CN105768195A - Buccal cigarette adopting big proportion of tobacco materials and preparation method for buccal cigarette - Google Patents

Buccal cigarette adopting big proportion of tobacco materials and preparation method for buccal cigarette Download PDF

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Publication number
CN105768195A
CN105768195A CN201610323627.XA CN201610323627A CN105768195A CN 105768195 A CN105768195 A CN 105768195A CN 201610323627 A CN201610323627 A CN 201610323627A CN 105768195 A CN105768195 A CN 105768195A
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China
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tobacco
buccal cigarette
fermentation
containing material
cigarette
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CN105768195B (en
Inventor
陈森林
陶红
沈光林
胡静
孔浩辉
李峰
赵谋明
赵强忠
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China Tobacco Guangdong Industrial Co Ltd
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China Tobacco Guangdong Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B13/00Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/20Biochemical treatment

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses a buccal cigarette adopting a big proportion of tobacco materials and a preparation method for the buccal cigarettes. The buccal cigarette is prepared from the following components in percent by mass: 80-95% of tobacco raw materials, 1-5% of a filler, 0.5-5% of a flavoring agent, 1-10% of an adhesive and 0.1-1% of essence, wherein the tobacco raw materials are formed by mixing tobacco leaf particles and tobacco stem particles in percent by mass being (60-80%): (40-20%); and the tobacco leaf particles and the tobacco stem particles are separately obtained by screening and getting penetration parts after carrying out fermentation treatment and micro-grinding. According to the buccal cigarette, the big proportion of tobacco raw materials are greatly used in the preparation of the buccal cigarette, so that the use ratio of the tobacco raw materials is guaranteed to be as high as 95%; moreover, the tobacco raw materials comprise a great proportion of tobacco stems, so that the utilization rate of the tobacco raw materials in the buccal cigarette is increased, technical support is provided for cigarette localization of the buccal cigarette, the bitter taste and the biting taste of the tobacco raw materials are scientifically treated, and the smell is rich and thick; while eating, the buccal cigarette is gradually melted while no granular sensation and roughness exist in an oral cavity, so that the buccal cigarette does not need to be spit and discarded after being consumed.

Description

Adopt buccal cigarette of vast scale tobacco-containing material and preparation method thereof
Technical field
The present invention relates to tobacco leaf production technical field, more particularly, to a kind of buccal cigarette adopting vast scale tobacco-containing material and preparation method thereof.
Background technology
Smoke-free tobacco product refers to without combustion process, and sucks the tobacco product of consumption either directly through oral cavity or nasal cavity.
World Health Organization's Framework Convention on Tobacco Control (WHOFCTC) proposes about forbidding restriction and the ban such as tobacco smoke diffusion in public places, and the development of conventional tobacco products Medicated cigarette is caused powerful impact.Under this background, countries in the world tobacco business using the research and development of smoke-free tobacco product and introduce to the market as solve tobacco business future development important means, in Europe, South and North America, India and Africa, smoke-less tobacco product various in style, consumption figure in various countries all in the trend increased year by year.For the U.S., in 2006 years, consumption figure is more than 4,000,000,000 dollars.
Buccal cigarette is a kind of smokeless tobacco containing nicotine, it is common that salt adding of being clayed into power by Nicotiana tabacum L. again and water mix, and sometimes also can add spice, seem oleum bergamottae, Oleum Rosae Rugosae or Radix Glycyrrhizae.Buccal cigarette the earliest is in bulk, is kneaded into a little group with finger, then fills in upper lip rear when suck.From 1973, buccal cigarette was installed in the pouch as little tea bag.
The sense organ impact strength of buccal cigarette is limited mainly by the organoleptic attribute impact of tobacco material, has the fire-cured tobacco of significant proportion in the tobacco material formula that external product is conventional in order to ensure its distinctive organoleptic feature.Owing to fire-cured tobacco is external distinctive tobacco material, this largely limits the raw material space of domestic Foreign Experience exploitation smoke-free tobacco product.And at present the smoke-free tobacco product technique of domestic-developed is mostly and directly uses tobacco material grinding, seasoning, pack, have that zest is excessive, bitter taste is dense, acid is strong, be not directed to the fermentation process technique of tobacco material.
On the other hand, existing buccal cigarette all uses tobacco leaf (tobacco shred) as raw material, does not find to use cabo as buccal cigarette raw material.This is that compared with tobacco leaf, cabo contains less volatile material (flavor component) and higher proportion of cell-wall biopolymers owing to cabo is very big with the nature difference of blade, such as cellulose, lignin and colloid etc., its rigid structure is more, and fiber is thick, it is difficult to edible.But, cabo accounts for more than the 20% of total tobacco leaf quality, if cabo application problem in buccal cigarette can be solved, tobacco material utilization rate preparation buccal cigarette in will be greatly improved.
Summary of the invention
The technical problem to be solved in the present invention is the technical deficiency overcoming existing buccal cigarette, a kind of buccal cigarette adopting vast scale tobacco-containing material is provided, described buccal cigarette is prepared by the adjuvant of the reasonably combined safe dose of tobacco material of super large ratio, described tobacco material forms in proportion through Nicotiana tabacum L. and the tobacco stalk raw material of scientific disposal, eliminate bitter taste and acid, enrich fragrance matter.
The preparation method that another technical problem that the invention solves the problems that is to provide described buccal cigarette.
The purpose of the present invention is achieved by the following technical programs:
A kind of buccal cigarette adopting vast scale tobacco-containing material is provided, each component of following mass ratio prepares: tobacco material 80~95%, filler 1~5%, correctives 0.5~5%, binding agent 1~10% and essence 0.1~1%;
Described tobacco material is made up of according to the mass ratio mixing of 60~80%:40~20% tobacco leaf granule and cabo particle;
Described cabo particle is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process,;
S13. the stem fermented by step S12 carries out Crushing of Ultrafine, sieves and obtains described cabo particle;
Described tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22. the tobacco shred of step S21 shredding gained is carried out carbon dioxide expanding treatment;
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process;Sieve after the tobacco shred Crushing of Ultrafine after fermentation, take permeation parts;
Wherein, fermentation processing method described in step S12 is: preparation inoculation liquid, be the inoculation after fermentation of 1~15g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50~200) g:(0.1~10) g:(0.01~1) g:(100~500) g.After fermentation process, effectively removes bitter taste, acid, and obtain ferment local-flavor.
Fermentation described in step S23 is preparation inoculation liquid, is 1~15g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50~200) g:(0.1~10) g:(0.01~1) g:(100~500) g.After fermentation process, effectively removes bitter taste, acid, and obtain ferment local-flavor.
Described protein peptide be soybean protein peptide, wheat protein peptide, rice protein peptide, casein peptide, whey protein peptide one or more;
Described strain is one or more of monascus (MonascuspurpureusWent.), aspergillus oryzae (Aspergillusoryzae), Zygosaccharomyces rouxii (Mucorroxianus) or rhizopus (Rhizopus), yeast (Saccharomyces) or lactic acid bacteria (Lactobacillus).
Described water preferably employs distilled water.
Described filler is one or more in starch, maltodextrin, cyclodextrin, microcrystalline Cellulose, white sugar, mannitol or xylitol;Described correctives is one or more of Sal, sodium carbonate or sodium benzoate etc.;Described binding agent is one or more in sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, gelatin or white sugar;Described essence is naturally occurring or synthetic perfume monomer, fruit extract or vegetable material extract.
The described preferred menthol of naturally occurring or synthetic perfume monomer, menthyl acetate, Borneolum Syntheticum etc. further, described fruit extract is preferably the extract of Fructus Mali pumilae, Fructus Citri junoris, Fructus Persicae, Fructus Citri Limoniae or Fructus Armeniacae Mume etc., and described vegetable material extract is preferably the extract of Folium Camelliae sinensis, Flos Chrysanthemi, coffee bean or cacao bean etc..Can adopting the corresponding essence of the existing use of tobacco enterprise, if extracted, extracting method is with reference to existing routine.
Preferably, sieving described in step S23 was 160 mesh sieves, took permeation parts.
Preferably, the process conditions of microwave bulking described in step S11 are: cabo moisture content 14~18%, Bulking Time 45~75s, expand power 600~900W.
Preferably, shredding described in step S11 is that cabo is cut to 0.5~5.0cm length, the uniform stem that 0.3~0.9mm is wide.
Preferably, in the process of fermentation described in step S12, fermentation temperature is for 35~45 DEG C, and fermentation time is 10~30 days.
Preferably, described in step 22, the process conditions of carbon dioxide expanding treatment are: dip time 1~5min, expansion temperature 300~400 DEG C.
Preferably, in the process of fermentation described in step 23, fermentation temperature is for 35~45 DEG C, and fermentation time is 7~30 days.
Described Crushing of Ultrafine is with reference to existing routine techniques.
Preferably, step S13 or sieve described in S23 and be 160 mesh sieves, take permeation parts.
The preparation method that present invention simultaneously provides described buccal cigarette, comprises the following steps:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.Described cutting can be cut into rectangle or other shapes, such as Nicotiana tabacum L. shape etc..
Preferably, the thickness of diaphragm described in step S2 is 0.1~1mm.
Preferably, described baking is to toast 1~2 hour at 40~60 DEG C.
Beneficial effects of the present invention is as follows:
The invention provides a kind of new buccal cigarette material, each component of following mass ratio prepare: tobacco material 80~95%, filler 1~5%, correctives 0.5~5%, binding agent 1~10% and essence 0.1~1%.Described buccal cigarette material is made up of according to the mass ratio mixing of 60~80%:40~20% tobacco leaf granule and cabo particle, tobacco leaf granule and cabo particle be adopt Nicotiana tabacum L. or cabo respectively fermented wait the laggard row Crushing of Ultrafine of process after sieve, take permeation parts and get final product.The process of science of the present invention eliminates bitter taste and the acid of Nicotiana tabacum L., fragrance matter is enriched mellow, by itself and the collocation of adjuvant science, the seasoning carrying out reasonable benefit/risk processes, it is thus achieved that a kind of new buccal cigarette material, mouthfeel is more abundant, flavor coordination, quality are high, can by gradually containing change when edible, without granular sensation, harsh feeling in oral cavity, edible end abandons without spuing, apply cabo in large quantities simultaneously, improve tobacco material utilization rate in preparation buccal cigarette.
The present invention is vast scale use tobacco material in the preparation of buccal cigarette not only, ensure that the usage ratio of tobacco material is up to 95%, and tobacco-containing material used includes significant percentage of cabo, " this change of cigarette " for buccal cigarette provides technical support, and solve cabo application problem in buccal cigarette well, improve tobacco material utilization rate in buccal cigarette.
The buccal cigarette of the present invention is uniform sheet form, can in the oral cavity quickly containing change, and instant also can be completely edible, will not to environment.
Detailed description of the invention
The present invention is further described below in conjunction with specific embodiment.Unless stated otherwise, the present invention adopts reagent, equipment are the art conventional reagent and equipment;Design philosophy of the present invention is summed up based on long-term great many of experiments and is obtained, and following embodiment is merely to illustrate the present invention, but does not therefore limit the present invention.The raw material (protein peptide, strain, filler, correctives, binding agent, essence, lubricant etc.) that following embodiment adopts, unless stated otherwise, is conventional commercial raw material.
Embodiment 1
The present embodiment provides a kind of cabo particle suitable in buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process, removes bitter taste, acid, and obtains ferment local-flavor;
S13. the stem fermented by step S12 carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain described cabo particle;
The process conditions of microwave bulking described in step S11 are: cabo moisture content 14%, Bulking Time 45s, expand power 750W.
Shredding described in step S11 is that cabo is cut to 1.0~3.0cm length, the uniform stem that 0.3~0.5mm is wide.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 15g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:0.5g:0.2g:200g of distilled water;Controlling temperature 35 DEG C, fermentation time is 10 days.
Described strain is monascus (MonascuspurpureusWent.).Described protein peptide is soybean protein peptide.
Embodiment 2
The present embodiment provides a kind of cabo particle suitable in buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process, removes bitter taste, acid, and obtains ferment local-flavor;
S13. the stem fermented by step S12 carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain described cabo particle;
The process conditions of microwave bulking described in step S11 are: cabo moisture content 16%, Bulking Time 45s, expand power 750W.
Shredding described in step S11 is that cabo is cut to 0.5~1cm length, the uniform stem that 0.3~0.5mm is wide.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 12g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:0.3g:0.3g:100g of distilled water;Controlling temperature 37 DEG C, fermentation time is 14 days.
Described strain is aspergillus oryzae (Aspergillusoryzae).Described protein peptide is wheat protein peptide.
Embodiment 3
The present embodiment provides a kind of cabo particle suitable in buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process, removes bitter taste, acid, and obtains ferment local-flavor;
S13. the stem fermented by step S12 carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain described cabo particle;
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, Bulking Time 60s, expand power 900W.
Shredding described in step S11 is that cabo is cut to 2~4cm length, the uniform stem that 0.6~0.9mm is wide.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 1g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=100g:1g:0.5g:200g of distilled water;Controlling temperature at 40 DEG C, fermentation time is 20 days.
Described strain is yeast (Saccharomyces).Described protein peptide is rice protein peptide.
Embodiment 4
The present embodiment provides a kind of cabo particle suitable in buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process, removes bitter taste, acid, and obtains ferment local-flavor;
S13. the stem fermented by step S12 carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain described cabo particle;
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, Bulking Time 70s, expand power 900W.
Shredding described in step S11 is that cabo is cut to 1.0~2.0cm length, the uniform stem that 0.5~0.6mm is wide.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 15g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=120g:3g:0.6g:200g of distilled water;Controlling temperature 38 DEG C, fermentation time is 24 days.
Described strain is yeast (Saccharomyces) and the combined inoculation liquid of lactic acid bacteria (Lactobacillus), and the mixed proportion of the two does not do considered critical, it is preferred to 1:4.Described protein peptide is whey protein peptide.
Embodiment 5
The present embodiment provides a kind of cabo particle suitable in buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process, removes bitter taste, acid, and obtains ferment local-flavor;
S13. the stem fermented by step S12 carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain described cabo particle;
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, Bulking Time 70s, expand power 900W.
Shredding described in step S11 is that cabo is cut to 2.0~3.0cm length, the uniform stem that 0.4~0.6mm is wide.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 15g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=180g:8g:0.6g:300g of distilled water;Controlling temperature 45 C, fermentation time is 20 days.
Described strain is monascus (MonascuspurpureusWent.) and the combined inoculation liquid of yeast (Saccharomyces), and the mixed proportion of the two is 1:1.Described protein peptide is casein peptide.
Embodiment 6
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22. step S21 shredding gained tobacco shred being carried out carbon dioxide expanding treatment, the process conditions of described carbon dioxide expanding treatment are: dip time 5min, expansion temperature 400 DEG C;
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid, it is thus achieved that fermentation taste;By the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 10g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Fermentation temperature is 35 DEG C, and the time is 10 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=80g:0.05g:0.2g:120g of distilled water;Described protein peptide is soybean protein peptide is 1:1 with whey protein peptide mass ratio.
Described strain is monascus (MonascuspurpureusWent.).
Embodiment 7
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22. step S21 shredding gained tobacco shred being carried out carbon dioxide expanding treatment, the process conditions of described carbon dioxide expanding treatment are: dip time 1min, expansion temperature 350 DEG C.
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid, it is thus achieved that fermentation taste;By the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 5g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Fermentation temperature is 38 DEG C, and the time is 15 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:3g:0.5g:250g of distilled water;Described strain is lactic acid bacteria (Lactobacillus).The protein peptide of described inoculation liquid is soybean protein peptide.
Embodiment 8
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22., the tobacco shred of step S21 shredding gained carries out carbon dioxide expanding treatment, and the process conditions of described carbon dioxide expanding treatment are: dip time 5min, expansion temperature 400 DEG C.
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid, it is thus achieved that fermentation taste;By the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 15g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Fermentation temperature is 37 DEG C, and the time is 21 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=50g:1g:0.08g:120g of distilled water;Described protein peptide is whey protein peptide.Described strain is rhizopus (Rhizopus).
Embodiment 9
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22. the tobacco shred of step S21 shredding gained being carried out the process conditions of carbon dioxide expanding treatment described in carbon dioxide expanding treatment is: dip time 4min, expansion temperature 400 DEG C;
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid, it is thus achieved that fermentation taste, the tobacco shred after fermentation is carried out Crushing of Ultrafine, crosses 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 10g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Fermentation temperature is 40 DEG C, and the time is 14 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=80g:4g:0.3g:350g of distilled water;Described protein peptide is rice protein peptide.Described strain is Zygosaccharomyces rouxii (Mucorroxianus).
Embodiment 10
The present embodiment provides a kind of buccal cigarette, and this buccal cigarette is made up according to percentage by weight of following raw material: tobacco-containing material 80%;Filler 5%;Correctives 5%;Binding agent 9%;Essence 1%;Described tobacco-containing material is made up of embodiment 6 to 9 arbitrary example gained tobacco leaf granule and the arbitrary example gained cabo particle of embodiment 1 to 5, and wherein the mass ratio of tobacco leaf granule and cabo particle is 60%:40%.
Described filler is starch, and described correctives is Sal, and described binding agent is sodium carboxymethyl cellulose, and described essence is menthol.
The preparation method of described buccal cigarette is as follows:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cut growth is square on request or other shapes, such as Nicotiana tabacum L. shape etc..
The thickness of diaphragm described in step S2 is 0.1~1mm.
Described baking is to toast 1~2 hour at 40~60 DEG C.
Embodiment 11
The present embodiment provides a kind of buccal cigarette, and this buccal cigarette is made up according to percentage by weight of following raw material: tobacco-containing material 85%;Filler 3%;Correctives 1.5%;Binding agent 10%;Essence 0.5%;Described tobacco-containing material is made up of embodiment 6 to 9 arbitrary example gained tobacco leaf granule and the arbitrary example gained cabo particle of embodiment 1 to 5, and wherein the mass ratio of tobacco leaf granule and cabo particle is 80%:20%.
Described filler is maltodextrin, and described correctives is sodium carbonate, and described binding agent is ethyl cellulose, and described essence is Folium Camelliae sinensis extract.
The preparation method of described buccal cigarette is as follows:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.Described cutting can be cut into rectangle or other shapes, such as Nicotiana tabacum L. shape etc..
The thickness of diaphragm described in step S2 is 0.1~1mm.
Described baking is to toast 1~2 hour at 40~60 DEG C.
Embodiment 12
Tobacco material 80~95%, filler 1~5%, correctives 0.5~5%, binding agent 1~10% and essence 0.1~1%;
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is made up of according to percentage by weight following raw material: tobacco-containing material 95%;Filler 1%;Correctives 0.5%;Binding agent 3%;Essence 0.5%;Described tobacco-containing material is made up of embodiment 6 to 9 arbitrary example gained tobacco leaf granule and the arbitrary example gained cabo particle of embodiment 1 to 5, and wherein the mass ratio of tobacco leaf granule and cabo particle is 70%:30%.
Described filler is cyclodextrin, and described correctives is sodium benzoate, and described binding agent is gelatin, and described essence is Fructus Armeniacae Mume extract.
The preparation method of described buccal cigarette is as follows:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.Described cutting can be cut into rectangle or other shapes, such as Nicotiana tabacum L. shape etc..
The thickness of diaphragm described in step S2 is 0.1~1mm.
Described baking is to toast 1~2 hour at 40~60 DEG C.
Embodiment 13
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is made up of according to percentage by weight following raw material: tobacco-containing material 90%;Filler 2%;Correctives 2%;Binding agent 5%;Essence 1%;Described tobacco-containing material is made up of embodiment 6 to 9 arbitrary example gained tobacco leaf granule and the arbitrary example gained cabo particle of embodiment 1 to 5, and wherein the mass ratio of tobacco leaf granule and cabo particle is 65%:35%.
Described filler is starch and white sugar mixture (mixing quality ratio 1:1), and wherein white sugar is simultaneously as binding agent, and described correctives is Sal, and described essence is menthyl acetate.
The preparation method of described buccal cigarette is as follows:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.Described cutting can be cut into rectangle or other shapes, such as Nicotiana tabacum L. shape etc..
The thickness of diaphragm described in step S2 is 0.1~1mm.
Described baking is to toast 1~2 hour at 40~60 DEG C.
Embodiment 14
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is made up of according to percentage by weight following raw material: tobacco-containing material 95%;Filler 1%;Correctives 1%;Binding agent 2.5%;Essence 0.5%;Described tobacco-containing material is made up of embodiment 6 to 9 arbitrary example gained tobacco leaf granule and the arbitrary example gained cabo particle of embodiment 1 to 5, and wherein the mass ratio of tobacco leaf granule and cabo particle is 70%:30%.
Described filler is mannitol, and described correctives is Sal, and described binding agent is white sugar, and described essence is Borneolum Syntheticum.
The preparation method of described buccal cigarette is as follows:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.Described cutting can be cut into rectangle or other shapes, such as Nicotiana tabacum L. shape etc..
The thickness of diaphragm described in step S2 is 0.1~1mm.
Described baking is to toast 1~2 hour at 40~60 DEG C.
Embodiment 15 detection and experiment of smokeing panel test
The product that Example 1 to embodiment 14 any embodiment prepares, is packaged as sheet form by the specification of 0.3g/ sheet.
The mensuration of content of nitrite: the chromatography of ions (mensuration of NY/T1375-2007 plant product nitrite and nitrate);The mensuration of protein content: Ke Daerfa (mensuration of YCT166-2003 Nicotiana tabacum L. and tobacco product total protein content);The mensuration of content of cellulose: enzymolysis-flow analysis (list of references: Guo Song. China examines cigarette Nicotiana tabacum L. pectin, content of cellulose characteristic distributions and impact [D] Henan on reviewing prnciple: Agricultural University Of He'nan, and 2011,18~19);The mensuration of pectin content: the chromatography of ions (the mensuration chromatography of ions of YC/T346-2010 Nicotiana tabacum L. and tobacco product pectin);The mensuration of content of cellulose: enzyme hydrolysis-chromatography of ions (YC/T283-2009 Nicotiana tabacum L. and tobacco product. the mensuration of starch. enzyme hydrolysis-chromatography of ions);The mensuration of content of lignin: sulfuric acid process (list of references: Tao Yongzhen, Guan Yingting. the chemical constitution of lignin and application [J] thereof. Cellulose Science and technology, 2003,11 (1): 43-55).
Through inspection, the content of nitrite of embodiment 1 to 14 products obtained therefrom is all between 1.25~1.30%, and protein content is all between 8.9~9.0%, and content of cellulose is all between 8.65~8.89%, and pectin content is all between 12.3~12.5%.
Ask 10 experts that smoke panel test to carry out experiment of smokeing panel test the product that the embodiment of the present invention 1~14 prepares simultaneously.Smoke panel test method for directly to insert between upper lip and upper row's tooth by product, and the tobacco shred granular mass every time putting into lip is 0.2g, and standard edible time is decided to be 10min.The entirety of embodiment 1 to 14 effect of smokeing panel test is that bitter taste and acid are all relatively lighter, very agreeable to the taste.
The smoking result of embodiment 1 to 14 products obtained therefrom is shown in Table 1.Scoring criterion is, the alkali rate of release of buccal cigarette, sucks early stage and later stage strength, compliance (the below standard quasi-edible time of buccal cigarette edible time is considered as poor compliance by discharge), local flavor, fragrance, pleasant impression respectively account for 10 points, total score 70 points.Comparative example 1 is the sample that 160 mesh sieves are crossed in unprocessed cabo shredding, and comparative example 2 is the sample that 160 mesh sieves are crossed in unprocessed cabo shredding.
Table 1 is smoked panel test result of the test
Sample Suck early stage strength Suck later stage strength Compliance Local flavor Fragrance Pleasant impression Total score
Comparative example 1 Weak Weak 4 10 20 10 44
Comparative example 2 By force Weak 5 15 25 15 60
Embodiment 1 Weak Weak 7 15 28 20 70
Embodiment 2 Weak Weak 7 16 28 22 73
Embodiment 3 Weak Weak 7 16 28 21 72
Embodiment 4 Weak Weak 8 16 27 22 73
Embodiment 5 Weak Weak 7 15 27 21 70
Embodiment 6 By force Weak 8 16 30 24 78
Embodiment 7 By force Weak 8 16 32 24 80
Embodiment 8 By force Weak 8 16 33 24 81
Embodiment 9 By force Weak 8 16 34 25 83
Embodiment 10 In In 8 16 34 24 82
Embodiment 11 In In 8 17 32 25 82
Embodiment 12 In In 8 17 33 24 82
Embodiment 13 In In 8 17 33 25 83
Embodiment 14 In In 8 17 33 25 83
The invention provides a kind of new buccal cigarette material, each component of following mass ratio prepare: tobacco material 80~95%, filler 1~5%, correctives 0.5~5%, binding agent 1~10% and essence 0.1~1%.Described buccal cigarette material is made up of according to the mass ratio mixing of 60~80%:40~20% tobacco leaf granule and cabo particle, tobacco leaf granule and cabo particle be adopt Nicotiana tabacum L. or cabo respectively fermented wait the laggard row Crushing of Ultrafine of process after sieve, take permeation parts and get final product.The process of science of the present invention eliminates bitter taste and the acid of Nicotiana tabacum L., fragrance matter is enriched mellow, by itself and the collocation of adjuvant science, the seasoning carrying out reasonable benefit/risk processes, it is thus achieved that a kind of new buccal cigarette material, mouthfeel is more abundant, flavor coordination, quality are high, can by gradually containing change when edible, without granular sensation, harsh feeling in oral cavity, edible end abandons without spuing, apply cabo in large quantities simultaneously, improve tobacco material utilization rate in preparation buccal cigarette.
The present invention is vast scale use tobacco material in the preparation of buccal cigarette not only, ensure that the usage ratio of tobacco material is minimum and be not less than 80%, up to 95%, but the quality such as the overall taste flavor of buccal cigarette are well ensured, and tobacco-containing material used includes significant percentage of cabo, " this change of cigarette " for buccal cigarette provides technical support, solves cabo application problem in buccal cigarette well, improves tobacco material utilization rate in buccal cigarette.
The buccal cigarette of the present invention is uniform sheet form, can in the oral cavity quickly containing change, and instant also can be completely edible, will not to environment.

Claims (10)

1. the buccal cigarette adopting vast scale tobacco-containing material, it is characterised in that prepared by each component of following mass ratio: tobacco material 80~95%, filler 1~5%, correctives 0.5~5%, binding agent 1~10% and essence 0.1~1%;
Described tobacco material is made up of according to the mass ratio mixing of 60~80%:40~20% tobacco leaf granule and cabo particle;
Described cabo particle is prepared by following steps:
S11. cabo is carried out wind to wash to remove surface dust, then through shredding after microwave bulking;
S12. the stem cut by step S11 carries out fermentation process;
S13. the stem fermented by step S12 carries out micronizing, sieves and obtains described cabo particle;
Described tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding;
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment;
S22. step S21 shredding gained tobacco shred is carried out fermentation process;Sieve after the tobacco shred Crushing of Ultrafine after fermentation, take permeation parts;
Wherein, fermentation processing method described in step S12 is: preparation inoculation liquid, be the inoculation after fermentation of 1~15g inoculation liquid/100g stem according to inoculum concentration, described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50~200) g:(0.1~10) g:(0.01~1) g:(100~500) g;
Fermentation described in step S23 is preparation inoculation liquid, is 1~15g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration;Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50~200) g:(0.1~10) g:(0.01~1) g:(100~500) g;
Described protein peptide be soybean protein peptide, wheat protein peptide, rice protein peptide, casein peptide, whey protein peptide one or more;
Described strain be monascus (MonascuspurpureusWent.), aspergillus oryzae (Aspergillusoryzae), Zygosaccharomyces rouxii (Mucorroxianus) or rhizopus (Rhizopus), yeast (Saccharomyces) or lactic acid bacteria (Lactobacillus) one or more.
2. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that the process conditions of microwave bulking described in step S11 are: cabo moisture content 14~18%, Bulking Time 45~75s, expands power 600~900W.
3. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that shredding described in step S11 is that cabo is cut to 0.5~5.0cm length, the uniform stem that 0.3~0.9mm is wide.
4. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that in the process of fermentation described in step S12, fermentation temperature is for 35~45 DEG C, and fermentation time is 10~30 days.
5. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that described in step 22, the process conditions of carbon dioxide expanding treatment are: dip time 1~5min, expansion temperature 300~400 DEG C.
6. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that in the process of described fermentation described in step 23, fermentation temperature is for 35~45 DEG C, and fermentation time is 7~30 days.
7. the buccal cigarette of employing vast scale tobacco-containing material according to claim 1, it is characterised in that described filler is one or more in starch, maltodextrin, cyclodextrin, microcrystalline Cellulose, white sugar, mannitol or xylitol;Described correctives is one or more of Sal, sodium carbonate or sodium benzoate etc.;Described binding agent is one or more in sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, gelatin or white sugar;Described essence is naturally occurring or synthetic perfume monomer, fruit extract or vegetable material extract.
8. the preparation method adopting the buccal cigarette of vast scale tobacco-containing material described in any one of claim 1 to 7, it is characterised in that comprise the following steps:
S1. the mixed dissolution in water by filler and binding agent, heating, stir, add tobacco-containing material and correctives, be stirred for 10~20 minutes, become pasty state;
S2. step S1 gained pasty state tobacco-containing material is sprayed to film forming on drying machine equably, after being toasted by film forming gained diaphragm, spray essence;
S3. excision forming: after the step S2 diaphragm cooling spraying essence, cutting obtains buccal cigarette on request.
9. the preparation method adopting the buccal cigarette of vast scale tobacco-containing material according to claim 8, it is characterised in that the thickness of diaphragm described in step S2 is 0.1~1mm.
10. the preparation method adopting the buccal cigarette of vast scale tobacco-containing material according to claim 8, it is characterised in that described baking is to toast 1~2 hour at 40~60 DEG C.
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