CN116531292B

CN116531292B - Cosmetic for animals

Info

Publication number: CN116531292B
Application number: CN202310467003.5A
Authority: CN
Inventors: 钟广林; 程方翔; 张沛煌
Original assignee: Foshan Fudan Animal Pharmaceutical Co ltd
Current assignee: Foshan Fudan Animal Pharmaceutical Co ltd
Priority date: 2023-04-27
Filing date: 2023-04-27
Publication date: 2023-11-17
Anticipated expiration: 2043-04-27
Also published as: CN116531292A

Abstract

The invention relates to a cosmetic toilet product for animals, which belongs to the technical field of external care products for animals, and comprises the following raw materials: ginkgo leaf extract, garlicin, white water lily flower extract, water-soluble lanolin, camphor tree leaf extract, tea leaf extract, mountain Ji trimethyl ammonium chloride, active combination materials and auxiliary materials. The ginkgo leaf extract, the white water lily flower extract and the allicin are added to generate a synergistic effect when being used in combination, wherein flavonoid compounds in the ginkgo leaf extract and active ingredient compounds in the white water lily flower extract can inhibit the mechanisms of virus adhesion, synthesis or damage the structure and the like, and the allicin is added to further enhance the antibacterial effect; the camphor tree leaf extract and the tea leaf extract are added, so that the odor and the peculiar smell are weakened or eliminated; whereas mountain Ji trimethylammonium chloride improves animal hair entanglement; the water-soluble lanolin can effectively slow down water loss and resist drying.

Description

Cosmetic for animals

Technical Field

The invention belongs to the technical field of external care products for animals, and particularly relates to a cosmetic toilet product for animals.

Background

The animals are kept from ancient times, along with the ageing degree of population in China and the annual increase of individual young people, more and more animals enter families of common people as emotion, meanwhile, the properties of the animals are changed silently, and in many families, the animals have risen to the status of family members. In order to meet various demands generated in the process of raising animals by people, a huge consumer market consisting of animal foods, supplies, medical treatment, cosmetology and the like is formed, and an 'animal economy' is created. While animal products are the most important components in animal economy, animal accessory products are the primary category in the animal products market, main products are collars, lead ropes, clothing, toys, etc. for dogs and cats, and topical care products are the second competitive category in the overall animal products market.

However, throughout the market, it is found that the external care products for animals are very lacking, and only products for washing eyes or protecting ears and some shampoo products for washing eyes or protecting ears, which can be easily purchased, are almost blank for the cosmetic care products for animals. However, in the process of raising animals, external care products for animals are very necessary, and it is well known that most animal hairs are vigorous, and the hairs are dry and easy to wind due to insufficient nutrition in the raising process, and in addition, a large amount of hairs are more easily adhered with dust, adsorb environmental odor such as kitchen, toilet and the like, and the odor are mainly multi-component, low-boiling-point and small-molecular-weight mixtures mainly comprising ammonia, hydrogen sulfide, indole, skatole and the like, have the characteristics of being easy to volatilize and low in perception threshold, can harm health of human bodies after being in odor gas for a long time, and can bring hidden trouble to people who inhale cats and dog-making people daily. In addition, the secretion of the animal can accumulate in the peculiar smell environment to easily breed germs, and the animal is not friendly to the raising owners while the animal is harmful to the health. Therefore, the invention provides a cosmetic toilet product for animals, which solves the problems that animals are easy to generate peculiar smell and breed bacteria and hair is dry and easy to wind.

Disclosure of Invention

The invention aims to provide a cosmetic toilet product for animals, which is added with ginkgo leaf extract, white water lily flower extract and allicin, and the three are combined to generate a synergistic effect, wherein flavonoid compounds in the ginkgo leaf extract and active ingredient compounds in the white water lily flower extract can inhibit the mechanisms of virus adhesion, synthesis or damage the structure and the like, and allicin is added to further enhance the antibacterial effect; the camphor tree leaf extract and the tea leaf extract are also added, so that the odor and the peculiar smell are weakened or eliminated; the added mountain Ji trimethyl ammonium chloride improves the entanglement of animal hair, and the added water-soluble lanolin can effectively slow down the water loss and resist dryness, so that the problems that animals are easy to generate peculiar smell and breed bacteria and the hair is dry and entangled are solved.

The aim of the invention can be achieved by the following technical scheme:

a cosmetic toilet article for animals, which comprises the following raw materials in parts by mass:

further, the active combination material comprises any three or more than three of salicylic acid, hydroxyethyl urea, sodium hyaluronate, benzyl benzoate, bisabolol and ceramide according to the mass ratio of 0.7-1.2:0.3-0.9:0.5-1.1:0.8-1.4:0.5-1.0:0.4-1.0.

Further, the tea extract is prepared from soaked tea as an extraction raw material by a conventional solvent extraction method in the field.

Further, the soaked and used tea leaves include, but are not limited to, soaked and used green tea leaves, oolong tea leaves, black tea leaves and white tea.

Further, the cosmetic toilet also comprises white water lily flower extract, water-soluble lanolin and auxiliary materials.

Further, the white water lily flower extract is 5.2-6.6g, the water-soluble lanolin is 4.8-5.9g, and the auxiliary material is 4.3-5.4g.

Further, the auxiliary materials comprise glycerol caprylate and any one of polyvinylpyrrolidone, polysorbate-80 and stearic acid.

Further, the mass ratio of the glyceryl caprylate to the vinyl pyrrolidone to the polysorbate-80 to the stearic acid is 1.2-1.6:0.6-0.7:0.5-0.7:0.3-0.5.

Further, the preparation method of the cosmetic toilet product comprises the following steps: mixing all the raw materials, stirring at controlled temperature, cooling to room temperature to obtain mixture, and making into cosmetic toilet product.

Further, the temperature of the temperature-controlled stirring is 25-35 ℃, and the stirring time is 0.5-1h; the finished cosmetic products include, but are not limited to, make-up drops, make-up sprays, shampoos, and make-up toilet creams.

The invention has the beneficial effects that:

(1) The ginkgo leaf extract, the white water lily flower extract and the allicin are added, and the three are combined to produce a synergistic effect, so that a stronger antibacterial effect is exerted. The ginkgo leaf extract contains various active substances such as flavonoid, phenols, polysaccharide, lactone and the like, wherein the types of flavonoid compounds are more than 40, and the flavonoid compounds can be used together with the mechanisms of inhibiting the adhesion, synthesis or destroying the structure of viruses of active component compounds existing in the ginkgo flower extract to cause harmful microorganisms to generate functional disorder, and the garlic oil is added as the active component of the garlicin, so that the ginkgo leaf extract and the ginkgo flower extract can be further assisted to exert antibacterial and anti-inflammatory effects, and the product shows excellent antibacterial effect.

(2) The camphor tree leaf extract added in the invention contains main active ingredients such as alkene, aldehyde, ketone, epoxy alkane groups and the like, the active groups can be added, condensed and neutralized with odor to produce odorless substance compounds with low volatility, and in addition, the camphor tree leaf extract also contains volatile aromatic substances, thereby playing a role in masking odor; the main component of the added tea extract is tea polyphenol, and hydroxyl groups on catechin rings of the tea extract can provide hydrogen ions to react with ammonia to generate ammonium salt, so that odor and peculiar smell can be reduced or eliminated.

(3) The added mountain Ji trimethyl ammonium chloride is a cationic surfactant, has a long chain of twenty-two carbons, has positive charges, can neutralize negative charges on animal hair, has good affinity with animal hair, and is beneficial to improving animal hair entanglement; in addition, the water-soluble lanolin and phytosphingosine are added, so that the moisture loss can be effectively reduced, the drying can be resisted, the moisture can be locked, the wetting and softening degree of animal hair can be increased, a better conditioning effect can be achieved, the comb property of animal hair can be improved integrally, and the hair-conditioning agent is especially effective in repairing the drying and winding properties of animal hair and helping hair growth.

(4) The raw materials of the tea extract are soaked tea, the waste tea is reused, the cost is reduced, and the preparation method is simple and easy to operate and is beneficial to mass production.

Detailed Description

The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.

The ginkgo leaf extract product number used in the invention is A-0669, the white water lily flower extract product number is A-6545, the ginkgo leaf extract product number is purchased from Sichuan Biotechnology Co., ltd, the garlicin is purchased from Sichuan Biotechnology Co., ltd, the camphor leaf extract product is purchased from Ningxia vanilla Biotechnology Co., ltd, and the water-soluble lanolin is purchased from Guangzhou flower King chemical Co., ltd.

Example 1

Weighing the following raw materials in parts by mass:

the active combination material comprises salicylic acid, sodium hyaluronate and bisabolol according to the mass ratio of 1.2:0.8:0.7; the green tea leaf extract is prepared by soaking green tea leaves and adopting a solvent extraction method which is a conventional technical method in the field.

Mixing all the raw materials in the formula, stirring for 0.5h at the temperature of 25 ℃, cooling to room temperature after stirring to obtain a mixture, adding deionized water with the mass of 5 times into the mixture, and uniformly stirring to obtain the cosmetic spray.

Example 2

Weighing the following raw materials in parts by mass:

the active combination material comprises benzyl benzoate, ceramide and bisabolol according to the mass ratio of 1.1:0.7:0.5; the oolong tea leaf extract is prepared by soaking the used oolong tea leaves and adopting a solvent extraction method by a conventional technical method in the field.

Mixing all the raw materials in the formula, stirring for 1h at the temperature of 30 ℃, cooling to room temperature after stirring to obtain a mixture, adding deionized water with the mass of 2 times into the mixture, and stirring uniformly to obtain the cosmetic drops.

Dropping the cosmetic toilet drops on the hands of the animal owners, uniformly spreading the toilet drops on the hands, and then wiping the toilet drops on the hair and skin of the pets.

Example 3

Weighing the following raw materials in parts by mass:

the active combination material comprises salicylic acid, hydroxyethyl urea and ceramide according to the mass ratio of 0.7:0.9:0.7; the black tea leaf extract is prepared by soaking the used black tea leaves and adopting a solvent extraction method by a conventional technical method in the field.

Mixing all the raw materials in the formula, stirring for 0.5h at the temperature of 35 ℃, cooling to room temperature after stirring to obtain a mixture, adding deionized water with the mass of 5 times into the mixture, and uniformly stirring to obtain the cosmetic spray.

Example 4

Weighing the following raw materials in parts by mass:

The auxiliary materials comprise glycerol caprylate and stearic acid according to the mass ratio of 1.4:0.4.

Example 5

Weighing the following raw materials in parts by mass:

The auxiliary materials comprise glycerol caprylate and polyvinylpyrrolidone according to the mass ratio of 1.6:0.6.

Example 6

Weighing the following raw materials in parts by mass:

The auxiliary materials comprise glyceryl caprylate and polysorbate-80 according to the mass ratio of 1.4:0.6.

Spraying the cosmetic spray onto the desired part about 2cm from the animal, and combing with hair combing tool against the animal skin.

Comparative examples 1 to 3

The quality of the ginkgo leaf extract, allicin and white water lily flower extracts in comparative examples 1 to 3 are shown in table 1, and the other preparation steps and parameters are the same, as compared with example 4.

TABLE 1

Comparative example 4

Compared with example 4, the camphor tree leaf extract is 5g, and the rest preparation steps and parameters are the same.

Comparative example 5

Compared with example 4, the camphor tree leaf extract is 7g, and the rest preparation steps and parameters are the same.

Comparative example 6

In comparison to example 4, the black tea leaf extract was 5.5g, and the remaining preparation steps and parameters were the same.

Comparative example 7

In comparison to example 4, the black tea leaf extract was 7.4g, the remaining preparation steps and parameters were the same.

Comparative example 8

Compared with example 4, 5.5g of mountain Ji trimethylammonium chloride was obtained, and the other preparation steps and parameters were the same.

Comparative example 9

Compared with example 4, the mountain Ji trimethylammonium chloride was 7g, and the other preparation steps and parameters were the same.

Comparative example 10

In comparison with example 4, the water-soluble lanolin was 4.7g, and the remaining preparation steps and parameters were the same.

Comparative example 11

In comparison with example 4, the water-soluble lanolin was 6g, and the remaining preparation steps and parameters were the same.

Comparative example 12

In comparison with example 4, phytosphingosine was 2.9g, the remaining preparation steps and parameters were the same.

Comparative example 13

In comparison with example 4, phytosphingosine was 4.1g, the remaining preparation steps and parameters were identical.

Test example 1

The antibacterial effect of the cosmetic toiletries prepared in examples 4-6 and comparative examples 1-3 of the present invention was measured, and the specific steps were:

(1) Selecting a test strain: staphylococcus aureus, escherichia coli, and bacillus subtilis.

(2) Preparation of the culture medium: the formula of the yeast extract agar medium comprises: 10g of peptone, 20g of maltose, 5g of yeast extract and 20g of agar, after dissolving the raw materials, the raw materials are supplemented with water to 1000mL, and the raw materials are sterilized for activating each test bacterium.

(3) Preparation of test bacterial suspension: measuring the bacterial concentration by using a Maillard turbidity method; activating and culturing the slant of the test bacteria, preparing a gradient bacteria solution by using physiological saline, using a standard tube of 0.5 McGeorge as a reference, measuring the absorbance value of each gradient bacteria solution at 560nm by using a spectrophotometer, and selecting a diluted bacteria solution of 0.5 McGersGersGersche turbidity, namely the concentration of each test bacteria is 1.5X10 ⁸ And (3) one/mL for later use.

Preparation of standard tube 0.5 of McAld: 0.048 mol/L barium chloride solution is prepared and stored in a dark place.

(4) And (3) antibacterial effect measurement: and (3) adding 1mL of the test bacterial suspension prepared in the step (3) of the test example into 50mL of the culture medium which is sterilized and cooled to 45-48 ℃, uniformly mixing, and placing 20mL of the mixture into a culture dish to prepare a bacteria-containing flat plate. Then, sterilized filter paper sheets with the diameter of 5mm are respectively put into the cosmetic toiletries prepared in the examples 4-6 and the comparative examples 1-3 of the invention, soaked for 24 hours, then evenly placed on the surface of a culture medium after being air-dried, fixed by light pressure, and each strain is repeated for 3 times and cultured at a proper temperature (bacteria are cultured at 36 ℃ for 18-24 hours and fungi are cultured at 27 ℃ for 24-48 hours). The diameter of the inhibition zone on each plate was measured by a graduated scale, the maximum inhibition zone was the strongest inhibition zone, and the result was the average value of 3 repeated tests, and the result is shown in table 2.

TABLE 2

The results in Table 2 show that the cosmetic toiletries prepared in accordance with the present invention have excellent antibacterial effects. In detail, as can be seen from comparative examples 1 to 3, the inhibition effect on test bacteria is not as good as that of examples 4 to 6 no matter which of ginkgo leaf extract, white water lily flower extract and allicin is added, especially comparative example 1, the inhibition effect on three test bacteria is obviously weakened under the condition that ginkgo leaf extract is not added, which indicates that the combined use of ginkgo leaf extract, white water lily flower extract and allicin can produce a synergistic effect and exert stronger antibacterial effect.

Test example 2

The dog owners voluntarily agree to test the autotrophic pet dogs and randomly divide 42 pet dogs with peculiar smell on the body into 7 groups, 6 pet dogs in each group are subjected to odor removal test by using the cosmetic spray agents prepared in examples 4-6 and comparative examples 4-7, and the heavy condition of the peculiar smell on the pet dogs is recorded before use; the cosmetic spray is applied by spraying the whole body of the cosmetic spray at a distance of about 2cm from the pet dog, and then combing against the skin of the pet dog with a hair combing tool. The method is characterized in that the method is used once in the morning and noon every day, one treatment course is continuously used, one treatment course is 5 days, and the odor concentration condition on the pet dog is recorded at about 4 pm on the 2 nd day, the 4 th day after the use and the interval day (namely the 6 th day) after the use of one treatment course;

evaluation index: the peculiar smell is given a 5-point, the peculiar smell is given a 4-point, the peculiar smell is given a 3-point, the peculiar smell is given a 2-point, the peculiar smell is given a 1-point, and the peculiar smell is given a 0-point; taking an average value of the final scores of each group, and reserving an integer for the results; the results are shown in Table 3.

TABLE 3 Table 3

As can be seen from Table 3, the cosmetic toilet products prepared by the present invention have excellent deodorizing effects. The invention is characterized in that the added camphor tree leaf extract contains volatile aromatic substances which play a role in masking peculiar smell, the main component of the added tea leaf extract is tea polyphenol, and hydroxyl groups on catechin rings of the tea polyphenol can provide hydrogen ions to react with ammonia to generate ammonium salts, so that the peculiar smell and the peculiar smell can be weakened or eliminated.

Test example 3

The dog owners voluntarily agree to test the autotrophic pet dogs and randomly divide 35 pet dogs with dry hair and easy winding on the body into 7 groups of 5 pet dogs, and the dry hair and easy winding hair repairing test is carried out on the pet dogs by using the cosmetic spray-paint prepared in examples 4-6 and comparative examples 8-11 respectively.

The dryness and the entanglement degree of the hair on the pet dog are observed and scored before use (i.e. day 0) by spraying the cosmetic spray over the whole body at a distance of about 2cm from the pet dog and combing the skin of the pet dog with a hair combing tool. The method is characterized in that the method is used once in the morning and in the noon every day, one treatment course is continuously used, the treatment course is 6 days, the hair dryness and the hair winding course on the pet dog are observed and recorded at about 5 pm after the free movement of the pet on the 2 nd day, the 4 th day and the 6 th day after the use, and the records are made;

evaluation index:

degree of hair dryness: dry to the touch and matt 0 minutes;

the product is dry to touch and has a glossiness of 1 minute;

a slightly moist feel and a slightly glossy feel for 3 minutes;

wet to the touch and extremely shiny for 5 minutes;

degree of hair entanglement: the hairs are extremely disordered and intertwined for 0 minutes;

the hairs are disordered and intertwined for 1 minute;

hair is normal but there is still a small number of intertwining 3 minutes;

hair is normal and no 5 minutes of entanglement;

taking an average value of the final scores of each group, and reserving an integer for the results; the results are shown in Table 4.

TABLE 4 Table 4

As can be seen from Table 4, the cosmetic toilet product of the present invention has excellent effects of restoring dry hair and anti-entanglement effect of animal hair. The invention is characterized in that the mountain Ji trimethyl ammonium chloride is added, the mountain Ji trimethyl ammonium chloride has positive charges, can neutralize negative charges on animal hair, has good affinity with animal hair, further improves animal hair entanglement, and can effectively slow down water loss, resist dryness, increase the wetting degree of animal hair and help hair growth.

In the description of the present specification, the descriptions of the terms "one embodiment," "example," "specific example," and the like, mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiments or examples. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The foregoing is merely illustrative and explanatory of the invention, as various modifications and additions may be made to the particular embodiments described, or in a similar manner, by those skilled in the art, without departing from the scope of the invention or exceeding the scope of the invention as defined in the claims.

Claims

1. A cosmetic toilet article for animals, characterized in that the cosmetic toilet article comprises the following raw materials in parts by mass:

7.1-8.2g of ginkgo leaf extract

Allicin 3.9-4.5g

5.4-6.6g of camphor tree leaf extract

5.8-7.1g of tea extract

Mountain Ji trimethyl ammonium chloride 5.6-6.9g

Phytosphingosine 3-4g

13.3 g to 15.7g of active composite material

5.2-6.6g of white water lily flower extract

4.8-5.9g of water-soluble lanolin;

the active composition comprises any three or more than three of salicylic acid, hydroxyethyl urea, sodium hyaluronate, benzyl benzoate, bisabolol and ceramide according to the mass ratio of 0.7-1.2:0.3-0.9:0.5-1.1:0.8-1.4:0.5-1.0:0.4-1.0.

2. The cosmetic toilet article for animals according to claim 1, wherein the tea extract is prepared from tea leaves after soaking.

3. The cosmetic toilet article for animals according to claim 1, wherein the cosmetic toilet article further comprises an auxiliary material.

4. A cosmetic toilet article for animals according to claim 3, wherein the auxiliary material is 4.3-5.4g in mass parts.

5. A cosmetic toilet article for animals according to claim 3, wherein the auxiliary material comprises glyceryl caprylate and further comprises any one of polyvinylpyrrolidone, polysorbate-80 and stearic acid.

6. A method of preparing a cosmetic toilet article for animals according to any one of claims 3 to 5, wherein the method of preparing a cosmetic toilet article comprises: mixing all the raw materials, stirring at controlled temperature, cooling to room temperature to obtain mixture, and making into cosmetic toilet product.

7. The method for preparing a cosmetic toilet article for animals according to claim 6, wherein the temperature of the temperature-controlled stirring is 25-35 ℃ and the stirring time is 0.5-1h.