CN107929100A - A kind of rose essential-oil microcapsule and preparation method thereof - Google Patents
A kind of rose essential-oil microcapsule and preparation method thereof Download PDFInfo
- Publication number
- CN107929100A CN107929100A CN201711211314.6A CN201711211314A CN107929100A CN 107929100 A CN107929100 A CN 107929100A CN 201711211314 A CN201711211314 A CN 201711211314A CN 107929100 A CN107929100 A CN 107929100A
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- Prior art keywords
- rose essential
- oil microcapsule
- oil
- arabic gum
- cyclodextrin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0204—Specific forms not provided for by any of groups A61K8/0208 - A61K8/14
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Medicinal Preparation (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention discloses a kind of rose essential-oil microcapsule and preparation method thereof, using Rosa Damascana as capsule-core, cyst wall is used as using Arabic gum, casein sodium, maltodextrin, beta cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl methyl cellulose mixing, it is mixed above as emulsifying agent using one or both of sucrose ester, stearoyl lactate, glycerol stearate, glycol fatty acid, after mixing emulsifying rose essential-oil microcapsule is obtained through spray drying.The present invention is improved in prior art basis, there is provided it is a kind of it is easy to operate, stability is strong, dissolubility is good, be not easy to be aoxidized, the rose essential-oil microcapsule that the shelf-life is longer and preparation method thereof.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of rose essential-oil microcapsule and preparation method thereof.
Background technology
Rosa Damascana is the rare advanced concentration essence in the world, is the fine work in essential oil, is the advanced rare perfume of manufacture
Not only important but also expensive raw material, be not only used for manufacturing the cosmetics such as beauty, skin care, hair care, be also widely used in medical and food.
Rosa Damascana is Pure natural plant essential oil, is the basic medicinal ingredient of rose.It can stimulate immune with landman
And nervous system, while help to improve the secretion of incretory, remove organ sclerosis, repair cell.Rosa Damascana is rich in dimension
Raw element c, carrotene, vitamin b and vitamin k, vitamin k can promote blood clotting.Rosa Damascana, which can be adjusted in women, to be divided
Secrete, nourish uterus, alleviate dysmenorrhoea, it is uncomfortable to improve frigidity and climacteric, can be with especially with good beautifying skin-protection function
It is interior support outer Kohakuhi, promote melanin decompose, improve dry skin, recovery skin elasticity, allow women possess it is pale, full of bullet
The healthy skin of property, is the volatile oil of suitable female health.
Rosa Damascana is the mixture of the type organics such as polyol, more hydrocarbon, polyenoid, and volatility is very strong, sees light and exposed to sky
In gas, easily aoxidize, thus at present essential oil mostly using the bottle storage of sealing, shelf-life of this storing mode generally compared with
It is short.In addition, Rosa Damascana is fat-soluble liquid, have some limitations in practical applications.
Microcapsules are a kind of miniature vessels with polymeric shell wall or bag thing, its size is generally 5-200 μm and differs, shape
Shape is various, depending on raw material and preparation method.Essential oil can be embedded in microcapsules by microencapsulation, effectively prevent essential oil to be subject to
The stimulation of extraneous air, moisture, daylight, so as to improve the stability of essential oil, reduces volatilization loss, extends storage period, while can
To widen the application field of Rosa Damascana.
The content of the invention
The present invention is improved in prior art basis, there is provided one kind is easy to operate, stability is strong, dissolubility is good,
It is not easy to be aoxidized, the rose essential-oil microcapsule that the shelf-life is longer and preparation method thereof.
The present invention is achieved through the following technical solutions：
Rose essential-oil microcapsule of the present invention is using Rosa Damascana as capsule-core, with Arabic gum, casein sodium, malt
Dextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl methyl cellulose mixing are used as cyst wall.
The capsule-core of microcapsules of the present invention and the mass ratio of cyst wall are 1~5：8~20.
Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, evil spirit in the cyst wall of microcapsules of the present invention
Taro glue, the mass percent of hydroxypropyl methyl cellulose be respectively 1~2%, 3~10%, 5~15%, 10~20%, 5~
20%th, 2~10%, 3~10%, remaining is water.
The preparation method of microcapsules of the present invention comprises the following steps：
(1) by cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxyl
Propyl methocel mixes in proportion, adds water to stir homogeneous, obtains wall material solution；
(2) emulsifying agent that mass percent is 1~5% is added in wall material solution, is uniformly mixed, adds rose
Essential oil, high-pressure homogeneous emulsification, homogenizing temperature are 30~60 DEG C, and homogenization pressure is 20~40Mpa, and homogenizing time is 2~5h；
(3) emulsion after homogeneous is spray-dried, inlet air temperature is 70~100 DEG C, and leaving air temp is 40~50
DEG C, feeding temperature is 40~60 DEG C, obtains rose essential-oil microcapsule.
The micro- emulsifying agent used of the present invention is two in sucrose ester, stearoyl lactate, glycerol stearate, glycol fatty acid
Kind is mixed above.
Embodiment
With specific embodiment, the invention will be further described below, but the invention is not limited in these embodiments.
Embodiment 1
By cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Ylmethyl cellulose adds water to mix by 1%, 10%, 15%, 10%, 5%, 2%, 10% mass percent respectively, and stirring is equal
Matter obtains wall material solution；The emulsifying agent that mass percent is 4% is added in wall material solution, emulsifying agent is sucrose ester, stearoyl
Sodium lactate mixes, and is uniformly mixed, and adds Rosa Damascana, and the mass ratio of Rosa Damascana and cyst wall is 1：12, carry out
High-pressure homogeneous emulsification, homogenizing temperature are 60 DEG C, homogenization pressure 40Mpa, homogenizing time 2h；Emulsion after homogeneous is carried out
Spray drying, inlet air temperature are 100 DEG C, and leaving air temp is 40 DEG C, and feeding temperature is 60 DEG C, obtains rose essential-oil microcapsule.
Embodiment 2
By cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Ylmethyl cellulose adds water to mix by 2%, 3%, 5%, 20%, 20%, 10%, 3% mass percent respectively, stirs homogeneous
Obtain wall material solution；The emulsifying agent that mass percent is 1% is added in wall material solution, emulsifying agent is stearoyl lactate, firmly
Resin acid glycerine, glycol fatty acid mix, and are uniformly mixed, and add the matter of Rosa Damascana, Rosa Damascana and cyst wall
Amount is than being 2：15, high-pressure homogeneous emulsification is carried out, homogenizing temperature is 50 DEG C, homogenization pressure 20Mpa, homogenizing time 5h；Will be equal
Emulsion after matter is spray-dried, and inlet air temperature is 90 DEG C, and leaving air temp is 50 DEG C, and feeding temperature is 60 DEG C, obtains rose
Rare essential oil microcapsules.
Embodiment 3
By cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Ylmethyl cellulose adds water to mix by 1%, 7%, 10%, 16%, 17%, 5%, 8% mass percent respectively, stirs homogeneous
Obtain wall material solution；The emulsifying agent that mass percent is 3% is added in wall material solution, emulsifying agent is sucrose ester, stearic acid is sweet
Oil mixes, and is uniformly mixed, and adds Rosa Damascana, and the mass ratio of Rosa Damascana and cyst wall is 1：8, it is equal into horizontal high voltage
Matter emulsifies, and homogenizing temperature is 40 DEG C, homogenization pressure 30Mpa, homogenizing time 3h；It is dry that emulsion after homogeneous is subjected to spraying
Dry, inlet air temperature is 80 DEG C, and leaving air temp is 50 DEG C, and feeding temperature is 50 DEG C, obtains rose essential-oil microcapsule.
Embodiment 4
By cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Ylmethyl cellulose adds water to mix by 2%, 5%, 12%, 12%, 15%, 5%, 5% mass percent respectively, stirs homogeneous
Obtain wall material solution；The emulsifying agent that mass percent is 5% is added in wall material solution, emulsifying agent is sucrose ester, stearoyl breast
Sour sodium, glycerol stearate, glycol fatty acid mix, and are uniformly mixed, and add Rosa Damascana, Rosa Damascana and capsule
The mass ratio of wall is 4：20, high-pressure homogeneous emulsification is carried out, homogenizing temperature is 30 DEG C, homogenization pressure 20Mpa, and homogenizing time is
5h；Emulsion after homogeneous is spray-dried, inlet air temperature is 100 DEG C, and leaving air temp is 50 DEG C, feeding temperature 60
DEG C, obtain rose essential-oil microcapsule.
Embodiment 5
By cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Ylmethyl cellulose adds water to mix by 1%, 3%, 10%, 15%, 15%, 5%, 8% mass percent respectively, stirs homogeneous
Obtain wall material solution；The emulsifying agent that mass percent is 2% is added in wall material solution, emulsifying agent is sucrose ester, stearoyl breast
Sour sodium, glycerol stearate mix, and are uniformly mixed, and add Rosa Damascana, and the mass ratio of Rosa Damascana and cyst wall is
5：13, high-pressure homogeneous emulsification is carried out, homogenizing temperature is 30 DEG C, homogenization pressure 40Mpa, homogenizing time 4h；After homogeneous
Emulsion is spray-dried, and inlet air temperature is 70 DEG C, and leaving air temp is 40 DEG C, and feeding temperature is 40 DEG C, obtains Rosa Damascana
Microcapsules.
Claims (5)
1. a kind of rose essential-oil microcapsule, it is characterised in that using Rosa Damascana as capsule-core, with Arabic gum, casein sodium, wheat
Bud dextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl methyl cellulose mixing are used as cyst wall.
2. rose essential-oil microcapsule according to claim 1, it is characterised in that the mass ratio of the capsule-core and cyst wall is 1
~5：8~20.
3. rose essential-oil microcapsule according to claim 1, it is characterised in that Arabic gum, casein in the cyst wall
Sour sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, the mass percent of hydroxypropyl methyl cellulose be respectively 1~
2%th, 3~10%, 5~15%, 10~20%, 5~20%, 2~10%, 3~10%, remaining is water.
4. rose essential-oil microcapsule according to claim 1, it is characterised in that its preparation method comprises the following steps：
(1) by cyst material Arabic gum, casein sodium, maltodextrin, beta-cyclodextrin, converted starch, konjac glucomannan, hydroxypropyl
Methylcellulose mixes in proportion, adds water to stir homogeneous, obtains wall material solution；
(2) emulsifying agent that mass percent is 1~5% is added in wall material solution, is uniformly mixed, adds rhodamine toner
Oil, high-pressure homogeneous emulsification, homogenizing temperature are 30~60 DEG C, and homogenization pressure is 20~40Mpa, and homogenizing time is 2~5h；
(3) emulsion after homogeneous being spray-dried, inlet air temperature is 70~100 DEG C, and leaving air temp is 40~50 DEG C, into
Material temperature degree is 40~60 DEG C, obtains rose essential-oil microcapsule.
5. step according to claim 4, it is characterised in that the emulsifying agent is sucrose ester, stearoyl lactate, tristearin
Two or more mixing in acid glycerol, glycol fatty acid.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711211314.6A CN107929100A (en) | 2017-11-28 | 2017-11-28 | A kind of rose essential-oil microcapsule and preparation method thereof |
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| CN201711211314.6A CN107929100A (en) | 2017-11-28 | 2017-11-28 | A kind of rose essential-oil microcapsule and preparation method thereof |
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| CN107929100A true CN107929100A (en) | 2018-04-20 |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108740350A (en) * | 2018-05-04 | 2018-11-06 | 尹富贵 | A kind of composite feed additive and its application |
| CN109363973A (en) * | 2018-11-27 | 2019-02-22 | 上海应用技术大学 | A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule |
| CN110419596A (en) * | 2019-08-21 | 2019-11-08 | 天津国际生物医药联合研究院 | A kind of preparation method and application of spine date seed oil microcapsules and oral solid formulation |
| CN110680166A (en) * | 2019-11-01 | 2020-01-14 | 广西壮族自治区林业科学研究院 | Fireproof Buddha incense and processing technology thereof |
| CN110720815A (en) * | 2019-11-01 | 2020-01-24 | 广西壮族自治区林业科学研究院 | Low-dust Buddha incense and processing technology thereof |
| CN110754905A (en) * | 2019-11-01 | 2020-02-07 | 广西壮族自治区林业科学研究院 | Refreshing and health-preserving Buddha incense and processing technology thereof |
| CN110819039A (en) * | 2019-11-27 | 2020-02-21 | 上海新泊地化工技术服务有限公司 | TPE (thermoplastic elastomer) elastomer material special for anti-skid foot pad of bathroom and preparation method thereof |
| CN110859482A (en) * | 2019-11-01 | 2020-03-06 | 广西壮族自治区林业科学研究院 | Anti-scald Buddha incense and processing technology thereof |
| CN111592304A (en) * | 2020-05-23 | 2020-08-28 | 陕西宏基混凝土构件有限责任公司 | C70 self-compacting concrete and preparation method thereof |
| CN111715157A (en) * | 2020-06-15 | 2020-09-29 | 上海应用技术大学 | Temperature-controlled release rose essence-starch-based microcapsule and preparation method thereof |
| CN113576144A (en) * | 2021-08-03 | 2021-11-02 | 上海慧姿化妆品有限公司 | Composition for nail sticker and preparation method thereof |
| CN114570301A (en) * | 2022-03-11 | 2022-06-03 | 东莞市农业科学研究中心 | Camphor tree essential oil microcapsule and preparation method thereof |
| CN115522392A (en) * | 2022-06-16 | 2022-12-27 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
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| CN107156372A (en) * | 2017-04-24 | 2017-09-15 | 南昌大学 | A kind of rose hip oil inulin beauty treatment weight reducing milk tea |
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| CN101125133A (en) * | 2007-09-27 | 2008-02-20 | 武汉麦可得生物技术有限公司 | Unsaturated fatty acid microcapsule preparing technology and application |
| CN103861537A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Preparation method of essential oil microcapsule |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108740350A (en) * | 2018-05-04 | 2018-11-06 | 尹富贵 | A kind of composite feed additive and its application |
| CN109363973A (en) * | 2018-11-27 | 2019-02-22 | 上海应用技术大学 | A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule |
| CN110419596A (en) * | 2019-08-21 | 2019-11-08 | 天津国际生物医药联合研究院 | A kind of preparation method and application of spine date seed oil microcapsules and oral solid formulation |
| CN110859482A (en) * | 2019-11-01 | 2020-03-06 | 广西壮族自治区林业科学研究院 | Anti-scald Buddha incense and processing technology thereof |
| CN110680166A (en) * | 2019-11-01 | 2020-01-14 | 广西壮族自治区林业科学研究院 | Fireproof Buddha incense and processing technology thereof |
| CN110720815A (en) * | 2019-11-01 | 2020-01-24 | 广西壮族自治区林业科学研究院 | Low-dust Buddha incense and processing technology thereof |
| CN110754905A (en) * | 2019-11-01 | 2020-02-07 | 广西壮族自治区林业科学研究院 | Refreshing and health-preserving Buddha incense and processing technology thereof |
| CN110819039A (en) * | 2019-11-27 | 2020-02-21 | 上海新泊地化工技术服务有限公司 | TPE (thermoplastic elastomer) elastomer material special for anti-skid foot pad of bathroom and preparation method thereof |
| CN110819039B (en) * | 2019-11-27 | 2021-08-24 | 上海新泊地化工技术服务有限公司 | TPE (thermoplastic elastomer) elastomer material special for anti-skid foot pad of bathroom and preparation method thereof |
| CN111592304A (en) * | 2020-05-23 | 2020-08-28 | 陕西宏基混凝土构件有限责任公司 | C70 self-compacting concrete and preparation method thereof |
| CN111715157A (en) * | 2020-06-15 | 2020-09-29 | 上海应用技术大学 | Temperature-controlled release rose essence-starch-based microcapsule and preparation method thereof |
| CN113576144A (en) * | 2021-08-03 | 2021-11-02 | 上海慧姿化妆品有限公司 | Composition for nail sticker and preparation method thereof |
| CN114570301A (en) * | 2022-03-11 | 2022-06-03 | 东莞市农业科学研究中心 | Camphor tree essential oil microcapsule and preparation method thereof |
| CN115522392A (en) * | 2022-06-16 | 2022-12-27 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
| CN115522392B (en) * | 2022-06-16 | 2024-03-01 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
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