CN102217796A - Preparation of compound polysaccharide humectant and application of compound polysaccharide humectant to cigarettes - Google Patents

Preparation of compound polysaccharide humectant and application of compound polysaccharide humectant to cigarettes Download PDF

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CN102217796A
CN102217796A CN2010101554285A CN201010155428A CN102217796A CN 102217796 A CN102217796 A CN 102217796A CN 2010101554285 A CN2010101554285 A CN 2010101554285A CN 201010155428 A CN201010155428 A CN 201010155428A CN 102217796 A CN102217796 A CN 102217796A
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compound
humectants
polysaccharide
cigarettes
preparation
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CN2010101554285A
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崔海滨
王学娟
许展伟
赵世兴
黄艳
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华芳烟用香料有限公司
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Abstract

The invention discloses the preparation of a compound polysaccharide humectant and application of the compound polysaccharide humectant to cigarettes. The preparation method comprises the following steps of: (1) crushing compound Chinese medicines such as Adenophora elata, dwarf lilyturf tuber, and platycodon grandiflorus, adding water, slightly boiling, performing reflux extraction, mixing extracting solution, and filtering; (2) adding protamex and high-temperature amylase into the extracting solution, and performing enzymolysis; (3) absorbing naturally cooled enzymolysis extracting solution by using a macroporous resin column, and collecting flow-through liquid; (4) concentrating the flow-through liquid in a rotary evaporator until the moisture is not evaporated to obtain the polysaccharide humectant; and (5) dissolving the polysaccharide humectant in water and adding into cut tobacco, wherein the humidification effect of cigarettes is remarkably improved, and the dry sensation of the cigarettes is reduced and the sweet degree of the cigarettes is strengthened when the cigarettes are smoked. The invention has the outstanding advantages that: the compound polysaccharide humectant can improve the aesthetic quality of the cigarettes, reduce the dry sensation of smoke, improve the sweet degree and comfort degree, and has remarkable effects of promoting the secretion of saliva or body fluid and humidifying; and the application of the technology cannot change the conventional cigarette processing technology, and the technology has actual application value.

Description

复方多糖保润剂的制备及其在卷烟中的应用 Preparation of compound polysaccharide humectants its application in cigarette

技术领域: FIELD:

[0001] 本发明涉及天然香料的开发及应用,特别是涉及复方多糖保润剂的制备及其在卷烟中的应用。 The present invention relates to the development and application of natural fragrances, particularly relates to the preparation of compound polysaccharide humectants and Its Application [0001] In the cigarette.

背景技术: Background technique:

[0002] 在过去的几十年里,世界各国的烟草工作者对不同物质的保润作用及其对卷烟吃味和烟气化学组成的影响进行了广泛研究,其中研究最多的是多元醇类,如甘油、丙二醇、 山梨醇、丁二醇和二甘醇等,使用此类保润剂的主要目的在于维持加工过程中烟丝的含水率,提高烟丝的耐加工性,而对于成品卷烟含水率的维持、吸食口感的改善则效果不太理 [0002] In the past few decades, the world's tobacco workers to protect profit effect of different substances have been extensively studied and their effects on cigarette smoke and taste and chemical composition, which is the most studied polyols such as glycerol, propylene glycol, sorbitol, butylene glycol and diethylene glycol, the use of such humectants main purpose is to maintain the moisture content of the tobacco processing, improve the process resistance of the tobacco, and for the moisture content of the finished cigarette to maintain and improve the taste of the smoking effect is not science

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[0003] 此外,糖和糖醇类(单糖)、有机盐类、天然萃取物等也常被用作卷烟保润剂。 [0003] In addition, sugar alcohols and sugar (monosaccharide), organic salts, natural extracts and the like are often used as humectants cigarette. 近年来,开发出的各种新型保润剂也倍受关注,如麦芽低聚糖醇、D-吡喃半乳糖醛酸、壳聚糖衍生物、NCS、PDS、蔗糖酯复合保润剂和仿生保润剂(FSB)等。 In recent years, development of new types humectants also much attention, maltooligosaccharides such as an alcohol, D- galactopyranosyl uronic acid, chitosan derivatives, NCS, PDS, sucrose esters and humectants compound bionic humectants (FSB) and the like. 这些保润剂一方面改变了烟丝解湿和吸湿的过程,另一方面还影响了烟丝的平衡含水率;保润剂的吸湿性能主要与其亲水能力有关,但吸湿性能与保湿性能之间并无必然联系;不同类型的保润剂在不同温湿度条件下吸湿性能与保湿性能表现出不同特点。 These humectants aspect of the process of changing the wet tobacco and hygroscopic solution, on the other hand also affects the equilibrium moisture content of the tobacco; hygroscopic humectants can be related mainly to its hydrophilic capability, but the hygroscopicity and moisture retention and between not necessarily linked to; different types of hygroscopic humectants and moisturizing properties different performance characteristics under different temperature and humidity conditions.

[0004] 植物多糖由于其分子结构中存在大量羟基或羧基等极性基团,可与水分子形成氢键,并常常相互交联成网状结构而表现出良好的吸水和保湿性能。 [0004] Due to plant polysaccharides large number of polar hydroxyl group or carboxyl group in the molecular structure, can form hydrogen bonds with water molecules, and often cross-linked into a network structure to each other and exhibit good water-absorbing and moisturizing properties. 由于多糖一般都具有一定的粘度和较好的成膜性,可在物质表面形成均勻的薄膜从而减少物质表面的水分蒸发。 Since polysaccharides generally have a certain viscosity and good film-forming property, it can form a uniform film material surface to reduce water evaporation surface of the material. 在香料开发过程中,我们发现具有生津润肺、止咳功效的中草药提取物可明显改善烟气干燥感、增加甜润度、改善口感和刺激性,而其中有些也富含多糖类成分。 In the perfume development process, we have found that fluid lungs, cough effectiveness of herbal extracts can significantly improve the dry feeling of smoke, sweet degree increase, to improve the taste and pungent, some of which are also rich in polysaccharide component. 从物理保润和感官舒适度角度出发,对从此类中草药中提取的多糖进行筛选,选取能改善口感,增加润感,降低卷烟刺激性的多糖,进行合理复配,通过酶解去除杂质达到提高有效成分的纯度,并通过分离手段去除药味。 From the physical and sensory-Run comfort point of view, Chinese herbal medicine extracted from such polysaccharides in screening, selecting can improve taste, increase the sense of profit, reduce irritation of cigarette polysaccharide, reasonably complex, by enzymatic hydrolysis to remove impurities to improve purity of the active ingredient, and is removed by separation means Smell. 近年来,国内外对单味中药的多糖从不同角度做了大量的研究,逐步阐明其化学、生理学和药理学等多方面的性质,但是对复方中药多糖的研究相对较少,而将复方中药多糖应用于卷烟还处于研究起始阶段,未见文献报道。 In recent years, researches on single herb polysaccharides from a lot of different angles, gradually clarify its multifaceted nature of chemistry, physiology and pharmacology, but relatively few studies of traditional Chinese medicine compound polysaccharide, and the compound Chinese medicine polysaccharide used in cigarettes is still in the initial research stage, it has not been reported.

发明内容: SUMMARY:

[0005] 本发明正是基于上述现状而运用天然有效成分的提取分离技术、生物酶催化技术,充分地考虑了工业化生产的可行性和可操作性,同时对制备过程中涉及的因素逐一进行了探讨,确定了最佳的工艺参数,产品具有物理保润和感官保润双重效果,且质量稳定、 风格突出,是一种复方多糖保润剂的制备方法。 [0005] The present invention is based on the above state of the use of natural active ingredient extraction and separation techniques, enzyme catalysis, fully considered the feasibility of industrial production and operability, while the factors involved in the production process one by one Discussion, the optimal process parameters, the product has physical and sensory-Run-Run double effect, and stable quality, style projection, is a method for preparing the compound polysaccharide humectants.

[0006] 本发明的目的是通过如下技术方案解决:复方多糖保润剂的制备及其在卷烟中的应用,通过下述步骤实现: [0006] The object of the present invention is solved by the following technical solutions: Preparation of compound polysaccharide humectants and its application in cigarette realized by the following steps:

[0007] a、将沙参、麦冬、桔梗、复方中药粉碎,加水微沸回流提取,合并提取液,过滤。 [0007] a, the Radix, Campanulaceae, pulverized compound Chinese medicine, micro-boiling reflux extraction with water, the combined extracts were filtered.

[0008] b、向提取液中加入复合蛋白酶和高温淀粉酶,酶解。 [0008] b, was added and the temperature protamex amylase, the hydrolysis extract. [0009] C、自然冷却后的酶解提取液经大孔树脂柱吸附,收集流穿液。 [0009] C, allowed to cool after hydrolysis extract by macroporous adsorption resin column, the flow through was collected.

[0010] d、将流穿液于旋转蒸发仪中浓缩到无水分蒸出,制得多糖保润剂。 [0010] d, the flow-through was concentrated on a rotary evaporator to a moisture-free distilled off, to obtain a polysaccharide humectants.

[0011] 上述步骤a中,沙参与麦冬和桔梗的质量比为5 : 3 : 2〜2 : 3 : 5。 [0011] In the above step a, sand and Radix participation Campanulaceae mass ratio of 5: 3: 2~2: 3: 5.

[0012] 上述步骤a中,加入6〜10倍质量的水提取两次,每次时间为1〜池。 [0012] step a above was added 6~10 times the mass of water and extracted twice, each time for 1 ~ pool. 上述步骤b中,复合蛋白酶和高温淀粉酶的用量为干药材粉末重量的0. 25〜1%,酶解反应温度为50°C〜90°C,酶解反应时间为2〜4h。 Step (b) above, the amount of compound of protease and amylase high temperature dry powder medicinal 25~1 0.5% by weight, hydrolysis reaction temperature is 50 ° C~90 ° C, the reaction time of hydrolysis 2~4h.

[0013] 本发明的复方多糖保润剂在应用时,是将保润剂经水溶解后,通过喷洒方式在烟丝加料工序施加到烟丝上,卷烟保润效果明显改善,吸食卷烟时,刺激性明显降低,尤其是喉部的呛刺感明显降低,入喉和顺,烟气细腻清甜,杂气降低,烟气和余味的润感加强,口腔和喉部的残留明显减少;保润剂用量为烟丝重量的1_3%。 [0013] After the compound polysaccharide humectants in the application of the present invention, the humectants are dissolved by water, is applied to the tobacco by spraying tobacco feed step mode, the effect of significantly improved cigarette-Run, when smoked cigarettes, irritation significantly reduced, especially the throat choking tingling significantly reduced, choking rolls, sweet and fine smoke, reducing mixed gas, smoke aftertaste and feeling run enhanced residual mouth and throat significantly reduced; the amount of humectants 1_3% by weight of tobacco.

[0014] 本发明的突出优点是:可提高卷烟的感官质量,降低烟气的干燥感,甜润度、舒适度提高,具有明显的生津、保润效果,且这一技术的应用不改变现有卷烟的加工工艺,具有实际生产的意义和价值。 [0014] The outstanding advantages of the present invention are: to improve the organoleptic quality of the cigarette can reduce the feeling of flue gas drying, sweet, comfort increase, with obvious fluid, effect-Run, and application of this technology does not change the existing cigarette processing technology, have practical significance and value of production.

[0015] 烟丝含水率测试:将多糖保润剂经水溶解后,通过喷洒方式在加料工序施加到空白烟丝上,空白烟丝施加同等剂量的丙二醇和水,将其一并放置于相对湿度40%低湿和70%高湿环境下,结果显示保润剂在环境相对湿度较低(40%)的条件下,添加多糖保润剂烟丝的保湿能力强于丙二醇;在环境相对湿度较高(70% )的条件下,添加多糖保润剂烟丝的水分增加量较丙二醇样品小,表明多糖保润剂具有保湿效果,且综合性能优于其他常用保润剂。 [0015] tobacco moisture content test: The polysaccharide humectants was dissolved in water, applied to a blank in the feed step manner by spraying tobacco, tobacco blank filament for the same dose of propylene glycol and water, and placed in one of the relative humidity of 40% under low humidity and high-humidity environment of 70%, the results show that humectants in an environment of low relative humidity (40%) are satisfied, adding the polysaccharide humectants tobacco moisturizing ability in propylene glycol; in high relative humidity (70% ) under the conditions of addition of the polysaccharide humectants tobacco moisture increased amount smaller than the sample of propylene glycol, humectants indicate polysaccharide having a moisturizing effect, and the overall performance is superior to other commonly used humectants.

[0016] 施加复方多糖保润剂、丙二醇和水的卷烟感官舒适度评吸结果见表1。 [0016] applying a compound polysaccharide humectants, tobacco sensory assessment Comfort propylene glycol and water absorption results are shown in Table 1.

[0017] 表1感官舒适度评吸结果 [0017] Table 1 Sensory results smoking Comfort

[0018] [0018]

Figure CN102217796AD00041

附图说明: BRIEF DESCRIPTION OF:

[0019] 图1为本发明制备方法的工艺流程图 [0019] FIG. 1 process flow diagram of a method of the present invention were prepared

[0020] 图2为添加复方多糖保润剂、丙二醇和水后,在低湿环境下烟丝含水率测试图。 [0020] FIG. 2 is a compound polysaccharide added humectants, propylene glycol and the water, in a low-humidity environment to test moisture content tobacco FIG.

[0021] 图3为添加复方多糖保润剂、丙二醇和水后,在高湿环境下烟丝含水率测试图。 [0021] FIG. 3 is a compound polysaccharide added humectants, propylene glycol and the water, in a high-humidity environment to test moisture content of tobacco FIG.

具体实施方式: Detailed ways:

[0022] 本发明以下结合实施例做进一步描述,但并不是限制本发明。 The following [0022] embodiment of the present invention is further described in conjunction with, but not limit the present invention. [0023] 实施例1 [0023] Example 1

[0024] 将购买的中药材组成复方,用清水清洗,除去尘土,低温烘干,采用粉碎机粉碎,按料液重量比1 : 10称取药材和去离子水于加热回流装置,微沸状态下回流提取lh,400目筛网滤出提取液,按此条件共提取三次,合并滤液。 [0024] The herbal composition of the later compound, washing with water, to remove dust, low temperature drying, using a grinder, by solid-liquid weight ratio of 1: taking medicine and deionized water was heated under reflux to said means 10, micro-boiling state extracting at reflux lh, 400 mesh extract was filtered off, extracted three times under these conditions were combined with the filtrate. 按干药材粉末重量的0. 5%称取复合蛋白酶加入提取液,于50°C搅拌酶解池。 0.5% by weight of dry medicinal powder weighed protamex extract was added, was stirred at 50 ° C hydrolysis tank. 按干药材粉末重量的0. 5%称取高温淀粉酶加入提取液,于90°C搅拌酶解池。 0.5% by weight of dry medicinal powder weighed temperature amylase extract was added, was stirred at 90 ° C hydrolysis tank. 自然冷却后的酶解提取液经D-101大孔树脂柱吸附,收集流穿液。 After cooling the natural enzyme extract by macroporous adsorption resin column D-101, the flow through was collected. 将流穿液于旋转蒸发仪中浓缩到无水分蒸出,得多糖保润剂。 The flow-through was concentrated on a rotary evaporator and evaporated to a moisture-free, to obtain a polysaccharide humectants. 将本发明的复方多糖保润剂经水溶解后,通过喷洒方式在加料工序施加到卷烟烟丝上。 The compound polysaccharide humectants present invention was dissolved in water, applied to the cut tobacco by spraying manner in the feed step. 具体使用比例为:复方多糖保润剂用量为烟丝重量的1%。 Specific use ratio: compound polysaccharide humectants in an amount of 1% by weight of the tobacco.

[0025] 实施例2 [0025] Example 2

[0026] 将购买的中药材组成复方,用清水清洗,除去尘土,低温烘干,采用粉碎机粉碎,按料液重量比1 : 8称取药材和去离子水于加热回流装置,微沸状态下回流提取池,400目筛网滤出提取液,按此条件共提取三次,合并滤液。 [0026] The herbal composition of the later compound, washing with water, to remove dust, low temperature drying, using a grinder, by solid-liquid weight ratio of 1: taking medicine and deionized water was heated to reflux for 8 said apparatus, micro-boiling state reflux extraction cell, a 400 mesh screen extract was filtered off, extracted three times under these conditions were combined with the filtrate. 按干药材粉末重量的称取复合蛋白酶加入提取液,于50°C搅拌酶解4h。 Dry weight of the powder medicine weighed protamex extract was added, stirred for hydrolysis at 50 ° C 4h. 按干药材粉末重量的0. 5%称取高温淀粉酶加入提取液, 于90°C搅拌酶解4h。 0.5% by weight of dry medicinal powder weighed temperature amylase extract was added, stirred for hydrolysis at 90 ° C 4h. 自然冷却后的酶解提取液经D-101大孔树脂柱吸附,收集流穿液。 After cooling the natural enzyme extract by macroporous adsorption resin column D-101, the flow through was collected. 将流穿液于旋转蒸发仪中浓缩到无水分蒸出,得多糖保润剂。 The flow-through was concentrated on a rotary evaporator and evaporated to a moisture-free, to obtain a polysaccharide humectants. 将本发明的复方多糖保润剂经水溶解后,通过喷洒方式在加料工序施加到卷烟烟丝上。 The compound polysaccharide humectants present invention was dissolved in water, applied to the cut tobacco by spraying manner in the feed step. 具体使用比例为:复方多糖保润剂用量为烟丝重量的3%。 Specific use ratio: compound polysaccharide humectants in an amount of 3% by weight of the tobacco.

Claims (6)

1.复方多糖保润剂的制备及其在卷烟中的应用,其特征在于:它包括以下步骤:a、将沙参、麦冬、桔梗复方中药粉碎,加水微沸回流提取,合并提取液,过滤。 Preparation of compound polysaccharide humectants 1. Its application in cigarette, characterized in that: it comprises the following steps: a, the Radix, Campanulaceae pulverized compound Chinese medicine, micro-boiling reflux extraction with water, the combined extracts were filter. b、向提取液中加入复合蛋白酶和高温淀粉酶,酶解。 B, addition of protease and high temperature composite amylase, the hydrolysis extract. c、自然冷却后的酶解提取液经大孔树脂柱吸附,收集流穿液。 C, natural cooling after hydrolysis extract by macroporous adsorption resin column, the flow through was collected. d、将流穿液于旋转蒸发仪中浓缩到无水分蒸出,得多糖保润剂。 d, the flow-through was concentrated on a rotary evaporator to a moisture-free distilled off to give a polysaccharide humectants.
2.根据权利要求1所述的复方多糖保润剂的制备,其特征在于冬和桔梗,质量比为5 : 3 : 2〜2 : 3 : 5。 2. Preparation of the compound polysaccharide humectants 1 claim, characterized in that the winter and Campanulaceae, mass ratio of 5: 3: 2~2: 3: 5.
3.根据权利要求1所述的复方多糖保润剂的制备,其特征在于和高温淀粉酶催化酶解。 3. Preparation of the compound polysaccharide humectants 1 claim, characterized in that the temperature and the enzymatic hydrolysis of starch.
4.根据权利要求1所述的复方多糖保润剂的制备,其特征在于脂吸附,收集流穿液。 4. The preparation according to claim 1 compound polysaccharide humectants claims, characterized in that the lipid adsorption, flow through was collected.
5. 一种权利要求1所述的复方多糖保润剂的应用,其特征在于:将保润剂经水溶解后, 通过喷洒方式在烟丝加料工序施加到烟丝上,卷烟保润效果明显改善,吸食卷烟时,刺激性明显降低,尤其是喉部的呛刺感明显降低,入喉和顺,烟气细腻清甜,杂气降低,烟气和余味的润感加强,口腔和喉部的残留明显减少。 Application of the polysaccharide compound 1 5. A humectants claim, wherein: the humectants was dissolved in water, applied to the tobacco by spraying step manner to feed the tobacco, cigarette-Run significantly improved effect, when smoking a cigarette, significantly reduced irritation, tingling throat choking in particular significantly reduced, choking rolls, sweet and fine smoke, reducing mixed gas, smoke aftertaste and feeling run enhanced significantly residual mouth and throat cut back.
6.根据权利要求5所述的复方多糖保润剂的应用,其特征在于:复方多糖保润剂用量为烟丝重量的1-3%。 6. Use according to claim 5 polysaccharide humectants compound as claimed in claim wherein: compound polysaccharide humectants in an amount of 1-3% by weight of the tobacco. :中药复方为沙参与麦:提取液经复合蛋白酶:酶解提取液经大孔树 : Traditional Chinese medicine to participate sand wheat: extract protamex by: enzyme extract by macroporous tree
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CN103504463A (en) * 2013-09-27 2014-01-15 广东中烟工业有限责任公司 Application of shaddock ped polysaccharide to tobacco leaf moisturizing
CN103772512A (en) * 2012-10-20 2014-05-07 中国烟草总公司郑州烟草研究院 Preparation method and application of oxidized-carboxymethylated amyloid cigarette humectant
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CN104432493A (en) * 2014-11-03 2015-03-25 云南中烟工业有限责任公司 Application of agrocybe cylindracea polysaccharide or compound of agrocybe cylindracea polysaccharide in cigarettes
CN104987543A (en) * 2015-07-31 2015-10-21 云南中烟工业有限责任公司 Preparation method and application of ternary blend polysaccharide containing konjak glucomannan, chitosan and sodium carboxymethylcellulose
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CN104987542A (en) * 2015-07-31 2015-10-21 云南中烟工业有限责任公司 Preparation method and application of ternary blend polysaccharide containing polysaccharide of enteromorpha, fucoidan and carboxymethyl chitosan
CN105061820A (en) * 2015-07-31 2015-11-18 云南中烟工业有限责任公司 Preparation method and application of Wedelia prostrate polysaccharide, chitin and carrageenan oligosaccharide blended polysaccharide
CN105131346A (en) * 2015-07-31 2015-12-09 云南中烟工业有限责任公司 Preparation method and application of ternary blended polysaccharide of xylan, galactomannan, and hydroxyethyl cellulose
CN105131345A (en) * 2015-07-31 2015-12-09 云南中烟工业有限责任公司 Preparation method and application of ternary blended polysaccharide of pulullan, sodium alginate, and propylene glycol alginate
CN105153477A (en) * 2015-07-31 2015-12-16 云南中烟工业有限责任公司 Preparation method of ternary blending polysaccharide containing opuntia polysaccharide, hydroxy propyl cellulose and xanthan gum as well as application thereof
CN105175796A (en) * 2015-07-31 2015-12-23 云南中烟工业有限责任公司 Preparation method for ternary blending polysaccharide of schizophyllan, arabinose and maltodextrin and applications

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CN1187365A (en) * 1997-12-15 1998-07-15 辛孟芬 Oral liquid for removing intense heat from throat and preparing process thereof
CN1202370A (en) * 1998-04-16 1998-12-23 莫程鹏 Method for producing throat smoothing tablet with emblic
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CN103082413A (en) * 2011-11-08 2013-05-08 江西中烟工业有限责任公司 Method for decreasing cigarette offensive odor by utilizing composite Chinese herbal medicine
CN103082403A (en) * 2011-11-08 2013-05-08 江西中烟工业有限责任公司 Tobacco flavor fermented by utilizing radix ophiopogonis and preparation method and application thereof
CN103767065B (en) * 2012-10-20 2015-04-22 中国烟草总公司郑州烟草研究院 Preparation method for pyrolysis-oxidized starchiness cigarette humectant and application thereof
CN103772512A (en) * 2012-10-20 2014-05-07 中国烟草总公司郑州烟草研究院 Preparation method and application of oxidized-carboxymethylated amyloid cigarette humectant
CN103767065A (en) * 2012-10-20 2014-05-07 中国烟草总公司郑州烟草研究院 Preparation method for pyrolysis-oxidized starchiness cigarette humectant and application thereof
CN103772512B (en) * 2012-10-20 2016-06-29 中国烟草总公司郑州烟草研究院 The preparation method of a kind of oxidation-carboxymethylated starch matter humectant for smoke and application thereof
CN103504463B (en) * 2013-09-27 2015-09-30 广东中烟工业有限责任公司 The application of a kind of shaddock ped polysaccharide in tobacco leaf humectation
CN103504463A (en) * 2013-09-27 2014-01-15 广东中烟工业有限责任公司 Application of shaddock ped polysaccharide to tobacco leaf moisturizing
CN104432493A (en) * 2014-11-03 2015-03-25 云南中烟工业有限责任公司 Application of agrocybe cylindracea polysaccharide or compound of agrocybe cylindracea polysaccharide in cigarettes
CN104987544A (en) * 2015-07-31 2015-10-21 云南中烟工业有限责任公司 Preparation method and application of ternary blend polysaccharide containing D-glucan, fucoidan and pectin
CN104987542A (en) * 2015-07-31 2015-10-21 云南中烟工业有限责任公司 Preparation method and application of ternary blend polysaccharide containing polysaccharide of enteromorpha, fucoidan and carboxymethyl chitosan
CN105061820A (en) * 2015-07-31 2015-11-18 云南中烟工业有限责任公司 Preparation method and application of Wedelia prostrate polysaccharide, chitin and carrageenan oligosaccharide blended polysaccharide
CN105131346A (en) * 2015-07-31 2015-12-09 云南中烟工业有限责任公司 Preparation method and application of ternary blended polysaccharide of xylan, galactomannan, and hydroxyethyl cellulose
CN105131345A (en) * 2015-07-31 2015-12-09 云南中烟工业有限责任公司 Preparation method and application of ternary blended polysaccharide of pulullan, sodium alginate, and propylene glycol alginate
CN105153477A (en) * 2015-07-31 2015-12-16 云南中烟工业有限责任公司 Preparation method of ternary blending polysaccharide containing opuntia polysaccharide, hydroxy propyl cellulose and xanthan gum as well as application thereof
CN105175796A (en) * 2015-07-31 2015-12-23 云南中烟工业有限责任公司 Preparation method for ternary blending polysaccharide of schizophyllan, arabinose and maltodextrin and applications
CN104987543A (en) * 2015-07-31 2015-10-21 云南中烟工业有限责任公司 Preparation method and application of ternary blend polysaccharide containing konjak glucomannan, chitosan and sodium carboxymethylcellulose

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