CN104323544A - Mosquito repellent wrist ring and preparation method thereof - Google Patents

Mosquito repellent wrist ring and preparation method thereof Download PDF

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Publication number
CN104323544A
CN104323544A CN201410514680.9A CN201410514680A CN104323544A CN 104323544 A CN104323544 A CN 104323544A CN 201410514680 A CN201410514680 A CN 201410514680A CN 104323544 A CN104323544 A CN 104323544A
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Prior art keywords
mixture
parts
mosquito repelling
preparation
extract liquid
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CN201410514680.9A
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Chinese (zh)
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吴克
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Priority to CN201410514680.9A priority Critical patent/CN104323544A/en
Publication of CN104323544A publication Critical patent/CN104323544A/en
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Abstract

The invention discloses a mosquito repellent wrist ring and preparation method thereof. The mosquito repellent wrist ring includes following raw materials, by weight, 16-40 parts of silica gel, 10-15 parts of natural rubber, 15-20 parts of a lemongrass extract liquid, 5-10 parts of pearl powder, 5-9 parts of shell powder, 1-5 parts of a flame retardant, 1-3 parts of an anti-aging agent RD3 and 10-15 parts of a pomegranate extract liquid. The preparation method comprises following steps: (1) preparing the lemongrass extract liquid and the pomegranate extract liquid and weighing and refrigerating the lemongrass extract liquid and the pomegranate extract liquid for later use; (2) weighing the silica gel and mixing the silica gel with the natural rubber, adding deionized water with stirring and heating to obtain a first mixture; (3) weighing the pearl powder, the shell powder, the flame retardant and the anti-aging agent RD3 and adding the pearl powder, the shell powder, the flame retardant and the anti-aging agent RD3 to the first mixture with homogenization to obtain a second mixture; and (4) after the second mixture being cooled naturally, adding the lemongrass extract liquid and the pomegranate extract liquid, stirring and heating the second mixture again, performing a mechanically defoaming process, pouring the second mixture into a wrist ring mould while the second mixture is still hot, and drying the second mixture and performing a demoulding process to obtain the mosquito repellent wrist ring. The mosquito repellent wrist ring is durable in mosquito repellent effect, has a natural lemon fragrance and is popular.

Description

A kind of mosquito repelling bracelet and preparation method thereof
Technical field
The invention belongs to daily necessities field, be specifically related to a kind of mosquito repelling bracelet and preparation method thereof.
Background technology
Summer be the best opportunity that various insect breeds, particularly mosquito this kind of bloodsucker, fertility fertility strong especially.The skin of children is very tender and lovely, once by bite by mosquitos, just there will be redness, the symptoms such as sufferings at once.Mosquito or the communication media of various pathogens, likely cause the infectious disease that harmfulness is stronger.Therefore, florida water for children is more and more subject to the favor of mothers.But the most alcohol content of the floral water of existing market is higher, have certain danger, some product is even containing potential carcinogenic substance.
Dimethyl phthalate is composition main in mosquito-repellent perfume, 6 kinds of common in the market floral water content situations are as follows: contained by Johnson & Johnson baby mosquito-driving liquid, the ratio of dimethyl phthalate composition is the highest, reach 11.5%, Europe is protected mosquito-driving liquid and is come second with 7%, the content of Long Liqi mosquito-repellent perfume and Australia's snow mosquito-repellent perfume is 5%, the content of six refreshing mosquito-repellent perfumes (Type B formula) is 4.5%, and what content was minimum is the pleasant mosquito-repellent perfume in baby Jinsui River, and dimethyl phthalate content is 4%.
Application number be 201110037755.5 China application discloses that a kind of plastic plant mosquito repelling decoration, although the natural plant essential oils utilized prepares bracelet as additive, preparation method is too simple, and just simple mixing, pours cooling forming in mould into.The nutritional labeling in essential oil can not be protected well, so need the preparation method improving mosquito repelling bracelet, improve repelling effect.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of mosquito repelling bracelet and preparation method thereof, the composition of gained bracelet is simple, and pliability is good, cheap.
For solving prior art problem, the technical scheme that the present invention takes is:
A kind of mosquito repelling bracelet, comprises the following raw material counted by weight: silica gel 16-40 part, natural rubber 10-15 part, lemon-grass extract 15-20 part, pearl powder 5-10 part, oyster shell whiting 5-9 part, fire retardant 1-5 part, anti-aging agent RD 3 1-3 part, pomegranate extract 10-15 part.
As preferably, above-mentioned mosquito repelling bracelet, comprises the following raw material counted by weight: silica gel 16-40 part, natural rubber 10-15 part, lemon-grass extract 15-20 part, pearl powder 5-10 part, oyster shell whiting 5-9 part, fire retardant 1-5 part, anti-aging agent RD 3 1-3 part, pomegranate extract 10-15 part.
As preferably, the order number of described pearl powder and oyster shell whiting is 200-400 order.
As preferably, described fire retardant is be magnesium hydroxide and the Firebrake ZB mixture of 1:1 mixing according to mass ratio.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, take rear refrigeration for subsequent use;
Step 2, after taking silica gel and natural rubber mixing, add the rear weight 1-3 of mixing deionized water doubly, stir and heat 20-30 minute, obtaining the first mixture, heating-up temperature is 60-80 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 10-15 minute at 40-50 DEG C, and homogeneous speed is 8000-9000rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 20-30 minute, be again heated to 40-50 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
As preferably, in step one, refrigerated storage temperature is 2-4 DEG C.
As preferably, heat 30 minutes in step 2, heating-up temperature is 80 DEG C.
As preferably, homogeneous process 15 minutes in step 3, homogeneous speed is 9000rpm.
Lemon-grass is grass family Cymbopogon plants, is common spice crop and flavouring, is adapted at growing in warm, moist environment, and the ground such as Guangdong, Guangxi, Yunnan, Sichuan are originated in the main place of production in China.Nature and flavor are pungent, and temperature, has expelling wind to resolve the exterior, effect of eliminating blood stasis and smoothing collaterals.Can be used for the headache that cures cold, stomachache, traumatic injury, mosquito dispersing etc., the main chemical compositions of its ethereal oil has citral, neral, linalool, menthones, citronellol etc., there is the hay-scented of cyan, micro-have the fragrant and sweet of geraniol, and fragrance is strong and lasting, in the blending of the various commodity of common-use words.
beneficial effect
Mosquito repelling bracelet prepared by the present invention, mosquito component derives from the extract of lemon-grass, safe and reliable, non-stimulated to human body, the citrus scented that lemon-grass is natural, decrease the interpolation of essence, reduce cost, preparation method is divided into multistep to carry out, high temperature rapid solution rubber, low temperature adds lemon-grass extract and pomegranate extract, avoids nutritional labeling to be destroyed, and improves the repelling effect of bracelet.
Detailed description of the invention
The following examples can make the present invention of those skilled in the art comprehend, but do not limit the present invention in any way.
 
Embodiment 1
A kind of mosquito repelling bracelet, comprise the following raw material counted by weight: 16 parts, silica gel, natural rubber 10 parts, lemon-grass extract 15 parts, 200 order pearl powders 5 parts, 200 order oyster shell whitings 5 parts, fire retardant 1 part, anti-aging agent RD 31 parts, pomegranate extract 10 parts, wherein said fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, refrigerate for subsequent use at 2 DEG C after taking;
Step 2, after taking silica gel and natural rubber mixing, add the deionized water of the rear weight 1 times of mixing, stir and heat 20 minutes, obtaining the first mixture, heating-up temperature is 60 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 10 minutes at 40 DEG C, and homogeneous speed is 8000rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 20 minutes, be again heated to 40 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
 
Embodiment 2
A kind of mosquito repelling bracelet, comprise the following raw material counted by weight: 18 parts, silica gel, natural rubber 12 parts, lemon-grass extract 16 parts, 240 order pearl powders 6 parts, 200 order oyster shell whitings 7 parts, fire retardant 2 parts, anti-aging agent RD 32 parts, pomegranate extract 12 parts, wherein said fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, refrigerate for subsequent use at 3 DEG C after taking;
Step 2, after taking silica gel and natural rubber mixing, add the deionized water of the rear weight 1.5 times of mixing, stir and heat 22 minutes, obtaining the first mixture, heating-up temperature is 65 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 12 minutes at 42 DEG C, and homogeneous speed is 8500rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 24 minutes, be again heated to 44 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
 
Embodiment 3
A kind of mosquito repelling bracelet, comprise the following raw material counted by weight: 22 parts, silica gel, natural rubber 13 parts, lemon-grass extract 18 parts, 300 order pearl powders 8 parts, 300 order oyster shell whitings 8 parts, fire retardant 3 parts, anti-aging agent RD 3 2.5 parts, pomegranate extract 13 parts, wherein, described fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, refrigerate for subsequent use at taking latter 4 DEG C;
Step 2, after taking silica gel and natural rubber mixing, add the deionized water of the rear weight 2 times of mixing, stir and heat 25 minutes, obtaining the first mixture, heating-up temperature is 70 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 13 minutes at 45 DEG C, and homogeneous speed is 8800rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 25 minutes, be again heated to 45 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
 
Embodiment 4
A kind of mosquito repelling bracelet, comprise the following raw material counted by weight: 38 parts, silica gel, natural rubber 14 parts, lemon-grass extract 18 parts, 400 order pearl powders 8 parts, 400 order oyster shell whitings 8 parts, fire retardant 4 parts, anti-aging agent RD 33 parts, pomegranate extract 14 parts, wherein, described fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, take rear 3 DEG C of refrigerations for subsequent use;
Step 2, after taking silica gel and natural rubber mixing, add the deionized water of the rear weight 3 times of mixing, stir and heat 30 minutes, obtaining the first mixture, heating-up temperature is 80 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 15 minutes at 50 DEG C, and homogeneous speed is 9000rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 30 minutes, be again heated to 50 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
 
Embodiment 5
A kind of mosquito repelling bracelet, comprise the following raw material counted by weight: 16 parts, silica gel, natural rubber 10 parts, lemon-grass extract 15 parts, 400 order pearl powders 5 parts, 400 order oyster shell whitings 5 parts, fire retardant 1 part, anti-aging agent RD 31 parts, pomegranate extract 10 parts, wherein said fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
As preferably, described fire retardant is be magnesium hydroxide and the Firebrake ZB mixture of 1:1 mixing according to mass ratio.
The preparation method of above-mentioned mosquito repelling bracelet, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, take rear 3 DEG C of refrigerations for subsequent use;
Step 2, after taking silica gel and natural rubber mixing, add the deionized water of the rear weight 3 times of mixing, stir and heat 30 minutes, obtaining the first mixture, heating-up temperature is 80 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 15 minutes at 50 DEG C, and homogeneous speed is 9000rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 30 minutes, be again heated to 50 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
Choose two identical cartons, 50 mosquitoes are all put in the inside, and the mosquito repelling bracelet then the present invention prepared and existing mosquito repelling bracelet are put into, and observe mosquito and flee from situation; Place after 2 days, take bracelet away, observe mosquito regressive case.The data obtained is as shown in table 1.
Table 1 mosquito is fled from and regressive case list
As can be seen from upper table data, mosquito repelling bracelet of the present invention is rapid-action, and mosquito repellent time is long, is better than the repelling effect of existing bracelet.

Claims (8)

1. a mosquito repelling bracelet, is characterized in that, comprises the following raw material counted by weight: silica gel 16-40 part, natural rubber 10-15 part, lemon-grass extract 15-20 part, pearl powder 5-10 part, oyster shell whiting 5-9 part, fire retardant 1-5 part, anti-aging agent RD 3 1-3 part, pomegranate extract 10-15 part.
2. mosquito repelling bracelet according to claim 1, it is characterized in that, comprise the following raw material counted by weight: silica gel 16-40 part, natural rubber 10-15 part, lemon-grass extract 15-20 part, pearl powder 5-10 part, oyster shell whiting 5-9 part, fire retardant 1-5 part, anti-aging agent RD 3 1-3 part, pomegranate extract 10-15 part.
3. mosquito repelling bracelet according to claim 1, is characterized in that: the order number of described pearl powder and oyster shell whiting is 200-400 order.
4. mosquito repelling bracelet according to claim 1, is characterized in that: described fire retardant be according to mass ratio be 1:1 mixing magnesium hydroxide and Firebrake ZB mixture.
5. the preparation method of mosquito repelling bracelet according to claim 1, is characterized in that, comprises the following steps:
Step one, preparation lemon-grass extract and pomegranate extract, take rear refrigeration for subsequent use;
Step 2, after taking silica gel and natural rubber mixing, add the rear weight 1-3 of mixing deionized water doubly, stir and heat 20-30 minute, obtaining the first mixture, heating-up temperature is 60-80 DEG C;
Step 3, takes pearl powder, oyster shell whiting, fire retardant and age resistor, adds in the first mixture, homogeneous process 10-15 minute at 40-50 DEG C, and homogeneous speed is 8000-9000rpm, obtains the second mixture;
Step 4, after the second mixture cools naturally, adds lemon-grass extract and pomegranate extract, and stir after 20-30 minute, be again heated to 40-50 DEG C, after mechanical defoaming, pour into while hot in bracelet mould, demoulding after drying obtains mosquito repelling bracelet.
6. the preparation method of mosquito repelling bracelet according to claim 5, is characterized in that: in step one, refrigerated storage temperature is 2-4 DEG C.
7. the preparation method of mosquito repelling bracelet according to claim 5, is characterized in that: heat 30 minutes in step 2, heating-up temperature is 80 DEG C.
8. the preparation method of mosquito repelling bracelet according to claim 5, is characterized in that: homogeneous process 15 minutes in step 3, homogeneous speed is 9000rpm.
CN201410514680.9A 2014-09-30 2014-09-30 Mosquito repellent wrist ring and preparation method thereof Withdrawn CN104323544A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105054508A (en) * 2015-09-24 2015-11-18 广东小天才科技有限公司 Product with fragrance and processing method of product
CN108601344A (en) * 2016-03-31 2018-09-28 大日本除虫菊株式会社 Flying insect repellent product and flying insect repellent method
CN111937910A (en) * 2020-09-01 2020-11-17 张增香 Mosquito-proof bracelet for baby
CN113017207A (en) * 2021-04-06 2021-06-25 成都彩虹电器(集团)股份有限公司 Electronic sound wave mosquito repellent bracelet and preparation method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3105994U (en) * 2004-06-17 2004-12-09 ファイルド株式会社 Health accessories using silicone elastomer
CN101416809A (en) * 2008-12-02 2009-04-29 陈宝华 A kind of agent structure that is applicable to necklace or bangle or ring
CN202014675U (en) * 2011-03-30 2011-10-26 深圳市和乐联动科技有限公司 Mosquito-dispelling whipping ring
CN102977613A (en) * 2012-12-17 2013-03-20 肇庆皓明有机硅材料有限公司 Method for preparing halogen-free and flame-retardant silicon rubber
CN103319894A (en) * 2012-03-21 2013-09-25 杨红光 Preparation methods for special silicon rubber and papa wristband
CN103494760A (en) * 2013-09-29 2014-01-08 黄珍珍 Moistening and whitening facial mask and preparation method thereof
CN103948527A (en) * 2014-04-30 2014-07-30 卜明珍 Chinese medicinal compound mosquito-repellent floral water

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3105994U (en) * 2004-06-17 2004-12-09 ファイルド株式会社 Health accessories using silicone elastomer
CN101416809A (en) * 2008-12-02 2009-04-29 陈宝华 A kind of agent structure that is applicable to necklace or bangle or ring
CN202014675U (en) * 2011-03-30 2011-10-26 深圳市和乐联动科技有限公司 Mosquito-dispelling whipping ring
CN103319894A (en) * 2012-03-21 2013-09-25 杨红光 Preparation methods for special silicon rubber and papa wristband
CN102977613A (en) * 2012-12-17 2013-03-20 肇庆皓明有机硅材料有限公司 Method for preparing halogen-free and flame-retardant silicon rubber
CN103494760A (en) * 2013-09-29 2014-01-08 黄珍珍 Moistening and whitening facial mask and preparation method thereof
CN103948527A (en) * 2014-04-30 2014-07-30 卜明珍 Chinese medicinal compound mosquito-repellent floral water

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105054508A (en) * 2015-09-24 2015-11-18 广东小天才科技有限公司 Product with fragrance and processing method of product
CN108601344A (en) * 2016-03-31 2018-09-28 大日本除虫菊株式会社 Flying insect repellent product and flying insect repellent method
CN111937910A (en) * 2020-09-01 2020-11-17 张增香 Mosquito-proof bracelet for baby
CN113017207A (en) * 2021-04-06 2021-06-25 成都彩虹电器(集团)股份有限公司 Electronic sound wave mosquito repellent bracelet and preparation method thereof

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Application publication date: 20150204