CN109205579A - 氮化铝的制备方法 - Google Patents
氮化铝的制备方法 Download PDFInfo
- Publication number
- CN109205579A CN109205579A CN201811231432.8A CN201811231432A CN109205579A CN 109205579 A CN109205579 A CN 109205579A CN 201811231432 A CN201811231432 A CN 201811231432A CN 109205579 A CN109205579 A CN 109205579A
- Authority
- CN
- China
- Prior art keywords
- aluminium
- aluminium nitride
- preparation
- carbon black
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910017083 AlN Inorganic materials 0.000 title claims abstract description 36
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 56
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 51
- 239000004411 aluminium Substances 0.000 claims abstract description 48
- 239000006229 carbon black Substances 0.000 claims abstract description 39
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 16
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000012298 atmosphere Substances 0.000 claims abstract description 11
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 11
- 238000006722 reduction reaction Methods 0.000 claims abstract description 11
- 239000013049 sediment Substances 0.000 claims abstract description 11
- 239000001257 hydrogen Substances 0.000 claims abstract description 7
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 238000009830 intercalation Methods 0.000 claims abstract description 5
- 230000002687 intercalation Effects 0.000 claims abstract description 5
- 239000006185 dispersion Substances 0.000 claims abstract description 4
- 238000011049 filling Methods 0.000 claims abstract description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims description 6
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 229910021529 ammonia Inorganic materials 0.000 claims description 4
- 239000007789 gas Substances 0.000 claims description 4
- 239000001272 nitrous oxide Substances 0.000 claims description 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 239000002245 particle Substances 0.000 abstract description 16
- 238000000034 method Methods 0.000 abstract description 11
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 9
- 229910052710 silicon Inorganic materials 0.000 abstract description 9
- 239000010703 silicon Substances 0.000 abstract description 9
- 238000003756 stirring Methods 0.000 abstract description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract description 2
- 239000000843 powder Substances 0.000 description 17
- 238000001556 precipitation Methods 0.000 description 10
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 8
- 230000007062 hydrolysis Effects 0.000 description 8
- 238000006460 hydrolysis reaction Methods 0.000 description 8
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 230000005684 electric field Effects 0.000 description 4
- 239000012498 ultrapure water Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000004913 activation Effects 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 description 2
- 230000009977 dual effect Effects 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910021392 nanocarbon Inorganic materials 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 229960000935 dehydrated alcohol Drugs 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/072—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with aluminium
- C01B21/0722—Preparation by direct nitridation of aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Products (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201811231432.8A CN109205579B (zh) | 2018-10-22 | 2018-10-22 | 氮化铝的制备方法 |
Applications Claiming Priority (1)
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CN201811231432.8A CN109205579B (zh) | 2018-10-22 | 2018-10-22 | 氮化铝的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN109205579A true CN109205579A (zh) | 2019-01-15 |
CN109205579B CN109205579B (zh) | 2020-10-13 |
Family
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Family Applications (1)
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CN201811231432.8A Active CN109205579B (zh) | 2018-10-22 | 2018-10-22 | 氮化铝的制备方法 |
Country Status (1)
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CN (1) | CN109205579B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112897482A (zh) * | 2021-01-14 | 2021-06-04 | 中氢能源科技发展(内蒙古)有限公司 | 以铝合金为原料制备氮化铝的方法 |
CN113480828A (zh) * | 2021-03-02 | 2021-10-08 | 海南大学 | 一种氮化铝纳米花/聚合物复合材料及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4643859A (en) * | 1985-01-26 | 1987-02-17 | National Institute For Researches In Inorganic Materials | Process for the production of fine non-oxide powders from alkoxides |
CN101829607A (zh) * | 2010-05-17 | 2010-09-15 | 昆明珀玺金属材料有限公司 | 超声-电场耦合活化水解金属铝制备催化剂载体Al2O3粉末制备方法 |
CN104047015A (zh) * | 2014-06-19 | 2014-09-17 | 郑州昆研新材料科技有限公司 | 一种利用交流电解制备高纯氧化铝粉末的方法 |
CN104402452A (zh) * | 2014-10-31 | 2015-03-11 | 中国航空工业集团公司基础技术研究院 | 一种氮化铝陶瓷粉体的制备方法 |
-
2018
- 2018-10-22 CN CN201811231432.8A patent/CN109205579B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4643859A (en) * | 1985-01-26 | 1987-02-17 | National Institute For Researches In Inorganic Materials | Process for the production of fine non-oxide powders from alkoxides |
CN101829607A (zh) * | 2010-05-17 | 2010-09-15 | 昆明珀玺金属材料有限公司 | 超声-电场耦合活化水解金属铝制备催化剂载体Al2O3粉末制备方法 |
CN104047015A (zh) * | 2014-06-19 | 2014-09-17 | 郑州昆研新材料科技有限公司 | 一种利用交流电解制备高纯氧化铝粉末的方法 |
CN104402452A (zh) * | 2014-10-31 | 2015-03-11 | 中国航空工业集团公司基础技术研究院 | 一种氮化铝陶瓷粉体的制备方法 |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112897482A (zh) * | 2021-01-14 | 2021-06-04 | 中氢能源科技发展(内蒙古)有限公司 | 以铝合金为原料制备氮化铝的方法 |
CN113480828A (zh) * | 2021-03-02 | 2021-10-08 | 海南大学 | 一种氮化铝纳米花/聚合物复合材料及其制备方法 |
CN113480828B (zh) * | 2021-03-02 | 2022-06-14 | 海南大学 | 一种氮化铝纳米花/聚合物复合材料及其制备方法 |
Also Published As
Publication number | Publication date |
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CN109205579B (zh) | 2020-10-13 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of aluminum nitride Effective date of registration: 20220722 Granted publication date: 20201013 Pledgee: China Everbright Bank Limited by Share Ltd. Xiamen branch Pledgor: XIAMEN JUCI TECHNOLOGY CO.,LTD. Registration number: Y2022980011005 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231225 Granted publication date: 20201013 Pledgee: China Everbright Bank Limited by Share Ltd. Xiamen branch Pledgor: XIAMEN JUCI TECHNOLOGY CO.,LTD. Registration number: Y2022980011005 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of aluminum nitride Effective date of registration: 20231229 Granted publication date: 20201013 Pledgee: China Everbright Bank Limited by Share Ltd. Xiamen branch Pledgor: XIAMEN JUCI TECHNOLOGY CO.,LTD. Registration number: Y2023980074961 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20201013 Pledgee: China Everbright Bank Limited by Share Ltd. Xiamen branch Pledgor: XIAMEN JUCI TECHNOLOGY CO.,LTD. Registration number: Y2023980074961 |