CN109602633A - The skincare material and its preparation method and application of soybean fiber mixture viscose rayon - Google Patents
The skincare material and its preparation method and application of soybean fiber mixture viscose rayon Download PDFInfo
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- CN109602633A CN109602633A CN201811528687.0A CN201811528687A CN109602633A CN 109602633 A CN109602633 A CN 109602633A CN 201811528687 A CN201811528687 A CN 201811528687A CN 109602633 A CN109602633 A CN 109602633A
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- viscose rayon
- soybean fiber
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- fiber
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/425—Cellulose series
- D04H1/4258—Regenerated cellulose series
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic System
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The invention discloses the skincare materials and its preparation method and application of soybean fiber mixture viscose rayon.The present invention uses raw material of the soybean fiber as skincare material, it is mutually mixed with viscose rayon, with the feel as cashmere, the gloss as silk, excellent lead wet steam permeability and viscose rayon there is essential, the good smooth nice and cool, gas permeability of cotton to be organically combined together soybean fiber, the pollution of fungi and bacterium to non-woven fabrics can be prevented in production process.The present invention passes through the combination of two kinds of fibers, and the uniform high-efficiency infiltration for being aided with plant essence liquid is attached, so that skincare material not only has effects that Essence, but also maintenance soybean fiber and viscose rayon nature, soft, pro-skin nature of relaxing, the antibiotic skin-care function of product is further improved.
Description
Technical field
The present invention relates to skincare material technical fields, more particularly, to the skin care material of soybean fiber mixture viscose rayon
Material and its preparation method and application.
Background technique
Skincare material, must be comfortable to people while containing shin moisturizer as the product with human skin intimate contact
Sense.Existing non-woven fabrics is generally formed by cotton, fiber crops, textile of chemical fibre, and water imbibition, feel, the glossiness of cotton are good, but it is ventilative
Property is poor, intolerant to mould.The gas permeability of flaxen fiber is strong, but its feel is not good enough.Although chemical fibre can be obtained by modification in all respects
To the preferable fiber of mechanical property, but its water suction is not strong, and easily causes allergy to human body in the application of skin-protection product.Even if
Ventilative, the resistance to bacterium for improving cotton fiber, the feel etc. of flaxen fiber are mixed by multiple fiber, but the textile technology of each fiber is not
Together, blended complex process, end breakage rate are high, and sticking together easily occurred in finished product, filoplume and other issues.Silk is a kind of excellent nothing
Woven fabric raw material, but it is expensive, high production cost.
Soybean fiber is that it is manufactured novel after synthesizing to extract phytogloibulin to slough the soybean meal of grease and make raw material
Aftergrowth azelon.Soybean fiber is that protein and high polymer are extracted from soybean for raw material, contour using bioengineering
New technology processing, forms through wet spinning.This monofilament, fineness is thin, light specific gravity, tensile strength are high, acid-fast alkali-proof is strong, moisture absorption
Wet guilding is good.Soybean fiber is better than the feel of cashmere, and gloss can compare favourably with silk, the warmth retention property of cotton and good skin-friendly etc.
Excellent performance is known as " the healthy comfortable environment-protection fiber of new century " and " the good fabric that skin is liked ".And soybean fiber is rich
Containing amino acid, nourishing effect can be played to skin.
The correlative study report that soybean fiber mixture viscose rayon is prepared to skincare material is had no at present.
Summary of the invention
The present invention is directed to existing skincare material pro-skin, the problem of skin care performance deficiency, and it is viscous to provide a kind of soybean fiber mixture
The skincare material of glue fiber.
Another goal of the invention of the present invention is to provide the preparation method of the skincare material.
The present invention, which it is yet another object of, provides the application of the skincare material.
The purpose of the present invention is achieved by the following technical programs:
A kind of skincare material of soybean fiber mixture viscose rayon is provided, the skincare material is prepared in raw material, soybean
The mass ratio of fiber and viscose rayon is 30~80:20~70.
It is blended that the present invention uses soybean fiber, viscose rayon to carry out with scientific and reasonable ratio, and it is good that exquisiteness, pliability is made
Skincare material.
It is further preferred that the mass ratio of the soybean fiber and viscose rayon is 40~60:40~60.
Preferably, the soybean fiber is handled through aqueous slkali soaking；The viscose rayon is koplon.
Preferably, the soda ash solution concentration is 1~2g/L, and the temperature of the immersion treatment is 80~85 DEG C, immersion
Time is 40~50min.
Preferably, the length of the viscose rayon is 20~40mm, Gan Qiangwei 3.0~5.0cN/dtex, it is wet it is strong for 2.0~
3.5cN/dtex。
It is further preferred that the viscose rayon, the length is 25~30mm, Gan Qiangwei 4.0~5.0cN/dtex is wet strong
For 3.0~3.5cN/dtex.
It is further preferable that the dry of the viscose rayon is 5.0cN/dtex by force, wet be 3.5cN/dtex by force.
Present invention simultaneously provides the preparation methods of the skincare material of the soybean fiber mixture viscose rayon, including walk as follows
It is rapid:
S1. soybean fiber is pre-processed: by soybean fiber aqueous slkali soaking；
S2. viscose rayon is pre-processed: viscose rayon is heat-treated in overflow dyeing machine with emulsifier；
S3. by treated, soybean fiber is mixed with viscose rayon；
S5. composite fibre by hydrophilic treated, shredding, combing, lapping, drawing-off, spun lacing, drying and batches to obtain nonwoven
Cloth；
S6. Essence is sprayed on non-woven fabrics by micro emulsion atomization process, it is fine is drying to obtain soybean fiber mixture viscose glue
The skincare material of dimension.
Further, the mass fraction of the emulsifier is 1~2wt.%；Heat treatment temperature is 90~95 DEG C, heat treatment
Time is 30~40min.Preferably, the mass fraction of emulsifier described in step S2 is 1wt.%；Heat treatment temperature is 90 DEG C, heat
The processing time is 40min.
Further, soybean fiber described in step S3 is mixed with viscose rayon is mixed by water jet process, and spun lacing pressure is
12~30kg；Preferably, the soybean fiber and viscose rayon be by four spun lacing steps, and spun lacing pressure is respectively 15~
18kg, 12~15kg, 25~30kg, 15~18kg.
Further, Essence described in step S6 includes plant essence and organic solvent.
Further, the mass ratio of the plant essence and organic solvent is 1:4~6.
Further, the plant essence includes wormwood, honeysuckle, Fructus Forsythiae, seaweed, chrysanthemum, peppermint, Radix Salviae Miltiorrhizae, aloe, rose
Rare flower, lavender or white tea flower Essence it is one or more.
Further, the organic solvent be ethyl alcohol, glycerol, polyethylene glycol, propylene glycol, benzyl alcohol it is one or more.
Further, the temperature of the micro emulsion atomization process is 25~28 DEG C, 0.35~0.45MPa of atomizing pressure, air column
Jet 0.5~0.6MPa of air pressure, drying temperature are 100~110 DEG C；It is further preferred that the temperature of the micro emulsion atomization process
It is 25 DEG C, atomizing pressure 0.4MPa, air column jet air pressure 0.5MPa；Drying temperature is 110 DEG C.
Present invention simultaneously provides application of the skincare material of the soybean fiber mixture viscose rayon in the manufacture soft towel of cotton.
The soybean fiber that the present invention uses is as raw material, preferably using soybean fibrillarin as raw material, using bioengineering etc.
New and high technology processing, through soybean fiber made of wet spinning.Soybean fiber has gloss as silk, soft, with skin
There is fabulous affinity.The hygroscopicity of soybean fiber is suitable with cotton fiber, and leads wet, gas permeability and be much better than cotton fiber.Soybean is fine
Dimension makes it have the unexistent nursing function of other fibers, the ammonia in soybean fiber containing there are many amino acid necessary to human body
After base acid and skin contact, energy activating skin collagen inhibits pruitus, shines skin vitality.Containing soybean fiber
Facial treatment essence liquid is sprayed on non-woven fabrics, combines it with fibre chemistry key, and drug effect is significant and lasting.Soybean fiber also has simultaneously
There are preferable antibiotic property and anti-uv-ray, the drug effect for avoiding functional product is difficult to lasting disadvantage.Science of the invention
Soybean fiber is carried out dipping by lye processing by ground, after the method for the present invention is handled, soybean fiber on the one hand can be enhanced and glue
The cohesive force of glue fiber reduces electrostatic generation and fibres bond, conducive to blended combing；Meanwhile the immersion of weak lye is to soybean
Bacterium and fungi on fiber have certain a sterilizing and fungistatic effect, keep that product is sterile in process of production or low bacterium.It impregnates
The alkalinity of the lye of soybean fiber is too strong, temperature is too high, the processing time too long reduced performance that can make soybean fiber, influences to produce
Product quality；The effect that antibacterial sterilizing is not achieved if alkalinity is too weak, temperature is too low, the processing time is too short, improves product quality.This
It is 1~2g/L that invention, which provides the soda ash solution concentration, and the temperature of the immersion treatment is 80~85 DEG C, and the time of immersion is 40
Under the conditions of~50min, guarantee preferred technical effect.Each index is balanced, the preferred scheme of alkali process is the soda ash
Solution concentration is 2g/L, and soaking temperature is 80 DEG C, soaking time 50min, to obtain optimal technical effect.
Viscose rayon is to extract plastic fiber molecule of laying equal stress on from natural lignose to obtain, and derived from day however is better than day
So, with the essence of cotton, the quality of silk.The bright and clean softness of viscose fiber, feel is smooth, has good hygroscopicity, gas permeability.
The present invention will be absorbed water the excellent soybean fiber and viscose fiber blending of gas permeability by water jet process, obtain a kind of comfortable feel,
Affine skin, moisturizing be ventilative, antibacterial bacteriostatic non-woven fabrics.Viscose rayon carries out emulsification heat treatment, can effectively remove fiber and take
Pectin, the grease of band reduce blended weave difficulty, improve the uniform dispersion of soybean fiber and viscose rayon.Further preferably
Ground, the mass fraction of the emulsifier are 2wt.%；Heat treatment temperature is 95 DEG C, heat treatment time 30min.Soybean fiber
Dry fracture is 3.5~4.5cN/dtex by force, and be broken wet is 2.5~3.0cN/dtex by force.In blending process, viscose rayon is too long
Or too short cotton knot, filoplume, item can be caused to do unevenness and other issues, the intensity difference of soybean fiber and viscose rayon in cotton carding
The problems such as will cause flyings, short flannel, high end breakage rate greatly.For the intensity and quality for keeping non-woven fabrics, it is preferable that the viscose glue is fine
Dimension is koplon, and the length is 25~30mm, 4.0~5.0cN/dtex of Gan Qiangwei, and wet be 3.0~3.5cN/ by force
dtex；It is further preferred that the viscose rayon is high wet modulus subtended angle fiber, Gan Qiangwei 5.0cN/dtex is wet to be by force
3.5cN/dtex。
Water jet process it is entangled to each other together to make fiber, to make fiber on the fine water flow jet to web of high pressure
Net has certain mechanical strength to reinforce.Pass through the breaking strength of soybean fiber and viscose rayon, regain, oil content, fibre
The factors such as degree, length determine that the spun lacing pressure of blended spun lacing is 12~30kg, and spun lacing pressure is bigger, and water needle energy is higher, spun lacing
Non-woven fabrics intensity out is also higher, but excessively high hydraulic pressure can make fibrous fracture and fiber loss, causes under non-woven fabrics intensity
Drop directly makes the fiber in web generate the quality for being displaced two influence non-woven fabrics；The surface of hypotony, web cannot
Consolidation well.
The present invention is reinforced according to the performance and content of soybean fiber and viscose rayon using 4 water jet processes, and using from
Low to high to be distributed in reduced pressure, pressure is respectively as follows: 15~18kg, 12~15kg, 25~30kg, 15~18kg.First
The hypertonia of road spun lacing can reduce non-woven fabrics quality, be lost fibrous fracture, aggravate the burden of water circulation system, cause two,
The snagging of three water jet processes is serious.Two spun lacing pressure are too small, and web is reinforced loosely, loosely organized, soybean fiber
It cannot combine closely with viscose rayon, non-woven fabrics is made to form coarse surface, the uniformity of nonwoven cloth cover is caused to decline, fluffing is tight
Weight, influences the feel of product；Two spun lacing pressure are excessive, make that fiber alignment is mixed and disorderly, the decline of entanglement degree, to make strength ratio in length and breadth
To increasing, fibre damage is caused.Three spun lacing high pressures reinforce web, and soybean fiber and viscose rayon is made to reach good
Mechanical property.The main function of four spun lacings is the modification that positive and negative are carried out to nonwoven cloth cover, is not up to saturated to entanglement degree
Fiber further puncture, so that it is reached saturation as far as possible, this just determines that spun lacing pressure cannot be too low；Meanwhile four spun lacing pair
The surface of non-woven fabrics carries out certain reparation, this just determines that spun lacing pressure cannot be excessively high.It is further preferred that the soybean fiber
With viscose rayon by four spun lacing steps, spun lacing pressure is respectively 17kg, 12kg, 28kg, 17kg.
The skincare material of soybean fiber mixture viscose rayon of the present invention has antibacterial bacteriostatic effect, and isolation was producing
The pollution of bacterium, fungi in journey.Various plant essences are uniformly distributed in combination with utilization " micro emulsion atomization molecule mutually seeps " technique
It on non-woven fabrics, is made that fine and smooth, pliability is good, further increases to have skin and moisten and cleaning action.Plant essence of the present invention
Extracting solution including wormwood, honeysuckle, Fructus Forsythiae, seaweed, chrysanthemum, peppermint, Radix Salviae Miltiorrhizae, aloe, rose, lavender or white tea flower
It is one or more.The plant essence liquid has bactericidal antiphlogistic, prevents infection, moist moisturizing skin and other effects.
Wormwood: folium artemisiae argyi has antibacterial and antivirus action, and has a kind of special fragrance, this special fragrance, which has, to be driven
The effect of mosquito.
Honeysuckle: honeysuckle can be clearing heat and detoxicating, and to various pathogens such as hemolytic streptococcus, Staphylococcus aureus
And infection of the upper respiratory tract Causative virus etc. has stronger restraint.
Fructus Forsythiae: Fructus Forsythiae has antibacterial action, can inhibit typhoid bacillus, paratyphosum Bacterium, Escherichia coli, shigella dysenteriae, diphtheria
Bacillus and comma bacillus, staphylococcus, streptococcus etc..
Peppermint: can pruitus, fash and eczema etc..
Aloe: sterilization, it is anti-inflammatory, moisten beauty.
Compared with prior art, beneficial effect is:
The present invention uses raw material of the soybean fiber as skincare material, mutually mixed with viscose rayon, and soybean fiber is had
The gloss as feel, silk as cashmere, excellent lead wet steam permeability and viscose rayon have the essential, good smooth cool of cotton
Refreshing, gas permeability is organically combined together, and the pollution of fungi and bacterium to non-woven fabrics can be prevented in production process.The present invention is logical
The combination of two kinds of fibers is crossed, soybean fiber and viscose rayon all have outstanding moisture transported permeable, have high parent with skin
And power, the sweat stain of generation and the sense of discomfort of moisture absorption patch skin can be eliminated.
Further, the invention to soybean fiber carries out dipping by lye processing, and dipping by lye processing increases
Add the cohesive force of soybean fiber and viscose rayon, reduces electrostatic of the soybean fiber in fabrication processes and generate, improve the two fiber
Dispersed homogeneous degree, obtain it is a kind of with primary colors, skin care, antibacterial fiber.The present invention using special process to soybean fiber into
Row pretreatment, but not to fiber does not cause to damage, additionally it is possible to so that soybean fiber sufficiently softens, improve the moisturizing of soybean fiber
Property, and the quality of soybean fiber and spinnability are effectively improved, so that soybean fiber has preferably soft skin fitness, are improved
The row yielding and quality of product.
Further, the present invention is blended by water jet process, improves the mechanical strength of non-woven fabrics, avoids addition chemical fiber belt
The sense of discomfort to skin.By water jet process by soybean fiber and viscose fiber blending, in conjunction with " micro emulsion atomization molecule mutually seeps "
Technology, realize uniform high-efficiency infiltration, the absorption of plant essence liquid, the effect of not only having protected Essence, but also maintenance soybean fiber and
Viscose rayon nature, soft, pro-skin nature of relaxing, further improve the antibiotic skin-care function of product.
The skincare material of the soybean fiber mixture viscose rayon cures the disease to Escherichia coli, golden yellow grape candida albicans etc.
Bacterium has an obvious effect, and viscose rayon has certain antibacterial bacteriostatic effect, the two can prevent in process of production fungi and
Pollution of the bacterium to non-woven fabrics.
Further, in preparation process, the uniform high-efficiency infiltration that the present invention is aided with plant essence liquid is attached, so that skincare material
Not only have effects that Essence, but also maintenance soybean fiber and viscose rayon nature, soft, pro-skin nature of relaxing, further improve
The antibiotic skin-care function of product.
Skincare material of the present invention is soft, and skin-friendly is strong, and air permeable humidity retaining is good, and has effects that antibacterial bacteriostatic,
The effect of preventing the bacterium not completely cut off in process of production, fungal infection, not will cause skin-care nutrient liquid, reduces or pollution.Using
The soft towel of cotton made of the skincare material can substantially improve humidity, Yi Zisheng bacterium possessed by current cotton spun lacing class amenities
The problems such as, impart the comfortable pro-skin of amenities, natural antibacterial, it is dry and comfortable ventilative the features such as, be beneficial to the health of user.
Specific embodiment
It is explained further and illustrates below with reference to embodiment, but specific embodiment does not have any type of limit to the present invention
It is fixed.Unless otherwise specified, method and apparatus used in embodiment is ability conventional method and equipment, raw materials used is routine
Marketable material.
Wherein, plant essence liquid extracting method are as follows:
Essence is made of the active component extract of following parts by weight of component: 0.01~0.2 part of wormwood, honeysuckle 0.01
~0.2 part, 0.01~0.2 part of Fructus Forsythiae, 0.01~0.2 part of seaweed, 0.01~0.2 part of chrysanthemum, 0.01~0.3 part of peppermint, Radix Salviae Miltiorrhizae
0.01~0.1 part, 0.01~0.3 part of aloe, 0.01~0.2 part of rose, 0.01~0.2 part of lavender, white tea spend 0.01~
0.2 part；
Firstly, aloe is smashed it through 30 meshes, according to the solid-liquid ratio (g:ml) of 1:18, the second for being 90% with volume fraction
Alcohol ultrasonic extraction 85min, concentrated extracting solution are to get, wherein the frequency of ultrasonic extraction at the medicinal extract of relative density 1.1~1.3
40kHz, power 500W；
Secondly, respectively by wormwood, Fructus Forsythiae, seaweed, Radix Salviae Miltiorrhizae boiling, extracted, the de- slag of filtering obtains corresponding filtrate.By gold and silver
Flower, chrysanthemum, rose and lavender distillation extraction, obtain extracting solution；
Finally, the plant extraction liquid is uniformly mixed, it is added 90% ethyl alcohol, ultrasonic dissolution, until clear solution, i.e.,
, wherein the frequency of ultrasonic dissolution is 40kHz, power 500W.
Although a kind of above-mentioned specific embodiment for being only exemplified by each extract, it will be appreciated by those skilled in the art that
Be be not limited to other extracting methods (method especially in the limited range of the present invention) of ad hoc fashion similarly can be with
It realizes essentially identical extraction effect, can be used for realizing the present invention, this is no longer particularly limited.
Embodiment 1
The present embodiment provides the preprocess methods of soybean fiber.
Soybean fiber is impregnated into 50min at 80 DEG C with the sodium hydroxide solution of 2g/L.
Embodiment 2
The present embodiment provides the preprocess methods of soybean fiber.
Soybean fiber is impregnated into 40min at 85 DEG C with the sodium hydroxide solution of 1g/L.
Embodiment 3
The present embodiment provides the preprocess methods of viscose rayon.
Viscose rayon is pre-processed: being 25~30mm by length, Gan Qiangwei 5.0cN/dtex, wet be 3.5cN/ by force
Dtex viscose rayon is heat-treated in overflow dyeing machine with the emulsifier of 2wt.%, and temperature is 95 DEG C, time 30min.
Embodiment 4
The present embodiment provides the preprocess methods of viscose rayon.
Viscose rayon is pre-processed: being 25~30mm by length, Gan Qiangwei 4.0cN/dtex, wet be 3.0cN/ by force
Dtex viscose rayon is heat-treated in overflow dyeing machine with the emulsifier of 1wt.%, and temperature is 90 DEG C, time 40min.
Embodiment 5
S1. soybean fiber is pre-processed: preprocess method is the same as embodiment 1；
S2. viscose fiber is pre-processed: preprocess method is the same as embodiment 3；
S3. by treated, soybean fiber is mixed with viscose rayon spun lacing；
S4. pass through hydrophilic treated, combing, lapping, spun lacing, drying and batch to obtain non-woven fabrics；
S41. hydrophilic process: the blend fibre prepared in step S3 is handled with hydrogen peroxide and water, treatment temperature
It is 60 DEG C, the processing time is 12 hours, and wherein the mass ratio of hydrogen peroxide, water and fiber is 1:4:5.
S42. shredding, carding step: successively carrying out thick shredding and smart shredding, after various fibers are mixed through more storehouse mixing machines
Afterwards, using sending cotton blower to be sent to double cylinder and double doffer carding machine for composite fibre is uniform and stable, double cylinder and double doffer is used
Fibrous raw material is processed into the thin net being made of single fiber by carding machine, through cross lapping and drawing-off, to manufacture centainly quantitative three
Tie up the fibre web of disordered arrangements.
S43. lapping process: by the way of cross lapping.
S44. drafting process: using roller type drafting machine, will originally in transversely arranged fibre web to longitudinal arrangement, formed compared with
Good vertically and horizontally strength requires, to meet using upper strength requirement, drafting multiple 2.1.
S45. rotary drum spun-laced machine, including 4 water jets spun lacing process: are used；Using 4 water jet processes, spun lacing pressure
Successively are as follows: 17kg, 14kg, 28kg, 17kg.
S46. drying process: controlling dry temperature is 110 DEG C.
It S5. is 25~28 DEG C, 0.35~0.45MPa of atomizing pressure by temperature by Essence, air column jet air pressure 0.5~
The micro emulsion atomization process of 0.6MPa is sprayed on non-woven fabrics, is drying to obtain the skin care non-woven fabrics containing soybean fiber:
Essence is the extracting solution of wormwood, honeysuckle, Fructus Forsythiae, Radix Salviae Miltiorrhizae, aloe, lavender, plant essence and organic solvent
Mass ratio be 1:4；
Using natural fiber spunlace non-woven cloth as carrier, pass through after 8 times of propylene glycol dilutions are added in high-purity prescription Essence
High pressure nozzle jet atomization, the prescription Essence after atomization are evenly distributed on day under the high pressure nitrogen airflow function of upper and lower convection current
On right fiber spun-laced non-woven fabrics, 25 DEG C of atomization temperature, atomizing pressure 0.4MPa, air column jet air pressure 0.5MPa；Natural fiber water
Every square metre of prick nonwoven cloth is evenly distributed high-purity Essence 2.0g；
Embodiment 6
The present embodiment is identical as 5 technique of embodiment, and difference is the pretreatment of S1 soybean fiber: the pre- place of soybean fiber
Reason is the same as embodiment 2.
Embodiment 7
The present embodiment is identical as the technique of embodiment 5, and difference is that step S3 will treated soybean fiber and viscose glue
Fiber spun-laced mixing: spun lacing pressure is 15kg, 12kg, 25kg, 15kg.
Embodiment 8
The present embodiment is identical as the technique of embodiment 5, and difference is that step S3 will treated soybean fiber and viscose glue
Fiber spun-laced mixing: spun lacing pressure is 18kg, 15kg, 30kg, 18kg.
Embodiment 9
The present embodiment is identical as the technique of embodiment 5, and difference is plant essence that step S6 is used for seaweed, chrysanthemum
The mass ratio of the extracting solution that flower, peppermint, rose, lavender, white tea are spent, plant essence and organic solvent is 1:6.
Comparative example 1
The present embodiment is identical as the processing step of embodiment 5, and difference is the soybean fiber of step S1 use without pre-
Processing.
Comparative example 2
The present embodiment is identical as the processing step of embodiment 5, and difference is the viscose rayon of step S2 use without pre-
Processing.
Comparative example 3
The present embodiment is identical as the processing step of embodiment 5, and difference is that the viscose rayon that step S2 is used is common
The viscose rayon of intensity.
Comparative example 4~7
The present embodiment is identical as the processing step of embodiment 5, and difference is that the soybean fiber that step S1 is used uses not
Same pretreatment:
| Concentration of lye (g/L) | Temperature (DEG C) | Time (min) | |
| Comparative example 4 | 0.1 | 80 | 50 |
| Comparative example 5 | 1 | 80 | 50 |
| Comparative example 6 | 0.2 | 100 | 50 |
| Comparative example 7 | 0.2 | 80 | 90 |
Comparative example 8~9
The present embodiment is identical as the processing step of embodiment 5, and difference is soybean fiber and viscose rayon in step S3
Mass ratio are as follows:
| Soybean fiber | Viscose rayon | |
| Comparative example 8 | 10 | 90 |
| Comparative example 9 | 90 | 10 |
Comparative example 10~14
The present embodiment is identical as the processing step of embodiment 5, and difference is the blended pressure of the spun lacing of step S3 are as follows:
Comparative example 15
The present embodiment is identical as the processing step of embodiment 5, and difference is that the present embodiment will plant by the way of coating
Object Essence is sprayed at the surface layer of soybean fiber spunlace non-woven cloth.
Comparative example 16
The present embodiment is identical as the processing step of embodiment 5, and difference is that the present embodiment is not added with plant essence liquid.
According to standard FZ/T64012.1-64012.2-2013 to the embodiment of the present invention 5~8, the side of comparative example 1~11
Legal system obtains sample and carries out quality testing, and testing result is averaged, and the results are shown in Table 1.
Table 1
As the result is shown: the product that 5~9 method of the embodiment of the present invention is prepared is superior to comparative example 1 in performance parameter
~16, wherein 5 effect of embodiment is best.It can be seen that damage of the preparation method of the present invention to fiber from the data of ultimate strength
Small, binding force is big between fiber, and effect is substantially better than comparative example 1~16；In addition, from water absorption rate, pliability, elongation, regain
Etc. data, can embody the embodiment of the present invention 5~9 water absorbing properties, in terms of be superior to comparative example 1~16.
Compared to embodiment, the bonding or end breakage rate of fiber want high in the fabrication processes of comparative example 4~7, and comparative example 10~14 flies
Phenomena such as spending, fluffing, is mixed and disorderly.
Conclusion: the skincare material of soybean fiber mixture viscose rayon produced by the present invention is suitable on thickness, quantitative parameter,
Compared with the existing technology, quantitative irregularity is low, and pliability is low, and ultimate strength is high, and elongation is high, and water absorption rate is high, obtained production
The low damage of product, low-loss, length is uniform, Fiber Straightness is good, soft suitable skin.
Microbial indicators detected
The skin care non-woven fabrics containing soybean fiber that the preparation method of embodiment 5~9 and comparative example 15~16 obtains is carried out
Microbial indicators detected, microbiological indicator are measured according to standard GB/T/T15979, the results are shown in Table 2:
Table 2
Skin irritation test
Skin care non-woven fabrics containing soybean fiber prepared by the method for embodiment 4~8 is applied to the soft towel of cotton, observes above-mentioned cotton
Soft towel provides reference to the irritation and allergic reaction of skin to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and after being kept in contact 1d, continuous 7d with the tender sensitive skin paper of children and rabbit skin and mucosa respectively, sees
Examining skin, whether there is or not the stimulate the reactions such as erythema, oedema.
(2) skin allergy experiment is carried out using cavy, is kept in contact 2 times with the soft towel of cotton and guinea pig skin mucous membrane weekly, often
Secondary contact 4h or more, continuous 5 weeks, whether there is or not the allergic reactions such as erythema, oedema for observation skin.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Therefore, skin care non-woven fabrics of the invention will not cause irritative response to rabbit intact skin and damage skin, right
Guinea pig skin has good cutaneous safety without allergic reaction.
Moisturizing performance test
This experiment randomly selects 5 volunteers, and volunteer is in same working environment by the women that the age is 25~35,
Relative humidity is 20%, in the environment that temperature is 25 DEG C.First using the skin of moisture of skin tester measurement volunteer's face
Moisture value, the skin care non-woven fabrics and commercially available skin care cloth of the fruit fiber containing butter prepared using embodiment 5 are cleaned face, recorded respectively
Initially, 2 hours after cleaning, 4 hours volunteer's skin of face moisture values after cleaning, the results are shown in Table 3:
Table 3
Clinical trial
The skin care non-woven fabrics of embodiment 5 and embodiment 9 is applied to the soft towel of cotton, using the soft towel of commercially available common cotton as control
Group selects the age for 2~5 years old children totally 90 people, and age-based layer is randomly divided into 4 groups, every group of 25 people, after 2 weeks, detection this
Stimulation implementations of the soft towel of cotton to skin and mucosa of offer are provided, and its experimental result is counted, the results are shown in Table 4:
Table 4
As the result is shown: thering are 6 children (to account for total number of persons using there is irritative response after the product of control group in control group
20%) irritative response, does not occur in embodiment 4 and 8.As it can be seen that the soft towel of cotton provided by the invention to skin and mucosa substantially without
Any irritation and side effect.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this
Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention
Protection scope within.
Claims (10)
1. the skincare material of soybean fiber mixture viscose rayon, which is characterized in that the skincare material is prepared in raw material, soybean
The mass ratio of fiber and viscose rayon is 30 ~ 80:20 ~ 70.
2. the skincare material of soybean fiber mixture viscose rayon according to claim 1, which is characterized in that the soybean fiber
Mass ratio with viscose rayon is 40 ~ 60:40 ~ 60.
3. the skincare material of soybean fiber mixture viscose rayon according to claim 1 or claim 2, which is characterized in that the soybean
Fiber is through soda ash solution immersion treatment；The viscose rayon is koplon.
4. the skincare material of soybean fiber mixture viscose rayon according to claim 3, which is characterized in that the soda ash solution
Concentration is 1 ~ 2g/L, and the temperature of the immersion treatment is 80 ~ 85 DEG C, and the time of immersion is 40 ~ 50min；Preferably, the soda ash
Solution concentration is 2g/L, and the temperature of the immersion treatment is 80 DEG C, and the time of immersion is 50min.
5. the skincare material of soybean fiber mixture viscose rayon according to claim 3, which is characterized in that the viscose rayon
Length be 20 ~ 40mm, Gan Qiangwei 3.0 ~ 5.0cN/dtex, wet be 2.0 ~ 3.5cN/dtex by force；Preferably, the viscose glue is fine
Dimension, the length is 25 ~ 30mm, 4.0 ~ 5.0cN/dtex of Gan Qiangwei, and wet be 3.0 ~ 3.5cN/dtex by force；It is further preferred that institute
Stating the dry of viscose rayon is by force 5.0cN/dtex, and wet be 3.5cN/dtex by force.
6. the preparation method of the skincare material of any one of claim 1 to the 5 soybean fiber mixture viscose rayon, feature exist
In, comprising the following steps:
S1. soybean fiber is pre-processed: by soybean fiber aqueous slkali soaking；
S2. viscose rayon is pre-processed: is heat-treated in overflow dyeing machine in viscose rayon with emulsifier；
S3. by treated, soybean fiber is mixed with viscose rayon；
S4. pass through blended net hydrophilic treated, combing, lapping, spun lacing, drying and batch to obtain non-woven fabrics；
S5. Essence is sprayed on non-woven fabrics, the dry skincare material to get soybean fiber mixture viscose rayon.
7. preparation method according to claim 6, which is characterized in that the mass fraction of emulsifier described in step S2 be 1 ~
2wt.%；Heat treatment temperature is 90 ~ 95 DEG C, and heat treatment time is 30 ~ 40min；Preferably, the quality of emulsifier described in step S2
Score is 1wt.%；Heat treatment temperature is 90 DEG C, heat treatment time 40min.
8. the skincare material of soybean fiber mixture viscose rayon according to claim 6, which is characterized in that mixed described in step S4
It spins and uses water jet process, spun lacing pressure is 12 ~ 30kg；Preferably, described blended using four water jet processes, spun lacing pressure difference
For 15 ~ 18kg, 12 ~ 15kg, 25 ~ 30kg, 15 ~ 18kg；It is further preferred that spun lacing pressure is respectively 17kg, 12kg, 28kg,
17kg；
Spraying described in step S5 is using micro emulsion atomization process；It is preferred that the temperature of the micro emulsion atomization process is 25 ~ 28 DEG C, atomization
0.35 ~ 0.0.45MPa of pressure, 0.5 ~ 0.6MPa of air column jet air pressure；Drying temperature is 100 ~ 110 DEG C；It is further preferred that institute
The temperature for stating micro emulsion atomization process is 25 DEG C, atomizing pressure 0.4MPa, air column jet air pressure 0.5MPa；Drying temperature is 110 DEG C.
9. the skincare material of soybean fiber mixture viscose rayon according to claim 6, which is characterized in that the Essence packet
Include plant essence and organic solvent；The plant essence includes wormwood, honeysuckle, Fructus Forsythiae, seaweed, chrysanthemum, peppermint, Radix Salviae Miltiorrhizae, reed
Luxuriant growth, rose, lavender or white tea flower Essence it is one or more；The organic solvent is ethyl alcohol, glycerol, poly- second two
Alcohol, propylene glycol or benzyl alcohol it is one or more.
10. application of any one of claim 1 ~ 9 skincare material in the manufacture soft towel of cotton.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055646A (en) * | 2019-04-25 | 2019-07-26 | 德州恒丰纺织有限公司 | A kind of wormwood scribbled with antibacterial, antiviral functions |
| CN113062045A (en) * | 2021-03-25 | 2021-07-02 | 福建恒安集团有限公司 | Natural color surface layer sanitary towel |
-
2018
- 2018-12-13 CN CN201811528687.0A patent/CN109602633A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055646A (en) * | 2019-04-25 | 2019-07-26 | 德州恒丰纺织有限公司 | A kind of wormwood scribbled with antibacterial, antiviral functions |
| CN113062045A (en) * | 2021-03-25 | 2021-07-02 | 福建恒安集团有限公司 | Natural color surface layer sanitary towel |
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