CN109161211B - Preparation method of bead blasting packaging material for cigarettes - Google Patents
Preparation method of bead blasting packaging material for cigarettes Download PDFInfo
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- CN109161211B CN109161211B CN201811078405.1A CN201811078405A CN109161211B CN 109161211 B CN109161211 B CN 109161211B CN 201811078405 A CN201811078405 A CN 201811078405A CN 109161211 B CN109161211 B CN 109161211B
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L89/00—Compositions of proteins; Compositions of derivatives thereof
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention relates to a preparation method of a bead blasting wrapping material for cigarettes, and belongs to the technical field of materials for cigarettes. According to the invention, nano silicon dioxide and ethylene-vinyl acetate copolymerized hot melt adhesive are mixed, polyethylene pyrrolidone is used as a dispersing agent, so that mixed sol is obtained as an auxiliary agent for preparing a wrapping material, gelatin, soybean protein and starch are blended by adopting a blending method, the auxiliary agent is added to prepare the bead blasting wrapping material for cigarettes, and the blending method can improve the characteristics of single gelatin film, such as softness, thermal instability, easiness in water absorption and the like; the addition of the starch increases the Young modulus and the elastic strength of the wrapping material, the addition of the glycerol increases the elongation rate of the wrapping material, reduces the brittleness, and prevents the wrapping material from cracking due to friction and extrusion, and the stearic acid is used as a heat stabilizer, so that the weather resistance of the wrapping material is obviously improved.
Description
Technical Field
The invention relates to a preparation method of a bead blasting wrapping material for cigarettes, and belongs to the technical field of materials for cigarettes.
Background
The bead blasting, also called as flavor dripping pill, brittle capsule, etc., refers to a kind of liquid small glue bead embedded into the cigarette filter in the form of capsule, through wrapping liquid solvents with different flavors, the smoker squeezes and crushes the bead by hand in the process of smoking the cigarette, so that the flavor liquid in the bead flows out, and the flavor component is released under the action of the mainstream smoke of the cigarette. The application of the popping beads in the cigarette filter stick realizes the adjustability of the smoking taste of the cigarette, has obvious effects of increasing the fragrance and keeping the moisture, can meet the requirement of consumers pursuing the individual fragrance of the cigarette, and obtains pleasant smoking experience such as comfortable sensation, sweet feeling, fluid production feeling and the like; the bead blasting has strong visual output such as sound, transparency and visibility, and the like, and gives the cigarette playing integrated function. In recent years, a plurality of tobacco enterprises have developed and produced bead-blasting cigarettes in China, and certain achievements are achieved in breaking through the key technical barriers of bead blasting. In combination with the actual production situation, the use of the dropping method for producing popping beads in the prior art has the following drawbacks: the dropping pill is easy to be broken due to friction and extrusion in the drying, screening and filter stick embedding processes after being formed, the oily spice in the soft capsule is easy to seep out, the adhesion condition among the dropping pills occurs, the brittleness of the dropping pill is reduced after being stored for a period of time, the phenomenon of fogging occasionally occurs, when the dropping pill is pinched by hands, the crisp sound of 'snap' is difficult to hear, and the appearance quality and the actual application effect of the dropping pill are seriously influenced. This is probably due to the thin thickness of the rubber, the unstable water content, and the deterioration of the rubber matrix.
The wall material of the soft capsule prepared by the traditional technology is mostly gelatin which is mainly extracted from skin and bones of certain animals. Gelatin is a mixture of water-soluble proteins and is a partially denatured product of collagen. Since gelatin is derived from natural products and has the ability to bear dyes due to its glossy appearance, and is easy to handle, it is widely used as a good drug coating material for solid dosage forms in medicine, including hard and soft gelatin capsules and gelatin-coated tablets. However, the gelatin has low strength and high brittleness, is easy to absorb water and swell, and has low strength and elastic modulus after swelling, so that the gelatin is limited to be directly used. Therefore, in order to solve the problem of the gelatin soft capsule, the development of a high-performance bead blasting packaging material for cigarettes is urgently needed to improve the problem of poor experience of consumers.
Disclosure of Invention
The technical problems to be solved by the invention are as follows: aiming at the problems that the existing bead blasting packaging material is poor in weather resistance and easy to break due to friction and extrusion, the preparation method of the bead blasting packaging material for the cigarettes is provided.
In order to solve the technical problems, the invention adopts the technical scheme that:
(1) mixing polyvinylpyrrolidone, nano silicon dioxide powder and liquid sol, carrying out ultrasonic dispersion for 20-40 min, and carrying out magnetic stirring to obtain mixed sol;
(2) respectively weighing 20-28 parts by weight of gelatin, 10-16 parts by weight of starch, 1-6 parts by weight of mixed sol, 3-8 parts by weight of soybean protein, 2-5 parts by weight of stearic acid, 1-3 parts by weight of glycerol and 30-60 parts by weight of deionized water, mixing the gelatin, the deionized water and the soybean protein, heating to obtain a mixed solution, adding the starch, stirring to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, magnetically stirring and standing, sieving by a screen mesh under a heat preservation state, and obtaining a filtrate which is the packing material for the cigarette blasting beads.
The liquid sol in the step (1) is ethylene-vinyl acetate copolymerized hot melt adhesive, and is heated for 30-40 min at the temperature of 70-80 ℃.
And (2) mixing the polyvinylpyrrolidone, the nano silicon dioxide powder and the liquid sol in the step (1) according to the mass ratio of 1: 5: 12.
The magnetic stirring in the step (1) is carried out for 1-2 hours at a stirring speed of 100-160 r/min.
The heating and stirring treatment in the step (2) is to mix gelatin and deionized water, heat and stir at 50-60 ℃ for 20-30 min to obtain a gelatin solution, add soy protein, heat and stir in a water bath at 70-80 ℃ for 30-40 min.
And (3) stirring for 20-30 min at the rotating speed of 200-300 r/min, and then continuously stirring for 20-30 min at the rotating speed of 1000-3000 r/min.
And (3) magnetically stirring and standing the mixture in the step (2), wherein the magnetic stirring is carried out for 30-50 min at the water bath temperature of 70-80 ℃, and the standing is carried out for 3-6 h.
And (3) passing through a 60-100 mesh screen in the heat preservation state.
Compared with other methods, the method has the beneficial technical effects that:
(1) according to the invention, nano silicon dioxide and ethylene-vinyl acetate copolymerized hot melt adhesive are mixed, polyvinylpyrrolidone is used as a dispersing agent, the obtained mixed sol is used as an auxiliary agent for preparing the wrapping material, gelatin, soybean protein and starch are blended by adopting a blending method, the auxiliary agent is added to prepare the bead blasting wrapping material for cigarettes, the characteristics of softness, thermal instability, easiness in water absorption and the like of a single gelatin film can be improved by the blending method, and the starch is a natural organic matter and has good biocompatibility with the gelatin; the silt and seepage effects of the nano particles can be uniformly embedded in the wrapping material, so that the compactness and the barrier property of the wrapping material are enhanced, the nano silicon dioxide has certain antibacterial property and can better inhibit the activity of some bacteria, and the wrapping material added with the nano silicon dioxide particles enhances the mechanical property, the moisture permeability and the oxygen permeability of the original wrapping material to a greater extent, so that the wrapping material is more compact;
(2) the addition of the starch increases the Young modulus and the elastic strength of the wrapping material, the addition of the glycerol increases the elongation rate of the wrapping material, reduces the brittleness, and prevents the wrapping material from cracking due to friction and extrusion, and the stearic acid is used as a heat stabilizer, so that the weather resistance of the wrapping material is obviously improved.
Detailed Description
Heating ethylene-vinyl acetate copolymerized hot melt adhesive at the temperature of 70-80 ℃ for 30-40 min to obtain liquid sol, mixing polyvinylpyrrolidone, nano silicon dioxide powder and the liquid sol according to the mass ratio of 1: 5: 12, ultrasonically dispersing for 20-40 min, and magnetically stirring for 1-2 h at the stirring speed of 100-160 r/min to obtain mixed sol; respectively weighing 20-28 parts by weight of gelatin, 10-16 parts by weight of starch, 1-6 parts by weight of mixed sol, 3-8 parts by weight of soybean protein, 2-5 parts by weight of stearic acid, 1-3 parts by weight of glycerol and 30-60 parts by weight of deionized water, mixing the gelatin and the deionized water, heating and stirring at 50-60 ℃ for 20-30 min to obtain a gelatin solution, adding the soybean protein, heating and stirring in a water bath at 70-80 ℃ for 30-40 min to obtain a mixed solution, adding the starch, stirring at a rotating speed of 200-300 r/min for 20-30 min, adjusting the rotating speed to 1000-3000 r/min, continuously stirring for 20-30 min to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, stirring at a water bath temperature of 70-80 ℃ for 30-50 min, standing for 3-6 h, sieving with a 60-100-mesh sieve in a heat preservation state, and obtaining a filtrate which is the cigarette-used as a cigarette-used packaging.
Example 1
Heating ethylene-vinyl acetate copolymerized hot melt adhesive at the temperature of 70 ℃ for 30min to obtain liquid sol, mixing polyvinylpyrrolidone, nano silicon dioxide powder and the liquid sol according to the mass ratio of 1: 5: 12, ultrasonically dispersing for 20min, and magnetically stirring for 1h at the stirring speed of 100r/min to obtain mixed sol; respectively weighing 20 parts of gelatin, 10 parts of starch, 1 part of mixed sol, 3 parts of soybean protein, 2 parts of stearic acid, 1 part of glycerol and 30 parts of deionized water, mixing the gelatin and the deionized water, heating and stirring at 50 ℃ for 20min to obtain a gelatin solution, adding the soybean protein, heating and stirring in a water bath at 70 ℃ for 30min to obtain a mixed solution, adding the starch, stirring at a rotating speed of 200r/min for 20min, adjusting the rotating speed to 1000r/min, continuously stirring for 20min to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, magnetically stirring at a water bath temperature of 70 ℃ for 30min, standing for 3h, sieving with a 60-mesh sieve in a heat preservation state, and obtaining a filtrate which is the bead blasting packaging material for cigarettes.
Example 2
Heating ethylene-vinyl acetate copolymerized hot melt adhesive at the temperature of 75 ℃ for 35min to obtain liquid sol, mixing polyvinylpyrrolidone, nano silicon dioxide powder and the liquid sol according to the mass ratio of 1: 5: 12, ultrasonically dispersing for 30min, and magnetically stirring for 1.5h at the stirring speed of 130r/min to obtain mixed sol; respectively weighing 24 parts of gelatin, 13 parts of starch, 4 parts of mixed sol, 5 parts of soybean protein, 3 parts of stearic acid, 2 parts of glycerol and 45 parts of deionized water, mixing the gelatin and the deionized water, heating and stirring for 25min at 55 ℃ to obtain a gelatin solution, adding the soybean protein, heating and stirring for 35min in a water bath at 75 ℃ to obtain a mixed solution, adding the starch, stirring for 25min at a rotation speed of 250r/min, continuously stirring for 25min at a rotation speed of 2000r/min to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, magnetically stirring for 40min at a water bath temperature of 75 ℃, standing for 5h, sieving by a 80-mesh sieve in a heat preservation state to obtain a filtrate which is the bead blasting packaging material for cigarettes.
Example 3
Heating ethylene-vinyl acetate copolymerized hot melt adhesive at the temperature of 80 ℃ for 40min to obtain liquid sol, mixing polyvinylpyrrolidone, nano silicon dioxide powder and the liquid sol according to the mass ratio of 1: 5: 12, ultrasonically dispersing for 40min, and magnetically stirring for 2h at the stirring speed of 160r/min to obtain mixed sol; respectively weighing 28 parts of gelatin, 16 parts of starch, 6 parts of mixed sol, 8 parts of soybean protein, 5 parts of stearic acid, 3 parts of glycerol and 60 parts of deionized water, mixing the gelatin and the deionized water, heating and stirring at 60 ℃ for 30min to obtain a gelatin solution, adding the soybean protein, heating and stirring in a water bath at 80 ℃ for 40min to obtain a mixed solution, adding the starch, stirring at 300r/min for 30min, adjusting the rotation speed to 3000r/min, continuously stirring for 30min to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, magnetically stirring at 80 ℃ for 50min, standing for 6h, sieving with a 100-mesh sieve in a heat preservation state, and obtaining a filtrate which is the bead blasting packaging material for cigarettes.
The bead blasting packaging material for the cigarette and the bead blasting packaging material sold in the market are detected, and the specific detection results are shown in the following tables 1 and 2:
the detection method comprises the following steps:
and (3) detecting the moisture content of the bead blasting packaging material by using an HR73/HG53 moisture detector in the above embodiment, wherein the drying temperature is 105 ℃, the heating mode is soft heating, and the heating time is 1: 20 min. And (3) absorbing moisture of the dropped bead blasting material for 48 hours at the temperature of 20 +/-2 ℃ and the relative humidity of 85-95%, and respectively detecting the moisture of the bead blasting packaging material before and after moisture absorption as shown in the table 1.
The hardness of the popping beads in the embodiment is detected by using a DPYD-A dropping pill tablet hardness tester, the popping beads are placed in the middle of a sample tray of the hardness tester and are abutted against a fixed baffle, a tester switch is started, a push rod advances at a fixed speed of 1mm/s to press the popping beads, the pressure of the push rod when the popping beads are broken, namely the hardness, is recorded, and the detection result is shown in the table 1:
table 1 shows the results of the moisture content and hardness before and after moisture absorption of the exploded bead
And (2) test II: wet heat aging test of exploded bead
And (3) carrying out a damp-heat aging cycle test on the popping beads dripped in each example in a high-low temperature damp-heat aging box for 48h, observing the appearance of the popping beads, and detecting the hardness of the popping beads after moisture absorption.
The experimental conditions were as follows:
(1) and (3) low-temperature conditions: -20 ℃ x 12h
(2) High temperature conditions: 22 ℃ x 12h, 40 ℃ x 12h
The relative humidity was maintained at (93. + -. 3)%, at the higher temperatures mentioned above, and the remaining time in the cycle was not less than 95%, with the results in the cycle test shown in Table 2:
TABLE 2 Damp and Hot aging cycle test of the exploding beads in a high and Low temperature Damp and Hot aging Box
TABLE 1 characterization of bead blasting wrapping Material Properties
TABLE 2 characterization of wet heat aging resistance of bead blasting packaging material
As can be seen from Table 1, the moisture content of the exploded bead of the cigarette packaging material prepared by the invention is reduced, the moisture absorption performance of the exploded bead is improved, the adaptability of the exploded bead to the environmental temperature is strong, and the weather resistance is good.
Claims (7)
1. A preparation method of a bead blasting wrapping material for cigarettes is characterized by comprising the following specific preparation steps:
(1) heating ethylene-vinyl acetate copolymerized hot melt adhesive at the temperature of 70-80 ℃ for 30-40 min to obtain liquid sol, mixing polyvinylpyrrolidone, nano silicon dioxide powder and the liquid sol, performing ultrasonic dispersion for 20-40 min, and performing magnetic stirring to obtain mixed sol;
(2) respectively weighing 20-28 parts by weight of gelatin, 10-16 parts by weight of starch, 1-6 parts by weight of mixed sol, 3-8 parts by weight of soybean protein, 2-5 parts by weight of stearic acid, 1-3 parts by weight of glycerol and 30-60 parts by weight of deionized water, mixing the gelatin, the deionized water and the soybean protein, heating to obtain a mixed solution, adding the starch, stirring to obtain a blended solution, sequentially adding the mixed sol, the stearic acid and the glycerol, magnetically stirring and standing, sieving by a screen mesh under a heat preservation state, and obtaining a filtrate which is the packing material for the cigarette blasting beads.
2. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: and (2) mixing the polyvinylpyrrolidone, the nano silicon dioxide powder and the liquid sol in the step (1) according to the mass ratio of 1: 5: 12.
3. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: the magnetic stirring in the step (1) is carried out for 1-2 hours at a stirring speed of 100-160 r/min.
4. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: the heating and stirring treatment in the step (2) is to mix gelatin and deionized water, heat and stir at 50-60 ℃ for 20-30 min to obtain a gelatin solution, add soy protein, heat and stir in a water bath at 70-80 ℃ for 30-40 min.
5. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: and (3) stirring for 20-30 min at the rotating speed of 200-300 r/min, and then continuously stirring for 20-30 min at the rotating speed of 1000-3000 r/min.
6. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: and (3) magnetically stirring and standing the mixture in the step (2), wherein the magnetic stirring is carried out for 30-50 min at the water bath temperature of 70-80 ℃, and the standing is carried out for 3-6 h.
7. The preparation method of the bead blasting packaging material for the cigarettes according to claim 1, characterized by comprising the following steps: and (3) passing through a 60-100 mesh screen in the heat preservation state.
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| CN109662346A (en) * | 2019-02-22 | 2019-04-23 | 广东省金叶科技开发有限公司 | It is a kind of not by the cigarette of filter tip microenvironment with quick-fried pearl and preparation method thereof |
| CN109846083A (en) * | 2019-02-22 | 2019-06-07 | 广西中烟工业有限责任公司 | A kind of cigarette of appearance setting waterproof wax coat is with quick-fried pearl and preparation method thereof |
| CN115197478A (en) * | 2022-04-15 | 2022-10-18 | 江苏万腾新材料科技有限公司 | Plant gum base bead blasting wall material and preparation method thereof |
| CN115479458B (en) * | 2022-09-30 | 2024-01-26 | 湖北中烟工业有限责任公司 | Drying device |
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