CN109169722A - A kind of animal husbandry thimerosal and preparation method thereof - Google Patents
A kind of animal husbandry thimerosal and preparation method thereof Download PDFInfo
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- CN109169722A CN109169722A CN201810760064.XA CN201810760064A CN109169722A CN 109169722 A CN109169722 A CN 109169722A CN 201810760064 A CN201810760064 A CN 201810760064A CN 109169722 A CN109169722 A CN 109169722A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/10—Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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Abstract
The invention discloses a kind of animal husbandry thimerosal and preparation method thereof, the raw material including following parts by weight: 3.3-4.5 parts of polyvinylpyrrolidone, smart 0.25-0.44 parts of iodine, 7.6-9.5 parts of tea oil, 3.6-5.2 parts of allicin, 8.6-13.4 parts of camphortree leaf, 4.7-7.8 parts of ginger, 8-14.5 parts of the coptis, 10-17.2 parts of gardenia, 4.3-6.6 parts of radix bupleuri and 3.5-5 parts of root of kirilow rhodiola.Raw material sources of the present invention are extensive, by extracting to different Chinese medicine and being used cooperatively with smart iodine, allicin etc., the thimerosal sterilizing ability and stability of preparation are strong, has a broad antifungal spectrum, the skin of animal is not stimulated and not will cause the adverse reaction of animal, secondary pollution after not will cause disinfection is suitable for livestock breed aquatics.
Description
Technical field
The present invention relates to a kind of thimerosal, specifically a kind of animal husbandry thimerosal.
Background technique
Animal husbandry is the animal tamed by the mankind using livestock and poultry etc., the open countries such as Huo Zhelu, musk deer, fox, ermine, otter, quail
The physiological function of lively object enables it that plants such as herbage and feed are changed into animal energy, by artificial feeding, breeding to take
Obtain the production division of the livestock products such as meat, egg, milk, wool, cashmere, hide, silk and medicinal material.Self-sufficient domestic animal is different to raise
Support, animal husbandry be mainly characterized by centralization, scale and with it is commercial for production purpose.Animal husbandry be the mankind and nature into
The link of the utmost importance of row mass exchange, can provide animal food, can also provide raw material, and animal husbandry is also the important of agricultural
Composition.
People are when carrying out livestock breed aquatics, it is often necessary to carry out disinfection, reduce to the environment of an activation of animal house and animal
The probability of animals got sick, at present people's disinfection are all using pure chemistry drug, although this kind of drug can achieve disinfection, but
That irritation can be generated to animal, also can fur to animal and physical condition cause adverse effect, this just brings for culturist
Inconvenience.
Summary of the invention
The purpose of the present invention is to provide a kind of animal husbandry thimerosals, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the invention provides the following technical scheme:
A kind of animal husbandry thimerosal, the raw material including following parts by weight: 3.3-4.5 parts of polyvinylpyrrolidone, smart iodine
0.25-0.44 parts, 7.6-9.5 parts of tea oil, 3.6-5.2 parts of allicin, 8.6-13.4 parts of camphortree leaf, 4.7-7.8 parts of ginger, Huang
Even 8-14.5 parts, 10-17.2 parts of gardenia, 4.3-6.6 parts of radix bupleuri and 3.5-5 parts of root of kirilow rhodiola.
As a further solution of the present invention: the purity of smart iodine is 99.95% or more.
As a further solution of the present invention: smart iodine is the smart iodine extracted in seaweed.
The preparation method of the animal husbandry thimerosal, the specific steps are as follows:
Step 1 is freeze-dried under subzero 10 to subzero 2 degrees Celsius to water after cleaning up camphortree leaf and ginger
Mass fraction is 1.2-2.5%, be crushed to after 40-70 mesh be added to 5-7 times of its volume of mass fraction it is molten for 90% ethyl alcohol
It refluxing extraction 3-4 times and is assisted using ultrasonic wave in liquid, 45-60 minute each, filtering and merging filtrate obtain camphortree leaf
Extracting solution and ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting, obtain coptis extract liquor, cape jasmine by step 2
Flower extract liquor and radix bupleuri extract liquor；
Then step 3 exists polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil ball milling in the ball mill
It is kept for 20-35 minutes in the magnetic field of 4500-6300 Gauss, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed by step 4, be then cooled to subzero 5 to
It subzero 2 degrees Celsius and stirs 30-45 minutes, obtains the second mixture；
Step 5 is uniform by the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
It mixes and filters, then be uniformly mixed with suitable water to get finished product is arrived.
As a further solution of the present invention: the power of ultrasonic wave auxiliary is 75-120W, frequency 15-22KHz.
As a further solution of the present invention: the ratio of grinding media to material of ball mill is 60-75:1, and ball milling temperature is 40-52 degrees Celsius.
As a further solution of the present invention: mixing speed is 75-135rpm in step 4.
Compared with prior art, the beneficial effects of the present invention are: raw material sources of the present invention are extensive, by different Chinese medicine
It extracting and is used cooperatively with smart iodine, allicin etc., the thimerosal sterilizing ability and stability of preparation are strong, has a broad antifungal spectrum,
The skin of animal is not stimulated and not will cause the adverse reaction of animal, the secondary pollution after not will cause disinfection is applicable in
In livestock breed aquatics.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of animal husbandry thimerosal, the raw material including following parts by weight: 3.3 parts of polyvinylpyrrolidone, smart iodine 0.25
Part, 7.6 parts of tea oil, 3.6 parts of allicin, 8.6 parts of camphortree leaf, 4.7 parts of ginger, 8 parts of the coptis, 10 parts of gardenia, 4.3 parts of radix bupleuri
With 3.5 parts of root of kirilow rhodiola.The purity of smart iodine is 99.95% or more.
The preparation method of the animal husbandry thimerosal, the specific steps are as follows:
Step 1 is freeze-dried under subzero 6 degrees Celsius after cleaning up camphortree leaf and ginger to the mass fraction of water
It is 1.7%, is crushed to and refluxing extraction is added in the ethanol solution for being 90% to 6 times of its volume of mass fraction after 50 mesh 3 times simultaneously
And assisted using ultrasonic wave, the power of ultrasonic wave auxiliary is 80W, frequency 19KHz, 48 minutes every time, filters and merges filter
Liquid obtains camphor tree leaf extract and ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting, obtain coptis extract liquor, cape jasmine by step 2
Flower extract liquor and radix bupleuri extract liquor；
Then step 3 exists polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil ball milling in the ball mill
It is kept for 26 minutes in the magnetic field of 5400 Gausses, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed by step 4, are then cooled to subzero 3 and are taken the photograph
Family name's degree and stir 42 minutes, obtain the second mixture；
Step 5 is uniform by the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
It mixes and filters, then be uniformly mixed with suitable water to get finished product is arrived.
Embodiment 2
A kind of animal husbandry thimerosal, the raw material including following parts by weight: 3.8 parts of polyvinylpyrrolidone, smart iodine 0.36
Part, 8.4 parts of tea oil, 4.2 parts of allicin, 10.8 parts of camphortree leaf, 5.9 parts of ginger, 11.6 parts of the coptis, 14.5 parts of gardenia, bavin
5.4 parts and 4.2 parts of root of kirilow rhodiola recklessly.Smart iodine is the smart iodine extracted in seaweed.
The preparation method of the animal husbandry thimerosal, the specific steps are as follows:
Step 1 is freeze-dried under subzero 6 degrees Celsius after cleaning up camphortree leaf and ginger to the mass fraction of water
It is 2.3%, is crushed to and refluxing extraction is added in the ethanol solution for being 90% to 6 times of its volume of mass fraction after 50 mesh 4 times simultaneously
And assisted using ultrasonic wave, 58 minutes every time, filtering and merging filtrate obtain camphor tree leaf extract and ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting, obtain coptis extract liquor, cape jasmine by step 2
Flower extract liquor and radix bupleuri extract liquor；
Polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil in 45 degrees Celsius and ratio of grinding media to material are 66:1's by step 3
Then ball milling in ball mill is kept for 33 minutes in the magnetic field of 5900 Gausses, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed by step 4, are then cooled to subzero 5 and are taken the photograph
Family name's degree and stir 36 minutes, obtain the second mixture；
Step 5 is uniform by the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
It mixes and filters, then be uniformly mixed with suitable water to get finished product is arrived.
Embodiment 3
A kind of animal husbandry thimerosal, the raw material including following parts by weight: 4.2 parts of polyvinylpyrrolidone, smart iodine 0.39
Part, 8.6 parts of tea oil, 4.8 parts of allicin, 12.8 parts of camphortree leaf, 7.5 parts of ginger, 13.8 parts of the coptis, 16.6 parts of gardenia, bavin
6.4 parts and 4.7 parts of root of kirilow rhodiola recklessly.The purity of smart iodine is 99.95% or more.Smart iodine is the smart iodine extracted in seaweed.
The preparation method of the animal husbandry thimerosal, the specific steps are as follows:
Step 1 is freeze-dried under subzero 8 degrees Celsius after cleaning up camphortree leaf and ginger to the mass fraction of water
It is 1.9%, is crushed to and refluxing extraction is added in the ethanol solution for being 90% to 5 times of its volume of mass fraction after 60 mesh 3 times simultaneously
And assisted using ultrasonic wave, 58 minutes every time, filtering and merging filtrate obtain camphor tree leaf extract and ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting, obtain coptis extract liquor, cape jasmine by step 2
Flower extract liquor and radix bupleuri extract liquor；
Then step 3 exists polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil ball milling in the ball mill
It is kept for 29 minutes in the magnetic field of 6300 Gausses, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed by step 4, are then cooled to subzero 3 and are taken the photograph
Family name's degree and with the revolving speed of 105rpm stirring 38 minutes, obtain the second mixture；
Step 5 is uniform by the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
It mixes and filters, then be uniformly mixed with suitable water to get finished product is arrived.
Embodiment 4
A kind of animal husbandry thimerosal, the raw material including following parts by weight: 4.5 parts of polyvinylpyrrolidone, smart iodine 0.44
Part, 9.5 parts of tea oil, 5.2 parts of allicin, 13.4 parts of camphortree leaf, 7.8 parts of ginger, 14.5 parts of the coptis, 17.2 parts of gardenia, bavin
6.6 parts and 5 parts of root of kirilow rhodiola recklessly.The purity of smart iodine is 99.95% or more.Smart iodine is the smart iodine extracted in seaweed.
The preparation method of the animal husbandry thimerosal, the specific steps are as follows:
Step 1 is freeze-dried under subzero 10 degrees Celsius after cleaning up camphortree leaf and ginger to the mass fraction of water
It is 2.5%, is crushed to and refluxing extraction is added in the ethanol solution for being 90% to 5 times of its volume of mass fraction after 70 mesh 4 times simultaneously
And assisted using ultrasonic wave, the power of ultrasonic wave auxiliary is 115W, frequency 20KHz, 52 minutes every time, filters and merges filter
Liquid obtains camphor tree leaf extract and ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting, obtain coptis extract liquor, cape jasmine by step 2
Flower extract liquor and radix bupleuri extract liquor；
Polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil in 50 degrees Celsius and ratio of grinding media to material are 72:1's by step 3
Then ball milling in ball mill is kept for 30 minutes in the magnetic field of 6000 Gausses, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed by step 4, are then cooled to subzero 2 and are taken the photograph
Family name's degree and with the revolving speed of 90rpm stirring 40 minutes, obtain the second mixture；
Step 5 is uniform by the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
It mixes and filters, then be uniformly mixed with suitable water to get finished product is arrived.
Comparative example 1
Except allicin and gardenia is contained, remaining raw material and preparation method are same as Example 2.
Comparative example 2
Using existing animal husbandry thimerosal as a comparison case 2.
Selection staphylococcus aureus, candida albicans, bacillus coli and pseudomonas aeruginosa are inoculated with respectively
In on culture medium and cultivating, then the colonies typical in culture medium is inoculated in broth bouillon respectively, at identical temperature
Culture 24 hours, the product of Example 1-4 and the product of comparative example 1-2 are respectively 30 milliliters and dilute 30 times, dilute by 6 kinds
Liquid is released to be put in 4 containers and aseptically place respectively.After nutrient broth after cultivating 24 hours is diluted 50 times,
Every kind of bacterium is sub-packed in 6 culture dishes, marks 1-6 group respectively, the dilution of embodiment 1-4 and comparative example 1-2 are dripped respectively
In the culture dish for entering 1-6 group, observation, measurement strain revolution mark simultaneously record data, are shown in Table 1.
Table 1
Above-mentioned culture dish is put under aseptic condition after observation and stands 2 days, example 1-4's and comparative example 1-2 to be performed
After product volatilization, the bacterium of 1-4 group does not have significant change, and 5 groups of bacterium is slightly increased, and 6 groups of bacterium continues to breed.
3000 times of water of the product of the product of embodiment 1-4 and comparative example 1-2 is diluted, dilution multiple-contact is moved
The dilution of object skin, embodiment 1-4 does not stimulate animal skin, and also without adverse reaction, the dilution of comparative example 1 is to dynamic
Object skin slightly stimulates, but does not have adverse reaction, and the dilution of comparative example 2 is irritating to animal skin, vomits with animal
Equal adverse reactions.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of animal husbandry thimerosal, which is characterized in that the raw material including following parts by weight: polyvinylpyrrolidone 3.3-
4.5 parts, smart 0.25-0.44 parts of iodine, 7.6-9.5 parts of tea oil, 3.6-5.2 parts of allicin, 8.6-13.4 parts of camphortree leaf, ginger
4.7-7.8 parts, 8-14.5 parts of the coptis, 10-17.2 parts of gardenia, 4.3-6.6 parts of radix bupleuri and 3.5-5 parts of root of kirilow rhodiola.
2. animal husbandry thimerosal according to claim 1, which is characterized in that it is described essence iodine purity be 99.95% with
On.
3. animal husbandry thimerosal according to claim 1, which is characterized in that the essence iodine is the essence extracted in seaweed
Iodine.
4. a kind of preparation method of animal husbandry thimerosal a method according to any one of claims 1-3, which is characterized in that specific steps
It is as follows:
Step 1 is freeze-dried under subzero 10 to subzero 2 degrees Celsius after cleaning up camphortree leaf and ginger to the quality of water
Score is 1.2-2.5%, is added to 5-7 times of its volume of mass fraction after being crushed to 40-70 mesh to return in 90% ethanol solution
Stream is extracted 3-4 times and is assisted using ultrasonic wave, 45-60 minutes each, and filtering and merging filtrate obtain camphor tree leaf extract
And ginger extract；
The coptis, gardenia and radix bupleuri are used supercritical carbon dioxide extracting by step 2, obtain coptis extract liquor, gardenia extraction
Take liquid and radix bupleuri extract liquor；
Step 3, by polyvinylpyrrolidone, root of kirilow rhodiola, smart iodine and tea oil ball milling in the ball mill, then in 4500-
It is kept for 20-35 minutes in the magnetic field of 6300 Gausses, obtains the first mixture；
Allicin, camphor tree leaf extract and gardenia extract liquor are uniformly mixed, are then cooled to subzero 5 to subzero 2 by step 4
Degree Celsius and stir 30-45 minutes, obtain the second mixture；
Step 5 uniformly mixes the first mixture, the second mixture, ginger extract, coptis extract liquor and radix bupleuri extract liquor
And it filters, then be uniformly mixed with suitable water to get finished product is arrived.
5. the preparation method of animal husbandry thimerosal according to claim 4, which is characterized in that the ultrasonic wave auxiliary
Power is 75-120W, frequency 15-22KHz.
6. the preparation method of animal husbandry thimerosal according to claim 4 or 5, which is characterized in that the ball mill
Ratio of grinding media to material is 60-75:1, and ball milling temperature is 40-52 degrees Celsius.
7. the preparation method of animal husbandry thimerosal according to claim 4, which is characterized in that stirred in the step 4
Speed is 75-135rpm.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110583648A (en) * | 2019-08-26 | 2019-12-20 | 河北誉康检测技术服务有限公司 | Composite quaternary ammonium salt disinfectant and its preparation method |
| CN111034729A (en) * | 2019-12-30 | 2020-04-21 | 河南安进生物技术股份有限公司 | Tick repellent, preparation method thereof and application thereof to tick repelling |
| CN116531292A (en) * | 2023-04-27 | 2023-08-04 | 佛山市佛丹动物药业有限公司 | Cosmetic for animals |
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