CN106579538A - Bagged mouth-holding cigarette and preparation method therefor - Google Patents
Bagged mouth-holding cigarette and preparation method therefor Download PDFInfo
- Publication number
- CN106579538A CN106579538A CN201611153248.7A CN201611153248A CN106579538A CN 106579538 A CN106579538 A CN 106579538A CN 201611153248 A CN201611153248 A CN 201611153248A CN 106579538 A CN106579538 A CN 106579538A
- Authority
- CN
- China
- Prior art keywords
- selenium
- rich
- nicotiana tabacum
- powder
- burley tobaccos
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 80
- 239000011669 selenium Substances 0.000 claims abstract description 53
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims abstract description 45
- 229910052711 selenium Inorganic materials 0.000 claims abstract description 45
- 150000001875 compounds Chemical class 0.000 claims abstract description 35
- 239000000463 material Substances 0.000 claims abstract description 34
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract description 33
- 241000196324 Embryophyta Species 0.000 claims abstract description 28
- 239000000203 mixture Substances 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 5
- 239000003765 sweetening agent Substances 0.000 claims abstract description 5
- 241000208125 Nicotiana Species 0.000 claims description 47
- 239000000843 powder Substances 0.000 claims description 35
- 239000000284 extract Substances 0.000 claims description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 22
- 239000006228 supernatant Substances 0.000 claims description 22
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 15
- FXFYOPQLGGEACP-UHFFFAOYSA-N 6-methylcoumarin Chemical compound O1C(=O)C=CC2=CC(C)=CC=C21 FXFYOPQLGGEACP-UHFFFAOYSA-N 0.000 claims description 14
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 claims description 14
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 12
- 238000005119 centrifugation Methods 0.000 claims description 10
- 238000005352 clarification Methods 0.000 claims description 10
- 239000012535 impurity Substances 0.000 claims description 10
- 239000002002 slurry Substances 0.000 claims description 10
- 239000000779 smoke Substances 0.000 claims description 9
- 241000219492 Quercus Species 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- MOMFXATYAINJML-UHFFFAOYSA-N 2-Acetylthiazole Chemical group CC(=O)C1=NC=CS1 MOMFXATYAINJML-UHFFFAOYSA-N 0.000 claims description 7
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 claims description 7
- 229960001867 guaiacol Drugs 0.000 claims description 7
- 239000003607 modifier Substances 0.000 claims description 7
- RHDGNLCLDBVESU-UHFFFAOYSA-N but-3-en-4-olide Chemical compound O=C1CC=CO1 RHDGNLCLDBVESU-UHFFFAOYSA-N 0.000 claims description 6
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims description 5
- 229940109275 cyclamate Drugs 0.000 claims description 5
- HCAJEUSONLESMK-UHFFFAOYSA-N cyclohexylsulfamic acid Chemical compound OS(=O)(=O)NC1CCCCC1 HCAJEUSONLESMK-UHFFFAOYSA-N 0.000 claims description 5
- 229940093503 ethyl maltol Drugs 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 239000001509 sodium citrate Substances 0.000 claims description 5
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical group O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 5
- 235000011083 sodium citrates Nutrition 0.000 claims description 5
- 239000002689 soil Substances 0.000 claims description 5
- 230000001954 sterilising effect Effects 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- DEMKZLAVQYISIA-UHFFFAOYSA-N Liquirtin Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(C2OC3=CC(O)=CC=C3C(=O)C2)C=C1 DEMKZLAVQYISIA-UHFFFAOYSA-N 0.000 claims description 4
- 230000002255 enzymatic effect Effects 0.000 claims description 4
- 230000000813 microbial effect Effects 0.000 claims description 4
- -1 pectase Proteins 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 claims description 3
- 108010059892 Cellulase Proteins 0.000 claims description 3
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims description 3
- 229960004998 acesulfame potassium Drugs 0.000 claims description 3
- 235000010358 acesulfame potassium Nutrition 0.000 claims description 3
- 239000000619 acesulfame-K Substances 0.000 claims description 3
- 230000033228 biological regulation Effects 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 235000019262 disodium citrate Nutrition 0.000 claims description 3
- 239000002526 disodium citrate Substances 0.000 claims description 3
- 229940079896 disodium hydrogen citrate Drugs 0.000 claims description 3
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 3
- 229940013618 stevioside Drugs 0.000 claims description 3
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims description 3
- 235000019202 steviosides Nutrition 0.000 claims description 3
- 241000193755 Bacillus cereus Species 0.000 claims description 2
- 241000593922 Quercus acutissima Species 0.000 claims description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 2
- 235000009508 confectionery Nutrition 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 230000000717 retained effect Effects 0.000 claims description 2
- 241000256844 Apis mellifera Species 0.000 claims 1
- 108091005804 Peptidases Proteins 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 239000004365 Protease Substances 0.000 claims 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims 1
- 241000209140 Triticum Species 0.000 claims 1
- 235000021307 Triticum Nutrition 0.000 claims 1
- 238000007598 dipping method Methods 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 12
- 239000003205 fragrance Substances 0.000 abstract description 6
- 230000004927 fusion Effects 0.000 abstract description 2
- 238000005215 recombination Methods 0.000 abstract 2
- 230000006798 recombination Effects 0.000 abstract 2
- 241001523681 Dendrobium Species 0.000 abstract 1
- 241001517310 Eria Species 0.000 abstract 1
- 241001071917 Lithospermum Species 0.000 abstract 1
- 240000004064 Poterium sanguisorba Species 0.000 abstract 1
- 235000008291 Poterium sanguisorba Nutrition 0.000 abstract 1
- 206010039424 Salivary hypersecretion Diseases 0.000 abstract 1
- 235000008282 Sanguisorba officinalis Nutrition 0.000 abstract 1
- 240000006688 Telosma cordata Species 0.000 abstract 1
- 235000017352 Telosma cordata Nutrition 0.000 abstract 1
- 230000003750 conditioning effect Effects 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 208000026451 salivation Diseases 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 description 13
- 210000000214 mouth Anatomy 0.000 description 9
- 239000003814 drug Substances 0.000 description 7
- 230000036541 health Effects 0.000 description 6
- 210000001124 body fluid Anatomy 0.000 description 5
- 239000010839 body fluid Substances 0.000 description 5
- 229940079593 drug Drugs 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000001737 promoting effect Effects 0.000 description 5
- 210000004072 lung Anatomy 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- 229940088598 enzyme Drugs 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000011630 iodine Substances 0.000 description 3
- 229910052740 iodine Inorganic materials 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- 235000019505 tobacco product Nutrition 0.000 description 3
- 239000011573 trace mineral Substances 0.000 description 3
- 235000013619 trace mineral Nutrition 0.000 description 3
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 241000533849 Gleditsia Species 0.000 description 2
- 238000001467 acupuncture Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 241000721047 Danaus plexippus Species 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 102000003992 Peroxidases Human genes 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 230000004308 accommodation Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000002457 bidirectional effect Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 210000004195 gingiva Anatomy 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229940043353 maltol Drugs 0.000 description 1
- 230000007886 mutagenicity Effects 0.000 description 1
- 231100000299 mutagenicity Toxicity 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 108040007629 peroxidase activity proteins Proteins 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 238000002054 transplantation Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides a bagged mouth-holding cigarette and a preparation method therefor. The bagged mouth-holding cigarette is prepared through the following method, and the method comprises the steps: mixing a compound plant and selenium-rich tobacco leaves and uniformly placing the mixture in a sealed oak barrel; carrying out the recombination alcoholization of the mixture for 30-60d under the conditions that the temperature is 25-35 DEG and the humidity is 60%-80%, and then adding salt, an acid-base conditioning agent and a sweetening agent to an alcoholized base material; carrying out the processing for 20-40 min through steam with the temperature from 100 DEG C to 110 DEG C; adding essence according to a proportion after the base material is cooled, and adjusting the humidity to be 15%-50%, and finally carrying out the bagging. The compound plant consists of dark plum, garden burnet, radix sophorae flavescentis, lithospermum, spina gleditsiae, hooked dendrobium, herb of grassleaf eria and Chinese violet. The selenium content of the selenium-rich tobacco leaves is 0.3-0.8mg/kg. The oak barrel is employed for recombination alcoholization and ingredient matching and mixing to form bagged mouth-holding cigarettes in different forms. The mouth-holding cigarette is better in fragrance fusion, is coordinative in taste, is comfortable in taste, also provides necessary microelements for human bodies, and has an effect of removing heat to promote salivation.
Description
Technical field
The invention belongs to smoke-free tobacco product and its processing technique field, and in particular to a kind of packed buccal cigarette and its system
Preparation Method.
Background technology
Selenium is teleorganic trace element, and by scientist " king of anticancer " is referred to as in body trace element, is human body paddy
Guang (sweet peptide peroxidase GSH-Px) important activity composition, plays a part of to remove interior free yl;With removing toxic substances, toxin expelling,
Defying age, antioxidation, the effect of enhance immunity, selenium can play reduction gene mutagenicity, the work of DNA plerosis in human body
With.Meanwhile, selenium can reduce the toxicity of nicotine and tar, and suppression is played to tumor, have opposing to various carcinogen in flue gas
Effect;Also studies have reported that suction iodine enriched cigarette can make human body blood selenium level relatively aspirate regular-size cigarette human body blood selenium level at present
It is high by 10%.So people also begin to study iodine enriched cigarette, existing iodine enriched cigarette is substantially the Medicated cigarette of suction, although can also
Increase the content of human body selenium, but because Nicotiana tabacum L. needs burning, still can produce substantial amounts of flue gas, danger is brought to health
Evil.
Packed buccal cigarette belongs to a kind of form of smoke-free tobacco product, is used by being put between lip and gingiva, has
Need not burn, not produce second hand smoking harm, be received by increasing consumer.Because buccal cigarette is unlike traditional cigarette
Burning is equally participated in, therefore can be theoretical by Chinese medicine scientific compatibility according to " monarch " of the traditional Chinese medical science so as to control with certain
Treat and health-care effect.The A of Chinese patent CN 105054279 disclose a kind of selenium-rich buccal cigarette and preparation method thereof, in the patent
Buccal cigarette in selenium source mostly come from chemicals selenic ester polysaccharide, be not very healthy, and cannot play health care work
With.Although also there is the buccal cigarette of some health-care types, such as characteristic food is produced in a kind of river disclosed in Chinese patent CN 105124748A
The moistening lung and nourishing throat health buccal cigarette produced, is to produce in the river based on Fructus Citri grandiss, pears, Rhizoma Nelumbiniss, Caulis Sacchari sinensis, Corm Eleocharitiss, Herba Houttuyniae and Folium Eriobotryae
Characteristic food and tobacco extract compatibility, the method for preparing moistening lung and nourishing throat health buccal cigarette.Chinese patent CN104997153A
Disclose a kind of river and produce the moistening lung and nourishing throat health buccal cigarette that Special Traditional Chinese Medicine is produced, be with tobacco extract and Radix Scutellariae, Fructus Canarii, Fructus Citri tangerinae
Produce the method that the extract of Special Traditional Chinese Medicine prepares moistening lung and nourishing throat health buccal cigarette in river based on stalk, Bulbus Fritillariae Cirrhosae and Flos Lonicerae.These
Buccal cigarette is all directly that by food or Chinese medicine together with common Nicotiana tabacum L. compatibility, its health-care effect is not fine, and
Supplementary human body selenium source is not played a part of.
The content of the invention
For above-mentioned situation, the present invention provides a kind of packed buccal cigarette and preparation method thereof, and the buccal cigarette adopts natural plant
Thing compatibility, is combined the techniques such as alcoholization, prepares that outlet plenum is comfortable, the pure ecological selenium-rich mouth containing smoke product that fragrance is coordinated.
The technical solution used in the present invention is as follows:A kind of packed buccal cigarette, it is characterised in that be by following weight hundred
Divide the material composition of ratio:
The total weight percent of above-mentioned substance is 100%.
Wherein:The compound plant is by the material composition of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae
5%-10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae
6%-12%, Herba Violae 7%-15%;
Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade Se content 0.3-0.8mg/kg;
The essence is the material composition of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, yunyan extract 0.8-
2%th, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethylmaltol 0.3%-
0.7%th, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;Thing in above-mentioned essence
Matter is the product of direct purchase;
The sweeting agent is non-sugar sweetener;
The water is the water content of the final products prepared through process in all materials, is 15%-50%.
Further technical scheme of the invention:Described acid-base modifier is sodium citrate or DisodiumHydrogen Citrate.It is described
Non-sugar sweetener includes a kind of in liquirtin, cyclamate, stevioside or acesulfame potassium or any several mixing.The acid-alkali accommodation
Agent and sweeting agent are the product of direct purchase.Described selenium-rich Nicotiana tabacum L. is that Flue-cured Tobacco transplantation of seedlings is raw in selenium-rich soil of bestowing favour
Long cured tobacco leaf, the soil Se content of its planting site is more than 0.45mg/kg, altitude 800-1000m;Selenium-rich cigarette can
With direct using natural selenium-rich cigarette " Qing Jiangyuan " Nicotiana tabacum L. of bestowing favour.
The present invention preferably technical scheme:The burley tobaccos absolute oil is with burley tobacco leaf as raw material, by Nicotiana tabacum L. and concentration
20% ethanol mass ratio is 1:The ratio mixing of 3-20, the agitating heating reflux extraction 1-10 hours at a temperature of 110 ± 5 DEG C, drop
The clarification of 1-3 hours is stood to room temperature, supernatant is extracted;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and will filter
Liquid is poured in Rotary Evaporators after merging with supernatant and is concentrated to give under conditions of 60 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To thick liquid be burley tobaccos extract;Then burley tobaccos are carried with the ethanol of concentration 95% according to mass ratio 1:The ratio of 3-20
Example mixing, stands the clarification of 1-3 hours, extracts supernatant, and reject dregs after lower floor's slurry centrifugation collect filtrate, and and supernatant
Liquid is poured in Rotary Evaporators after merging and is concentrated into relative density under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
0.9-1.3g/cm3Obtain burley tobaccos absolute oil.
A kind of packed buccal cigarette preparation method that the present invention is provided, it is characterised in that processing method is as follows:
(1) compound plant raw material is prepared according to the formula of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae 5%-
10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%-
12%, Herba Violae 7%-15%;Above-mentioned raw materials are individually gone after the removal of impurity to crush, is retained powder more than 80 mesh and then is mixed
It is configured to compound plant powder;Or go the removal of impurity to be crushed again after above-mentioned raw materials are mixed, retain powder more than 80 mesh and obtain
Compound plant powder;
(2) burley tobaccos absolute oil is prepared:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110
Agitating heating reflux extraction 1-10 hours at a temperature of ± 5 DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with
The supernatant collected in step a merges, and then pours the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum
Burley tobaccos extract is more than thick liquid is concentrated under conditions of 0.95Mpa;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:3-20
Ratio mixing, stand the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and
Pour into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
(3) essence is prepared according to the formula of following percentage by weight:The burley tobaccos absolute oil 0.5%- prepared in step (2)
1%th, yunyan extract 0.8-2%, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%,
Ethylmaltol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of the third two
Alcohol;Above-mentioned raw materials mix homogeneously is configured to into essence;
(4) raw material of buccal cigarette is prepared according to formula as below:The middle compound plant powder for preparing of 10%-30% steps (1),
The essence of preparation, 0.1%-2% Sal, 0.5%-1% are sour in the step of selenium-rich Nicotiana tabacum L., 0.1%-4% of 30%-60% (1)
Alkali regulator, 0.5%-1.5% sweeting agents, excess water;
(5) the whole selenium-rich tobacco leaf pickings in step (4) are removed into the impurity in material, Ran Houzai with flexible wind election process
Pulverization process is carried out, the powder for retaining more than 80 mesh is selenium-rich Nicotiana tabacum L. powder;The flexible wind election process be existing process, its work
Skill principle is that the Nicotiana tabacum L. cut tobacco after pneumatic conveying drying is sent into into free-falling after selecting crude drugs with winnower casing by feeding mechanism, using casing it is vertical and
Horizontal bidirectional air intake carries out float choosing and flotation to cut tobacco, makes density larger object such as impurity, stalk label etc. by secondary separation case
Body falls, and the lighter cut tobacco of density will send casing by discharging mechanism, so as to realize the dedoping step of material;
(6) by the selenium-rich Nicotiana tabacum L. powder mix homogeneously in the compound plant powder in step (4) and step (5), it is placed in sealing
It it is 25-35 DEG C in temperature in oak barrel, humidity is that compound alcoholization 30d-60d is carried out under conditions of 60%-80%;
(7) after the compound alcoholization in step (6) terminates, the base material after compound alcoholization is taken out, according to the ratio in step (4)
Sal, acid-base modifier, sweeting agent are added, 100-110 DEG C of steam treatment 20-40min is then used under closed environment;
(8) after the cooling of above-mentioned base material, essence is added in the ratio in step (4), regulation humidity is 15%-50%, so
Laggard luggage bag, and packed mouth containing smoke product is obtained after sterilization processing;Adjusting the mode of humidity can be placed directly in constant temperature
In the system of constant humidity, regulation temperature is room temperature, and humidity is that required humidity carries out damp condition;Can also the too high employing of humidity
Drying unit carries out reducing moisture, and humidity is too low can be sprayed a certain amount of water to increase humidity;
The present invention preferably technical scheme:Mix in the compound plant powder and selenium-rich Nicotiana tabacum L. powder of step (6) and be placed in Quercus acutissima Carr.
Bucket in refined before, in base material sprinkling account for base material weight 0.5%-5% enzymatic solution microbial solution or its
Mixture, is placed in oak barrel again after mix homogeneously and is refined;Described enzymatic solution is cellulase, pectase, protein
A kind of or its mixture in enzyme, described microbial solution is a kind of or its mixture in yeast, bacillus cereuss.
The present invention is combined alcoholization technique by the natural plant powder with clearing away heat and promoting production of body fluid effect and the " Qingjian River using oak barrel
Source " selenium-rich Nicotiana tabacum L. powder compatibility is processed, also including appropriate essence, Sal, acid-base modifier, sweeting agent, by above-mentioned compound
The packed mouth containing tobacco product of alcoholization technique and composition collocation mixing composition multi-form, not only fragrance fusion is preferable, jealous coordination,
Comfortable taste, while also providing trace element needed by human, and also has functions that clearing away heat and promoting production of body fluid.
Specific embodiment
The technical scheme in the present invention is clearly and completely described below by specific embodiment.It should be appreciated that
Specific embodiment described by this part can only be used to explain the present invention, be not intended to limit the present invention.
Burley tobaccos absolute oil in following examples is prepared from accordance with the following methods:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110
Agitating heating reflux extraction 1-10 hours at a temperature of ± 5 DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with
The supernatant collected in step a merges, and then pours the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum
Burley tobaccos extract is more than thick liquid is concentrated under conditions of 0.95Mpa;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:3-20
Ratio mixing, stand the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and
Pour into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa
To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
Described selenium-rich Nicotiana tabacum L. in following examples, should using " Qing Jiangyuan " pure ecological selenium-rich Nicotiana tabacum L. of bestowing favour is originated in
Nicotiana tabacum L. is that tobacco seedlings are transplanted to the position of the height above sea level 800-1000m that bestows favour, soil Se content more than 0.45mg/kg normally to plant out
The selenium-rich cigarette for coming, selenium-rich Tobacco Leaves Se content 0.3-0.8mg/kg need not additionally apply selenium element in planting process.
A kind of embodiment 1, packed buccal cigarette, its concrete preparation method is as follows:
Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), Spina Gleditsiae, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content
0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible wind election process, remove the impurity in material, are then crushed respectively again
Process, retain powder more than 80 mesh, by plant powder Fructus Mume 20% by weight percentage, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 2%,
Radix Arnebiae (Radix Lithospermi) 20%, Spina Gleditsiae 8%, hook Herba Dendrobii 15%, Herba Eriae Graminifoliae 10%, the compounding of Herba Violae 15% obtains compound plant powder,
Then compound plant powder 2000g and selenium-rich Nicotiana tabacum L. powder 4000g mix homogeneously are taken, in being placed in sealing oak barrel, is in temperature
30 DEG C, humidity is to carry out compound alcoholization 50d under conditions of 70%;Compound base material after purification is taken out, Sal 100g, Fructus Citri Limoniae is added
Sour disodium hydrogen 70g, liquirtin 100g mix homogeneously, in being placed in sealing container, are passed through 100-110 DEG C of steam treatment 15min, so
200g essence is added in backward mixed resin, and (essence is formulated by the material of following percentage by weight:Burley tobaccos are net
Oil 0.8%, yunyan extract 1%, Mel 2%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%,
2- acetyl group pyrazine 0.1%, furanone 0.05%, Propylene Glycol 95.05%), its moisture 35.3% is adjusted, finally will be above-mentioned
Material carries out pack process, and carries out ultraviolet sterilization, obtains final product packed mouth containing smoke product.
A kind of embodiment 2, packed buccal cigarette, its concrete preparation method is as follows:Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), soap
Fructus Gleditsia acupuncture, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content 0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible selecting crude drugs with winnower work
Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder
Fructus Mume 10% by weight percentage, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 5%, Radix Arnebiae (Radix Lithospermi) 25%, Spina Gleditsiae 10%, hook Herba Dendrobii 20%, standing grain leaf
Black dry measure used in former times 10%, the compounding of Herba Violae 10% obtains compound plant powder, then takes compound plant 1500g, selenium-rich cigarette 5000g mixing
Uniformly, in 25 DEG C of temperature, being placed in the environment of humidity 65% in sealing oak barrel carries out compound alcoholization 40 days, after taking out alcoholization
Base material, adds Sal 100g, sodium citrate 70g, cyclamate 100g, then uses at 100-110 DEG C of vapor under closed environment
Reason 20min, then adds 150g essence in mixed resin, and (essence is by the material preparation of following percentage by weight
Into:Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, Mel 2.5%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, second
Base maltol 0.5%, 2- acetyl group pyrazine 0.1%, furanone 0.05%, Propylene Glycol 94.05%), adjust moisture
30.8%, finally above-mentioned material is carried out into pack process, and ultraviolet sterilization is carried out, obtain final product packed mouth containing smoke product.
A kind of embodiment 3, packed buccal cigarette, its concrete preparation method is as follows:Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), soap
Fructus Gleditsia acupuncture, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content 0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible selecting crude drugs with winnower work
Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder
Fructus Mume 10% by weight, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 5%, Radix Arnebiae (Radix Lithospermi) 25%, Spina Gleditsiae 10%, hook Herba Dendrobii 20%, Herba Eriae Graminifoliae
10%, the compounding of Herba Violae 10% obtains compound plant powder, then takes compound plant 1000g, selenium-rich cigarette 5000g mixing equal
It is even, in base material spray solution consumption account for base material weight 1% compound enzyme (compound enzyme be by pectase and cellulase by
Compare 1 according to weight:1 ratio is mixed), in 25 DEG C of temperature, being placed in the environment of humidity 65% in oak barrel carries out compound alcohol
Change 40 days, take out the base material for having refined, after adding Sal 100g, sodium citrate 70g, cyclamate 100g mix homogeneously, be placed in close
In envelope container, 100-110 DEG C of steam treatment 20min is passed through into container, 200g essence (institute is then added in mixed resin
Stating essence is formulated by the material of following percentage by weight:Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, Mel
2.5%th, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%, 2- acetyl group pyrazine 0.1%, furan
Ketone 0.05%, Propylene Glycol 94.05%), moisture 35.3% is adjusted, finally above-mentioned material is carried out into pack process, and carry out
Ultraviolet sterilization, obtains final product packed mouth containing smoke product.
The mouth containing smoke product prepared in three embodiments is smoked panel test by the group of smokeing panel test of specialty, its smoking result is such as
Shown in table 1:
Table 1 sucks smoke product effect assessment
Mouth containing smoke product | Evaluation effect |
Embodiment 1 | Fragrance is preferably, jealous general, there is certain stimulation to oral cavity, and clearing away heat and promoting production of body fluid effect is preferable |
Embodiment 2 | Fragrance is elegant, jealous coordination, less to oral stimulation, and clearing away heat and promoting production of body fluid effect is preferable |
Embodiment 3 | Fragrance is elegant, jealous coordination, less to oral stimulation, and clearing away heat and promoting production of body fluid effect is preferable |
Claims (7)
1. a kind of packed buccal cigarette, it is characterised in that be by the material composition of following percentage by weight:
Wherein:The compound plant is by the material composition of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae 5%-
10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%-
12%, Herba Violae 7%-15%;
Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade selenium content 0.3-0.8mg/kg;
The essence is the material composition of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, yunyan extract 0.8-2%, honeybee
Sweet 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethylmaltol 0.3%-0.7%,
2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;
The sweeting agent is non-sugar sweetener.
2. a kind of packed buccal cigarette according to claim 1, it is characterised in that:Described acid-base modifier is sodium citrate
Or DisodiumHydrogen Citrate.
3. a kind of packed buccal cigarette according to claim 1, it is characterised in that:The non-sugar sweetener include liquirtin,
A kind of or arbitrarily several mixing in cyclamate, stevioside or acesulfame potassium.
4. a kind of packed buccal cigarette according to claim 1, it is characterised in that:Described selenium-rich Nicotiana tabacum L. be by tobacco seedlings transplant in
Bestow favour the Nicotiana tabacum L. grown in selenium-rich soil, the soil Se content of its planting site is more than 0.45mg/kg, altitude 800-
1000m。
5. a kind of packed buccal cigarette according to claim 1, it is characterised in that:The burley tobaccos absolute oil is to be with burley tobacco leaf
Raw material, is 1 according to Nicotiana tabacum L. and the ethanol mass ratio of concentration 20%:3-20 mixes, the agitating heating backflow extraction at a temperature of 110 ± 5 DEG C
1-10 hours are taken, is down to after room temperature and is stood the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, receive
Collection filtrate, and pour into after filtrate is merged with supernatant in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum more than 0.95Mpa
Under conditions of the thick liquid that is concentrated to give be burley tobaccos extract;Then burley tobaccos are carried with the ethanol of concentration 95% according to matter
Amount compares 1:The ratio mixing of 3-20, stands the clarification of 1-3 hours, extracts supernatant, and reject dregs after lower floor's slurry centrifugation are collected
Filtrate, and pour into after merging with supernatant in Rotary Evaporators in 50 ± 2 DEG C of temperature, vacuum more than under conditions of 0.95Mpa
It is concentrated into relative density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil.
6. a kind of packed buccal cigarette preparation method, it is characterised in that comprise the following steps that:
(1) compound plant raw material is prepared according to formula as below:Fructus Mume 10%-20%, Radix Sangusorbae 5%-10%, Radix Sophorae Flavescentiss 1%-5%,
Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%-12%, Herba Violae 7%-
15%;Above-mentioned raw materials are individually gone after the removal of impurity to crush, is retained powder more than 80 mesh and then is hybridly prepared into compound plant powder;
Or go the removal of impurity to be crushed again after above-mentioned raw materials are mixed, retain powder more than 80 mesh and obtain compound plant powder;
(2) burley tobaccos absolute oil is prepared:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110 ± 5
Agitating heating reflux extraction 1-10 hours at a temperature of DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collects filtrate, and by filtrate and step
The supernatant collected in a merges, and then pours in Rotary Evaporators the filtrate of merging into and is more than in 60 ± 2 DEG C of temperature, vacuum
Thick liquid is concentrated under conditions of 0.95Mpa and is burley tobaccos extract;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:The ratio of 3-20
Example mixing, stands the clarification of 1-3 hours, extracts supernatant;By reject dregs after the centrifugation of lower floor slurry, collect filtrate, and with it is upper
Clear liquid is poured into relatively close more than being concentrated under conditions of 0.95Mpa in 50 ± 2 DEG C of temperature, vacuum in Rotary Evaporators after merging
Degree 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
(3) essence is prepared according to the formula of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, the cloud prepared in step (2)
Smoke-dipping paste 0.8-2%, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethyl wheat
Bud phenol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;Will be upper
State raw material mix homogeneously and be configured to essence;
(4) raw material of buccal cigarette is prepared according to the formula of following percentage by weight:The compound recipe prepared in 10%-30% steps (1)
Essence, 0.1%-2% Sal, the 0.5%- prepared in Plant Powder, the selenium-rich Nicotiana tabacum L. of 30%-60%, 0.1%-4% steps (1)
1% acid-base modifier, 0.5%-1.5% sweeting agents;Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade Se content 0.3-0.8mg/kg;
Described acid-base modifier is sodium citrate or DisodiumHydrogen Citrate;The sweeting agent include liquirtin, cyclamate, stevioside,
A kind of or arbitrarily several mixing in acesulfame potassium;
(5) the whole selenium-rich tobacco leaf pickings in step (4) are removed into the impurity in material with flexible wind election process, is then carried out again
Pulverization process, the powder for retaining more than 80 mesh is selenium-rich Nicotiana tabacum L. powder;
(6) by the selenium-rich Nicotiana tabacum L. powder mix homogeneously in the compound plant powder in step (4) and step (5), it is placed in sealing Quercus acutissima Carr.
It it is 25-35 DEG C in temperature in bucket, humidity is that compound alcoholization 30d-60d is carried out under conditions of 60%-80%;
(7) after the compound alcoholization in step (6) terminates, the base material after compound alcoholization is taken out, is added according to the ratio in step (4)
Sal, acid-base modifier, sweeting agent, then use 100-110 DEG C of steam treatment 20-40min under closed environment;
(8) after the cooling of above-mentioned base material, essence is added in the ratio in step (4), regulation humidity is 15%-50%, Ran Houjin
Luggage bag, and packed mouth containing smoke product is obtained after sterilization processing.
7. a kind of packed buccal cigarette preparation method according to claim 5, it is characterised in that:Plant in the compound recipe of step (6)
Thing powder and the mixing of selenium-rich Nicotiana tabacum L. powder are placed in before being refined in oak barrel, and the sprinkling in base material accounts for base material weight
The enzymatic solution or microbial solution or its mixture of 0.5%-5%, is placed in oak barrel again after mix homogeneously and is refined;It is described
Enzymatic solution be a kind of in cellulase, pectase, protease or its mixture, described microbial solution be yeast,
A kind of or its mixture in bacillus cereuss.
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