6
A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia, the soft towel of bacteriostatic skin-care cotton containing camellia include material composition Camellia fiber and cotton fiber are prepared through following method:
S1. camellia fiber and cotton fiber are pre-processed respectively, the preprocessing process of camellia includes: fiber impurity It picks, shredding, combing, oiling dosage is 0.5% in step shredding;
Cotton fiber pretreatment for by raw cotton by opening picking and carding step processing after at item, break Hou Chengbao;Using Leading portion bleaching, bleaching process reference implementation example 3;
S2. pretreated camellia fiber and cotton fiber are carried out according to raw material proportioning camellia fiber: cotton fiber 1: It is mixed that 19 proportion carries out case;
S3., composite fibre is successively passed through to opening picking, cotton carding, combing process a smart post-tensioning is made and be broken into smart net;
S4. smart net by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and is batched;Wherein spun lacing work Sequence carries out in rotary drum spun-laced machine, is divided into four spun lacing steps, the 1st to the 4th spun lacing pressure are as follows:: 17kg, 19kg, 34kg, 15kg;Being dried temperature is 63 DEG C, and the drying process time is 13s;
S5. plant essence liquid is extracted, the Essence is made of the active component extract of following parts by weight of component: aloe 0.12 part of extract, 0.2 part of mint extract, 0.11 part of Millettia extract, 0.15 part of Salvia root P.E.
By the plant essence liquid of extraction according to plant extraction liquid: glycerol is the dilution proportion of 1:4 into weak solution, is reused micro- Plant extraction liquid after dilution by high pressure nozzle jet atomization, 16 DEG C of atomization temperature, is atomized by the cream atomization mutual infiltration method of molecule Pressure 0.35MPa, air column jet air pressure 0.4MPa, Jet Stream is carbon dioxide, and the plant extraction liquid after atomization is right up and down The bacteriostatic skin-care on the non-woven fabrics of the fiber containing camellia to get the fiber containing camellia is evenly distributed under the high pressure draught effect of stream Non-woven fabrics.
The bacteriostatic skin-care non-woven fabrics of the fiber obtained containing camellia is applied to the soft towel of cotton.
The plant essence liquid activity extracted in the present invention is high, intact extraction and saves effective ingredient in plant, Middle aloe essence has the function of sterilization, anti-inflammatory, anti-aging, and Radix Salviae Miltiorrhizae essence can circumcise relieving restlessness, Caulis Spatholobi can with clearing and activating the channels and collaterals, Regulating lipid metabolism, peppermint essence have it is refrigerant, also there is good effect to pruitus, fash and eczema.Micro plant Object Essence ensure that with enough care effects, will not cause the waste of plant essence liquid.
Comparative example 1
The process conditions of this comparative example are similar to Example 4, the difference is that in step S1 not to camellia fiber into Row pretreatment.
Comparative example 2~3
The process conditions of this comparative example are similar to Example 4, the difference is that camellia fiber and cotton are fine in step S2 The mixed proportion of dimension is as follows:
Camellia fiber/% Cotton fiber/%
4% 96%
12% 88%
Comparative example 4~7
The process conditions of comparative example 4~7 are similar to Example 4, the difference is that spun lacing process is adopted respectively in step S3 With following process conditions:
Comparative example 8
The process conditions of comparative example 8 are similar to Example 4, the difference is that using method of roll coating by plant in step S5 Extracting solution is sprayed at the surface layer of the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia.
According to standard FZ/T64012.1-64012.2-2013 to the embodiment of the present invention 4~6,1~8 the method for comparative example Sample is made and carries out quality testing, testing result is averaged, and the results are shown in Table 1.
Table 1
Microbial indicators detected
Microorganism is carried out to the soft towel of bacteriostatic skin-care cotton for the fiber containing camellia that the preparation method of embodiment 4~6 obtains to refer to Mark detection, microbiological indicator are measured according to standard GB/T/T 15979.It the results are shown in Table 2.
Table 2
The bacteriostatic skin-care non-woven fabrics of the fiber containing camellia prepared by the method for embodiment 4~6 is applied to the soft towel of cotton, observation The above-mentioned soft towel of cotton provides reference to the irritation and allergic reaction of skin to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test Back backbone diamond wool shaves off, and after being kept in contact 1d, continuous 7d with the tender sensitive skin paper of children and rabbit skin and mucosa respectively, sees Examining skin, whether there is or not the stimulate the reactions such as erythema, oedema.
(2) skin allergy experiment is carried out using cavy, is kept in contact 2 times with the soft towel of cotton and guinea pig skin mucous membrane weekly, often Secondary contact 4h or more, continuous 5 weeks, whether there is or not the allergic reactions such as erythema, oedema for observation skin.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48, 72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic Allergic reaction.
Therefore, skin care non-woven fabrics of the invention will not cause irritative response to rabbit intact skin and damage skin, right Guinea pig skin has good cutaneous safety without allergic reaction.
Clinical trial
The skin care non-woven fabrics of embodiment 4 and embodiment 5 is applied to the soft towel of cotton, using the soft towel of commercially available common cotton as control Group selects the age for 2~5 years old children totally 120 people, and age-based layer is randomly divided into 3 groups, every group of 40 people, after 2 weeks, detection The soft towel of cotton provided by the invention counts the stimulation implementations of skin and mucosa to its experimental result.It the results are shown in Table 3.
As the result is shown: thering is 1 children (to account for total number of persons using there is irritative response after the product of control group in control group 2.5%) irritative response, does not occur in embodiment 4 and embodiment 5.As it can be seen that the soft towel of cotton provided by the invention is to skin and mucosa Substantially without any irritation and side effect.
Moisturizing performance test
5 volunteers are chosen in this experiment, and volunteer is in same working environment, relatively by the women that the age is 25~35 Humidity is 20%, in the environment that temperature is 25 DEG C.First using the moisture of skin of moisture of skin tester measurement volunteer's face Value cleans face based on the multifilament blended soft towel of bacteriostatic skin-care cotton and commercially available skin care cloth using prepared by embodiment 4, remembers respectively Record is initial, and 2 hours after cleaning, 4 hours volunteer's skin of face moisture values after cleaning, the results are shown in Table 2:
Table 2
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention Protection scope within.

Claims (10)

1. a kind of soft towel of bacteriostatic skin-care cotton of fiber containing camellia, which is characterized in that the soft towel of skin care cotton containing camellia The raw material for preparing of ontology includes camellia fiber and cotton fiber, and the camellia fiber and cotton fiber are respectively by pretreatment, institute It states cotton fiber and carries out leading portion bleaching after pretreatment;
The preprocessing process of the camellia fiber includes that fiber impurity is picked, shredding, combs step;
The preprocessing process of the cotton fiber include: by raw cotton by opening picking and carding step processing after at item, after breaking at Packet;Or, raw cotton is broken Hou Chengbao at item after the processing of opening picking, cotton carding and combing process;
The leading portion bleaching are as follows: by the wax or grease removal on cotton fiber, carried out after bleaching agent then is added into cotton fiber Ultrasonication.
2. the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia according to claim 1, which is characterized in that the ultrasonication When, it is 1:5 ~ 10, is warming up to 65 ~ 80 DEG C, utilizes 50 ~ 60min of ultrasonication, ultrasonic frequency in bath raio after bleaching agent is added For 30 ~ 40KHz.
3. the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia according to claim 1, which is characterized in that the bleaching agent is dense The hydrogenperoxide steam generator that degree is 30%.
4. the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia according to claim 1, which is characterized in that the camellia fiber Mixed proportion with cotton quality proportion is 1:19 ~ 2:18.
5. according to claim 1 to the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia described in 4 any one, which is characterized in that described The soft towel of bacteriostatic skin-care cotton further include coated on the soft towel of bacteriostatic skin-care cotton ontology Essence.
6. the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia according to claim 5, which is characterized in that the painting of the Essence The method covered is to be atomized the mutual infiltration method of molecule using micro emulsion;It is preferred that the atomization temperature 16 of the micro emulsion atomization mutual infiltration method of molecule ~ 18 DEG C, 0.2 ~ 0.35MPa of atomizing pressure, 0.4 ~ 0.7MPa of air column jet air pressure.
7. the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia according to claim 5 or 6, which is characterized in that the Essence It is made of the active component extract of following parts by weight of component: 0.01 ~ 0.3 part of aloe extract, mint extract 0.01 ~ 0.3 Part, 0.01 ~ 0.2 part of Millettia extract, 0.01 ~ 0.2 part of Salvia root P.E.
8. according to claim 1 to the soft towel of bacteriostatic skin-care cotton of the fiber containing camellia described in 7 any one, which is characterized in that through such as Lower step is prepared:
S1. camellia fiber and cotton fiber are pre-processed respectively, carries out leading portion bleaching after cotton fiber pretreatment;
S2. it will be mixed with treated camellia fiber and cotton fiber;
S3., composite fibre is successively passed through to opening picking, cotton carding, combing process a smart post-tensioning is made and be broken into smart net;Using leading portion Bleaching;
S4. smart net by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and is batched;
S5. extract plant essence liquid, the Essence is made of the active component extract of following parts by weight of component: aloe is extracted 0.01 ~ 0.3 part of object, 0.01 ~ 0.3 part of mint extract, 0.01 ~ 0.2 part of Millettia extract, Salvia root P.E 0.01 ~ 0.2 Part;
By plant extraction liquid through the suppression using the mutual infiltration method processing soft towel of cotton of micro emulsion atomization molecule to get the fiber containing camellia The soft towel of bacterium skin care cotton.
9. the soft towel of bacteriostatic skin-care cotton of the fiber according to claim 8 containing camellia, which is characterized in that preparation method step In S4, the spun lacing step includes 4 spun lacing steps;In step S4, the drying process temperature is 60 ~ 65 DEG C, is dried Time is 10 ~ 15s.
10. the soft towel of bacteriostatic skin-care cotton of the fiber according to claim 8 containing camellia, which is characterized in that preparation method step In rapid S5, the plant extraction liquid is by 4 ~ 8 times of organic solvent dilutings of addition, then passes through high pressure nozzle jet atomization, after atomization Plant extraction liquid upper and lower convection current high pressure draught effect under be evenly distributed on the fiber containing camellia the soft towel of cotton on.
CN201811528686.6A 2018-12-13 2018-12-13 A kind of soft towel of bacteriostatic skin-care cotton of the fiber containing camellia and its preparation method and application Pending CN109363996A (en)

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