CN109294762A - A kind of formula and technique of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid - Google Patents

A kind of formula and technique of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid Download PDF

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Publication number
CN109294762A
CN109294762A CN201811178153.XA CN201811178153A CN109294762A CN 109294762 A CN109294762 A CN 109294762A CN 201811178153 A CN201811178153 A CN 201811178153A CN 109294762 A CN109294762 A CN 109294762A
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citrus reticulata
xinhui citrus
fermentation liquid
dish washing
reticulata meat
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温伟成
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Guangdong Milton Hall Health Science Co Ltd
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Guangdong Milton Hall Health Science Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88Ampholytes; Electroneutral compounds
    • C11D1/94Mixtures with anionic, cationic or non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2065Polyhydric alcohols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/33Amino carboxylic acids
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29Sulfates of polyoxyalkylene ethers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88Ampholytes; Electroneutral compounds
    • C11D1/90Betaines

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Abstract

The invention discloses the formulas and technique of a kind of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid.By weight percentage, the formula of dish washing liquid of the present invention is prepared from the following raw materials: Xinhui citrus reticulata meat fermentation liquid 1~5%, glycerol 0.2~1.2%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0~14.5%, neopelex 3.0~6.5%, alkyl glycosides 1.8~5.0%, alkylamide propyl-betaine 2.0~4.8%, sodium chloride 1.2~4.8%, EDTA-2Na 0.09~1.5%, essence 0.1~1%, preservative 0.1~2%, surplus are deionized water.The low stimulation easily biological-degradable of formula and technique of the invention, product are not hurt hands mildly, the dish washing liquid containing Xinhui citrus reticulata meat fermentation liquid, have dispelling abnormal flavor, fungistatic effect good, are not necessarily to pre-treatment, are convenient for industrial production.

Description

A kind of formula and technique of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid
Technical field
The invention belongs to daily cosmetics technical fields, and in particular to a kind of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid is matched Side and technique.
Background technique
Dish washing liquid main component is surfactant, and decontamination principle is very simple, it contains a variety of active ingredients, emulsifier, These ingredients suspend to various greasy spots, harmful substance dissolution, emulsification, dispersion, and subsequent clear water rinsing is separated from tableware surface It goes out, achievees the effect that clean tebleware;Also containing the ingredient of sterilization in certain dish washing liquids, can remove be harmful to the human body it is micro- Biology, prevents that illness finds its way in by the mouth.As the improvement of people's living standards, the quality requirement to dish washing liquid is also higher and higher.With washing The diversified demand trend of clean essence product, with natural Chinese medicinal herb without side-effects, with curative effect and trophism, plant extraction liquid It is more and more popular with consumers with the compounding dish washing liquid of natural no stimulation.
The dried orange peel of Guangdong Province Xinhui District production, is national geography sign protection product, is the dry fruit skin of Xinhui citrus reticulata, is had very High medicinal and economic value and traditional fragrance and flavouring.Xinhui tangerine peel has just had become North-South trade since the Song Dynasty One of " Guangdong products ", more take Nan Yang, Middle and North America to by many overseas Chinese, since it is by prolonged storage, can give out The fragrance that the fragrance assailed one's nostrils, centuries are taken as rare fragrance propagating, trading.Recent studies show dried orange peel have eliminating the phlegm, It relievings asthma, anti-gastric-ulcer, cholagogue, the effect for reducing capillary permeability;Its volatile oil has mild stimulation to skin, gastrointestinal tract Effect;Ethanol extract can reduce blood pressure but on myocardium keto consumption without influence.Since dried orange peel has unique medicinal and edible value, Cultivated area expands year by year in recent years, and processing method is also being constantly brought forth new ideas.There are many product form currently on the market: dried orange peel Tea, dried orange peel beverage, dried orange peel preserved fruit, dried orange peel wine, the general tea of mandarin orange and dried orange peel are the various menus and flavouring of raw material.
However, after mandarin orange pericarp is made dried orange peel by people, mandarin orange and mandarin orange meat majority are thrown away in many degree, cause very big Waste, and in mandarin orange and mandarin orange meat be rich in vitamin C and microelement much beneficial to human body.So if can be sufficiently Mandarin orange or mandarin orange meat are used, develop a cleaning daily necessities with mandarin orange or mandarin orange meat fermentation liquid, it will have wide Application prospect.
Summary of the invention
The purpose of the present invention is to provide a kind of formulas of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid to resist with decontamination Hard water soaks, emulsification, and solubilising disperses, blistering, anti-corrosion and taste of dispelling is antibacterial, moisturizing and other effects.
In addition, the present invention also provides a kind of process of preparing of above-mentioned Xinhui citrus reticulata meat fermentation liquid production dish washing liquid.
The object of the invention to solve the technical problems adopts the following technical solutions to realize.
The formula of a kind of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid disclosed by the invention, by weight percentage, by following Raw material is made:
Xinhui citrus reticulata meat fermentation liquid 1~5%, glycerol 0.2~1.2%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0~ 14.5%, neopelex 3.0~6.5%, alkyl glycosides 1.8~5.0%, alkylamide propyl-betaine 2.0~ 4.8%, sodium chloride 1.2~4.8%, EDTA-2Na 0.09~1.5%, essence 0.1~1%, preservative 0.1~2%, surplus For deionized water.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention, is prepared from the following raw materials:
Xinhui citrus reticulata meat fermentation liquid 3~5%, glycerol 0.5~1.0%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0~ 10.0%, neopelex 3.5~5.5%, alkyl glycosides 3.8~5.0%, alkylamide propyl-betaine 3.0~ 4.0%, sodium chloride 2.8~4.8%, EDTA-2Na 0.5~1.0%, essence 0.1~1%, preservative 0.1~2%, surplus are Deionized water.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention, is prepared from the following raw materials:
Xinhui citrus reticulata meat fermentation liquid 4%, glycerol 0.8%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0%, dodecylamino Sodium propionate 4%, alkyl glycosides 3.8%, alkylamide propyl-betaine 4.0%, sodium chloride 4.8%, EDTA-2Na 0.5%, perfume Smart 0.3%, preservative 0.5%, surplus is deionized water.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention, the Xinhui citrus reticulata meat fermentation liquid The preparation method comprises the following steps:
1) Special grinder for disintegrating of pulp, core separation, and cleaning, disinfection fermentor are cleaned;
2) weigh Xinhui citrus reticulata meat in mass ratio, by Xinhui citrus reticulata meat first pass through the pulp, core separation Special grinder for disintegrating into Row meat, core separation, pulp, the fruit juice after separation are poured into the fermentor;
3) white granulated sugar, corn pulp, probiotics are added in the step 2) fermentor, and continuously stirs fermentation, terminates hair It is transferred in holding vessel and is stored to get the Xinhui citrus reticulata meat fermentation liquid is arrived after ferment.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid of the present invention production dish washing liquid, in step 3), the prebiotic bacterium bag Include lactic acid bacteria, saccharomycete, streptococcus thermophilus.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid of the present invention production dish washing liquid, in step 3), whipping temp 35 DEG C -45 DEG C, mixing time is 5-7 days, measures pH value, lactic acid content, citric acid content, reaches set quota, terminates to ferment;Knot It is transferred in the holding vessel after beam fermentation and stores 60-100 days to get the Xinhui citrus reticulata meat fermentation liquid is arrived.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid of the present invention production dish washing liquid, the set quota are as follows: pH value is 2.6-3.5, lactic acid content 1645.00-2155.00mg/kg, citric acid content 2450.00-2950.00mg/kg.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid of the present invention production dish washing liquid in step 3), stores up in holding vessel 60-100 days are deposited to get the Xinhui citrus reticulata meat fermentation liquid is arrived.
Furthermore, the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention, the preservative are Phenoxyethanol With the mixture of methylisothiazolinone, the mass ratio of Phenoxyethanol and methylisothiazolinone is 8:2.
In addition, the process of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the invention, comprising the following steps:
S1, ingredient: with Xinhui citrus reticulata meat fermentation liquid, stir evenly, spare;
S2, enough deionized waters are added in reaction pot, open stirring, deionization is added in provisioned EDTA-2Na In water, stirring is until be completely dissolved;
S3, sodium sulfate of polyethenoxy ether of fatty alcohol, neopelex, alkyl glycosides, alkylamide are sequentially added Propyl betaine, glycerol are in addition preceding to guarantee that previous raw material has been completely dissolved;
S4, preservative, viscosity modifier is added, continues stirring to material and is completely dissolved, uniformly.
By above-mentioned technical proposal, the invention has the advantages that and advantageous effects:
1) dish washing liquid of the invention containing Xinhui citrus reticulata meat fermentation liquid, has dispelling abnormal flavor, fungistatic effect, to escherichia coli Act on 30min, to staphylococcus aureus act on 30min, to Candida albicans act on 40min, killing rate up to 99.9% with On;
2) process of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention, this method prepares simple and efficient;
3) formula of the invention and the low stimulation easily biological-degradable of technique, product is not hurt hands mildly, and fluidity regulator The form of glycerol is liquid, and epidemic situation comparison is stablized, can dissolve each other well with surfactant, and pre-treatment is not necessarily to, raw convenient for industry It produces.
Specific embodiment
The formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of the present invention includes component:
Xinhui citrus reticulata meat fermentation liquid, glycerol, sodium sulfate of polyethenoxy ether of fatty alcohol, neopelex, alkyl glycosides, Alkylamide propyl-betaine, sodium chloride, EDTA-2Na, essence, preservative, surplus are deionized water.
Technical principle of the invention are as follows:
Using the mixture of glycerol and Xinhui citrus reticulata meat fermentation liquid as fluidity regulator and functional component, and can be easily Be applied to industrial production.The present invention has many advantages, such as source natural health, easily biological-degradable.
Below with reference to embodiment, the present invention is described in further detail, and embodiments of the present invention are not limited thereto.
Wherein, Xinhui citrus reticulata meat fermentation liquid the preparation method comprises the following steps:
1) Special grinder for disintegrating of pulp, core separation, and cleaning, disinfection fermentor are cleaned;
2) take fresh Xinhui citrus reticulata meat 100g, by Xinhui citrus reticulata meat first pass through pulp, core separation Special grinder for disintegrating carry out meat, Core separation, pulp, the fruit juice after separation are poured into the fermentor;
3) in the step 2) fermentor be added 5g white granulated sugar, 2g corn pulp, 3g probiotics (lactic acid bacteria, saccharomycete and The hybrid bacterial strain of streptococcus thermophilus), and after continuously stirring 7 days at being 40 DEG C in temperature, measurement pH value is 3.0, and lactic acid content is 1800.00mg/kg, citric acid content 2500.00mg/kg terminate fermentation, are transferred in holding vessel and store 90 days to get arriving Xinhui citrus reticulata meat fermentation liquid.
Below by specific preferred embodiment more detailed description detergent of the invention.
Unless stated otherwise, all percentages of the invention are all calculated with the mass percentage of composition, all proportions It is mass percent.
Various test apparatuses and reagent are commercial goods, are that can buy to obtain by commercial sources.
A kind of formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid, includes each raw material component as shown in table 1 below:
Embodiment 1-3
The formula of the Xinhui citrus reticulata meat fermentation liquid production dish washing liquid of 1 embodiment 1-3 of table and the dish washing liquid formula of comparative example 1
The present embodiment 1-3's the preparation method is as follows:
S1, ingredient: with Xinhui citrus reticulata meat fermentation liquid, stir evenly, spare;
S2, enough deionized waters are added in reaction pot, open stirring, deionization is added in provisioned EDTA-2Na In water, stirring is until be completely dissolved;
S3, sodium sulfate of polyethenoxy ether of fatty alcohol, neopelex, alkyl glycosides, alkylamide are sequentially added Propyl betaine, glycerol are in addition preceding to guarantee that previous raw material has been completely dissolved;
S4, preservative, viscosity modifier is added, continues stirring to material and is completely dissolved, uniformly.
The following are the contents of effete test embodiment.
Effete test embodiment 1 (dish washing liquid performance test)
Temperature-Viscosity measurement is carried out to the detergent of embodiment 1-3, detergency measures, Stability Determination, pH value measurement, Test result is shown in Table 2.
The performance measurement of 2 embodiment 1-3 of table and the dish washing liquid of comparative example 1
From table 2 it can be seen that the detergent product of embodiment 1-3 has good detergency and low-temperature stability, pH value Close to human skin.Embodiment 1-3 has added glycerol, and comparative sample of the sensibility of viscosity temperature obviously than being not added reduces perhaps It is more.Therefore, the addition of glycerol improves the high/low temperature rheological characteristic of embodiment 1-3 well.
Effete test embodiment 2 (taste of dispelling experiment)
Experimental method:
10g test sample is put in salable bottle, 10mL ammonium hydroxide is added or is passed through 10mL hydrogen sulfide, is sealed, puts 10min, 5 μ L of headspace sampling are set, the surplus of ammonium hydroxide and hydrogen sulfide after being removed with gas-chromatography test, while with no Xinhui citrus reticulata meat Fermentation liquid, glycerol dish washing liquid do blank control, product has deducted control group removal amount to the removal rate of ammonium hydroxide and hydrogen sulfide. Test result see the table below shown in 3.
The effect that eliminates the unusual smell (removal rate/%) of the dish washing liquid of the present invention of table 3 and comparative example
Project Embodiment 1 Embodiment 2 Embodiment 3 Comparative example 1
Ammonium hydroxide 96% 99% 97% 20%
Hydrogen sulfide 95% 98% 96% 25%
From 3 data of table it is found that the dish washing liquid of embodiment 1-3 is more preferable to the removal rate of ammonium hydroxide and hydrogen sulfide, illustrate the proportion Relatively rationally.And comparative example 1 is compared to being not added with Xinhui citrus reticulata meat fermentation liquid, Hua Su pairs of the dish washing liquid of comparative example 1 for embodiment 1-3 The removal rate of ammonium hydroxide and hydrogen sulfide is lower, illustrates that Xinhui citrus reticulata meat fermentation liquid has very strong removal effect to ammonium hydroxide, hydrogen sulfide etc., sweet Oil dispels taste effect to it with synergistic function.
Effete test embodiment 3 (bacteriostatic experiment)
The following are the fungistatic effects (bacteriostasis rate/%) that table 4 is dish washing liquid of the present invention and comparative example.
The fungistatic effect (bacteriostasis rate/%) of the dish washing liquid of the present invention of table 4 and comparative example
Project Embodiment 1 Embodiment 2 Embodiment 3 Comparative example 1
Escherichia coli 94% 99% 96% 20%
Staphylococcus aureus 96% 98% 97% 30%
Candida albicans 95% 99% 97% 25%
Chlosma 97% 98% 96% 20%
Remarks: action time 5min, activity 1:1.
From 4 data of table it is found that the good antimicrobial effect of 1~3 dish washing liquid of the embodiment of the present invention, to escherichia coli, golden yellow Color staphylococcus, Candida albicans killing rate up to 95%, reach and " resist antibacterial detergent " wanting for bacteriostasis rate >=90% in standard It asks, therefore, dish washing liquid of the present invention has extremely strong inhibiting effect to chlosma, can be effectively anti-dandruff.
Wherein, the bacteriostasis rate of embodiment 1-3 is higher, illustrates that each component and proportion synergistic effect are most strong.1 shampoo of comparative example Hua Suzhong is free of Xinhui citrus reticulata meat fermentation liquid, and bacteriostasis rate wants low compared to Examples 1 to 3, illustrates Xinhui citrus reticulata meat hair of the present invention There is synergistic effect in the components such as zymotic fluid and glycerol, three compounds the bacteriostasis that can play enhancement.
The above described is only a preferred embodiment of the present invention, be not intended to limit the present invention in any form, therefore Without departing from the technical solutions of the present invention, to the above embodiments according to the technical essence of the invention any simply to repair Change, equivalent variations and modification, all of which are still within the scope of the technical scheme of the invention.

Claims (10)

1. a kind of formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid, it is characterised in that: by weight percentage, by following raw material It is made:
Xinhui citrus reticulata meat fermentation liquid 1~5%, glycerol 0.2~1.2%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0~14.5%, ten Dialkyl benzene sulfonic acids sodium 3.0~6.5%, alkyl glycosides 1.8~5.0%, alkylamide propyl-betaine 2.0~4.8%, chlorination Sodium 1.2~4.8%, EDTA-2Na 0.09~1.5%, essence 0.1~1%, preservative 0.1~2%, surplus are deionized water.
2. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 1, it is characterised in that: with weight percent Than meter, it is prepared from the following raw materials:
Xinhui citrus reticulata meat fermentation liquid 3~5%, glycerol 0.5~1.0%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0~10.0%, ten Dialkyl benzene sulfonic acids sodium 3.5~5.5%, alkyl glycosides 3.8~5.0%, alkylamide propyl-betaine 3.0~4.0%, chlorination Sodium 2.8~4.8%, EDTA-2Na 0.5~1.0%, essence 0.1~1%, preservative 0.1~2%, surplus are deionized water.
3. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 2, it is characterised in that: with weight percent Than meter, it is prepared from the following raw materials:
Xinhui citrus reticulata meat fermentation liquid 4%, glycerol 0.8%, sodium sulfate of polyethenoxy ether of fatty alcohol 6.0%, dodecyl alanine Sodium 4%, alkyl glycosides 3.8%, alkylamide propyl-betaine 4.0%, sodium chloride 4.8%, EDTA-2Na 0.5%, essence 0.3%, preservative 0.5%, surplus are deionized water.
4. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 1, it is characterised in that: the Xinhui citrus reticulata Meat fermentation liquid the preparation method comprises the following steps:
1) Special grinder for disintegrating of pulp, core separation, and cleaning, disinfection fermentor are cleaned;
2) weigh Xinhui citrus reticulata meat in mass ratio, by Xinhui citrus reticulata meat first pass through the pulp, core separation Special grinder for disintegrating carry out meat, Core separation, pulp, the fruit juice after separation are poured into the fermentor;
3) white granulated sugar, corn pulp, probiotics are added in the step 2) fermentor, and continuously stirs fermentation, after terminating fermentation It is transferred in holding vessel and stores to get the Xinhui citrus reticulata meat fermentation liquid is arrived.
5. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 4, it is characterised in that: in step 3) In, the probiotics includes lactic acid bacteria, saccharomycete, streptococcus thermophilus.
6. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 4, it is characterised in that: in step 3) In, whipping temp is 35 DEG C -45 DEG C, and mixing time is 5-7 days, measures pH value, lactic acid content, citric acid content, reaches regulation Index terminates fermentation;Terminate to be transferred in the holding vessel after fermenting and stores 60-100 days to get the Xinhui citrus reticulata meat fermentation is arrived Liquid.
7. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 6, it is characterised in that: the regulation refers to It is designated as: pH value 2.6-3.5, lactic acid content 1645.00-2155.00mg/kg, citric acid content 2450.00- 2950.00mg/kg。
8. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 4, it is characterised in that: in step 3) In, 60-100 days are stored in holding vessel to get the Xinhui citrus reticulata meat fermentation liquid is arrived.
9. the formula of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid according to claim 1, it is characterised in that: the preservative For the mixture of Phenoxyethanol and methylisothiazolinone, the mass ratio of Phenoxyethanol and methylisothiazolinone is 8:2.
10. a kind of process of Xinhui citrus reticulata meat fermentation liquid production dish washing liquids described in any item according to claim 1~9, It is characterized in that, comprising the following steps:
S1, ingredient: with Xinhui citrus reticulata meat fermentation liquid, stir evenly, spare;
S2, enough deionized waters are added in reaction pot, open stirring, deionized water is added in provisioned EDTA-2Na In, stirring is until be completely dissolved;
S3, sodium sulfate of polyethenoxy ether of fatty alcohol, neopelex, alkyl glycosides, alkylamide propyl are sequentially added Glycine betaine, glycerol are in addition preceding to guarantee that previous raw material has been completely dissolved;
S4, preservative, viscosity modifier is added, continues stirring to material and is completely dissolved, uniformly.
CN201811178153.XA 2018-10-10 2018-10-10 A kind of formula and technique of Xinhui citrus reticulata meat fermentation liquid production dish washing liquid Pending CN109294762A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110106029A (en) * 2019-05-05 2019-08-09 华南协同创新研究院 A kind of dried orange peel aurantium meat detergent and the preparation method and application thereof
CN110272784A (en) * 2019-07-08 2019-09-24 江西理工大学 A kind of bathroom detergent and preparation method thereof containing citrus reticulata"Chachi" blueness mandarin orange juice
CN111733028A (en) * 2019-03-25 2020-10-02 广州市艺洋实业有限公司 Detergent composition

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103242974A (en) * 2013-04-08 2013-08-14 广州立白企业集团有限公司 Fruit, vegetable and tableware detergent with good rheological property
CN106085641A (en) * 2016-06-03 2016-11-09 江西草珊瑚消毒用品有限公司 Antibiotic liquid detergent
CN107648129A (en) * 2017-11-17 2018-02-02 江门酵敬堂生物科技有限公司 A kind of production method of dried orange peel ferment shampoo

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103242974A (en) * 2013-04-08 2013-08-14 广州立白企业集团有限公司 Fruit, vegetable and tableware detergent with good rheological property
CN106085641A (en) * 2016-06-03 2016-11-09 江西草珊瑚消毒用品有限公司 Antibiotic liquid detergent
CN107648129A (en) * 2017-11-17 2018-02-02 江门酵敬堂生物科技有限公司 A kind of production method of dried orange peel ferment shampoo

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111733028A (en) * 2019-03-25 2020-10-02 广州市艺洋实业有限公司 Detergent composition
CN110106029A (en) * 2019-05-05 2019-08-09 华南协同创新研究院 A kind of dried orange peel aurantium meat detergent and the preparation method and application thereof
CN110106029B (en) * 2019-05-05 2021-11-02 华南协同创新研究院 Orange peel and citrus pulp detergent as well as preparation method and application thereof
CN110272784A (en) * 2019-07-08 2019-09-24 江西理工大学 A kind of bathroom detergent and preparation method thereof containing citrus reticulata"Chachi" blueness mandarin orange juice
CN110272784B (en) * 2019-07-08 2021-05-04 江西理工大学 Bathroom cleaner containing camellia branch, citrus reticulata blanco and citrus reticulata juice and preparation method thereof

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Application publication date: 20190201