CN106579538A - Bagged mouth-holding cigarette and preparation method therefor - Google Patents

Bagged mouth-holding cigarette and preparation method therefor Download PDF

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Publication number
CN106579538A
CN106579538A CN201611153248.7A CN201611153248A CN106579538A CN 106579538 A CN106579538 A CN 106579538A CN 201611153248 A CN201611153248 A CN 201611153248A CN 106579538 A CN106579538 A CN 106579538A
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selenium
rich
nicotiana tabacum
powder
burley tobaccos
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CN106579538B (en
Inventor
刘冰
陈义坤
罗诚浩
柯炜昌
齐富友
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B13/00Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26Use of organic solvents for extraction

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention provides a bagged mouth-holding cigarette and a preparation method therefor. The bagged mouth-holding cigarette is prepared through the following method, and the method comprises the steps: mixing a compound plant and selenium-rich tobacco leaves and uniformly placing the mixture in a sealed oak barrel; carrying out the recombination alcoholization of the mixture for 30-60d under the conditions that the temperature is 25-35 DEG and the humidity is 60%-80%, and then adding salt, an acid-base conditioning agent and a sweetening agent to an alcoholized base material; carrying out the processing for 20-40 min through steam with the temperature from 100 DEG C to 110 DEG C; adding essence according to a proportion after the base material is cooled, and adjusting the humidity to be 15%-50%, and finally carrying out the bagging. The compound plant consists of dark plum, garden burnet, radix sophorae flavescentis, lithospermum, spina gleditsiae, hooked dendrobium, herb of grassleaf eria and Chinese violet. The selenium content of the selenium-rich tobacco leaves is 0.3-0.8mg/kg. The oak barrel is employed for recombination alcoholization and ingredient matching and mixing to form bagged mouth-holding cigarettes in different forms. The mouth-holding cigarette is better in fragrance fusion, is coordinative in taste, is comfortable in taste, also provides necessary microelements for human bodies, and has an effect of removing heat to promote salivation.

Description

A kind of packed buccal cigarette and preparation method thereof
Technical field
The invention belongs to smoke-free tobacco product and its processing technique field, and in particular to a kind of packed buccal cigarette and its system Preparation Method.
Background technology
Selenium is teleorganic trace element, and by scientist " king of anticancer " is referred to as in body trace element, is human body paddy Guang (sweet peptide peroxidase GSH-Px) important activity composition, plays a part of to remove interior free yl;With removing toxic substances, toxin expelling, Defying age, antioxidation, the effect of enhance immunity, selenium can play reduction gene mutagenicity, the work of DNA plerosis in human body With.Meanwhile, selenium can reduce the toxicity of nicotine and tar, and suppression is played to tumor, have opposing to various carcinogen in flue gas Effect;Also studies have reported that suction iodine enriched cigarette can make human body blood selenium level relatively aspirate regular-size cigarette human body blood selenium level at present It is high by 10%.So people also begin to study iodine enriched cigarette, existing iodine enriched cigarette is substantially the Medicated cigarette of suction, although can also Increase the content of human body selenium, but because Nicotiana tabacum L. needs burning, still can produce substantial amounts of flue gas, danger is brought to health Evil.
Packed buccal cigarette belongs to a kind of form of smoke-free tobacco product, is used by being put between lip and gingiva, has Need not burn, not produce second hand smoking harm, be received by increasing consumer.Because buccal cigarette is unlike traditional cigarette Burning is equally participated in, therefore can be theoretical by Chinese medicine scientific compatibility according to " monarch " of the traditional Chinese medical science so as to control with certain Treat and health-care effect.The A of Chinese patent CN 105054279 disclose a kind of selenium-rich buccal cigarette and preparation method thereof, in the patent Buccal cigarette in selenium source mostly come from chemicals selenic ester polysaccharide, be not very healthy, and cannot play health care work With.Although also there is the buccal cigarette of some health-care types, such as characteristic food is produced in a kind of river disclosed in Chinese patent CN 105124748A The moistening lung and nourishing throat health buccal cigarette produced, is to produce in the river based on Fructus Citri grandiss, pears, Rhizoma Nelumbiniss, Caulis Sacchari sinensis, Corm Eleocharitiss, Herba Houttuyniae and Folium Eriobotryae Characteristic food and tobacco extract compatibility, the method for preparing moistening lung and nourishing throat health buccal cigarette.Chinese patent CN104997153A Disclose a kind of river and produce the moistening lung and nourishing throat health buccal cigarette that Special Traditional Chinese Medicine is produced, be with tobacco extract and Radix Scutellariae, Fructus Canarii, Fructus Citri tangerinae Produce the method that the extract of Special Traditional Chinese Medicine prepares moistening lung and nourishing throat health buccal cigarette in river based on stalk, Bulbus Fritillariae Cirrhosae and Flos Lonicerae.These Buccal cigarette is all directly that by food or Chinese medicine together with common Nicotiana tabacum L. compatibility, its health-care effect is not fine, and Supplementary human body selenium source is not played a part of.
The content of the invention
For above-mentioned situation, the present invention provides a kind of packed buccal cigarette and preparation method thereof, and the buccal cigarette adopts natural plant Thing compatibility, is combined the techniques such as alcoholization, prepares that outlet plenum is comfortable, the pure ecological selenium-rich mouth containing smoke product that fragrance is coordinated.
The technical solution used in the present invention is as follows:A kind of packed buccal cigarette, it is characterised in that be by following weight hundred Divide the material composition of ratio:
The total weight percent of above-mentioned substance is 100%.
Wherein:The compound plant is by the material composition of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae 5%-10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%-12%, Herba Violae 7%-15%;
Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade Se content 0.3-0.8mg/kg;
The essence is the material composition of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, yunyan extract 0.8- 2%th, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethylmaltol 0.3%- 0.7%th, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;Thing in above-mentioned essence Matter is the product of direct purchase;
The sweeting agent is non-sugar sweetener;
The water is the water content of the final products prepared through process in all materials, is 15%-50%.
Further technical scheme of the invention:Described acid-base modifier is sodium citrate or DisodiumHydrogen Citrate.It is described Non-sugar sweetener includes a kind of in liquirtin, cyclamate, stevioside or acesulfame potassium or any several mixing.The acid-alkali accommodation Agent and sweeting agent are the product of direct purchase.Described selenium-rich Nicotiana tabacum L. is that Flue-cured Tobacco transplantation of seedlings is raw in selenium-rich soil of bestowing favour Long cured tobacco leaf, the soil Se content of its planting site is more than 0.45mg/kg, altitude 800-1000m;Selenium-rich cigarette can With direct using natural selenium-rich cigarette " Qing Jiangyuan " Nicotiana tabacum L. of bestowing favour.
The present invention preferably technical scheme:The burley tobaccos absolute oil is with burley tobacco leaf as raw material, by Nicotiana tabacum L. and concentration 20% ethanol mass ratio is 1:The ratio mixing of 3-20, the agitating heating reflux extraction 1-10 hours at a temperature of 110 ± 5 DEG C, drop The clarification of 1-3 hours is stood to room temperature, supernatant is extracted;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and will filter Liquid is poured in Rotary Evaporators after merging with supernatant and is concentrated to give under conditions of 60 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa To thick liquid be burley tobaccos extract;Then burley tobaccos are carried with the ethanol of concentration 95% according to mass ratio 1:The ratio of 3-20 Example mixing, stands the clarification of 1-3 hours, extracts supernatant, and reject dregs after lower floor's slurry centrifugation collect filtrate, and and supernatant Liquid is poured in Rotary Evaporators after merging and is concentrated into relative density under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa 0.9-1.3g/cm3Obtain burley tobaccos absolute oil.
A kind of packed buccal cigarette preparation method that the present invention is provided, it is characterised in that processing method is as follows:
(1) compound plant raw material is prepared according to the formula of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae 5%- 10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%- 12%, Herba Violae 7%-15%;Above-mentioned raw materials are individually gone after the removal of impurity to crush, is retained powder more than 80 mesh and then is mixed It is configured to compound plant powder;Or go the removal of impurity to be crushed again after above-mentioned raw materials are mixed, retain powder more than 80 mesh and obtain Compound plant powder;
(2) burley tobaccos absolute oil is prepared:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110 Agitating heating reflux extraction 1-10 hours at a temperature of ± 5 DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with The supernatant collected in step a merges, and then pours the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum Burley tobaccos extract is more than thick liquid is concentrated under conditions of 0.95Mpa;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:3-20 Ratio mixing, stand the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and Pour into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
(3) essence is prepared according to the formula of following percentage by weight:The burley tobaccos absolute oil 0.5%- prepared in step (2) 1%th, yunyan extract 0.8-2%, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, Ethylmaltol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of the third two Alcohol;Above-mentioned raw materials mix homogeneously is configured to into essence;
(4) raw material of buccal cigarette is prepared according to formula as below:The middle compound plant powder for preparing of 10%-30% steps (1), The essence of preparation, 0.1%-2% Sal, 0.5%-1% are sour in the step of selenium-rich Nicotiana tabacum L., 0.1%-4% of 30%-60% (1) Alkali regulator, 0.5%-1.5% sweeting agents, excess water;
(5) the whole selenium-rich tobacco leaf pickings in step (4) are removed into the impurity in material, Ran Houzai with flexible wind election process Pulverization process is carried out, the powder for retaining more than 80 mesh is selenium-rich Nicotiana tabacum L. powder;The flexible wind election process be existing process, its work Skill principle is that the Nicotiana tabacum L. cut tobacco after pneumatic conveying drying is sent into into free-falling after selecting crude drugs with winnower casing by feeding mechanism, using casing it is vertical and Horizontal bidirectional air intake carries out float choosing and flotation to cut tobacco, makes density larger object such as impurity, stalk label etc. by secondary separation case Body falls, and the lighter cut tobacco of density will send casing by discharging mechanism, so as to realize the dedoping step of material;
(6) by the selenium-rich Nicotiana tabacum L. powder mix homogeneously in the compound plant powder in step (4) and step (5), it is placed in sealing It it is 25-35 DEG C in temperature in oak barrel, humidity is that compound alcoholization 30d-60d is carried out under conditions of 60%-80%;
(7) after the compound alcoholization in step (6) terminates, the base material after compound alcoholization is taken out, according to the ratio in step (4) Sal, acid-base modifier, sweeting agent are added, 100-110 DEG C of steam treatment 20-40min is then used under closed environment;
(8) after the cooling of above-mentioned base material, essence is added in the ratio in step (4), regulation humidity is 15%-50%, so Laggard luggage bag, and packed mouth containing smoke product is obtained after sterilization processing;Adjusting the mode of humidity can be placed directly in constant temperature In the system of constant humidity, regulation temperature is room temperature, and humidity is that required humidity carries out damp condition;Can also the too high employing of humidity Drying unit carries out reducing moisture, and humidity is too low can be sprayed a certain amount of water to increase humidity;
The present invention preferably technical scheme:Mix in the compound plant powder and selenium-rich Nicotiana tabacum L. powder of step (6) and be placed in Quercus acutissima Carr. Bucket in refined before, in base material sprinkling account for base material weight 0.5%-5% enzymatic solution microbial solution or its Mixture, is placed in oak barrel again after mix homogeneously and is refined;Described enzymatic solution is cellulase, pectase, protein A kind of or its mixture in enzyme, described microbial solution is a kind of or its mixture in yeast, bacillus cereuss.
The present invention is combined alcoholization technique by the natural plant powder with clearing away heat and promoting production of body fluid effect and the " Qingjian River using oak barrel Source " selenium-rich Nicotiana tabacum L. powder compatibility is processed, also including appropriate essence, Sal, acid-base modifier, sweeting agent, by above-mentioned compound The packed mouth containing tobacco product of alcoholization technique and composition collocation mixing composition multi-form, not only fragrance fusion is preferable, jealous coordination, Comfortable taste, while also providing trace element needed by human, and also has functions that clearing away heat and promoting production of body fluid.
Specific embodiment
The technical scheme in the present invention is clearly and completely described below by specific embodiment.It should be appreciated that Specific embodiment described by this part can only be used to explain the present invention, be not intended to limit the present invention.
Burley tobaccos absolute oil in following examples is prepared from accordance with the following methods:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110 Agitating heating reflux extraction 1-10 hours at a temperature of ± 5 DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collect filtrate, and by filtrate with The supernatant collected in step a merges, and then pours the filtrate of merging in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum Burley tobaccos extract is more than thick liquid is concentrated under conditions of 0.95Mpa;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:3-20 Ratio mixing, stand the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, filtrate is collected, and Pour into after merging with supernatant in Rotary Evaporators and be concentrated into phase under conditions of 50 ± 2 DEG C of temperature, vacuum are more than 0.95Mpa To density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
Described selenium-rich Nicotiana tabacum L. in following examples, should using " Qing Jiangyuan " pure ecological selenium-rich Nicotiana tabacum L. of bestowing favour is originated in Nicotiana tabacum L. is that tobacco seedlings are transplanted to the position of the height above sea level 800-1000m that bestows favour, soil Se content more than 0.45mg/kg normally to plant out The selenium-rich cigarette for coming, selenium-rich Tobacco Leaves Se content 0.3-0.8mg/kg need not additionally apply selenium element in planting process.
A kind of embodiment 1, packed buccal cigarette, its concrete preparation method is as follows:
Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), Spina Gleditsiae, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content 0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible wind election process, remove the impurity in material, are then crushed respectively again Process, retain powder more than 80 mesh, by plant powder Fructus Mume 20% by weight percentage, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 2%, Radix Arnebiae (Radix Lithospermi) 20%, Spina Gleditsiae 8%, hook Herba Dendrobii 15%, Herba Eriae Graminifoliae 10%, the compounding of Herba Violae 15% obtains compound plant powder, Then compound plant powder 2000g and selenium-rich Nicotiana tabacum L. powder 4000g mix homogeneously are taken, in being placed in sealing oak barrel, is in temperature 30 DEG C, humidity is to carry out compound alcoholization 50d under conditions of 70%;Compound base material after purification is taken out, Sal 100g, Fructus Citri Limoniae is added Sour disodium hydrogen 70g, liquirtin 100g mix homogeneously, in being placed in sealing container, are passed through 100-110 DEG C of steam treatment 15min, so 200g essence is added in backward mixed resin, and (essence is formulated by the material of following percentage by weight:Burley tobaccos are net Oil 0.8%, yunyan extract 1%, Mel 2%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%, 2- acetyl group pyrazine 0.1%, furanone 0.05%, Propylene Glycol 95.05%), its moisture 35.3% is adjusted, finally will be above-mentioned Material carries out pack process, and carries out ultraviolet sterilization, obtains final product packed mouth containing smoke product.
A kind of embodiment 2, packed buccal cigarette, its concrete preparation method is as follows:Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), soap Fructus Gleditsia acupuncture, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content 0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible selecting crude drugs with winnower work Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder Fructus Mume 10% by weight percentage, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 5%, Radix Arnebiae (Radix Lithospermi) 25%, Spina Gleditsiae 10%, hook Herba Dendrobii 20%, standing grain leaf Black dry measure used in former times 10%, the compounding of Herba Violae 10% obtains compound plant powder, then takes compound plant 1500g, selenium-rich cigarette 5000g mixing Uniformly, in 25 DEG C of temperature, being placed in the environment of humidity 65% in sealing oak barrel carries out compound alcoholization 40 days, after taking out alcoholization Base material, adds Sal 100g, sodium citrate 70g, cyclamate 100g, then uses at 100-110 DEG C of vapor under closed environment Reason 20min, then adds 150g essence in mixed resin, and (essence is by the material preparation of following percentage by weight Into:Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, Mel 2.5%, guaiacol 0.3%, 6-Methylcoumarin 0.2%, second Base maltol 0.5%, 2- acetyl group pyrazine 0.1%, furanone 0.05%, Propylene Glycol 94.05%), adjust moisture 30.8%, finally above-mentioned material is carried out into pack process, and ultraviolet sterilization is carried out, obtain final product packed mouth containing smoke product.
A kind of embodiment 3, packed buccal cigarette, its concrete preparation method is as follows:Take Fructus Mume, Radix Sangusorbae, Radix Sophorae Flavescentiss, Radix Arnebiae (Radix Lithospermi), soap Fructus Gleditsia acupuncture, hook Herba Dendrobii, Herba Eriae Graminifoliae, Herba Violae and blade Se content 0.3-0.8mg/kg selenium-rich Nicotiana tabacum Lves, using flexible selecting crude drugs with winnower work Skill, removes the impurity in material, is then carried out pulverization process respectively again, retains powder more than 80 mesh, by plant powder Fructus Mume 10% by weight, Radix Sangusorbae 10%, Radix Sophorae Flavescentiss 5%, Radix Arnebiae (Radix Lithospermi) 25%, Spina Gleditsiae 10%, hook Herba Dendrobii 20%, Herba Eriae Graminifoliae 10%, the compounding of Herba Violae 10% obtains compound plant powder, then takes compound plant 1000g, selenium-rich cigarette 5000g mixing equal It is even, in base material spray solution consumption account for base material weight 1% compound enzyme (compound enzyme be by pectase and cellulase by Compare 1 according to weight:1 ratio is mixed), in 25 DEG C of temperature, being placed in the environment of humidity 65% in oak barrel carries out compound alcohol Change 40 days, take out the base material for having refined, after adding Sal 100g, sodium citrate 70g, cyclamate 100g mix homogeneously, be placed in close In envelope container, 100-110 DEG C of steam treatment 20min is passed through into container, 200g essence (institute is then added in mixed resin Stating essence is formulated by the material of following percentage by weight:Burley tobaccos absolute oil 0.8%, yunyan extract 1.5%, Mel 2.5%th, guaiacol 0.3%, 6-Methylcoumarin 0.2%, ethylmaltol 0.5%, 2- acetyl group pyrazine 0.1%, furan Ketone 0.05%, Propylene Glycol 94.05%), moisture 35.3% is adjusted, finally above-mentioned material is carried out into pack process, and carry out Ultraviolet sterilization, obtains final product packed mouth containing smoke product.
The mouth containing smoke product prepared in three embodiments is smoked panel test by the group of smokeing panel test of specialty, its smoking result is such as Shown in table 1:
Table 1 sucks smoke product effect assessment
Mouth containing smoke product Evaluation effect
Embodiment 1 Fragrance is preferably, jealous general, there is certain stimulation to oral cavity, and clearing away heat and promoting production of body fluid effect is preferable
Embodiment 2 Fragrance is elegant, jealous coordination, less to oral stimulation, and clearing away heat and promoting production of body fluid effect is preferable
Embodiment 3 Fragrance is elegant, jealous coordination, less to oral stimulation, and clearing away heat and promoting production of body fluid effect is preferable

Claims (7)

1. a kind of packed buccal cigarette, it is characterised in that be by the material composition of following percentage by weight:
Wherein:The compound plant is by the material composition of following percentage by weight:Fructus Mume 10%-20%, Radix Sangusorbae 5%- 10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%- 12%, Herba Violae 7%-15%;
Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade selenium content 0.3-0.8mg/kg;
The essence is the material composition of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, yunyan extract 0.8-2%, honeybee Sweet 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethylmaltol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;
The sweeting agent is non-sugar sweetener.
2. a kind of packed buccal cigarette according to claim 1, it is characterised in that:Described acid-base modifier is sodium citrate Or DisodiumHydrogen Citrate.
3. a kind of packed buccal cigarette according to claim 1, it is characterised in that:The non-sugar sweetener include liquirtin, A kind of or arbitrarily several mixing in cyclamate, stevioside or acesulfame potassium.
4. a kind of packed buccal cigarette according to claim 1, it is characterised in that:Described selenium-rich Nicotiana tabacum L. be by tobacco seedlings transplant in Bestow favour the Nicotiana tabacum L. grown in selenium-rich soil, the soil Se content of its planting site is more than 0.45mg/kg, altitude 800- 1000m。
5. a kind of packed buccal cigarette according to claim 1, it is characterised in that:The burley tobaccos absolute oil is to be with burley tobacco leaf Raw material, is 1 according to Nicotiana tabacum L. and the ethanol mass ratio of concentration 20%:3-20 mixes, the agitating heating backflow extraction at a temperature of 110 ± 5 DEG C 1-10 hours are taken, is down to after room temperature and is stood the clarification of 1-3 hours, extract supernatant;By reject dregs after lower floor's slurry centrifugation, receive Collection filtrate, and pour into after filtrate is merged with supernatant in Rotary Evaporators in 60 ± 2 DEG C of temperature, vacuum more than 0.95Mpa Under conditions of the thick liquid that is concentrated to give be burley tobaccos extract;Then burley tobaccos are carried with the ethanol of concentration 95% according to matter Amount compares 1:The ratio mixing of 3-20, stands the clarification of 1-3 hours, extracts supernatant, and reject dregs after lower floor's slurry centrifugation are collected Filtrate, and pour into after merging with supernatant in Rotary Evaporators in 50 ± 2 DEG C of temperature, vacuum more than under conditions of 0.95Mpa It is concentrated into relative density 0.9-1.3g/cm3Obtain burley tobaccos absolute oil.
6. a kind of packed buccal cigarette preparation method, it is characterised in that comprise the following steps that:
(1) compound plant raw material is prepared according to formula as below:Fructus Mume 10%-20%, Radix Sangusorbae 5%-10%, Radix Sophorae Flavescentiss 1%-5%, Radix Arnebiae (Radix Lithospermi) 15%-25%, Spina Gleditsiae 5%-10%, hook Herba Dendrobii 15%-20%, Herba Eriae Graminifoliae 6%-12%, Herba Violae 7%- 15%;Above-mentioned raw materials are individually gone after the removal of impurity to crush, is retained powder more than 80 mesh and then is hybridly prepared into compound plant powder; Or go the removal of impurity to be crushed again after above-mentioned raw materials are mixed, retain powder more than 80 mesh and obtain compound plant powder;
(2) burley tobaccos absolute oil is prepared:
A. with burley tobacco leaf as raw material, the rear and ethanol of concentration 20% is crushed according to mass ratio 1:3-20 mixes, 110 ± 5 Agitating heating reflux extraction 1-10 hours at a temperature of DEG C, are down to after room temperature and stand the clarification of 1-3 hours, extract supernatant;
B. reject dregs after the lower floor slurry centrifugation after supernatant will be extracted in step a, collects filtrate, and by filtrate and step The supernatant collected in a merges, and then pours in Rotary Evaporators the filtrate of merging into and is more than in 60 ± 2 DEG C of temperature, vacuum Thick liquid is concentrated under conditions of 0.95Mpa and is burley tobaccos extract;
C. burley tobaccos absolute oil is prepared:By burley tobaccos extract in step b and the ethanol of concentration 95% according to mass ratio 1:The ratio of 3-20 Example mixing, stands the clarification of 1-3 hours, extracts supernatant;By reject dregs after the centrifugation of lower floor slurry, collect filtrate, and with it is upper Clear liquid is poured into relatively close more than being concentrated under conditions of 0.95Mpa in 50 ± 2 DEG C of temperature, vacuum in Rotary Evaporators after merging Degree 0.9-1.3g/cm3Obtain burley tobaccos absolute oil;
(3) essence is prepared according to the formula of following percentage by weight:Burley tobaccos absolute oil 0.5%-1%, the cloud prepared in step (2) Smoke-dipping paste 0.8-2%, Mel 1%-5%, guaiacol 0.1%-0.5%, 6-Methylcoumarin 0.1%-0.3%, ethyl wheat Bud phenol 0.3%-0.7%, 2- acetyl group pyrazine 0.05%-0.2%, furanone 0.01%-0.1%, balance of Propylene Glycol;Will be upper State raw material mix homogeneously and be configured to essence;
(4) raw material of buccal cigarette is prepared according to the formula of following percentage by weight:The compound recipe prepared in 10%-30% steps (1) Essence, 0.1%-2% Sal, the 0.5%- prepared in Plant Powder, the selenium-rich Nicotiana tabacum L. of 30%-60%, 0.1%-4% steps (1) 1% acid-base modifier, 0.5%-1.5% sweeting agents;Described selenium-rich Nicotiana tabacum L. is the Nicotiana tabacum L. of blade Se content 0.3-0.8mg/kg; Described acid-base modifier is sodium citrate or DisodiumHydrogen Citrate;The sweeting agent include liquirtin, cyclamate, stevioside, A kind of or arbitrarily several mixing in acesulfame potassium;
(5) the whole selenium-rich tobacco leaf pickings in step (4) are removed into the impurity in material with flexible wind election process, is then carried out again Pulverization process, the powder for retaining more than 80 mesh is selenium-rich Nicotiana tabacum L. powder;
(6) by the selenium-rich Nicotiana tabacum L. powder mix homogeneously in the compound plant powder in step (4) and step (5), it is placed in sealing Quercus acutissima Carr. It it is 25-35 DEG C in temperature in bucket, humidity is that compound alcoholization 30d-60d is carried out under conditions of 60%-80%;
(7) after the compound alcoholization in step (6) terminates, the base material after compound alcoholization is taken out, is added according to the ratio in step (4) Sal, acid-base modifier, sweeting agent, then use 100-110 DEG C of steam treatment 20-40min under closed environment;
(8) after the cooling of above-mentioned base material, essence is added in the ratio in step (4), regulation humidity is 15%-50%, Ran Houjin Luggage bag, and packed mouth containing smoke product is obtained after sterilization processing.
7. a kind of packed buccal cigarette preparation method according to claim 5, it is characterised in that:Plant in the compound recipe of step (6) Thing powder and the mixing of selenium-rich Nicotiana tabacum L. powder are placed in before being refined in oak barrel, and the sprinkling in base material accounts for base material weight The enzymatic solution or microbial solution or its mixture of 0.5%-5%, is placed in oak barrel again after mix homogeneously and is refined;It is described Enzymatic solution be a kind of in cellulase, pectase, protease or its mixture, described microbial solution be yeast, A kind of or its mixture in bacillus cereuss.
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