CN105925364A - Method for extracting coffee oil from coffee grounds through ultrasonic waves - Google Patents
Method for extracting coffee oil from coffee grounds through ultrasonic waves Download PDFInfo
- Publication number
- CN105925364A CN105925364A CN201610268008.5A CN201610268008A CN105925364A CN 105925364 A CN105925364 A CN 105925364A CN 201610268008 A CN201610268008 A CN 201610268008A CN 105925364 A CN105925364 A CN 105925364A
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- China
- Prior art keywords
- coffee
- organic solvent
- oil
- coffee grounds
- bean oil
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the technical field of plant oil extraction, and especially relates to a method for extracting coffee oil from coffee grounds through ultrasonic waves. The method comprises the following steps: drying the coffee grounds, uniformly mixing the dried coffee grounds with an organic solvent to obtain a mixed stock solution, carrying out ultrasonic treatment on the mixed stock solution to obtain a coffee oil and organic solvent mixed solution, filtering or carrying out suction filtration on the coffee oil and organic solvent mixed solution, and distilling the obtained filtrate to recover the organic solvent and obtain coffee oil. The method has the advantages of simplicity, convenient operation, short extraction time, high extraction rate, low acid value of the extracted coffee oil, good oil quality, no heating, less energy consumption and environmental protection.
Description
Technical field:
The invention belongs to Vegetable oil lipoprotein extractive technique field, particularly relate to one utilize ultrasound wave from
The method extracting coffee bean oil. in coffee grounds.
Background technology:
Coffee is one of big beverage in the world three, in the international market, based on the accumulative trade amount of money,
Coffee is only second to oil and occupy second.In coffee product, instant coffee owing to quoting conveniently,
Meet modern society's rhythm, increasingly welcome by people.According to statistics, the consumption of instant coffee
The 20% of Liang Yizhan world coffee consumption, almost the coffee grounds of 50% is to process instant coffee
During coffee produce, in coffee grounds containing about 20% oils and fats, 10% protein, 58% carbon aquation
Compound and abundant mannan are (after acid hydrolysis, containing 15%-30% in its hydrolyzed solution
D-MANNOSE) and the composition such as galactose, coffee grounds is its warm when for combustion of industrial boiler
Value about 5000 kilocalories/kilogram, this is that other agro-industry garbages are unrivaled, 2008
There is scholar to attempt using coffee grounds to extract coffee bean oil. in year, and use transesterification process mode by coffee
Oil is converted into biodiesel, and this process can produce the biodiesel of 10%-15%, and its yield takes
Certainly in the kind of coffee；Scholar within 2010, is had to use the coffee bean oil. extracted from coffee grounds equally
Doing raw material, use enzyme catalysis transform mode to produce diesel oil, conversion ratio is up to 98.5%, from coffee
It is more stable for obtaining biodiesel in slag, does not changes under the observation more than month.Mesh
The plan of the front biodiesel extracting 3.4 hundred million gallons from coffee grounds has been started up, and extracts oils and fats
After coffee grounds be preferable garden fertilizer, ethanol raw material and burning particles, additionally coffee bean oil. is
A kind of valuable spice oil, can be used as the odorant of food, it may also be used for manufacture through dilution
The perfume etc. of coffee odor type.But, not yet utilize ultrasound wave to extract coffee bean oil. from coffee grounds
Pertinent literature or the open report of technique or use.
Ultrasonic extraction principle ultrasound wave is propagated in medium and medium particle can be made to propagate sky at it
The interior vibrational state that enters, strengthening solutes accumulation, mass transfer, i.e. ultrasound wave mechanism.Ultrasound wave exists
In medium particle communication process, its energy is constantly absorbed by medium particle and becomes heat energy, causes medium
Particle temperature raises, i.e. ultrasound wave calorifics mechanism, simultaneously when substantial amounts of ul-trasonic irradiation is in extraction
Medium, when vibration is in diluted state, medium is torn into many little holes, these apertures
Cave moment closes, and produces the instantaneous pressure of up to several kilo-atmospheric pressures, i.e. cavitation phenomenon during Guan Bi.
Owing to the residing Extraction medium such as the thing that is broken containing substantial amounts of dissolved gas in ultrasonic field
And small impurity, they are enclosed in the colloid periadventitial of the thing etc. that is broken, make for ultrasound wave
With providing essential condition, the enormous pressure produced in air causes the thing cell wall and whole of being broken
Individual organism ruptures, and whole rupture process completed in moment, and what ultrasound wave produced simultaneously shakes
Action release and the dissolving strengthening intracellular organic matter.Ultrasonic disruption process is a physics mistake
Journey, without chemical reaction in leaching process, the bioactive substance being leached keeps at short notice
Constant, biological activity does not subtracts, and improves broken speed simultaneously, shortens the broken time, can pole
Big raising extraction efficiency.And, ultrasound wave is elastic mechanical vibration wave, is beyond audition valve
Sonic vibration, excusing from death wave energy produce and transmit powerful energy, give medium particle with big speed
Degree and acceleration, acceleration increases along with increasing of frequency of sound wave, and ultrasound wave is at Cucumber
In, can be more deeper than what some electromagnetic waves penetrated, the time of staying is the most longer, again due to big energy
Ul-trasonic irradiation in liquid, when vibration is in diluted state, liquid can be torn into perhaps
The least hole, these foveolas the most i.e. close, and produce and be up to several kilo-atmospheric pressures during Guan Bi
Instantaneous pressure, becomes cavitation phenomenon.These cavitation phenomenons can refine various material and manufacture
Emulsion, accelerates the effective ingredient in plant and enters solvent so that it is extract further, to increase
The extraction rate of effective ingredient.In addition to cavitation, many second order effects of ultrasound wave, such as machine
Tool vibrates, emulsifying, diffusion, smashes, and it is effective that chemical effect etc. is the most all conducive to making in plant
Composition shifts, and fully mixes with solvent, promotes the carrying out extracted.
Summary of the invention:
It is an object of the invention to the shortcoming overcoming prior art to exist, seeking design provides one
New technology with ultrasonic extraction coffee bean oil..
In order to realize above-mentioned purpose, the present invention extracts the concrete technology step of coffee bean oil. and is:
(1) put into coffee grounds in calorstat to dry at a temperature of 40-50 DEG C to powdery and done
Coffee grounds after dry；
(2) dried coffee grounds and organic solvent are mixed all according to the weight ratio of 1:2-1:8
Even obtaining mixes stock solution；
(3) mixing stock solution is carried out ultrasonic Treatment and obtain the mixing of coffee bean oil. and organic solvent
Solution, ultrasonic frequency is 30-70KHZ, and ultrasonic treatment time is 5-40 minute, super
Sonicated temperature is 20 DEG C-50 DEG C；
(4) carry out filtering or sucking filtration, by filtrate by the mixed solution of coffee bean oil. and organic solvent
Reclaim organic solvent after distillation, obtain coffee bean oil..
Organic solvent of the present invention includes chloroform, acetone, ether, ethyl acetate, petroleum ether
And ethanol.
Compared with prior art, its technique is simple, and easy to operate, extraction time is short for the present invention,
Extraction ratio is high, and the coffee bean oil. acid value of extraction is low, and oil product is good, it is not necessary to heating, less energy consumption, environment
Friendly.
Detailed description of the invention:
Below by embodiment, the invention will be further described.
Described in the present embodiment, raw material dosage is in parts by weight.
Embodiment 1:
Fresh coffee grounds is put in calorstat and is dried at 40-50 DEG C by the present embodiment, removes
Moisture obtains dried coffee grounds；Weigh 1 part of dried coffee grounds, add 2-4 part
Ethyl acetate obtains mixing stock solution；Mixing stock solution is placed in excusing from death ripple instrument and uses ultrasonic Treatment
Obtaining the mixed liquor after ultrasonic Treatment, treatment temperature, between 45-50 DEG C, processes frequency and exists
Between 45-70KH, the process time is 30-40 minute；By the mixed liquor mistake after ultrasonic Treatment
Filter (sucking filtration), takes filtrate and puts in flask, after reclaiming ethyl acetate, obtains coffee after distillation
Oil, coffee bean oil. extraction ratio is between 15%-16%；Measuring the acid value of coffee bean oil., acid value exists
2-3mgKOH/g。
Embodiment 2:
Fresh coffee grounds is put in calorstat and is dried at 40-50 DEG C by the present embodiment, removes
Moisture obtains dried coffee grounds；Weigh 1 part of dried coffee grounds, add 2-6 part
Ether obtains mixing stock solution；Above-mentioned mixing stock solution is placed in excusing from death ripple instrument and uses at ultrasound wave
Reason, treatment temperature is between 20-25 DEG C, and process frequency, between 30-60KH, processes the time
For 5-20 minute；Mixed liquor after ultrasonic Treatment is filtered (sucking filtration), takes filtrate and put into burning
In Ping, after reclaiming ether, obtaining coffee bean oil. after distillation, coffee bean oil. extraction ratio is at 13%-15%
Between；Measuring the acid value of coffee bean oil., acid value is at 1-3mgKOH/g.
Embodiment 3:
Fresh coffee grounds is put in calorstat and is dried at 40-50 DEG C by the present embodiment, removes
Moisture obtains dried coffee grounds；Weigh 1 part of dried coffee grounds, add 2-5 part
Chloroform obtains mixing stock solution；Mixing stock solution is placed in excusing from death ripple instrument and obtains by ultrasonic Treatment
Mixed liquor after ultrasonic Treatment, treatment temperature, between 30-50 DEG C, processes frequency and exists
Between 45-70KH, the process time is 20-30 minute；By the mixed liquor mistake after ultrasonic Treatment
Filter (sucking filtration), takes filtrate and puts in flask, after reclaiming chloroform, obtains coffee bean oil. after distillation,
Coffee bean oil. extraction ratio is between 15%-19%；Measuring the acid value of coffee bean oil., acid value exists
4-5mgKOH/g。
Embodiment 4:
Fresh coffee grounds is put in calorstat and is dried at 40-50 DEG C by the present embodiment, removes
Moisture obtains dried coffee grounds；Weigh 1 part of dried coffee grounds, add 2-5 part
Ethanol obtains mixing stock solution；Mixing stock solution is placed in excusing from death ripple instrument and obtains by ultrasonic Treatment
Mixed liquor after ultrasonic Treatment, treatment temperature, between 40-50 DEG C, processes frequency and exists
Between 45-70KH, the process time is 30-40 minute；By the mixed liquor mistake after ultrasonic Treatment
Filter (sucking filtration), takes filtrate and puts in flask, after reclaiming ethanol, obtains coffee bean oil. after distillation,
Coffee bean oil. extraction ratio is between 15%-17%；Measuring the acid value of coffee bean oil., acid value exists
3-5mgKOH/g。
Embodiment 5:
Fresh coffee grounds is put in calorstat and is dried at 40-50 DEG C by the present embodiment, removes
Moisture obtains dried coffee grounds；Weigh 1 part of dried coffee grounds, add 2-5 part
Petroleum ether obtains mixing stock solution；Mixing stock solution is placed in excusing from death ripple instrument and obtains by ultrasonic Treatment
Mixed liquor after ultrasonic Treatment, treatment temperature, between 30-50 DEG C, processes frequency and exists
Between 45-70KH, the process time is 30-40 minute；By the mixed liquor mistake after ultrasonic Treatment
Filter (sucking filtration), takes filtrate and puts in flask, after reclaiming petroleum ether, obtains coffee bean oil. after distillation,
Coffee bean oil. extraction ratio is between 13%-16%；Measuring the acid value of coffee bean oil., acid value exists
2-4mgKOH/g。
Claims (2)
1. one kind utilizes the method that ultrasound wave extracts coffee bean oil. from coffee grounds, it is characterised in that
Concrete technology step is:
(1) put into coffee grounds in calorstat to dry at a temperature of 40-50 DEG C to powdery and done
Coffee grounds after dry；
(2) dried coffee grounds and organic solvent are mixed all according to the weight ratio of 1:2-1:8
Even obtaining mixes stock solution；
(3) mixing stock solution is carried out ultrasonic Treatment and obtain the mixing of coffee bean oil. and organic solvent
Solution, ultrasonic frequency is 30-70KHZ, and ultrasonic treatment time is 5-40 minute, super
Sonicated temperature is 20 DEG C-50 DEG C；
(4) carry out filtering or sucking filtration, by filtrate by the mixed solution of coffee bean oil. and organic solvent
Reclaim organic solvent after distillation, obtain coffee bean oil..
Ultrasound wave is utilized to extract the side of coffee bean oil. from coffee grounds the most according to claim 1
Method, it is characterised in that described organic solvent includes chloroform, acetone, ether, ethyl acetate, stone
Oil ether and ethanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610268008.5A CN105925364A (en) | 2016-04-27 | 2016-04-27 | Method for extracting coffee oil from coffee grounds through ultrasonic waves |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610268008.5A CN105925364A (en) | 2016-04-27 | 2016-04-27 | Method for extracting coffee oil from coffee grounds through ultrasonic waves |
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| CN201610268008.5A Pending CN105925364A (en) | 2016-04-27 | 2016-04-27 | Method for extracting coffee oil from coffee grounds through ultrasonic waves |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106987303A (en) * | 2017-04-21 | 2017-07-28 | 蚌埠市九华油脂有限公司 | A kind of method from extracting blackberry seed oil from blackberry slag |
| CN107674758A (en) * | 2017-11-22 | 2018-02-09 | 中国科学院兰州化学物理研究所 | The method for extracting coffee grease from coffee grounds using ultrasonic subcritical fluid extraction technology |
| WO2018234914A1 (en) | 2017-06-21 | 2018-12-27 | Carmenza Jaramillo De Echeverri | Method for producing clarified oil from coffee grounds and from whole and/or damaged beans |
| CN111019759A (en) * | 2019-12-30 | 2020-04-17 | 云南大学 | Method for extracting coffee extract from coffee grounds |
| CN111387327A (en) * | 2020-03-30 | 2020-07-10 | 黑龙江八一农垦大学 | Preparation method of green coffee oil |
| CN111869774A (en) * | 2020-07-03 | 2020-11-03 | 云南肆只猫实业有限公司 | Instant coffee powder and preparation process thereof |
| GB2611578A (en) * | 2021-10-11 | 2023-04-12 | Revive Eco Ltd | Extraction of coffee oil from coffee-based feedstocks by using a green and scalable new process |
| CZ309724B6 (en) * | 2023-01-12 | 2023-08-16 | ALEMAR Real and Trading s.r.o. | Cold extraction of coffee oil and equipment for producing it |
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| CN85107887A (en) * | 1984-01-18 | 1987-05-20 | 通用食品公司 | Finish coffee hydrolysis and oil extraction simultaneously |
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| CN85107887A (en) * | 1984-01-18 | 1987-05-20 | 通用食品公司 | Finish coffee hydrolysis and oil extraction simultaneously |
Non-Patent Citations (2)
| Title |
|---|
| E. PICHAI 等: "OPTIMIZATION OF SOLID-TO-SOLVENT RATIO AND TIME FOR OIL EXTRACTION PROCESS FROM SPENT COFFEE GROUNDS USING RESPONSE SURFACE METHODOLOGY", 《ARPN JOURNAL OF ENGINEERING AND APPLIED SCIENCES》 * |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106987303A (en) * | 2017-04-21 | 2017-07-28 | 蚌埠市九华油脂有限公司 | A kind of method from extracting blackberry seed oil from blackberry slag |
| WO2018234914A1 (en) | 2017-06-21 | 2018-12-27 | Carmenza Jaramillo De Echeverri | Method for producing clarified oil from coffee grounds and from whole and/or damaged beans |
| EP3643770A4 (en) * | 2017-06-21 | 2021-04-14 | Carmenza Jaramillo De Echeverri | Method for producing clarified oil from coffee grounds and from whole and/or damaged beans |
| US11667868B2 (en) | 2017-06-21 | 2023-06-06 | Carmenza Jaramillo de Echeverri | Method for producing clarified oil from coffee grounds and from whole and/or damaged beans |
| CN107674758A (en) * | 2017-11-22 | 2018-02-09 | 中国科学院兰州化学物理研究所 | The method for extracting coffee grease from coffee grounds using ultrasonic subcritical fluid extraction technology |
| CN111019759A (en) * | 2019-12-30 | 2020-04-17 | 云南大学 | Method for extracting coffee extract from coffee grounds |
| CN111387327A (en) * | 2020-03-30 | 2020-07-10 | 黑龙江八一农垦大学 | Preparation method of green coffee oil |
| CN111869774A (en) * | 2020-07-03 | 2020-11-03 | 云南肆只猫实业有限公司 | Instant coffee powder and preparation process thereof |
| GB2611578A (en) * | 2021-10-11 | 2023-04-12 | Revive Eco Ltd | Extraction of coffee oil from coffee-based feedstocks by using a green and scalable new process |
| WO2023062026A1 (en) | 2021-10-11 | 2023-04-20 | Revive Eco Ltd | Extraction of coffee oil from coffee-based feedstocks by using a green and scalable new process |
| GB2611578B (en) * | 2021-10-11 | 2024-01-03 | Revive Eco Ltd | Extraction of coffee oil from coffee-based feedstocks by using a green and scalable new process |
| CZ309724B6 (en) * | 2023-01-12 | 2023-08-16 | ALEMAR Real and Trading s.r.o. | Cold extraction of coffee oil and equipment for producing it |
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