CN109363973A - A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule - Google Patents
A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule Download PDFInfo
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- CN109363973A CN109363973A CN201811425260.8A CN201811425260A CN109363973A CN 109363973 A CN109363973 A CN 109363973A CN 201811425260 A CN201811425260 A CN 201811425260A CN 109363973 A CN109363973 A CN 109363973A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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Abstract
The present invention provides a kind of shampoo and preparation method thereof containing rose essential-oil microcapsule.The composition and content of the shampoo containing rose essential-oil microcapsule are as follows: surfactant 25-35%, pearling agent 0.5-1.2%, pH adjusting agent 0.3-0.8%, preservative 0.03-3%, Chinese medicine 0.04-1%, pigment 0.01%, rose essential-oil microcapsule 1-1.5%, deionized water add to 100%.The present invention embed by Rosa Damascana and then application is added in shampoo, and the hair quality for allowing Rosa Damascana to have rose scent in the product is experienced, refrigerant comfortable, while and having antibacterial effect.
Description
Technical field
The invention belongs to daily chemicals fields, are related to a kind of shampoo, specifically one kind contains rose essential-oil microcapsule
Traditional-Chinese-medicine-type shampoo and preparation method thereof.
Background technique
Essential oil belongs to volatile oil, and some ingredients will volatilize in room temperature or lower than room temperature under conditions of, and stability is poor, stays
The fragrant time is short, influences the quality of product, is limited by very large its application.Essential oil is wrapped using microencapsulation technology
Processing is buried, is research hotspot in recent years.By microencapsulation, due to the sealing function of cyst wall, volatilization is suppressed essential oil, fragrant
Gas retains completely, to extend essential oil storage time and improve the stability used.Therefore, it is necessary to carry out the micro- glue of Rosa Damascana
The research of encapsulated embedding process, be desirably to obtain embedding effect it is good, the high microcapsule product of stability.In recent years, with washing nurse
Industry development is very fast, especially Traditional-Chinese-medicine-type shampoo very by the welcome of consumer, with people quality of life is required it is universal
The reinforcement with health perception is improved, special biological agent, such as plants essential oil and essential oil microcapsules are added in shampoo,
There is refrigerant and antibacterial, product foaming abundancy is fine and smooth, and detergency is moderate, is easy to rinse, to the equal nothing such as hair and eyes
Stimulation, plays good comfortable effect.
Summary of the invention
The object of the present invention is to provide a kind of shampoo and preparation method thereof containing rose essential-oil microcapsule.
In order to achieve the above object, the present invention provides a kind of shampoo containing rose essential-oil microcapsule, features
It is, is calculated by mass percentage, composition and content is as follows:
The preparation method of the rose essential-oil microcapsule includes:
Step 1): being dissolved in water for beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution；The material ratio of the beta-cyclodextrin and water is
1g:6mL-10mL, solution temperature are 70 DEG C -80 DEG C；
Step 2): Rosa Damascana is dissolved in organic solvent, obtains Rosa Damascana solution；The organic solvent is anhydrous second
The volume ratio of alcohol, the Rosa Damascana and dehydrated alcohol is 1:15-25；
Step 3): resulting Rosa Damascana solution is added in beta-cyclodextrin aqueous solution, is contained in beta-cyclodextrin aqueous solution
The mass ratio of the Rosa Damascana contained in some beta-cyclodextrins and Rosa Damascana solution is 4-7:1, is heating, is being protected from light and sealing strip
It is embedded under part, embedding temperature is 45 DEG C -55 DEG C；The embedding time is 1.5h-2.5h；
Step 4): placing reaction liquid into refrigerator refrigerate after the reaction was completed, and refrigerated storage temperature is 0 DEG C -5 DEG C, and cold preservation time is
22h-26h；Dry after vacuum filtration, drying temperature is 45 DEG C -55 DEG C, obtains rose essential-oil microcapsule.
Preferably, the surfactant is by cationic surfactant JR-400 aqueous solution (hydroxyethyl cellulose season
Amine salt), anionic surfactant AES (poly alkyl alcohol ether sodium sulfate), (the coconut oil glycol acyl of nonionic surfactant 6501
Amine) and amine-oxides composition, the quality hundred of the JR-400 aqueous solution, AES, 6501 and amine-oxides in the shampoo
Divide than being respectively 9-10%, 2-15%, 0.5-6% and 0.1-4%.
It is highly preferred that mass percent of the JR-400 contained in the JR-400 aqueous solution in the shampoo
For 0.1-1%.
Preferably, the pearling agent is ethylene glycol monostearate.
Preferably, the pH adjusting agent is citric acid.It is highly preferred that the Citric Acid Dosage is 0.5%.
Preferably, the preservative is made of extremely beauty-II, methylparaben and propylben, the extremely beauty-
II, the mass percent of methylparaben and propylben in shampoo is respectively 0.01-1%, 0.02-1% and 0-
1%.
Preferably, the Chinese medicine is menthol, and menthol has the function of refrigerant antipruritic.
Preferably, the shampoo containing rose essential-oil microcapsule, is calculated by mass percentage, and forms and contains
It measures as follows:
Preferably, the shampoo containing rose essential-oil microcapsule, is calculated by mass percentage, and forms and contains
It measures as follows:
The present invention also provides the preparation method of the above-mentioned shampoo containing rose essential-oil microcapsule, feature exists
In including the following steps:
Step 1): first putting into deionized water into reaction kettle, and stirring is warming up to 55-65 DEG C；
Step 2): preservative and pearling agent stirring and dissolving are added into the reaction kettle, while it is water-soluble to prepare JR-400
Liquid；
Step 3): AES, 6501, amine-oxides and JR-400 aqueous solution stirring and dissolving are sequentially added into the reaction kettle；
Step 4): Chinese medicine menthol is added into the reaction kettle, pH adjusting agent citric acid tune is added after stirring and dissolving
The pH value for saving solution is 5.5-6；
Step 5): being down to room temperature for reaction kettle, flavoring rose essence microcapsules is added before discharging, pigment stirs evenly to get washing
Hair-care shampoo.
The present invention also provides a kind of preparation methods of rose essential-oil microcapsule characterized by comprising
Step 1): being dissolved in water for beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution；The material ratio of the beta-cyclodextrin and water is
1g:6mL-10mL, solution temperature are 70 DEG C -80 DEG C；
Step 2): Rosa Damascana is dissolved in organic solvent, obtains Rosa Damascana solution；The organic solvent is anhydrous second
The volume ratio of alcohol, the Rosa Damascana and dehydrated alcohol is 1:15-25；
Step 3): resulting Rosa Damascana solution is added in beta-cyclodextrin aqueous solution, is contained in beta-cyclodextrin aqueous solution
The mass ratio of the Rosa Damascana contained in some beta-cyclodextrins and Rosa Damascana solution is 4-7:1, is heating, is being protected from light and sealing strip
It is embedded under part, embedding temperature is 45 DEG C -55 DEG C；The embedding time is 1.5h-2.5h；
Step 4): placing reaction liquid into refrigerator refrigerate after the reaction was completed, and refrigerated storage temperature is 0 DEG C -5 DEG C, and cold preservation time is
22h-26h；Dry after vacuum filtration, drying temperature is 45 DEG C -55 DEG C, obtains rose essential-oil microcapsule.
The present invention provides a kind of preparation methods containing rose essential-oil microcapsule shampoo, including prepare beta-cyclodextrin
Aqueous solution: being dissolved in water for beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution；Then Rosa Damascana solution is prepared: Rosa Damascana is molten
In organic solvent, Rosa Damascana solution is obtained；Rose essential-oil microcapsule is prepared again: resulting Rosa Damascana solution is added into institute
In the beta-cyclodextrin aqueous solution obtained, is heating, is being protected from light and embedded under air-proof condition, placing reaction liquid into ice after the reaction was completed
It is refrigerated in case, dries after vacuum filtration to constant weight, obtain rose essential-oil microcapsule；It is fragrant that embedded microcapsules are applied to hair washing
In wave formula.
Compared with prior art, the beneficial effects of the present invention are:
1, Rosa Damascana embed and then is applied by the shampoo prepared by the present invention containing rose essential-oil microcapsule
It is added in shampoo, solves essential oil volatilization, the short technical problem of fragrance remaining time allows essential oil to play its lasting in the product
Permanent characteristic, product brings refrigerant comfortable hair quality experience, while playing the role of antibacterial.
2, the preparation method of rose essential-oil microcapsule of the invention has embedding effect good, stability height and good economy performance etc.
Advantage.
3, the theory of the present invention and health green are mutually agreed with, while more refrigerant comfortable, exuberant the fragrance of rose, pleasure
Body and mind.
4, the whole particle size uniformity of flavoring rose essence microcapsules prepared by the present invention is high, mechanical strength is good, and stability is strong.
Detailed description of the invention
Fig. 1 is the experimental result of embodiment 6.
Fig. 2 is different drying time essence mass change relational graphs.
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
Rosa Damascana in following embodiment is purchased from Gansu bitter water rose Industries, Ltd.
Embodiment 1
A kind of preparation method of rose essential-oil microcapsule, specific steps are as follows:
Step 1): being dissolved in 80mL deionized water for 10.00g beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution, in 80 DEG C of water-baths
Middle stirring, makes it dissolve, and obtains beta-cyclodextrin aqueous solution, and it is spare to be cooled to 50 DEG C of heat preservations；
Step 2): 2g Rosa Damascana is dissolved in organic solvent, obtains Rosa Damascana solution；The organic solvent is anhydrous
The volume ratio of ethyl alcohol, the Rosa Damascana and dehydrated alcohol is 1:20；
Step 3): resulting Rosa Damascana solution at the uniform velocity and is added dropwise in beta-cyclodextrin aqueous solution, side edged stirs
It mixes, the mass ratio of the beta-cyclodextrin contained in beta-cyclodextrin aqueous solution and the Rosa Damascana contained in Rosa Damascana solution is 5:1,
Reaction solution is taken out after being protected from light the sealing embedding 2h time under 50 DEG C of bath temperatures；
Step 4): after reaction solution is cooled to room temperature, placing reaction liquid into refrigerator refrigerate after the reaction was completed, and refrigerated storage temperature is
4 DEG C, cold preservation time is for 24 hours；It is dried in 50 DEG C of drying boxes to constant weight after vacuum filtration, obtaining white solid particle is rose
Essential oil microcapsules, using Rosa Damascana as core material, using beta-cyclodextrin as wall material.
The measurement of microcapsule embedded rate:
Really weigh the rose essential-oil microcapsule W of the present embodiment1It is placed in the small beaker of dry weighing, adds 20ml70-80 DEG C
Hot water, after stirring to dissolve, be added 30ml petroleum ether concussion extraction, repetition be extracted twice, filter sample after sample is dried
It does to constant weight W2, embedding rate is calculated according to following equation:
Wherein, the Rosa Damascana content being embedded in microcapsules is equal to W1-W2。
The measurement of microcapsule embedded yield:
In formula:
M1-Rosa Damascana quality, g；
M2-beta-cyclodextrin quality, g；
Gained rose essential-oil microcapsule quality, g after m3-drying.
M1 is 2g, m2 10.00g in the present embodiment, and through calculating, the embedding rate of the present embodiment is 89.3%, embeds yield
It is 95.1%.
Embodiment 2 (sustained release, stability experiment)
The rose essential-oil microcapsule, the test of slow release effect, the specific number of time and lasting mass change under exposure air
According to as shown in Figure 2.The experimental result can prove that the whole particle size uniformity of flavoring rose essence microcapsules is high, mechanical strength is good, surely
It is qualitative strong.
Embodiment 3-5
A kind of shampoo containing rose essential-oil microcapsule, is calculated by mass percentage, and composition and content are as follows:
1 rose scent shampoo formula table of table
The above-mentioned shampoo containing rose essential-oil microcapsule the preparation method comprises the following steps:
1) amount for weighing good each ingredient, is added deionized water in a kettle first, and stirring is warming up to 60 DEG C；
2) preservative, pearling agent stirring and dissolving are added into the deionized water of the reaction kettle in step 1), while preparing JR-
400 aqueous solutions (0.1%JR-400 and 9.9% water)；
3) AES, 6501, amine-oxides and JR-400 aqueous solution stirring and dissolving are sequentially added to the reaction kettle of step 2)；
4) it is eventually adding menthol into the reaction kettle of step 3), the pH value of citric acid regulating solution is added after stirring and dissolving
For 5.5-6；
5) reaction kettle is down to room temperature, flavoring rose essence microcapsules is added before discharging, pigment stirs evenly to get hair washing perfume
Wave.
The effect of final sustained release flavoring rose essence may refer to the experimental result of example 2.
Embodiment 6
The antibacterial test method of the shampoo containing rose essential-oil microcapsule, includes the following steps:
1) by LB culture medium, (LB meat soup is purchased from exploration platform, product number are as follows: 011008072) is down to 60 after melting first
DEG C, pour into plate natural coagulation.
2) 1mL E. coli clones are diluted into 10 times of (total plate counts about 107-108), it is inhaled respectively with 1 milliliter of Sterile pipette
It takes 1 milliliter of bacterium solution on plate, is uniformly coated on bacterium solution on culture medium respectively with sterile spreading rod.
3) filter paper for being coated with rose essential-oil microcapsule shampoo is affixed on above-mentioned plate with aseptic nipper, is watched
With the presence or absence of inhibition zone, as shown in Figure 1, can be seen that there are inhibition zone by the figure, it was demonstrated that go out the hair washing of flavoring rose essence microcapsules
Shampoo has bacteriostasis really.
For those skilled in the art, with above-mentioned technical process and material and thinking, appropriate adjustment is made
And deformation, these adjustment and deformation belong in scope of protection of the claims of the invention.Protection scope of the present invention is with institute
It has the right subject to requirement.
In conclusion the preparation method and rose essential-oil microcapsule shampoo of a kind of rose essential-oil microcapsule of the invention
Preparation method, can effectively embed Rosa Damascana, make essential oil volatility reduction, prepare rose essential-oil microcapsule shampoo,
It is good to assign fragrant effect, the complete fine and smooth and fragrance remaining time of fragrance is long, it is refrigerant comfortable to make the hair quality of people, and play antibacterial effect.
Above said content is only the basic explanation under present inventive concept, and is appointed made by technical solution according to the present invention
What equivalent transformation, is within the scope of protection of the invention.
Claims (10)
1. a kind of shampoo containing rose essential-oil microcapsule, which is characterized in that be calculated by mass percentage, form and contain
It measures as follows:
The preparation method of the rose essential-oil microcapsule includes:
Step 1): being dissolved in water for beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution；The material ratio of the beta-cyclodextrin and water is 1g:
6mL-10mL, solution temperature are 70 DEG C -80 DEG C；
Step 2): Rosa Damascana is dissolved in organic solvent, obtains Rosa Damascana solution；The organic solvent is dehydrated alcohol,
The volume ratio of the Rosa Damascana and dehydrated alcohol is 1:15-25；
Step 3): resulting Rosa Damascana solution is added in beta-cyclodextrin aqueous solution, is contained in beta-cyclodextrin aqueous solution
The mass ratio of the Rosa Damascana contained in beta-cyclodextrin and Rosa Damascana solution is 4-7:1, heat, be protected from light under air-proof condition
It is embedded, embedding temperature is 45 DEG C -55 DEG C；The embedding time is 1.5h-2.5h；
Step 4): placing reaction liquid into refrigerator refrigerate after the reaction was completed, and refrigerated storage temperature is 0 DEG C -5 DEG C, cold preservation time 22h-
26h；Dry after vacuum filtration, drying temperature is 45 DEG C -55 DEG C, obtains rose essential-oil microcapsule.
2. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that the surface-active
Agent is by cationic surfactant JR-400 aqueous solution, anionic surfactant AES, nonionic surfactant 6501 and oxygen
Change ammonium composition, the mass percent difference of the JR-400 aqueous solution, AES, 6501 and amine-oxides in the shampoo
For 9-10%, 2-15%, 0.5-6% and 0.1-4%.
3. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that the pearling agent is
Ethylene glycol monostearate.
4. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that the pH adjusting agent
For citric acid.
5. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that the preservative by
Extremely beauty-II, methylparaben and propylben composition, extremely beauty-II, methylparaben and the propylben are being had one's hair wash
Mass percent in shampoo is respectively 0.01-1%, 0.02-1% and 0-1%.
6. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that the Chinese medicine is thin
Lotus brain.
7. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that described contains rose
The shampoo of essential oil microcapsules, is calculated by mass percentage, and composition and content are as follows:
8. as described in claim 1 containing the shampoo of rose essential-oil microcapsule, which is characterized in that described contains rose
The shampoo of essential oil microcapsules, is calculated by mass percentage, and composition and content are as follows:
9. the preparation method of the shampoo of any of claims 1-8 containing rose essential-oil microcapsule, feature
It is, includes the following steps:
Step 1): first putting into deionized water into reaction kettle, and stirring is warming up to 55-65 DEG C；
Step 2): preservative and pearling agent stirring and dissolving are added into the reaction kettle, while preparing JR-400 aqueous solution；
Step 3): AES, 6501, amine-oxides and JR-400 aqueous solution stirring and dissolving are sequentially added into the reaction kettle；
Step 4): Chinese medicine menthol is added into the reaction kettle, it is molten that the adjusting of pH adjusting agent citric acid is added after stirring and dissolving
The pH value of liquid is 5.5-6；
Step 5): being down to room temperature for reaction kettle, and flavoring rose essence microcapsules, pigment and deionized water is added before discharging and stirs evenly,
Up to shampoo.
10. a kind of preparation method of rose essential-oil microcapsule characterized by comprising
Step 1): being dissolved in water for beta-cyclodextrin, obtains beta-cyclodextrin aqueous solution；The material ratio of the beta-cyclodextrin and water is 1g:
6mL-10mL, solution temperature are 70 DEG C -80 DEG C；
Step 2): Rosa Damascana is dissolved in organic solvent, obtains Rosa Damascana solution；The organic solvent is dehydrated alcohol,
The volume ratio of the Rosa Damascana and dehydrated alcohol is 1:15-25；
Step 3): resulting Rosa Damascana solution is added in beta-cyclodextrin aqueous solution, is contained in beta-cyclodextrin aqueous solution
The mass ratio of the Rosa Damascana contained in beta-cyclodextrin and Rosa Damascana solution is 4-7:1, heat, be protected from light under air-proof condition
It is embedded, embedding temperature is 45 DEG C -55 DEG C；The embedding time is 1.5h-2.5h；
Step 4): placing reaction liquid into refrigerator refrigerate after the reaction was completed, and refrigerated storage temperature is 0 DEG C -5 DEG C, cold preservation time 22h-
26h；Dry after vacuum filtration, drying temperature is 45 DEG C -55 DEG C, obtains rose essential-oil microcapsule.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111281819A (en) * | 2020-04-02 | 2020-06-16 | 上海应用技术大学 | Bacteriostatic hand sanitizer containing fingered citron-rose essential oil microcapsules and preparation method thereof |
| CN111297769A (en) * | 2019-12-09 | 2020-06-19 | 上海应用技术大学 | Shampoo containing citron essential oil microcapsules and preparation method thereof |
| CN113384492A (en) * | 2021-06-04 | 2021-09-14 | 上海应用技术大学 | Cool and refreshing mint-flavored toothpaste essence and preparation method thereof |
| CN113842847A (en) * | 2021-10-09 | 2021-12-28 | 北京林业大学 | Preparation method of rose essential oil microcapsule |
| CN113842848A (en) * | 2021-10-09 | 2021-12-28 | 北京林业大学 | Preparation method of salted rose essential oil microcapsule |
| CN114099386A (en) * | 2021-11-29 | 2022-03-01 | 广州温雅日用化妆品有限公司 | Bacteriostatic and fragrance-releasing foam shampoo |
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| CN111297769A (en) * | 2019-12-09 | 2020-06-19 | 上海应用技术大学 | Shampoo containing citron essential oil microcapsules and preparation method thereof |
| CN111281819A (en) * | 2020-04-02 | 2020-06-16 | 上海应用技术大学 | Bacteriostatic hand sanitizer containing fingered citron-rose essential oil microcapsules and preparation method thereof |
| CN113384492A (en) * | 2021-06-04 | 2021-09-14 | 上海应用技术大学 | Cool and refreshing mint-flavored toothpaste essence and preparation method thereof |
| CN113842847A (en) * | 2021-10-09 | 2021-12-28 | 北京林业大学 | Preparation method of rose essential oil microcapsule |
| CN113842848A (en) * | 2021-10-09 | 2021-12-28 | 北京林业大学 | Preparation method of salted rose essential oil microcapsule |
| CN114099386A (en) * | 2021-11-29 | 2022-03-01 | 广州温雅日用化妆品有限公司 | Bacteriostatic and fragrance-releasing foam shampoo |
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