CN104814895A - Formula of natural hair shampoo and preparation method thereof - Google Patents
Formula of natural hair shampoo and preparation method thereof Download PDFInfo
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- CN104814895A CN104814895A CN201510230080.4A CN201510230080A CN104814895A CN 104814895 A CN104814895 A CN 104814895A CN 201510230080 A CN201510230080 A CN 201510230080A CN 104814895 A CN104814895 A CN 104814895A
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Abstract
The invention relates to a formula of natural hair shampoo and a preparation method thereof, wherein the formula includes 2-8% of tea saponin, 2-5% of camellia oil, 1-3% of grape seed extract, 0.4-0.5% of [beta]-cyclodextrin, 30-40% of sapindus mukorossi extraction liquid, 1-10% of flaxseed gum, 1-5% of wheat protein powder, 0.5-2% of vitamin E, 0.5-4% of essential oil from rose, 10-15% of aloe gel juice and 20-25% of deionized water. The preparation method comprises following steps: (1) preparing a [beta]-cyclodextrin-grape seed extract-camellia oil included substance which is insoluble in cold water; (2) adding the sapindus mukorossi extraction liquid into a reaction kettle with addition of the aloe gel juice, the tea saponin and the vitamin and adding the [beta]-cyclodextrin-grape seed extract-camellia oil included substance being insoluble in cold water; and (3) adding the flaxseed gum, the essential oil from rose and the wheat protein powder, and vacuum-filling the hair shampoo. The natural hair shampoo is excellent in hair washing and protecting, is slight in skin stimulation, is toxic-free and harmless, is free of emission of waste gas and waste water, is mild in property and is easy to biodegrade, is free of drug resistance after long time use and is beneficial to body health and environment protection.
Description
Technical field
The present invention relates to a kind of articles for washing, be specifically related to a kind of formula and preparation technology thereof of natural shampoo.
Background technology
The shampoo product brand circulated in the market is various, and its class also differs comparatively large, some low grade products majorities be all by various petrochemical industry synthesize surfactant and Zinc Pyrithione antibacterial, the compositions such as prescription pearling agent, essence.Surfactant and antibacterial zest and toxicity are comparatively large, and biological degradability is poor, if the shampoo that life-time service Zinc Pyrithione (ZPT) is prepared, can develop immunity to drugs; The surfactant that life-time service is excessive, can, to the excessive defat of scalp, cause harmful substance to remain in scalp, and then cause scalp root of hair to expand, and produces zest pruritus, repiece scurf, thus causes alopecia, alopecia and hair quality damage.Therefore the shampoo of prior art is unfavorable for the healthy of people and environmental conservation.
In recent years, people pursue greenization cosmetic, the psychology of back to nature strengthens day by day, therefore seek with the natural product of no side effects as the cosmetic product of active additive and cosmetic material becomes the large focus of fine chemicals industry one.Such as on 08 06th, 2014, in Chinese invention patent application publication No. CN 103961285A, just disclose Han Yibo " formula of the active shampoo of kind of plant and preparation method thereof ", its formula is: sapindoside 1.0-15.0%, tea saponin 1.0-20.0%, sodium lauroyl glutamate 3.0-20.0%, cocamido propyl betaine 3.0-30.0%, glutamic acid 0.1-2.0%, menthol 0.1-2.0%, glycerol 0.5-5.0%, vitamin E 0.2-2.0%, biotin 0.2-2.0%, Radix Scutellariae glycosides 0.1-1.0%, osthole 0.1-1.0%, magnolol 0.1-2.0%, stearic acid ethylene glycol fat 0.5-2.0%, potassium sorbate 0.2-2.0%, sodium D-isoascorbate 0.1-0.5%, quaternary ammoniated former B 50.3-5.0%, citric acid 0.1-0.5%, oil of Rhizoma Zingiberis Recens 0.1-2.0%, guar hydroxypropyltrimonium ammonium chloride 0.5-5.0%, food stage PAM 0.03-0.5%, NaCl 0.1-3.0%, deionized water surplus.Although this formula uses the nonionic surfactant such as tea saponin, sapindoside; But in order to bubble, nurse one's health, thickening with the addition of a large amount of petrochemical industry synthesis sodium lauroyl glutamate, cocamido propyl betaine; And the biological degradability of these petrochemical industry sinteticses is poor, shampoo discharging of waste liquid will cause ecological deterioration, and this shampoo is still unfavorable for the healthy of people and environmental conservation.
Summary of the invention
The object of the present invention is to provide a kind of formula and preparation technology thereof of natural shampoo, with natural plant active components such as Camellia oil, Semen Vitis viniferae extract and Fructus Sapindi Mukouossi extracting solution for major ingredient, and add tea saponin and Aloe gel juice; Hair-washing hair-care excellent, little to skin irritation, nontoxic, without waste liquid toxic emission, performance gentle and easily biological-degradable, life-time service can not develop immunity to drugs and be beneficial to the healthy of people and environmental conservation.
The technical solution adopted in the present invention is as follows:
A kind of formula of natural shampoo and preparation technology thereof, its formula comprises (percentage by weight) tea saponin 2-8%, Camellia oil 2-5%, Semen Vitis viniferae extract 1-3%, cycloheptaamylose 0.4-0.5%, Fructus Sapindi Mukouossi extracting solution 30-40%, Semen Lini glue 1-10%, wheat protein powder 1-5%, vitamin E 0.5-2%, Flos Rosae Rugosae quintessence oil 0.5-4%, Aloe gel juice 10-15%, deionized water 20-25%;
Preparation technology is:
(1) cycloheptaamylose is added 25-30 DEG C of deionized water for stirring by solid-liquid mass ratio 1:100, prepare cycloheptaamylose saturated solution, by Camellia oil, Semen Vitis viniferae extract adds in cycloheptaamylose saturated solution and stirs, and prepares cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container that cold water is insoluble;
(2) Fructus Sapindi Mukouossi extracting solution is added in stirred tank, with Aloe gel juice adjust pH between 5.4-5.5; Add tea saponin successively, vitamin; Evacuation stirring makes reinforced miscible, is warming up to 65-75 DEG C, then adds the insoluble cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container of cold water, and evacuation stirs 25-30 minute;
(3) be cooled to 25-30 DEG C, then add Semen Lini glue, Flos Rosae Rugosae quintessence oil, evacuation stirs; After adding wheat protein powder adjusting viscosity 6800-7000mPas, vacuum filling.
Wherein, described Fructus Sapindi Mukouossi extracting solution is by Fructus Sapindi Mukouossi water extraction gained; Get the sub-peel 1kg of trouble to clean, add deionized water 3kg, be heated to 70-75 DEG C, extract 5-8 hour; When the pH value of Aqueous extracts is 5.8, filter, filtrate is Fructus Sapindi Mukouossi extracting solution;
Preferably, described Fructus Sapindi Mukouossi extracting solution is by Fructus Sapindi Mukouossi water extraction gained; Get the sub-peel 1kg of trouble to clean, add deionized water 3kg, be heated to 75 DEG C, extract 6 hours; When the pH value of Aqueous extracts is 5.8, filter, filtrate is Fructus Sapindi Mukouossi extracting solution.
Wherein, described Semen Vitis viniferae extract is the Semen Vitis viniferae adopting the leftover bits and pieces of grape wine factory to separate, broken through Semen Vitis viniferae, ethanol merceration, and be separated cooling bath, cooling bath ethyl acetate etc. is further purified, and is separated obtains Semen Vitis viniferae extract with column chromatography.
Wherein, described Aloe gel juice, be with the fresh leaf of Aloe vera L.var. chinensis(Haw.)Berg. or Aloe Barbadensis Miller fresh leaf for raw material, form through cleaning, peeling, stabilisation extraction, membrane filtration, membrance concentration;
Preferably, described Aloe gel juice is with the fresh leaf of Aloe vera L.var. chinensis(Haw.)Berg. for raw material, forms through cleaning, peeling, stabilisation extraction, membrane filtration, membrance concentration.
It is below the mechanism explain of natural shampoo.
Described cycloheptaamylose it can the various compound molecule of envelope, increase by the stability of inclusion complex to photo-thermal, oxygen, change by the physicochemical property of envelope material.Can also prevent natural shampoo brightening agent from damaging hematic acid oxidation browning and improve whitening effect, reduce zest; Some odorous material envelope can also be got up, play the effect of eliminating the unusual smell.Camellia oil-cycloheptaamylose container is prepared in the present invention with Camellia oil compatibility.The interfacial activity that its principle mainly utilizes the alcohol in Camellia oil to have, bioflavonoids has free radical resisting feature, assemble the interface of oil-collecting-water, be beneficial to the bag of cycloheptaamylose in aqueous phase and connect, form cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container that a cold water is insoluble.
The peel of described Fructus Sapindi Mukouossi contains Saponin, and peel is containing triterpene saponin, fruit acid and ferulic acids such as sapindosides, and Fructus Sapindi Mukouossi foaming abundancy, feel is fine and smooth, and strong detergency, can improve skin quality, makes its fine and smooth gloss, high resilience.The effect such as antibacterial, antiinflammatory in addition, oxidation and removing free radicals, anticoagulation simultaneously.Ferulic acid in Fructus Sapindi Mukouossi is the cosmetic factor that scientific circles generally acknowledge, can improve skin quality, make its exquisiteness, gloss, high resilience.The effect such as antibacterial, antiinflammatory in addition, antioxidation, scavenging free radicals, anticoagulation simultaneously.Fruit acid in Fructus Sapindi Mukouossi can help skin removed to be deposited in outer field aging cutin, can anti-dandruff anti-dandruff and itching-relieving efficacies in advance for hair washing, its pH value between 5 ~ 7, in acidity naturally, the interfacial agent of pure natural, body of not hurting sb.'s feelings, the not characteristic of polluted source.Synergism together with cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container in the present invention, plays Action of Surfactant; Can healthy hair be cleaned, improve foam, reduce zest.
Described Aloe gel juice mainly contains aloe-emodin, Aloe anthrone, the compositions such as various saccharides, enzyme, aminoacid.For pistac liquid, relative density is 0.98 ~ 1.02, pH value 4 ~ 6.Play moisturizing, sun-proof, softening skin in the present invention, anti-inflammatory anti-itch effect.
Described Semen Vitis viniferae extract is the new and effective Natural antioxidant material that can not synthesize in a kind of human body of extracting from Semen Vitis viniferae, containing enriching bioflavonoids.It is the antioxidation that current occurring in nature finds, the material that Scavenging ability is the strongest, its antioxidant activity is 50 times, ascorbic 20 times of the plain E of dimension, it can effectively remove free radical unnecessary in human body, has superpower slow down aging and the effect of enhancing immunity.In the present invention with Aloe gel juice, tea saponin, vitamin E compatibility, scalp body odour, hair strengthening, black hair, anticreep, antipruritic and anti-dandruff can be eliminated.
Described wheat protein powder is also known as vital wheat gluten flour, gluten meal, it is the native protein extracted from Semen Tritici aestivi, be made up of several amino acids, protein content is up to 75% ~ 85%, containing 15 seed amino acids that human body is necessary, nutritious plant protein resource. there is viscosity, elasticity, extensibility, film forming and liposuction, wheat protein powder in the present invention with Flos Rosae Rugosae quintessence oil, Semen Lini glue compatibility as conditioner, there is water conservation, educate send out, horny layer softening, lasting makes hair smooth, fragrance, is easy to combing.
Compared with the prior art, the present invention has following beneficial effect:
(1) the present invention is with Camellia oil, the natural plant active components such as Semen Vitis viniferae extract and Fructus Sapindi Mukouossi extracting solution are major ingredient, utilize the interfacial activity that the alcohol in Camellia oil has, the efficient natural anti-oxidation characteristics of Semen Vitis viniferae extract, with the foaming decontamination of Fructus Sapindi Mukouossi extracting solution, antibacterial, antiinflammatory, surface tension is low, wetting power powerful feature synergism together, healthy hair can be cleaned, improve foam, reduce zest, there is broad spectrum antibiotic activity, simultaneously, resistance to strong acid, resistance to highly basic, resistance to hard water, salt-resistance is strong, not containing carcinogen and benzene such as " dioxanes ", the Organic substance that phenol etc. are harmful, safety and environmental protection, free from environmental pollution,
(2) tea saponin is contained in shampoo of the present invention, Semen Lini glue, Aloe gel juice, cycloheptaamylose, wheat protein powder, vitamin E, rhodamine toner wet goods plant component additive, there is hair strengthening, black hair, anticreep, educate send out, invigorate blood circulation, eliminating stagnation, horny layer softening, sterilization, parasite killing, the comprehensive effect such as antipruritic, can effectively anticreep, black hair, bright, educate send out, sterilization, anti-dandruff, antipruritic, little to skin irritation, life-time service can not develop immunity to drugs;
(3) formula of shampoo of the present invention does not use petrochemical industry sintetics, and shampoo is nontoxic, the gentle and easily biological-degradable without waste liquid toxic emission, performance, is beneficial to the healthy of people and environmental conservation.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated, but be not limited thereto.
A kind of formula of natural shampoo and preparation technology thereof, its formula comprises (percentage by weight): tea saponin 6%, Camellia oil 4%, Semen Vitis viniferae extract 2%, β-ring-type 0.5%, Fructus Sapindi Mukouossi extracting solution 36%, Semen Lini glue 8%, wheat protein powder 3%, vitamin E 1.5%, Flos Rosae Rugosae quintessence oil 3%, Aloe gel juice 13%, deionized water 23%;
Preparation technology is:
(1) cycloheptaamylose is added 25 DEG C of deionized water for stirring by solid-liquid mass ratio 1:100, prepare cycloheptaamylose saturated solution, by Camellia oil, Semen Vitis viniferae extract adds in cycloheptaamylose saturated solution and stirs, and prepares cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container that cold water is insoluble;
(2) Fructus Sapindi Mukouossi extracting solution is added in stirred tank, with Aloe gel juice adjust pH 5.4; Add tea saponin successively, vitamin; Evacuation stirring makes reinforced miscible, and be warming up to 70 DEG C, then add the insoluble cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container of cold water, evacuation stirs 30 minutes;
(3) be cooled to 25 DEG C, then add Semen Lini glue, Flos Rosae Rugosae quintessence oil, evacuation stirs; After adding wheat protein powder adjusting viscosity 6800-7000mPas, vacuum filling.
Wherein, described Fructus Sapindi Mukouossi extracting solution is by Fructus Sapindi Mukouossi water extraction gained; Get the sub-peel 1kg of trouble to clean, add deionized water 3kg, be heated to 75 DEG C, extract 6 hours; When the pH value of Aqueous extracts is 5.8, filter, filtrate is Fructus Sapindi Mukouossi extracting solution.
Wherein, described Semen Vitis viniferae extract is the Semen Vitis viniferae adopting the leftover bits and pieces of grape wine factory to separate, broken through Semen Vitis viniferae, ethanol merceration, and be separated cooling bath, cooling bath ethyl acetate etc. is further purified, and is separated obtains Semen Vitis viniferae extract with column chromatography.
Wherein, described Aloe gel juice is with the fresh leaf of Aloe vera L.var. chinensis(Haw.)Berg. for raw material, forms through cleaning, peeling, stabilisation extraction, membrane filtration, membrance concentration.
Result of use is tested: random selecting moderate seborrheic alopecia person 50 people carries out human trial, wherein male 35 people, women 15 people, age distribution in 20-60 year; get natural shampoo of the present invention and smear one to twice in alopecia place every day, 15 days each courses for the treatment of, use continuously 4 courses for the treatment of; each detailed inspection course for the treatment of is with or without whole body and local untoward reaction, and itemized record to 4 terminate a course for the treatment of.Its result shows, and 50 people all without local or systemic adverse reactions, and are obviously alleviated seborrheic alopecia and have 33 people well educating and send out, and can alleviate 16 people of seborrheic alopecia, 1 completely invalid people, its total efficiency 98%.
Claims (6)
1. the formula of a natural shampoo and preparation technology thereof, it is characterized in that: formula material comprises by weight percentage: tea saponin 2-8%, Camellia oil 2-5%, Semen Vitis viniferae extract 1-3%, cycloheptaamylose 0.4-0.5%, Fructus Sapindi Mukouossi extracting solution 30-40%, Semen Lini glue 1-10%, wheat protein powder 1-5%, vitamin E 0.5-2%, Flos Rosae Rugosae quintessence oil 0.5-4%, Aloe gel juice 10-15%, deionized water 20-25%;
Its preparation technology is:
(1) cycloheptaamylose is added 25-30 DEG C of deionized water for stirring by solid-liquid mass ratio 1:100, prepare cycloheptaamylose saturated solution, by Camellia oil, Semen Vitis viniferae extract adds in cycloheptaamylose saturated solution and stirs, and prepares cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container that cold water is insoluble;
(2) Fructus Sapindi Mukouossi extracting solution is added in stirred tank, with Aloe gel juice adjust pH between 5.4-5.5; Add tea saponin successively, vitamin; Evacuation stirring makes reinforced miscible, is warming up to 65-75 DEG C, then adds the insoluble cycloheptaamylose-Semen Vitis viniferae extract-Camellia oil container of cold water, and evacuation stirs 25-30 minute;
(3) be cooled to 25-30 DEG C, then add Semen Lini glue, Flos Rosae Rugosae quintessence oil, evacuation stirs; After adding wheat protein powder adjusting viscosity 6800-7000mPas, vacuum filling.
2. a kind of formula of natural shampoo and preparation technology thereof according to claim 1, is characterized in that: described Fructus Sapindi Mukouossi extracting solution is by Fructus Sapindi Mukouossi water extraction gained; Get the sub-peel 1kg of trouble to clean, add deionized water 3kg, be heated to 70-75 DEG C, extract 5-8 hour; When the pH value of Aqueous extracts is 5.8, filter, filtrate is Fructus Sapindi Mukouossi extracting solution.
3. a kind of formula of natural shampoo and preparation technology thereof according to claim 1, it is characterized in that: described Semen Vitis viniferae extract, it is the Semen Vitis viniferae adopting the leftover bits and pieces of grape wine factory to separate, broken through Semen Vitis viniferae, ethanol merceration, be separated cooling bath, cooling bath ethyl acetate etc. is further purified, and is separated obtains Semen Vitis viniferae extract with column chromatography.
4. a kind of formula of natural shampoo and preparation technology thereof according to claim 1, it is characterized in that: described Aloe gel juice, be with the fresh leaf of Aloe vera L.var. chinensis(Haw.)Berg. or Aloe Barbadensis Miller fresh leaf for raw material, form through cleaning, peeling, stabilisation extraction, membrane filtration, membrance concentration.
5. a kind of formula of natural shampoo and preparation technology thereof according to claim 2, is characterized in that: described Fructus Sapindi Mukouossi extracting solution is by Fructus Sapindi Mukouossi water extraction gained; Get the sub-peel 1kg of trouble to clean, add deionized water 3kg, be heated to 75 DEG C, extract 6 hours; When the pH value of Aqueous extracts is 5.8, filter, filtrate is Fructus Sapindi Mukouossi extracting solution.
6. a kind of formula of natural shampoo and preparation technology thereof according to claim 4, it is characterized in that: described Aloe gel juice, is with the fresh leaf of Aloe vera L.var. chinensis(Haw.)Berg. for raw material, forms through cleaning, peeling, stabilisation extraction, membrane filtration, membrance concentration.
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| CN105326694A (en) * | 2015-11-18 | 2016-02-17 | 华文蔚 | Shampoo containing grape seed extracting solution |
| CN105832626A (en) * | 2016-03-21 | 2016-08-10 | 王跃华 | Preparation method of Chinese soapberry fruit shower gel |
| CN106727060A (en) * | 2017-03-08 | 2017-05-31 | 张仕英 | A kind of technique of the preparation of the shampoo containing tea saponin |
| CN108096173A (en) * | 2017-12-28 | 2018-06-01 | 广州蜜妆生物科技有限公司 | Mild amino acid shampoo of a kind of green and preparation method thereof |
| CN108324619A (en) * | 2018-04-18 | 2018-07-27 | 深圳前海怡人生物工程有限公司 | A kind of whole plant formula shampoo having phalacrosis prevention and hair generation function |
| CN108578311A (en) * | 2018-04-03 | 2018-09-28 | 苏州高新区鼎正精密机电有限公司 | A kind of aloe liquid shampoo and preparation method thereof |
| CN109363973A (en) * | 2018-11-27 | 2019-02-22 | 上海应用技术大学 | A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule |
| CN111407711A (en) * | 2020-04-30 | 2020-07-14 | 广州德谷个人护理用品有限公司 | Plant essential oil aromatic repairing shampoo and preparation method thereof |
| CN113797134A (en) * | 2021-10-15 | 2021-12-17 | 长沙中战茶油集团有限公司 | Preparation method of milky gel and milky gel |
| US11911489B2 (en) * | 2016-05-13 | 2024-02-27 | Sanjeevita By Audubon, Llc | Saponin-containing compositions for use in textile wipes and methods of use and preparation |
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| CN105326694A (en) * | 2015-11-18 | 2016-02-17 | 华文蔚 | Shampoo containing grape seed extracting solution |
| CN105832626A (en) * | 2016-03-21 | 2016-08-10 | 王跃华 | Preparation method of Chinese soapberry fruit shower gel |
| US11911489B2 (en) * | 2016-05-13 | 2024-02-27 | Sanjeevita By Audubon, Llc | Saponin-containing compositions for use in textile wipes and methods of use and preparation |
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| CN108324619A (en) * | 2018-04-18 | 2018-07-27 | 深圳前海怡人生物工程有限公司 | A kind of whole plant formula shampoo having phalacrosis prevention and hair generation function |
| CN109363973A (en) * | 2018-11-27 | 2019-02-22 | 上海应用技术大学 | A kind of shampoo and preparation method thereof containing rose essential-oil microcapsule |
| CN111407711A (en) * | 2020-04-30 | 2020-07-14 | 广州德谷个人护理用品有限公司 | Plant essential oil aromatic repairing shampoo and preparation method thereof |
| CN113797134A (en) * | 2021-10-15 | 2021-12-17 | 长沙中战茶油集团有限公司 | Preparation method of milky gel and milky gel |
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