CN106727060A - A kind of technique of the preparation of the shampoo containing tea saponin - Google Patents
A kind of technique of the preparation of the shampoo containing tea saponin Download PDFInfo
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- CN106727060A CN106727060A CN201710136423.XA CN201710136423A CN106727060A CN 106727060 A CN106727060 A CN 106727060A CN 201710136423 A CN201710136423 A CN 201710136423A CN 106727060 A CN106727060 A CN 106727060A
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- tea saponin
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- cocounut oil
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- stirring
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
Abstract
A kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：（1）To be crushed through the leached tea oil slag of de-oiling, it is configured to after suspension under the conditions of 70~90 DEG C with water, microwave treatment, suspension is cooled to 40~50 DEG C after treatment, regulation pH is 4.5 ~ 6.5, cellulase 1%~3% is added, go out enzyme after 30~40min of microwave radiation technology enzymolysis, and collected after centrifugation supernatant can obtain tea saponin under the conditions of mixed liquor；（2）Each component consumption is calculated according to a certain percentage and is weighed up；（3）In mixing kettle, deionized water is added；Under conditions of stirring, add tea saponin, it is heated to 70~80 DEG C, stir, sequentially add cocounut oil diglycollic amide, cocounut oil CAB, guar gum, stirring is to being completely dissolved, then 45~50 DEG C are cooled to, sequentially add camellia flower extract, Lavender to stir evenly, then be 5.5~6.5 with lemon acid for adjusting pH value, stirring to cool down again obtains final product the shampoo containing tea saponin.
Description
Technical field
The present invention relates to the extraction technology of preparing of tea saponin, more particularly to carrying for tea saponin is extracted using microwave radiation technology enzyme process
Technology of preparing is taken, a kind of use microwave radiation technology enzyme process is further related to and is extracted tea saponin and its application in shampoo.
Background technology
Shampoo is by a kind of everybody widely used hair cleaning products.But making the strong shampoo of decontamination on the market more
Manually synthetic surfactant, easily injures hair quality, and natural shampoo dirt-removing power is not enough.
Tea saponin is the class Triterpenoids sapogenins saponin mixture extracted from leached tea oil slag, with good
Softening, dispersion, the nonionic surfactant of wetting and the function such as decontamination, with hair-washing hair-care dual-use function.Currently in tea
The method that tea saponin is extracted in the seed dregs of rice mainly has water extraction, the water extraction-precipitation method, organic solvent extractionprocess etc., but these methods
Generally existing extraction efficiency is low, the shortcomings of time-consuming, product purity is not high.
The content of the invention
Shortcoming for more than, the invention provides a kind of technique of the preparation of the shampoo containing tea saponin.
A kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：
（1）The extraction of tea saponin
To be crushed through the leached tea oil slag of de-oiling after obtaining the powder that particle diameter is 20~30 mesh, be configured to suspension quality with water and compare 1：
20, under the conditions of 70~90 DEG C, 10~15min of microwave treatment, processing power is 250~300W, and suspension is lowered the temperature after treatment
To 40~50 DEG C, regulation pH is 4.5 ~ 6.5, addition enzyme hydrolysis, microwave radiation technology 30~40min of enzymolysis, microwave power 350~
400W, go out 10~20min of enzyme under 100 DEG C of water bath conditions, and 20~30min is centrifuged under the conditions of 5000~10000r/min, receives
Collection supernatant can obtain tea saponin；
（2）Formula prepares
Cocounut oil diglycollic amide, cocounut oil CAB, guar gum, camellia flower extract, lavender are calculated according to a certain percentage
Essential oil, citric acid, tea saponin, deionized water are simultaneously weighed up；
（3）The preparation of shampoo
In mixing kettle, deionized water is added；Under conditions of stirring, tea saponin is added, be heated to 70~80 DEG C, stirring is equal
It is even, cocounut oil diglycollic amide, cocounut oil CAB, guar gum are sequentially added, stir to being completely dissolved, then cool to 45
~50 DEG C, sequentially add camellia flower extract, Lavender and stir evenly, then be 5.5~6.5 with lemon acid for adjusting pH value, stirring
Uniform cooling again obtains final product.
Further, step（1）Described in enzyme be cellulase；The addition of the enzyme is 1%-3%.
Further, step（1）Described in the frequency that is used of microwave treater be 915 megahertzs or 2450 megahertzs.
Further, step（2）Described in cocounut oil diglycollic amide addition be 3~5%；Cocounut oil CAB is added
Measure is 3~8%；Guar gum addition is 2~5%；Camellia flower extract addition is 1~2%；Lavender addition be 1~
2%；Citric acid adding amount is 0.5~2.5%；Tea saponin addition is 40~50%；Remaining deionized water complements to 100%.
The present invention extracts tea saponin using microwave radiation technology enzyme process, and both having employed microwave moment penetrability mode of heating makes to be carried
Take thing component and produce a large amount of heat energy rapidly in the presence of microwave field, accelerate extract to be spread from solid interior to solid liquid interface
Speed, and the cell membrane of leached tea oil slag is destroyed using cellulase, make its inner material be easier to discharge, and tea soap
Glycosides is not fiber substance, therefore will not be had an impact to its composition, high so as to improve DNA purity；Shampoo of the present invention uses tea
Saponin(e also has hair care effect as main dirt-removing functions composition outside the effect for ensureing anti-dandruff decontamination.Additionally, present invention hair washing
Water adds Lavender and camellia flower extract, with scalp blood circulation is promoted, dispels scalp grease, improves hair follicle and absorbs
Effect.Wash rear hair submissive, non-greasy is easily arranged.
Specific embodiment
Below with reference to specific embodiment a kind of production method of simple and convenient benzalkonium chloride of the present invention is done into
The elaboration of one step, it is more complete, accurate and deep to help those skilled in the art to have inventive concept of the invention, technical scheme
The understanding for entering.
Embodiment one
A kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：
（1）The extraction of tea saponin
The powder that particle diameter is 20 mesh is obtained by being crushed through the leached tea oil slag of de-oiling, being configured to suspension quality with water compares 1：20,70
Under the conditions of DEG C, microwave treatment 10min, processing power is 300W, and suspension is cooled into 40 DEG C after treatment, and regulation pH is 4.5, plus
Enter cellulase 1%, microwave radiation technology digests 40min, microwave power 350W, and go out enzyme 10min under 100 DEG C of water bath conditions,
30min is centrifuged under the conditions of 5000r/min, collecting supernatant can obtain tea saponin.The frequency of microwave treater used is 915,000,000
It is conspicuous or 2450 megahertzs；
（2）Formula prepares
The shampoo formula (by mass percentage) for calculating tea saponin according to a certain percentage is as follows：
Cocounut oil diglycollic amide 3%；
Cocounut oil CAB 3%；
Guar gum 2%；
Camellia flower extract 1%；
Lavender 1%；
Citric acid 0.5%；
Tea saponin 40%；
Deionized water is not enough to 100%；
（3）Shampoo preparation technology
In mixing kettle, deionized water is added.Under conditions of stirring, tea saponin is added, be heated to 70 DEG C, stirred, then
Cocounut oil diglycollic amide, cocounut oil CAB, guar gum are sequentially added, is stirred to being completely dissolved, then cool to 45 DEG C, according to
Secondary addition camellia flower extract, Lavender are stirred evenly, then are 5.5 with lemon acid for adjusting pH value, and stirring to cool down again obtains final product.
Embodiment two
A kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：
（1）The extraction of tea saponin
The powder that particle diameter is 25 mesh is obtained by being crushed through the leached tea oil slag of de-oiling, being configured to suspension quality with water compares 1：20,80
Under the conditions of DEG C, microwave treatment 12.5min, processing power is 275W, and suspension is cooled into 45 DEG C after treatment, and regulation pH is 5.5,
Cellulase 2%, microwave radiation technology is added to digest 35min, microwave power 375W, go out enzyme 15min under 100 DEG C of water bath conditions,
25min is centrifuged under the conditions of 7500r/min, collecting supernatant can obtain tea saponin.The frequency of microwave treater used is 915,000,000
It is conspicuous or 2450 megahertzs；
（2）Formula prepares
The shampoo formula (by mass percentage) for calculating tea saponin according to a certain percentage is as follows：
Cocounut oil diglycollic amide 4%；
Cocounut oil CAB 5.5%；
Guar gum 3.5%；
Camellia flower extract 1.5%；
Lavender 1.5%；
Citric acid 1.5%；
Tea saponin 45%；
Deionized water complements to 100%；
（3）Shampoo preparation technology
In mixing kettle, deionized water is added.Under conditions of stirring, tea saponin is added, be heated to 75 DEG C, stirred, then
Cocounut oil diglycollic amide, cocounut oil CAB, guar gum are sequentially added, are stirred to being completely dissolved, then cool to 47.5 DEG C,
Sequentially add camellia flower extract, Lavender to stir evenly, then be 6 with lemon acid for adjusting pH value, stirring to cool down again obtains final product.
Embodiment three
A kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：
（1）The extraction of tea saponin
The powder that particle diameter is 30 mesh is obtained by being crushed through the leached tea oil slag of de-oiling, being configured to suspension quality with water compares 1：20,90
Under the conditions of DEG C, microwave treatment 15min, processing power is 250W, and suspension is cooled into 50 DEG C after treatment, and regulation pH is 6.5, plus
Enter cellulase 3%, microwave radiation technology digests 30min, microwave power 400W, and go out enzyme 20min under 100 DEG C of water bath conditions,
20min is centrifuged under the conditions of 10000r/min, collecting supernatant can obtain tea saponin.The frequency of microwave treater used is 915
Megahertz or 2450 megahertzs；
（2）Formula prepares
The shampoo formula (by mass percentage) for calculating tea saponin according to a certain percentage is as follows：
Cocounut oil diglycollic amide 5%；
Cocounut oil CAB 8%；
Guar gum 5%；
Camellia flower extract 2%；
Lavender 2%；
Citric acid 2.5%；
Tea saponin 50%；
Deionized water complements to 100%；
（3）Shampoo preparation technology
In mixing kettle, deionized water is added.Under conditions of stirring, tea saponin is added, be heated to 80 DEG C, stirred, then
Cocounut oil diglycollic amide, cocounut oil CAB, guar gum are sequentially added, is stirred to being completely dissolved, then cool to 50 DEG C, according to
Secondary addition camellia flower extract, Lavender are stirred evenly, then are 6.5 with lemon acid for adjusting pH value, and stirring to cool down again obtains final product.
For the ordinary skill in the art, specific embodiment is that the present invention is exemplarily described,
The obvious present invention is implemented and is not subject to the restrictions described above, as long as employ method of the present invention design entering with technical scheme
The improvement of capable various unsubstantialities, or it is not improved by it is of the invention design and technical scheme directly apply to other occasions
, within protection scope of the present invention.
Claims (4)
1. a kind of technique of the preparation of the shampoo containing tea saponin, its feature with comprise the following steps：
（1）The extraction of tea saponin
To be crushed through the leached tea oil slag of de-oiling after obtaining the powder that particle diameter is 20~30 mesh, be configured to suspension quality with water and compare 1：
20, under the conditions of 70~90 DEG C, 10~15min of microwave treatment, processing power is 250~300W, and suspension is lowered the temperature after treatment
To 40~50 DEG C, regulation pH is 4.5 ~ 6.5, addition enzyme hydrolysis, microwave radiation technology 30~40min of enzymolysis, microwave power 350~
400W, go out 10~20min of enzyme under 100 DEG C of water bath conditions, and 20~30min is centrifuged under the conditions of 5000~10000r/min, receives
Collection supernatant can obtain tea saponin；
（2）Formula prepares
Cocounut oil diglycollic amide, cocounut oil CAB, guar gum, camellia flower extract, lavender are calculated according to a certain percentage
Essential oil, citric acid, tea saponin, deionized water are simultaneously weighed up；
（3）The preparation of shampoo
In mixing kettle, deionized water is added；Under conditions of stirring, tea saponin is added, be heated to 70~80 DEG C, stirring is equal
It is even, cocounut oil diglycollic amide, cocounut oil CAB, guar gum are sequentially added, stir to being completely dissolved, then cool to 45
~50 DEG C, sequentially add camellia flower extract, Lavender and stir evenly, then be 5.5~6.5 with lemon acid for adjusting pH value, stirring
Uniform cooling again obtains final product.
2. a kind of technique of the preparation of the shampoo containing tea saponin, it is characterised in that step（1）Described in enzyme be cellulase；
The addition of the enzyme is 1%-3%.
3. a kind of technique of the preparation of the shampoo containing tea saponin, it is characterised in that step（1）Described in microwave treater institute
The frequency for using is 915 megahertzs or 2450 megahertzs.
4. a kind of technique of the preparation of the shampoo containing tea saponin, it is characterised in that step（2）Described in cocounut oil diglycollic amide
Addition is 3~5%；Cocounut oil CAB addition is 3~8%；Guar gum addition is 2~5%；Camellia flower extract adds
It is 1~2% to enter amount；Lavender addition is 1~2%；Citric acid adding amount is 0.5~2.5%；Tea saponin addition is 40
~50%；Remaining deionized water complements to 100%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710136423.XA CN106727060A (en) | 2017-03-08 | 2017-03-08 | A kind of technique of the preparation of the shampoo containing tea saponin |
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| CN201710136423.XA CN106727060A (en) | 2017-03-08 | 2017-03-08 | A kind of technique of the preparation of the shampoo containing tea saponin |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108721177A (en) * | 2018-09-07 | 2018-11-02 | 海南迈嘉热带油茶研究院有限公司 | Camellia amino acid shampoo |
| CN113520959A (en) * | 2020-04-14 | 2021-10-22 | 广州樱奈儿化妆品有限公司 | Anti-dandruff essence lotion and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129310A (en) * | 2007-09-10 | 2008-02-27 | 广东新大地生物科技有限公司 | Anti-dandruff shampoo of common camellia seed |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
| CN103435663A (en) * | 2013-07-26 | 2013-12-11 | 青岛艾华隆生物科技有限公司 | Method used for rapid extraction of tea saponin |
| CN103479539A (en) * | 2013-08-16 | 2014-01-01 | 广州环亚化妆品科技有限公司 | Shampoo containing natural saponin and natural thickener |
| CN104814895A (en) * | 2015-05-08 | 2015-08-05 | 湖南红星盛康油脂股份有限公司 | Formula of natural hair shampoo and preparation method thereof |
-
2017
- 2017-03-08 CN CN201710136423.XA patent/CN106727060A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129310A (en) * | 2007-09-10 | 2008-02-27 | 广东新大地生物科技有限公司 | Anti-dandruff shampoo of common camellia seed |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
| CN103435663A (en) * | 2013-07-26 | 2013-12-11 | 青岛艾华隆生物科技有限公司 | Method used for rapid extraction of tea saponin |
| CN103479539A (en) * | 2013-08-16 | 2014-01-01 | 广州环亚化妆品科技有限公司 | Shampoo containing natural saponin and natural thickener |
| CN104814895A (en) * | 2015-05-08 | 2015-08-05 | 湖南红星盛康油脂股份有限公司 | Formula of natural hair shampoo and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108721177A (en) * | 2018-09-07 | 2018-11-02 | 海南迈嘉热带油茶研究院有限公司 | Camellia amino acid shampoo |
| CN113520959A (en) * | 2020-04-14 | 2021-10-22 | 广州樱奈儿化妆品有限公司 | Anti-dandruff essence lotion and preparation method thereof |
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