CN106579538B - A kind of packed buccal cigarette and preparation method thereof - Google Patents
A kind of packed buccal cigarette and preparation method thereof Download PDFInfo
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- CN106579538B CN106579538B CN201611153248.7A CN201611153248A CN106579538B CN 106579538 B CN106579538 B CN 106579538B CN 201611153248 A CN201611153248 A CN 201611153248A CN 106579538 B CN106579538 B CN 106579538B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 72
- 239000011669 selenium Substances 0.000 claims abstract description 51
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims abstract description 43
- 229910052711 selenium Inorganic materials 0.000 claims abstract description 43
- 239000000463 material Substances 0.000 claims abstract description 31
- 150000001875 compounds Chemical class 0.000 claims abstract description 30
- 241000196324 Embryophyta Species 0.000 claims abstract description 26
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 11
- 239000003765 sweetening agent Substances 0.000 claims abstract description 11
- 235000004256 Buglossoides arvense Nutrition 0.000 claims abstract description 10
- 240000004638 Dendrobium nobile Species 0.000 claims abstract description 10
- 240000006688 Telosma cordata Species 0.000 claims abstract description 10
- 235000017352 Telosma cordata Nutrition 0.000 claims abstract description 10
- 241001517310 Eria Species 0.000 claims abstract description 9
- 150000003839 salts Chemical class 0.000 claims abstract description 9
- 239000003607 modifier Substances 0.000 claims abstract description 7
- 239000002131 composite material Substances 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract description 3
- 241000208125 Nicotiana Species 0.000 claims abstract 20
- 241000118841 Lithospermum incisum Species 0.000 claims abstract 2
- 239000000843 powder Substances 0.000 claims description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000006228 supernatant Substances 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 17
- 239000000706 filtrate Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 14
- FXFYOPQLGGEACP-UHFFFAOYSA-N 6-methylcoumarin Chemical compound O1C(=O)C=CC2=CC(C)=CC=C21 FXFYOPQLGGEACP-UHFFFAOYSA-N 0.000 claims description 12
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 claims description 12
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 claims description 12
- 239000000047 product Substances 0.000 claims description 12
- 235000012907 honey Nutrition 0.000 claims description 10
- 239000012535 impurity Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 10
- 239000000779 smoke Substances 0.000 claims description 10
- 238000012545 processing Methods 0.000 claims description 9
- 238000005119 centrifugation Methods 0.000 claims description 8
- 239000002002 slurry Substances 0.000 claims description 8
- 108090000790 Enzymes Proteins 0.000 claims description 7
- 102000004190 Enzymes Human genes 0.000 claims description 7
- 229940088598 enzyme Drugs 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- MOMFXATYAINJML-UHFFFAOYSA-N 2-Acetylthiazole Chemical group CC(=O)C1=NC=CS1 MOMFXATYAINJML-UHFFFAOYSA-N 0.000 claims description 6
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 claims description 6
- 229960001867 guaiacol Drugs 0.000 claims description 6
- RHDGNLCLDBVESU-UHFFFAOYSA-N but-3-en-4-olide Chemical compound O=C1CC=CO1 RHDGNLCLDBVESU-UHFFFAOYSA-N 0.000 claims description 5
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 5
- 239000002689 soil Substances 0.000 claims description 5
- 230000001954 sterilising effect Effects 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 230000000813 microbial effect Effects 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical group O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 4
- 239000001509 sodium citrate Substances 0.000 claims description 4
- 235000011083 sodium citrates Nutrition 0.000 claims description 4
- -1 that is Substances 0.000 claims description 4
- KSDSYIXRWHRPMN-UHFFFAOYSA-N 4'-O-beta-D-Galactopyranoside-6''-p-Coumaroylprunin-4',5,7-Trihydroxyflavanone Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(C2OC3=CC(O)=CC(O)=C3C(=O)C2)C=C1 KSDSYIXRWHRPMN-UHFFFAOYSA-N 0.000 claims description 3
- 108010059892 Cellulase Proteins 0.000 claims description 3
- DEMKZLAVQYISIA-ONJCETCRSA-N Liquiritin Natural products O([C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)c1ccc([C@@H]2Oc3c(C(=O)C2)ccc(O)c3)cc1 DEMKZLAVQYISIA-ONJCETCRSA-N 0.000 claims description 3
- DEMKZLAVQYISIA-UHFFFAOYSA-N Liquirtin Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(C2OC3=CC(O)=CC=C3C(=O)C2)C=C1 DEMKZLAVQYISIA-UHFFFAOYSA-N 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- DEMKZLAVQYISIA-ZRWXNEIDSA-N liquiritin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C([C@H]2OC3=CC(O)=CC=C3C(=O)C2)C=C1 DEMKZLAVQYISIA-ZRWXNEIDSA-N 0.000 claims description 3
- GSZUGBAEBARHAW-UHFFFAOYSA-N sophoraflavone B Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(C=2OC3=CC(O)=CC=C3C(=O)C=2)C=C1 GSZUGBAEBARHAW-UHFFFAOYSA-N 0.000 claims description 3
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 claims description 2
- 241000193830 Bacillus <bacterium> Species 0.000 claims description 2
- 241000235342 Saccharomycetes Species 0.000 claims description 2
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims description 2
- 229960004998 acesulfame potassium Drugs 0.000 claims description 2
- 235000010358 acesulfame potassium Nutrition 0.000 claims description 2
- 239000000619 acesulfame-K Substances 0.000 claims description 2
- 235000019262 disodium citrate Nutrition 0.000 claims description 2
- 239000002526 disodium citrate Substances 0.000 claims description 2
- 229940079896 disodium hydrogen citrate Drugs 0.000 claims description 2
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 2
- 229940013618 stevioside Drugs 0.000 claims description 2
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims description 2
- 235000019202 steviosides Nutrition 0.000 claims description 2
- 108091005804 Peptidases Proteins 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 239000004365 Protease Substances 0.000 claims 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims 1
- 241000209140 Triticum Species 0.000 claims 1
- 235000021307 Triticum Nutrition 0.000 claims 1
- 238000007598 dipping method Methods 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 10
- 239000012530 fluid Substances 0.000 abstract description 6
- 239000003205 fragrance Substances 0.000 abstract description 6
- 230000001737 promoting effect Effects 0.000 abstract description 6
- 235000019505 tobacco product Nutrition 0.000 abstract description 4
- 239000011573 trace mineral Substances 0.000 abstract description 4
- 235000013619 trace mineral Nutrition 0.000 abstract description 4
- 230000004927 fusion Effects 0.000 abstract description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 52
- 244000157790 Buglossoides arvense Species 0.000 description 8
- 210000000214 mouth Anatomy 0.000 description 8
- 230000036541 health Effects 0.000 description 6
- 239000002585 base Substances 0.000 description 5
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 229940093503 ethyl maltol Drugs 0.000 description 4
- 210000004072 lung Anatomy 0.000 description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000011630 iodine Substances 0.000 description 3
- 229910052740 iodine Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 241000205585 Aquilegia canadensis Species 0.000 description 1
- 244000012254 Canarium album Species 0.000 description 1
- 235000009103 Canarium album Nutrition 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000276331 Citrus maxima Species 0.000 description 1
- 235000001759 Citrus maxima Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 241000675108 Citrus tangerina Species 0.000 description 1
- 241000721047 Danaus plexippus Species 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- 244000061508 Eriobotrya japonica Species 0.000 description 1
- 235000009008 Eriobotrya japonica Nutrition 0.000 description 1
- 241000935235 Fritillaria meleagris Species 0.000 description 1
- 235000013717 Houttuynia Nutrition 0.000 description 1
- 240000000691 Houttuynia cordata Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 235000003283 Pachira macrocarpa Nutrition 0.000 description 1
- 102000003992 Peroxidases Human genes 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 240000001085 Trapa natans Species 0.000 description 1
- 235000014364 Trapa natans Nutrition 0.000 description 1
- 230000004308 accommodation Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000002457 bidirectional effect Effects 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229940043353 maltol Drugs 0.000 description 1
- 231100000299 mutagenicity Toxicity 0.000 description 1
- 230000007886 mutagenicity Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 108040007629 peroxidase activity proteins Proteins 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000009165 saligot Nutrition 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 238000002054 transplantation Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention provides a kind of packed buccal cigarette and preparation method thereof.Compound plant and selenium-rich tobacco leaf are uniformly mixed by the packed buccal cigarette to be placed in sealing oak barrel, it it is 25 35 DEG C in temperature, humidity is adds in salt, the base-material that acid-base modifier, sweetener addition have been refined after alcoholization 30d 60d for composite under conditions of 60% 80%, then with 100 110 DEG C of 20 40min of steam treatment, after base-material cooling, it is proportionally added into essence, adjusts humidity as 15% 50%, then packed.The compound plant is made of dark plum, Radix Sangusorbae, kuh-seng, Asian puccoon, spina gleditsiae, the hook stem of noble dendrobium, grassleaf eria herb and Chinese violet, and the selenium-rich tobacco leaf is the tobacco leaf of 0.3 0.8mg/kg of blade selenium content.The present invention forms various forms of packed mouth containing tobacco products using the compound alcoholization of oak barrel and component collocation mixing, and not only fragrance fusion is preferable, jealous coordination, comfortable taste, while also provides the essential trace elements of the human body, and also has effects that clearing heat and promoting fluid.
Description
Technical field
The invention belongs to smoke-free tobacco product and its processing technique field, and in particular to a kind of packed buccal cigarette and its system
Preparation Method.
Background technology
Selenium is teleorganic trace element, is known as in body trace element " king of anticancer " by scientist, is human body paddy
Guang (sweet peptide peroxidase GSH-Px) important activity component, plays the role of removing interior free yl；With removing toxic substances, toxin expelling,
It is anti-aging, anti-oxidant, the effect of immunity is improved, selenium can play in human body reduces gene mutagenicity, the work of DNA plerosis
With.Meanwhile selenium can reduce the toxicity of nicotine and tar, suppression is played to tumour, there is resistance to a variety of carcinogens in flue gas
Effect；At present also studies have reported that suction iodine enriched cigarette can make human body blood selenium level relatively aspirate regular-size cigarette human body blood selenium level
It is high by 10%.So people also begin to research iodine enriched cigarette, existing iodine enriched cigarette is substantially the cigarette of suction, although can also
Increase the content of human body selenium, but since tobacco leaf needs to burn, still can produce substantial amounts of flue gas, danger is brought to health
Evil.
Packed buccal cigarette belongs to a kind of form of smoke-free tobacco product, is used, had between lip and gum by being put in
It need not burn, not produce secondhand smoke harm, received by more and more consumers.Since buccal cigarette is unlike traditional cigarette
Equally participate in burning, therefore can be theoretical by Chinese medicine scientific compatibility according to " monarch " of the traditional Chinese medical science, make it have certain control
Treatment and health-care effect.105054279 A of Chinese patent CN disclose a kind of selenium-rich buccal cigarette and preparation method thereof, in the patent
Buccal cigarette in selenium source mostly come from chemicals k-selenocarrageenan, be not very healthy, and can not play health care work
With.Although also there is the buccal cigarette of some health-care types, such as a kind of river production characteristic food disclosed in Chinese patent CN 105124748A
The moistening lung and nourishing throat health buccal cigarette produced, is to produce the river based on shaddock, pears, lotus rhizome, sugarcane, water chestnut, cordate houttuynia and loquat
Characteristic food and tobacco extract compatibility, the method for preparing moistening lung and nourishing throat health buccal cigarette.Chinese patent CN104997153A
The moistening lung and nourishing throat health buccal cigarette that a kind of river production Special Traditional Chinese Medicine is produced is disclosed, is with tobacco extract and radix scutellariae, Chinese olive, tangerine
The method that the extract of river production Special Traditional Chinese Medicine based on stalk, tendril-leaved fritillary bulb and honeysuckle prepares moistening lung and nourishing throat health buccal cigarette.These
Buccal cigarette is all directly by food or Chinese medicine together with common tobacco compatibility, and health effect is not fine, and
Do not play the role of supplementing human body selenium source.
The content of the invention
For the above situation, the present invention provides a kind of packed buccal cigarette and preparation method thereof, which is planted using natural
The technique such as thing compatibility, compound alcoholization, prepares the pure ecological selenium-rich mouth containing smoke product that outlet plenum is comfortable, fragrance is coordinated.
The technical solution adopted by the present invention is as follows：A kind of packed buccal cigarette, it is characterised in that be by following weight hundred
Divide the material composition of ratio：
The total weight percent of above-mentioned substance is 100%.
Wherein：The compound plant is by the material composition of following percentage by weight：Dark plum 10%-20%, Radix Sangusorbae
5%-10%, kuh-seng 1%-5%, Asian puccoon 15%-25%, spina gleditsiae 5%-10%, hook stem of noble dendrobium 15%-20%, grassleaf eria herb
6%-12%, Chinese violet 7%-15%；
The selenium-rich tobacco leaf is the tobacco leaf of blade Se content 0.3-0.8mg/kg；
The essence is the material composition of following percentage by weight：Burley tobaccos absolute oil 0.5%-1%, yunyan extract 0.8-
2%th, honey 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethylmaltol 0.3%-
0.7%th, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, surplus are propane diols；Thing in above-mentioned essence
Matter is the product directly bought；
The sweetener is non-sugar sweetener；
The water is the water content of the final products prepared in all materials by processing, is 15%-50%.
The further technical solution of the present invention：The acid-base modifier is sodium citrate or DisodiumHydrogen Citrate.It is described
Non-sugar sweetener includes a kind of in liquiritin, honey element, stevioside or acesulfame potassium or any several mixing.The acid-base accommodation
Agent and sweetener are the product directly bought.The selenium-rich tobacco leaf is the life in selenium-rich soil of bestowing favour by Flue-cured Tobacco transplantation of seedlings
The long cured tobacco leaf formed, the soil Se content of its planting site are more than 0.45mg/kg, altitude 800-1000m；Selenium-rich cigarette can
With direct using natural selenium-rich cigarette " Qing Jiangyuan " tobacco leaf of bestowing favour.
The present invention preferably technical solution：The burley tobaccos absolute oil is using burley tobacco leaf as raw material, by tobacco leaf and concentration
20% ethanol mass ratio is 1：The ratio mixing of 3-20, when agitating and heating reflux extraction 1-10 is small at a temperature of 110 ± 5 DEG C, drop
Clarified when standing 1-3 is small after to room temperature, extract supernatant；By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and will filter
Liquid is poured into Rotary Evaporators after merging with supernatant and is concentrated to give under conditions of 60 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To thick liquid be burley tobaccos extract；Then burley tobaccos are carried with 95% ethanol of concentration according to mass ratio 1：The ratio of 3-20
Example mixing, standing 1-3 are clarified when small, extract supernatant, reject dregs after lower floor's slurry centrifugation, collect filtrate, and and supernatant
Liquid pours into Rotary Evaporators after merging and is concentrated into relative density under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
0.9-1.3g/cm3Obtain burley tobaccos absolute oil.
A kind of packed buccal cigarette preparation method provided by the invention, it is characterised in that processing method is as follows：
(1) compound plant raw material is prepared according to the formula of following percentage by weight：Dark plum 10%-20%, Radix Sangusorbae 5%-
10%, kuh-seng 1%-5%, Asian puccoon 15%-25%, spina gleditsiae 5%-10%, hook stem of noble dendrobium 15%-20%, grassleaf eria herb 6%-
12%, Chinese violet 7%-15%；Crushed after above-mentioned raw materials are individually removed impurity, retain powder more than 80 mesh and then mix
It is configured to compound plant powder；Or remove impurity after above-mentioned raw materials are mixed and crushed again, retain powder more than 80 mesh and obtain
Compound plant powder；
(2) burley tobaccos absolute oil is prepared：
A. using burley tobacco leaf as raw material, after being crushed and 20% ethanol of concentration is according to mass ratio 1：3-20 is mixed, 110
When agitating and heating reflux extraction 1-10 is small at a temperature of ± 5 DEG C, be cooled to room temperature stand 1-3 it is small when clarify, extract supernatant；
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with
The supernatant collected in step a merges, and then pours into the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum
It is burley tobaccos extract more than thick liquid is concentrated under conditions of 0.95Mpa；
C. burley tobaccos absolute oil is prepared：By burley tobaccos extract in step b and 95% ethanol of concentration according to mass ratio 1：3-20
Ratio mixing, stand 1-3 it is small when clarify, extract supernatant；By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and
Poured into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil；
(3) essence is prepared according to the formula of following percentage by weight：The burley tobaccos absolute oil 0.5%- prepared in step (2)
1%th, yunyan extract 0.8-2%, honey 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%,
Ethylmaltol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, surplus are the third two
Alcohol；Above-mentioned raw materials are uniformly mixed and are configured to essence；
(4) raw material of buccal cigarette is prepared according to formula as below：The middle compound plant powder prepared of 10%-30% steps (1),
Essence, 0.1%-2% salt, the 0.5%-1% acid prepared in the step of selenium-rich tobacco leaf of 30%-60%, 0.1%-4% (1)
Alkali conditioning agent, 0.5%-1.5% sweeteners, excess water；
(5) by the flexibility wind election process of whole selenium-rich tobacco leaf pickings in step (4), the impurity in material, Ran Houzai are removed
Pulverization process is carried out, retains powder, that is, selenium-rich tobacco leaf powder more than 80 mesh；The flexibility wind election process is existing process, its work
Skill principle be by the tobacco leaf cut tobacco after pneumatic conveying drying by feeding mechanism be sent into selection by winnowing babinet after free-falling, using babinet vertically and
Horizontal bidirectional inlet air carries out float choosing and flotation to cut tobacco, makes the larger object of density such as impurity, stalk label etc. by secondary separation case
Body is fallen, and the lighter cut tobacco of density will send out babinet by discharging mechanism, so as to fulfill the dedoping step of material；
(6) the selenium-rich tobacco leaf powder in the compound plant powder in step (4) and step (5) is uniformly mixed, is placed in sealing
It it is 25-35 DEG C in temperature, humidity is alcoholization 30d-60d for composite under conditions of 60%-80% in oak barrel；
(7) after the compound alcoholization in step (6), the base-material after compound alcoholization is taken out, according to the ratio in step (4)
Salt, acid-base modifier, sweetener are added, 100-110 DEG C of steam treatment 20-40min is then used under closed environment；
(8) after the cooling of above-mentioned base-material, essence is added in the ratio in step (4), adjusting humidity is 15%-50%, so
Laggard luggage bag, and obtain packed mouth containing smoke product after sterilization processing；Constant temperature can be placed directly in by adjusting the mode of humidity
In the system of constant humidity, adjusting temperature is room temperature, and humidity carries out damp condition for required humidity；Can also the excessive use of humidity
Drying unit is carried out to reduce moisture, and humidity is too low can to spray a certain amount of water, to increase humidity；
The present invention preferably technical solution：Oak is placed in compound plant powder and selenium-rich tobacco leaf the powder mixing of step (6)
Bucket in do not refined before, into base-material sprinkling account for base-material weight 0.5%-5% enzyme solutions microbial solution or its
Mixture, is placed in oak barrel is refined after mixing again；The enzyme solutions are cellulase, pectase, protein
A kind of or its mixture in enzyme, the microbial solution is saccharomycete, a kind of or its mixture in bacillus.
The present invention is using the compound technique of refining of oak barrel by the natural plant powder with clearing heat and promoting fluid and the " Qingjian River
Source " selenium-rich tobacco leaf powder compatibility processing, further includes suitable essence, salt, acid-base modifier, sweetener, by above-mentioned compound
Refine technique and component collocation mixing forms various forms of packed mouth containing tobacco products, not only fragrance fusion is preferable, jealous coordination,
Comfortable taste, while the essential trace elements of the human body is also provided, and also there is clearing heat and promoting fluid.
Embodiment
The technical solution in the present invention is clearly and completely described below by specific embodiment.It should be appreciated that
The described specific embodiment in this part can only be used to explain the present invention, be not intended to limit the present invention.
Burley tobaccos absolute oil in following embodiments is prepared in accordance with the following methods：
A. using burley tobacco leaf as raw material, after being crushed and 20% ethanol of concentration is according to mass ratio 1：3-20 is mixed, 110
When agitating and heating reflux extraction 1-10 is small at a temperature of ± 5 DEG C, be cooled to room temperature stand 1-3 it is small when clarify, extract supernatant；
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with
The supernatant collected in step a merges, and then pours into the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum
It is burley tobaccos extract more than thick liquid is concentrated under conditions of 0.95Mpa；
C. burley tobaccos absolute oil is prepared：By burley tobaccos extract in step b and 95% ethanol of concentration according to mass ratio 1：3-20
Ratio mixing, stand 1-3 it is small when clarify, extract supernatant；By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and
Poured into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil；
The selenium-rich tobacco leaf in following embodiments, should using " Qing Jiangyuan " pure ecological selenium-rich tobacco leaf of bestowing favour is originated in
Tobacco leaf is that tobacco seedlings are transplanted to the position of the height above sea level 800-1000m that bestows favour, soil Se content more than 0.45mg/kg normally to plant out
The selenium-rich cigarette come, selenium-rich Tobacco Leaves Se content 0.3-0.8mg/kg, need not additionally apply selenium element in planting process.
Embodiment 1, a kind of packed buccal cigarette, its specific preparation method are as follows：
Take dark plum, Radix Sangusorbae, kuh-seng, Asian puccoon, spina gleditsiae, the hook stem of noble dendrobium, grassleaf eria herb, Chinese violet and blade Se content
0.3-0.8mg/kg selenium-rich tobacco leaves, using flexible wind election process, remove the impurity in material, are then crushed respectively again
Processing, retains powder more than 80 mesh, by plant powder dark plum 20% by weight percentage, Radix Sangusorbae 10%, and kuh-seng 2%,
Asian puccoon 20%, spina gleditsiae 8%, the hook stem of noble dendrobium 15%, grassleaf eria herb 10%, the compounding of Chinese violet 15% obtain compound plant powder,
Then take compound plant powder 2000g and selenium-rich tobacco leaf powder 4000g to be uniformly mixed, be placed in sealing oak barrel, be in temperature
30 DEG C, humidity is alcoholization 50d for composite under conditions of 70%；Compound base-material after purification is taken out, adds salt 100g, lemon
Sour disodium hydrogen 70g, liquiritin 100g are uniformly mixed, and are placed in sealing container, are passed through 100-110 DEG C of steam treatment 15min, so
Adding 200g essence in backward mixed resin, (essence is formulated by the material of following percentage by weight：Burley tobaccos are net
Oil 0.8%, yunyan extract 1%, honey 2%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%,
2- acetyl group pyrazine 0.1%, furanone 0.05%, propane diols 95.05%), its moisture 35.3% is adjusted, finally will be above-mentioned
Material carries out pack processing, and carries out ultraviolet sterilization, up to packed mouth containing smoke product.
Embodiment 2, a kind of packed buccal cigarette, its specific preparation method are as follows：Take dark plum, Radix Sangusorbae, kuh-seng, Asian puccoon, soap
Angle thorn, the hook stem of noble dendrobium, grassleaf eria herb, Chinese violet and blade Se content 0.3-0.8mg/kg selenium-rich tobacco leaves, using flexible selection by winnowing work
Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder
Dark plum 10% by weight percentage, Radix Sangusorbae 10%, kuh-seng 5%, Asian puccoon 25%, spina gleditsiae 10%, the hook stem of noble dendrobium 20%, standing grain leaf
Black dry measure used in former times 10%, the compounding of Chinese violet 10% obtain compound plant powder, then take compound plant 1500g, selenium-rich cigarette 5000g to mix
Uniformly, alcoholization for composite 40 days in sealing oak barrel are placed in the environment of 25 DEG C of temperature, humidity 65%, after taking out alcoholization
Base-material, adds salt 100g, sodium citrate 70g, honey element 100g, then with 100-110 DEG C of vapor under closed environment
Manage 20min, then into mixed resin add 150g essence, (essence be by following percentage by weight material prepare and
Into：Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, honey 2.5%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, second
Base maltol 0.5%, 2- acetyl group pyrazine 0.1%, furanone 0.05%, propane diols 94.05%), adjust moisture
30.8%, above-mentioned material is finally subjected to pack processing, and ultraviolet sterilization is carried out, up to packed mouth containing smoke product.
Embodiment 3, a kind of packed buccal cigarette, its specific preparation method are as follows：Take dark plum, Radix Sangusorbae, kuh-seng, Asian puccoon, soap
Angle thorn, the hook stem of noble dendrobium, grassleaf eria herb, Chinese violet and blade Se content 0.3-0.8mg/kg selenium-rich tobacco leaves, using flexible selection by winnowing work
Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder
Dark plum 10% by weight, Radix Sangusorbae 10%, kuh-seng 5%, Asian puccoon 25%, spina gleditsiae 10%, the hook stem of noble dendrobium 20%, grassleaf eria herb
10%, the compounding of Chinese violet 10% obtains compound plant powder, then takes compound plant 1000g, selenium-rich cigarette 5000g mixing equal
It is even, into base-material spray solution dosage account for base-material weight 1% complex enzyme (complex enzyme be by pectase and cellulase by
According to weight ratio 1:1 ratio mixes), alcohol for composite in oak barrel is placed in the environment of 25 DEG C of temperature, humidity 65%
Change 40 days, take out the base-material refined, add salt 100g, sodium citrate 70g, honey element 100g after mixing, be placed in close
Seal in container, 100-110 DEG C of steam treatment 20min is passed through into container, 200g essence (institute is then added into mixed resin
Stating essence is formulated by the material of following percentage by weight：Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, honey
2.5%th, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%, 2- acetyl group pyrazine 0.1%, furans
Ketone 0.05%, propane diols 94.05%), moisture 35.3% is adjusted, above-mentioned material is finally subjected to pack processing, and carry out
Ultraviolet sterilization, up to packed mouth containing smoke product.
The mouth containing smoke product prepared in three embodiments is smoked panel test by the group of smokeing panel test of specialty, its smoking result is such as
Shown in table 1：
Table 1 sucks smoke product effect assessment
| Suck smoke product | Evaluation effect |
| Embodiment 1 | Fragrance is preferable, jealous general, has certain stimulation to oral cavity, clearing heat and promoting fluid effect is preferable |
| Embodiment 2 | Fragrance is elegant, jealous coordination, smaller to oral stimulation, and clearing heat and promoting fluid effect is preferable |
| Embodiment 3 | Fragrance is elegant, jealous coordination, smaller to oral stimulation, and clearing heat and promoting fluid effect is preferable |
Claims (3)
1. a kind of preparation method of packed buccal cigarette, it is characterised in that comprise the following steps that：
(1) compound plant raw material is prepared according to formula as below：Dark plum 10%-20%, Radix Sangusorbae 5%-10%, kuh-seng 1%-5%,
Asian puccoon 15%-25%, spina gleditsiae 5%-10%, hook stem of noble dendrobium 15%-20%, grassleaf eria herb 6%-12%, Chinese violet 7%-
15%；Crushed after above-mentioned raw materials are individually removed impurity, retain powder more than 80 mesh and be then hybridly prepared into compound plant powder；
Or remove impurity after above-mentioned raw materials are mixed and crushed again, retain powder more than 80 mesh and obtain compound plant powder；
(2) burley tobaccos absolute oil is prepared：
A. using burley tobacco leaf as raw material, after being crushed and 20% ethanol of concentration is according to mass ratio 1：3-20 is mixed, 110 ± 5
When agitating and heating reflux extraction 1-10 is small at a temperature of DEG C, be cooled to room temperature stand 1-3 it is small when clarify, extract supernatant；
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate and step
The supernatant collected in a merges, and then pours into Rotary Evaporators the filtrate of merging and is more than in 60 ± 2 DEG C of temperature, vacuum
It is burley tobaccos extract that thick liquid is concentrated under conditions of 0.95Mpa；
C. burley tobaccos absolute oil is prepared：By burley tobaccos extract in step b and 95% ethanol of concentration according to mass ratio 1：The ratio of 3-20
Example mixing, standing 1-3 are clarified when small, extract supernatant；By reject dregs after the centrifugation of lower floor slurry, collect filtrate, and with it is upper
Clear liquid pours into relatively close more than being concentrated under conditions of 0.95Mpa in 50 ± 2 DEG C of temperature, vacuum in Rotary Evaporators after merging
Spend 0.9-1.3g/cm3Obtain burley tobaccos absolute oil；
(3) essence is prepared according to the formula of following percentage by weight：Burley tobaccos absolute oil 0.5%-1%, the cloud prepared in step (2)
Smoke-dipping paste 0.8-2%, honey 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethyl wheat
Bud phenol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, surplus are propane diols；Will be upper
State raw material and be uniformly mixed and be configured to essence；
(4) raw material of buccal cigarette is prepared according to the formula of following percentage by weight：The compound prepared in 10%-30% steps (1)
Essence, 0.1%-2% salt, the 0.5%- prepared in Plant Powder, the selenium-rich tobacco leaf of 30%-60%, 0.1%-4% steps (1)
1% acid-base modifier, 0.5%-1.5% sweeteners, excess water；The selenium-rich tobacco leaf is blade Se content 0.3-0.8mg/kg
Tobacco leaf；The acid-base modifier is sodium citrate or DisodiumHydrogen Citrate；The sweetener include liquiritin, honey element,
A kind of or arbitrarily several mixing in stevioside, acesulfame potassium；
(5) by the flexibility wind election process of whole selenium-rich tobacco leaf pickings in step (4), the impurity in material is removed, is then carried out again
Pulverization process, retains powder, that is, selenium-rich tobacco leaf powder more than 80 mesh；
(6) the selenium-rich tobacco leaf powder in the compound plant powder in step (4) and step (5) is uniformly mixed, is placed in sealing oak
It it is 25-35 DEG C in temperature, humidity is alcoholization 30d-60d for composite under conditions of 60%-80% in bucket；
(7) after the compound alcoholization in step (6), the base-material after compound alcoholization is taken out, is added according to the ratio in step (4)
Salt, acid-base modifier, sweetener, then use 100-110 DEG C of steam treatment 20-40min under closed environment；
(8) after the cooling of above-mentioned base-material, essence is added in the ratio in step (4), adjusting humidity is 15%-50%, Ran Houjin
Luggage bag, and obtain packed mouth containing smoke product after sterilization processing.
A kind of 2. preparation method of packed buccal cigarette according to claim 1, it is characterised in that the richness in the step (4)
Selenium tobacco leaf is the tobacco leaf for growing tobacco seedlings transplanting in selenium-rich soil of bestowing favour, and the soil Se content of its planting site is more than
0.45mg/kg, altitude 800-1000m.
A kind of 3. preparation method of packed buccal cigarette according to claim 1, it is characterised in that：Compound in step (6)
Plant Powder and the mixing of selenium-rich tobacco leaf powder are placed in oak barrel before not refined, are sprayed into base-material and are accounted for base-material weight
The enzyme solutions or microbial solution or its mixture of 0.5%-5%, are placed in oak barrel are refined after mixing again；It is described
Enzyme solutions be cellulase, pectase, a kind of or its mixture in protease, the microbial solution is saccharomycete,
A kind of or its mixture in bacillus.
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