CN105831798B - Fermented type buccal cigarette with slow-release function and preparation method thereof and buccal cigarette - Google Patents
Fermented type buccal cigarette with slow-release function and preparation method thereof and buccal cigarette Download PDFInfo
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- CN105831798B CN105831798B CN201610323524.3A CN201610323524A CN105831798B CN 105831798 B CN105831798 B CN 105831798B CN 201610323524 A CN201610323524 A CN 201610323524A CN 105831798 B CN105831798 B CN 105831798B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
- A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
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- Life Sciences & Earth Sciences (AREA)
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of fermented type buccal cigarette with slow-release function and preparation method thereof and buccal cigarettes.The buccal cigarette is by pipe blend particle 50%~80%, water 10%~30%, corrigent 1%~5%, sweetener 1%~5%, flavouring agent 1%~10% is formulated, and the pipe blend particle is the mixture of pipe tobacco particle and microcapsule granule, and the mixing quality ratio of the two is 2:1~4:1.Science of the present invention is using microencapsulated, overcome that existing product nicotine rate of release is too fast, the mouth containing excessive later stage strength of strength early period is smaller, the quick thin out deficiency of smoke during entire mouth containing, increase mouth containing initial stage nicotine dissolution resistance, under the premise of not changing overall nicotine burst size, delay the time that nicotine at the uniform velocity dissolves out, to ensure that during mouth containing stable strength and smoke, and the not additional alkali salt of the present invention can be kept in a longer period of time.
Description
Technical field
The present invention relates to tobacco leaf production technical fields, packed more particularly, to a kind of fermented type with slow-release function
The preparation method and buccal cigarette of buccal cigarette.
Background technology
Smoke-free tobacco product refers to and the tobacco system of consumption directly being sucked by oral cavity or nasal cavity without combustion process
Product.
World Health Organization's Framework Convention on Tobacco Control (WHO FCTC) is proposed in relation to forbidding tobacco smoke in public field
It limitations and the ban such as spreads, strong impact is caused to the development of conventional tobacco products cigarette.In this background, countries in the world
Tobacco business using the research and development of smoke-free tobacco product and is introduced to the market as the important of solution tobacco business future development
Means, in Europe, South and North America, India and Africa, smoke-less tobacco product it is various in style, consumption figure various countries be in year by year
Increased trend.By taking the U.S. as an example, in 2006 years, consumption figure is more than 4,000,000,000 dollars.
Buccal cigarette is a kind of smokeless tobacco containing nicotine, typically tobacco is clayed into power again plus salt and water mix and
At, sometimes also can add fragrance, seem bergamot oil, attar of rose or Radix Glycyrrhizae.Earliest buccal cigarette is in bulk, when sucking with
Finger is kneaded into a small group, then fills in upper lip rear.Since 1973, buccal cigarette was installed in as in the pouch small tea bag.
Currently, the researcher of domestic Field of Tobacco copes with the new change of international Field of Tobacco development, develops and be suitble to the country
The smoke-free tobacco product of tobacco consumer.Such as publication：A kind of mouth insertion tobacco product (200810050106.7) is packed
Mouth insertion tobacco product and preparation method thereof (200810049347.X), bagged buccal tobacco product (200810049346.5).
Bagging mouth-sucked drying tobacco products and preparation method thereof (200810049349.9), bagged buccal tobacco product
(200810049346.5) it is each provided with related smoke-free tobacco product.
The sense organ impact strength of smoke-free tobacco product is mainly influenced by the organoleptic attribute of tobacco material, external product in order to
Ensure the fire-cured tobacco for having significant proportion in its distinctive common tobacco material formula of organoleptic feature.Since fire-cured tobacco is state
Outer distinctive tobacco material, the raw material that this largely limits domestic Foreign Experience exploitation smoke-free tobacco product are empty
Between.And its of smoke-free tobacco product of domestic-developed is mainly characterized by through all kinds of conditioning agents, humectant, flavouring agent etc. at present
Formula modulation is carried out, domestic current smoke-free tobacco product technique is mostly directly using tobacco material grinding, seasoning, dress
Bag, that there are irritations is excessive, bitter taste is dense, acid is strong, is not directed to the fermentation process technique of tobacco material.
Usually there are two types of processing modes for the tobacco material of preparation buccal cigarette, and one is tobacco natural is air-dried or high temperature goes out
Bacterium, production method are to be mixed the tobacco leaf after natural air drying or high-temperature sterilization with sodium carbonate and water, then add fragrance again
Composition seems bergamot oil, attar of rose, Radix Glycyrrhizae and spice etc..Such as the China that number of patent application is 201410093051 is specially
Profit application provides a kind of packed mouth insertion tobacco article formulations of wet type granular and preparation method thereof, the raw tobacco material of use from
It is 12~16% so to air-dry to moisture.Another kind is made tobacco leaf is fermented (U.S.'s buccal cigarette).The country prepares mouth containing
Cigarette additionally uses a kind of raw material, such as application No. is 201310663425 Chinese patent applications using cigarette industry by-product work
To prepare the tobacco particle material of buccal cigarette, the cigarette industry by-product is the by-product generated between Primary processing shop or volume hired car
Product from the mixing of one or more of flue-cured tobacco, burley tobaccos, drying cigarette, Turkish tobaccos, and are fragment, sesame-seed slice, offal, stalk
One or more of mixing of label.But some have passed through ferment making in these cigarette industry by-products, some does not have, and is made
To prepare the raw material of buccal cigarette, quality is difficult to control, it is difficult to keep stable product special flavour.
Buccal cigarette is to be absorbed into nicotine in vivo by mouth containing, into blood after make one generation and rouse oneself sense.It is in oral cavity
The releasing effect of middle various composition directly determines the quality and quality of buccal cigarette.Compared with cigarette, smoke-free tobacco product pair
Raw tobacco material quality requirements higher, this is because：General 700~800 milligram/of Cigarette weight, all after burning only
1% or so substance enters flue gas, and after filter tip filters, the amount finally experienced by smoker is very little.And smokeless cigarette
Straw-made articles directly acts on human body without burning, therefore the quality of tobacco material is even more important.
According to known in production of cigarettes technology, there are many quality defects for band to some extent for the tobacco leaf without fermentation process, have
Blue foreign smell and irritation, aroma quality is dull, and perfume quantity is insufficient, if being used directly to production buccal cigarette, the defect will necessarily band
Enter finished product, or needs to add various additives to improve the defect.But existing research is it has been generally acknowledged that the mouth to ferment
Contain a greater amount of oxious component nitrosamine than the buccal cigarette of natural air drying or high-temperature sterilization containing cigarette, at present the country and buccal cigarette phase
Without reference to the relevant report for carrying out preparation buccal cigarette after specifically fermentation using tobacco leaf in the research of pass.
Nicotine be in tobacco one kind of a kind of very important alkaloid and buccal type smokeless tobacco product with the plum flavor it is important at
Point.Nicotine rate of release and burst size are the important indicators of buccal type smokeless tobacco product with the plum flavor quality safety.Research shows that:Nicotine is released
It is related to put the factors such as rate and the nicotine content of sample, pH value, moisture, granularity, but principal element is pH value.Existing buccal cigarette production
The additional alkali salt of product, at the same time, nicotine rate of release is too fast, and the mouth containing excessive later stage strength of strength early period is smaller, entire to suck
Smoke is quickly thin out in the process.In order to reach the effective control discharged to buccal type smokeless tobacco product with the plum flavor nicotine, researcher is
The research work in terms of some nicotine releases is carried out, the Chinese patent application of Publication No. CN101254023 discloses one kind
Disclose nicotine sustained-release type mouth insertion tobacco tablet.Nicotine sustained-release type mouth insertion tobacco tablet is bonded by the superposition of multilayer smoked sheet, each layer
Reconstituted tobacoo is equipped between smoked sheet, the compactness of each layer smoked sheet is from middle layer to upper and lower both sides in distribution of successively decreasing successively.To adjust
The rate of release of nicotine, it is 2 times of time compacted zone respectively to keep relatively stable strength and smoke, the density of compacted zone, is thin
4 times of loose layer are to increase the course that nicotine at the uniform velocity dissolves out；102940307 A of Publication No. CN disclose a kind of microcapsules packet
Alkali salt active constituent is encapsulated manufactured microcapsules by film raw material, and slow-release alkaline capsule slowly discharges alkalinity, can guarantee mouth containing type
PH of tobacco product during edible ensures that nicotine is discharged with molecular forms, makes the cigarette of mouth containing type cigarette between neutral environment
Alkali mouthfeel extends.The Chinese patent application of 103494324 A of Publication No. CN discloses a kind of sodium bicarbonate or sodium carbonate is acid
Alkali conditioning agent.
The mode of control nicotine rate of release all has that nicotine rate of release is very fast, difference is very big before and after pH value at present,
Difference is bigger before and after causing the mouthfeel of buccal type smokeless tobacco product with the plum flavor, suitable there are no finding at present only in conceptual phase
Method solve, make mouth containing type tobacco product popularization be restricted.
So summarizing the quality that tobacco fermentation technique is effectively improved tobacco leaf, and the seasoning processing of reasonable benefit/risk is combined to obtain cigarette
Silk particulate material, and the release of the nicotine in the pipe tobacco particle is controlled by the means of science, to obtain the mouth containing of high quality
Cigarette is urgent technical problem to be solved in the field.
Invention content
The technical problem to be solved by the present invention is to overcome the technical deficiencies of existing buccal cigarette, provide a kind of with slow-release function
The packed buccal cigarette of fermented type preparation method, pass through the macromolecular substances in microbial fermentation degrading tobacco, reduce bitter taste
And acid, comfortable taste and flavor are obtained in conjunction with the seasoning processing of reasonable benefit/risk, and by described in the control of the means of science
Nicotine release in pipe tobacco particle, can be made the buccal cigarette of high quality.
Another technical problem to be solved by the present invention is that providing the buccal cigarette of the application pipe tobacco.
The purpose of the present invention is achieved by the following technical programs：
A kind of fermented type buccal cigarette with slow-release function is provided, is obtained by the group assignment system of following mass percentage content
It arrives：
Pipe blend particle 50%~80%, water 10%~30%, corrigent 1%~5%, sweetener 1%~5% are fragrant
Taste agent 1%~10%；
The pipe blend particle is the mixture of pipe tobacco particle and microcapsule granule, and the mixing quality ratio of the two is 2:
1~4:1.
The preparation method of the pipe tobacco particle includes the following steps：
S1. prepare tobacco formulation group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 1~15g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, institute
Stating the group of inoculation liquid becomes fructose syrup：Protein peptides：Strain：The mass ratio of water=(50~200) g：(0.1~10) g：(0.01
~1) g：(100~500) g；
S4. after fermentation, carry out sterilization treatment to obtain the final product；
The water uses distilled water.
The preparation of the microcapsule granule is to take the pipe tobacco particle, is handled using following preparation process：
S5. it extracts：Pipe tobacco particle is extracted using water, solid content is filtered to obtain after extraction, solid content is dried through powder
After broken sieving, 40~60 mesh is taken to sieve to obtain extract ingredient；
S6. coating：Microcapsules, micro- glue is made in extract ingredient encapsulating obtained by step S5 with microcapsular envelopes raw material
Mass percent shared by microcapsular envelopes raw material is 10~90% in capsule.It is further preferred that microcapsules packet in the microcapsules
Mass percent shared by film raw material is 15~25%, most preferably 20%.
Preferably, the sweetener is honey, white sugar, brown sugar, glucose, fructose, sucrose, Abbas's sweet tea, xylitol, wheat
Any one or a few mixture of bud sugar alcohol, saccharin sodium, tripotassium glycyrrhetate or jujube.
Preferably, the corrigent is salt, cocoa power, licorice powder or ground coffee；The flavouring agent is capsicum tincture, menthol
Or fruit extract.
Preferably, the flavouring agent is capsicum tincture, menthol or fruit extract.
Preferably, it is according to one in flue-cured tobacco, burley tobaccos, drying cigarette, Turkish tobaccos to prepare tobacco formulation group described in step S1
By formula mixing, mass ratio is flue-cured tobacco for kind or several mixing：Burley tobaccos：Dry cigarette：Turkish tobaccos=(0~2)：(4~0)：
(3~0)：(0~3).
Preferably, chopping described in S2 steps is that tobacco leaf is cut to 0.5~6cm long, the uniform filament of 0.1~1mm wide.
Preferably, the condition fermented described in step S3 is：Fermentation process remains that control temperature at 35~45 DEG C, is fermented
Time is 7~35 days.The zymotechnique of science provided by the invention not only obtains good buccal cigarette flavor, but also does not produce
Raw exceeded nitrite.
Preferably, the group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：The mass ratio of distilled water=(50~
100)g：(1~10) g：(0.1~0.8) g：(200~500) g.
Preferably, strain described in step S3 is monascus (Monascus purpureus Went.), aspergillus oryzae
(Aspergillus oryzae), Zygosaccharomyces rouxii (Mucor roxianus) or head mold (Rhizopus), saccharomycete
(Saccharomyces) or the one or more of lactic acid bacteria (Lactobacillus)；It is further preferred that the strain is rice
Aspergillus (Aspergillus oryzae), saccharomycete (Saccharomyces) or lactic acid bacteria (Lactobacillus).
Preferably, temperature described in step S3 is 35~45 DEG C, and fermentation time is 15~30 days.
Preferably, the protein peptides of inoculation liquid described in step S3 are Soyprotein peptide, wheat protein peptide, rice protein peptide, junket
Protein peptides, the one or more of whey protein peptide.
Preferably, it is 70~121 DEG C that sterilizing described in step S4, which uses pasteurization, sterilization treatment temperature, sterilization time 5
~30min.
Preferably, extraction described in step S5 is extracted 1 hour at 50 DEG C, and the mass ratio of the pipe tobacco and water is 1:5.
The microcapsular envelopes raw material includes：Arabic gum, sodium alginate, carragheen, dextrin, oligosaccharide, starch derivatives
In biology, gelatin, casein, sodium carboxymethylcellulose, ethyl cellulose or methylcellulose it is arbitrary two or more
Combination.Preferably, the microcapsular envelopes raw material is the mixture of dextrin, oligosaccharide and methylcellulose.Further preferably
Ground, dextrin, oligosaccharide and methylcellulose are according to 1:2:1 mass ratio combination.
Preferably, encapsulating described in step S6 is in 60~70 DEG C of waters bath with thermostatic control, under constant stirring toward extract ingredient
Middle addition coating raw material carries out homogeneous after coating dissolution of raw material is complete, carries out high speed dispersion to mixture, obtains emulsion；
By emulsion spray drying, microcapsules are made.It is preferred that the emulsion solid content is 40%.
Preferably, the process conditions of the spray drying be 180~250 DEG C of hot-air inlet air temperature, leaving air temp 80~
90℃。
Present invention simultaneously provides the preparation methods of the fermented type buccal cigarette with slow-release function, which is characterized in that is
According to pipe blend particle 50%~80%, water 10%~30%, corrigent 1%~5%, sweetener 1%~5%, flavouring agent
After 1%~10% ratio mixing, packed using penetrability sack by 0.1~0.5g/ bags of specifications.
The present invention provides buccal cigarette made from the preparation method.
Compared with prior art, the beneficial effects of the invention are as follows：
The prior art, which rarely has, takes necessary and rational fermentation process, prepared buccal cigarette that generally can not remove on tobacco leaf
The blue foreign smell and irritation of tobacco leaf need the corrigent by large scale to carry out flavoring to cover blue foreign smell and irritation, fragrance
Matter is also more dull, and perfume quantity is insufficient.Although and using by-product some raw materials generated in production of cigarettes workshop section through everfermentation
Processing, blue foreign smell and irritation are reduced, but the starting point that these existing raw materials make is to participate in burning, is sent out tobacco leaf
Requirement of the requirement of ferment processing with buccal cigarette for raw material differs greatly, and flavor is uncoordinated.
The present invention handles tobacco leaf using the zymotechnique specific aim of science, and the present invention uses the zymotechnique specific aim of science
Tobacco leaf is handled, eliminates the bitter taste and acid of pipe tobacco, nitrogen substance is reduced conversion, improves buccal cigarette raw material
Comfortable taste, fragrance matter enrich it is mellow, successfully eliminate raw material blue foreign smell and irritation, be effectively improved the quality of tobacco leaf, and
It is handled in conjunction with the seasoning of reasonable benefit/risk, it is compatible using the corrigent of rational proportion and sweetener etc. and pipe tobacco particle, it obtains more
Add the buccal cigarette of abundant mouthfeel, flavor coordination, high quality.
Based on preferred fermentation raw material, the present invention further summarizes microencapsulated, overcomes existing product nicotine and releases
It puts that rate is too fast, the mouth containing excessive later stage strength of strength early period is smaller, the quick thin out deficiency of smoke during entire mouth containing, increases
Mouth containing initial stage nicotine dissolves out resistance, under the premise of not changing overall nicotine burst size, the time for delaying nicotine at the uniform velocity to dissolve out,
To ensure that during mouth containing stable strength and smoke, and the not additional alkali salt of the present invention can be kept in a longer period of time.
Specific implementation mode
With reference to specific embodiment, present invention be described in more detail.Reagent that unless stated otherwise, the present invention uses,
Equipment is the art conventional reagent and equipment；Design philosophy of the present invention is summarized to obtain based on long-term many experiments, Xia Shushi
It applies example and is merely to illustrate the present invention, but therefore do not limit the present invention.Fructose syrup that following embodiments use, protein peptides and
Monascus, aspergillus oryzae, Zygosaccharomyces rouxii or head mold, saccharomycete or lactic acid bacteria are regular market purchase raw material.
Embodiment 1
A kind of pipe tobacco particle is prepared in the present embodiment, and preparation method includes the following steps：
S1. prepare tobacco formulation group：According to flue-cured tobacco：The mass ratio of burley tobaccos is 2：4 prepare tobacco leaf group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 1g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, ferment item
Part is：Fermentation process remains control temperature at 45 DEG C, and fermentation time is 15 days；The zymotechnique of science not only obtains good
Good buccal cigarette flavor, and reduce content of nitrite.
The group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：Mass ratio=50g of distilled water：5g：0.1g：
250g；The strain is monascus and saccharomycete, is obtained after bacterium solution according to 1 according to routine culture respectively:1 ratio mixing；
The protein peptides of the inoculation liquid are Soyprotein peptide；
S4. after fermentation, through 70 DEG C of pasteurization 30min.
Embodiment 2
A kind of pipe tobacco particle is prepared in the present embodiment, and preparation method includes the following steps：
S1. prepare tobacco formulation group：According to flue-cured tobacco：Burley tobaccos：The mass ratio for drying cigarette is 1：1：1 prepares tobacco leaf group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 1g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, ferment item
Part is：Fermentation process remains control temperature at 45 DEG C, and fermentation time is 15 days；The zymotechnique of science not only obtains good
Good buccal cigarette flavor, and reduce content of nitrite.
The group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：Mass ratio=50g of distilled water：5g：0.1g：
250g；The strain is monascus and saccharomycete, is obtained after bacterium solution according to 2 according to routine culture respectively:1 ratio mixing；
The protein peptides of the inoculation liquid are wheat protein peptide；
S4. after fermentation, through 85 DEG C of pasteurization 15min.
Embodiment 3
The present embodiment provides a kind of preparation methods of the pipe tobacco suitable for buccal cigarette, include the following steps：
S1. prepare tobacco formulation group：According to flue-cured tobacco：Burley tobaccos：The mass ratio for drying cigarette is 1：1：1 prepares tobacco leaf group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 10g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, ferments
Condition is：Fermentation process remains control temperature at 35 DEG C, and fermentation time is 20 days；The zymotechnique of science not only obtains
Good buccal cigarette flavor, and without generating exceeded nitrite.
The group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：Mass ratio=100g of distilled water：1g：0.5g：
200g；The strain is aspergillus oryzae and lactic acid bacteria, is obtained after bacterium solution according to 1 according to routine culture respectively:1 ratio mixing；
The protein peptides of the inoculation liquid are casein peptide；
S4. after fermentation, through 121 DEG C of pasteurization 5min.
Embodiment 4
The present embodiment provides a kind of preparation methods of the pipe tobacco suitable for buccal cigarette, include the following steps：
S1. prepare tobacco formulation group：According to burley tobaccos：Dry cigarette：The mass ratio of Turkish tobaccos is 3：2：1 prepares tobacco leaf
Group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 15g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, ferments
Condition is：Fermentation process remains control temperature at 40 DEG C, and fermentation time is 35 days；The zymotechnique of science not only obtains
Good buccal cigarette flavor, and without generating exceeded nitrite.
The group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：Mass ratio=80g of distilled water：10g：0.8g：
500g；The strain is Zygosaccharomyces rouxii, head mold and saccharomycete, is obtained after bacterium solution according to 1 according to routine culture respectively:2 ratio
Mixing；
The protein peptides of the inoculation liquid are Soyprotein peptide and whey protein peptide mass ratio is 1:1；
S4. after fermentation, through 100 DEG C of pasteurization 10min.
Embodiment 5
The present embodiment provides a kind of preparation methods of the pipe tobacco suitable for buccal cigarette, include the following steps：
S1. prepare tobacco formulation group：According to flue-cured tobacco：Burley tobaccos：Dry cigarette：The mass ratio of Turkish tobaccos is 1：4：3：1；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, excessive moisture is removed, cuts
Silk；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 5g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, ferment item
Part is：Fermentation process remains control temperature at 45 DEG C, and fermentation time is 30 days；The zymotechnique of science not only obtains good
Good buccal cigarette flavor, and without generating exceeded nitrite.
The group of the inoculation liquid becomes fructose syrup：Protein peptides：Strain：Mass ratio=80g of distilled water：10g：0.8g：
500g；The strain is Zygosaccharomyces rouxii, head mold and saccharomycete, is obtained after bacterium solution according to 1 according to routine culture respectively:2:1 ratio
Example mixing；
The protein peptides of the inoculation liquid are rice protein peptide；
S4. after fermentation, through 121 DEG C of pasteurization 5min.
Embodiment 6 prepares microcapsule granule
The preparation method of the microcapsule granule includes the following steps：
The pipe tobacco particle that 1 to 5 any embodiment of Example is prepared is handled using following preparation process：
S5. it extracts：Pipe tobacco particle is extracted using water, solid content is filtered to obtain after extraction, solid content is dried through powder
After broken sieving, 40~60 mesh is taken to sieve to obtain extract ingredient；It is extracted 1 hour at 50 DEG C, the mass ratio of the pipe tobacco and water is
1:5。
S6. coating：Microcapsules, micro- glue is made in extract ingredient encapsulating obtained by step S5 with microcapsular envelopes raw material
Mass percent shared by microcapsular envelopes raw material is 10~90% in capsule.It is further preferred that microcapsules packet in the microcapsules
Mass percent shared by film raw material is 25%.
The microcapsular envelopes raw material is Arabic gum and maltodextrin according to 1:The combination of 1 mass ratio.
Encapsulating described in S6 steps is that coating is added in extract ingredient under constant stirring in 60~70 DEG C of waters bath with thermostatic control
Raw material carries out homogeneous after coating dissolution of raw material is complete, carries out high speed dispersion to mixture, obtains emulsion, the emulsion
Solid content is 50%；By emulsion spray drying, microcapsules are made.
The process conditions of the spray drying are 180 DEG C of hot-air inlet air temperature, 85~90 DEG C of leaving air temp.
Embodiment 7
Pipe tobacco obtained by 1 to 5 any embodiment of Example is handled using following preparation process：
S5. pipe tobacco extracts：After pipe tobacco fermentation, is extracted using water, solid content is filtered to obtain after extraction, solid content is dried
After pulverizing and sieving, 40~60 mesh is taken to sieve to obtain extract ingredient；
Wherein, extraction described in S5 steps is extracted 1 hour at 50 DEG C, and the mass ratio of the pipe tobacco and water is 1:5.
S6. coating：Extract ingredient is encapsulated with microcapsular envelopes raw material, microcapsules are made, microcapsules in the microcapsules
Coating material quality percentage is 20%.
The microcapsular envelopes raw material includes：Dextrin, oligosaccharide and methylcellulose are according to 1:2:1 ratio combination.
Encapsulating described in S6 steps is that coating is added in extract ingredient under constant stirring in 60~70 DEG C of waters bath with thermostatic control
Raw material carries out homogeneous after coating dissolution of raw material is complete, carries out high speed dispersion to mixture, obtains emulsion, the emulsion
Solid content is 40%；By emulsion spray drying, microcapsules are made.
The process conditions of the spray drying are 250 DEG C of hot-air inlet air temperature, 90 DEG C of leaving air temp.
Embodiment 8
Pipe tobacco obtained by 1 to 5 any embodiment of Example is handled by following preparation process：
S5. pipe tobacco extracts：After pipe tobacco fermentation, is extracted using water, solid content is filtered to obtain after extraction, solid content is dried
After pulverizing and sieving, 40~60 mesh is taken to sieve to obtain extract ingredient；
Wherein, extraction described in S5 steps is extracted 1 hour at 50 DEG C, and the mass ratio of the pipe tobacco and water is 1:5.
S6. coating：Extract ingredient is encapsulated with microcapsular envelopes raw material, microcapsules are made, microcapsules in the microcapsules
Coating material quality percentage is 30%.
The microcapsular envelopes raw material includes：Arabic gum, casein, ethyl cellulose are according to 2:1:1 ratio
Combination.
Encapsulating described in S6 steps is that coating is added in extract ingredient under constant stirring in 60~70 DEG C of waters bath with thermostatic control
Raw material carries out homogeneous after coating dissolution of raw material is complete, carries out high speed dispersion to mixture, obtains emulsion, the emulsion
Solid content is 50%；By emulsion spray drying, microcapsules are made.
The process conditions of the spray drying are that inlet air temperature is 220 DEG C, and leaving air temp is 80 DEG C.
Embodiment 9
Pipe tobacco obtained by 1 to 5 any embodiment of Example is handled by following preparation process：
S5. pipe tobacco extracts：After pipe tobacco fermentation, is extracted using water, solid content is filtered to obtain after extraction, solid content is dried
After pulverizing and sieving, 40~60 mesh is taken to sieve to obtain pipe tobacco particle；
Wherein, extraction described in S5 steps is extracted 1 hour at 50 DEG C, and the mass ratio of the pipe tobacco and water is 1:5.
S6. coating：Extract ingredient is encapsulated with microcapsular envelopes raw material, microcapsules are made, microcapsules in the microcapsules
Coating material quality percentage is 30%.
The microcapsular envelopes raw material includes：Gelatin and ethyl cellulose are according to 1:The combination of 1 ratio.
Encapsulating described in S6 steps is that coating is added in extract ingredient under constant stirring in 60~70 DEG C of waters bath with thermostatic control
Raw material carries out homogeneous 15min after coating dissolution of raw material is complete, carries out high speed dispersion to mixture, obtains emulsion, described
Emulsion solid content is 60%；By emulsion spray drying, microcapsules are made.
The process conditions of the spray drying are that inlet air temperature is 185 DEG C, and leaving air temp is 80 DEG C.
Embodiment 10
The pipe tobacco particle that 1 to 5 any embodiment of Example is prepared, Example 6 to 9 any embodiment gained are micro-
Capsule particle, the two is with 2:Pipe blend particle is obtained after 1 mass ratio mixing, auxiliaries is equipped with and forms buccal cigarette
Grain, the formula for being equipped with auxiliaries are：According to mass percent meter, pipe blend particle 80%, water 14%, corrigent
3%, sweetener 2%, flavouring agent 1%.Corrigent is salt, and sweetener is honey, and flavouring agent is menthol.
Embodiment 11
The pipe tobacco particle that 1 to 5 any embodiment of Example is prepared, Example 6 to 9 any embodiment gained are micro-
Capsule particle, the two is with 3:Pipe blend particle is obtained after 1 mass ratio mixing, auxiliaries is equipped with and forms buccal cigarette
Grain, the formula for being equipped with auxiliaries are：According to mass percent meter, pipe blend particle 90%, water 4%, corrigent
4%, sweetener 1%, flavouring agent 1%.Corrigent is salt and cocoa power according to 1:1 mass ratio, sweetener are honey, fragrance
Agent is capsicum tincture.
Embodiment 12
The pipe tobacco particle that 1 to 5 any embodiment of Example is prepared, Example 6 to 9 any embodiment gained are micro-
Capsule particle, the two is with 4:Pipe blend particle is obtained after 1 mass ratio mixing, auxiliaries is equipped with and forms buccal cigarette
Grain, the formula for being equipped with auxiliaries are：According to mass percent meter, pipe blend particle 90%, water 4%, corrigent
5%, flavouring agent 2%.Corrigent is salt and licorice powder according to 1:1 mass ratio, flavouring agent be capsicum tincture and menthol according to
1:5 mass ratio.
Embodiment 13
The pipe tobacco particle that 1 to 5 any embodiment of Example is prepared, Example 6 to 9 any embodiment gained are micro-
Capsule particle, the two is with 3:Pipe blend particle is obtained after 1 mass ratio mixing, auxiliaries is equipped with and forms buccal cigarette
Grain, the formula for being equipped with auxiliaries are：According to mass percent meter, pipe blend particle 85%, water 9%, corrigent
3%, sweetener 2%, flavouring agent 1%.Corrigent is that sweetener is honey, and flavouring agent is menthol.
Embodiment 14
Mouth containing smoke particle with slow-release function made from Example 10 to 13 any embodiment of embodiment, by 0.3g/
The specification of bag is by buccal cigarette granule packaging in penetrability pouch.
Embodiment 15 detects and experiment of smokeing panel test
The measurement of content of nitrite：The chromatography of ions (NY/T 1375-2007 plant products nitrites and nitric acid
The measurement of salt)；The measurement of protein content：Ke Daerfa be (YCT 166-2003 tobaccos and tobacco product total protein content
It measures)；The measurement of content of cellulose：Enzymolysis-flow analysis (bibliography：Examine cigarette tobacco leaf pectin, cellulose in the China Guo Song
Content distribution feature and Henan influence [D] to reviewing prnciple：Agricultural University Of He'nan, 2011,18~19)；The survey of pectin content
It is fixed：The chromatography of ions (the measurement chromatography of ions of YC/T 346-2010 tobaccos and tobacco product pectin)；The survey of content of cellulose
It is fixed：Enzyme hydrolysis-the chromatography of ions (measurement enzyme hydrolysis-ion chromatography of YC/T 283-2009 tobaccos and tobacco product starch
Method)；The measurement of content of lignin：Sulfuric acid process (bibliography：Pottery is precious, the chemical constitution of Guan Yingting lignin and its application
[J] Cellulose Sciences and technology, 2003,11 (1):43-55).
Through examining, the quality data of 1 to 5 gained pipe tobacco of embodiment are shown in Table 1；Simultaneously by the embodiment of the present invention 1
Pipe tobacco made from~5 asks 10 experts that smoke panel test to carry out experiment of smokeing panel test.Method of smokeing panel test is that pipe tobacco is directly placed in upper lip and upper row's tooth
Between tooth, the pipe tobacco granular mass being put into every time in lip is 0.2g, and standard edible time is set to 10min.
The quality of 1 pipe tobacco of table
Through examining, the quality data of 10 to 13 gained buccal cigarette of embodiment are shown in Table 2.Method of smokeing panel test is that will suck
Cigarette is directly placed between upper lip and upper row's tooth, and the buccal cigarette quality being put into every time in lip is 0.2g, and standard edible time is set to
10min.Scoring criterion is that the alkali rate of release of buccal cigarette sucks early period and later stage strength, compliance (buccal cigarette edible time
Below standard quasi- edible time, which is spued, is considered as poor compliance), flavor, fragrance, pleasant impression respectively account for 10 points, total score 70 is divided.
The quality of 2 buccal cigarette of table
| Sample | Alkali rate of release | Suck strength early period | Suck later stage strength | Compliance | Flavor | Fragrance | Pleasant impression | Total score |
| Embodiment 10 | 8 | 7 | 9 | 9 | 9 | 9 | 9 | 60 |
| Embodiment 11 | 9 | 9 | 8.5 | 9 | 9 | 9 | 8.5 | 62 |
| Embodiment 12 | 9 | 8 | 9 | 9 | 9 | 9 | 9.5 | 62.5 |
| Embodiment 13 | 8.5 | 8 | 8 | 9 | 9 | 9 | 8.5 | 60 |
The present invention handles tobacco leaf using the zymotechnique specific aim of science, and the present invention uses the zymotechnique specific aim of science
Tobacco leaf is handled, eliminates the bitter taste and acid of pipe tobacco, nitrogen substance is reduced conversion, improves buccal cigarette raw material
Comfortable taste, fragrance matter enrich it is mellow, successfully eliminate raw material blue foreign smell and irritation, be effectively improved the quality of tobacco leaf, and
It is handled in conjunction with the seasoning of reasonable benefit/risk, it is compatible using the corrigent of rational proportion and sweetener etc. and pipe tobacco particle, it obtains more
Add the buccal cigarette of abundant mouthfeel, flavor coordination, high quality.Based on preferred fermentation raw material, the present invention further summarizes micro- glue
Capsule is encapsulated, and overcomes that existing product nicotine rate of release is too fast, the mouth containing excessive later stage strength of strength early period is smaller, entire sucked
The quick thin out deficiency of smoke in journey increases mouth containing initial stage nicotine dissolution resistance, before not changing overall nicotine burst size
It puts, delaying time that nicotine at the uniform velocity dissolves out, (time of the nicotine dissolution of the pipe tobacco particle added without microcapsule granule is usual
For 10~12min, and it is added to nicotine dissolution time 15~18min of average out to of the pipe blend particle of microcapsule granule, prolonged
It has grown 50%), to ensure that during mouth containing stable strength and smoke can be kept in a longer period of time, and the present invention is not
Need additional alkali salt.
Claims (11)
1. a kind of fermented type buccal cigarette with slow-release function, which is characterized in that by the component of following mass percentage content
Preparation obtains：
Pipe blend particle 50%~80%, water 10%~30%, corrigent 1%~5%, sweetener 1%~5%, flavouring agent
1%~10%；
The pipe blend particle is the mixture of pipe tobacco particle and microcapsule granule, and the mixing quality ratio of the two is 2:1~
4:1；
The preparation method of the pipe tobacco particle includes the following steps：
S1. prepare tobacco formulation group；
S2. tobacco leaf is handled：Tobacco leaf is rinsed with water, surface dust is removed, slightly dries, removes excessive moisture, chopping；
S3. pipe tobacco ferments：Inoculation liquid is prepared, is to ferment after 1~15g inoculation liquids/100g pipe tobaccos are inoculated with according to inoculum concentration, it is described to connect
The group of kind liquid becomes fructose syrup：Protein peptides：Strain：The mass ratio of water=(50~200) g：(0.1~10) g：(0.01~1)
g：(100~500) g；
Strain described in step S3 is monascus (Monascus purpureus Went.), aspergillus oryzae (Aspergillus
Oryzae), Zygosaccharomyces rouxii (Mucor roxianus) or head mold (Rhizopus), saccharomycete (Saccharomyces) or lactic acid
The one or more of bacterium (Lactobacillus)；
The condition fermented described in step S3 is：Fermentation process remains control temperature at 35~45 DEG C, and fermentation time is 7~35
It；
S4. after fermentation, carry out sterilization treatment to obtain the final product；
The preparation method of the microcapsule granule includes the following steps：
S5. it extracts：Pipe tobacco particle is extracted using water, solid content is filtered to obtain after extraction, solid content is dried through crushed
After sieve, 40~60 mesh is taken to sieve to obtain extract ingredient；
S6. coating：Extract ingredient obtained by step S5 is encapsulated with microcapsular envelopes raw material, microcapsules are made, in the microcapsules
Mass percent shared by microcapsular envelopes raw material is 20~25%.
2. the fermented type buccal cigarette with slow-release function according to claim 1, which is characterized in that the sweetener is bee
Honey, white sugar, brown sugar, glucose, fructose, sucrose, Abbas's sweet tea, xylitol, maltitol, saccharin sodium, tripotassium glycyrrhetate or big
Any one or a few mixture of jujube.
3. according to claim 1 with slow-release function fermented type buccal cigarette, which is characterized in that the corrigent be salt,
Cocoa power, licorice powder or ground coffee；The flavouring agent is capsicum tincture, menthol or fruit extract.
4. the fermented type buccal cigarette with slow-release function according to claim 1, which is characterized in that the flavouring agent is capsicum
Tincture, menthol or fruit extract.
5. the fermented type buccal cigarette with slow-release function according to claim 1, which is characterized in that being extracted described in step S5 is
It is extracted 1 hour at 50 DEG C after adding water.
6. the fermented type buccal cigarette with slow-release function according to claim 1, which is characterized in that the microcapsular envelopes
Raw material is Arabic gum, sodium alginate, carragheen, dextrin, oligosaccharide, starch derivatives, gelatin, casein, carboxymethyl cellulose
Two or more arbitrary combination in plain sodium, ethyl cellulose or methylcellulose.
7. the fermented type buccal cigarette with slow-release function according to claim 6, which is characterized in that the starch derivatives
For dextrin.
8. the fermented type buccal cigarette with slow-release function according to claim 1, which is characterized in that with micro- glue described in step S6
Capsule coating raw material by the encapsulating that microcapsules are made in the encapsulating of extract ingredient obtained by step S5 be in 60~70 DEG C of waters bath with thermostatic control,
Be stirred continuously in the lower ingredient toward extract addition coating raw material, after coating dissolution of raw material is complete, carry out homogeneous, to mixture into
Row high speed dispersion, obtains emulsion, and by emulsion spray drying, microcapsules are made.
9. the fermented type buccal cigarette with slow-release function according to claim 8, which is characterized in that the work of the spray drying
Skill condition is 180~250 DEG C of hot-air inlet air temperature, 80~90 DEG C of leaving air temp.
10. the preparation method of the fermented type buccal cigarette with slow-release function described in any one of claim 1 to 9, which is characterized in that
It is according to pipe blend particle 50%~80%, water 10%~30%, corrigent 1%~5%, sweetener 1%~5%, fragrance
After the ratio mixing of agent 1%~10%, packed using penetrability sack by 0.1~0.5g/ bags of specifications.
11. buccal cigarette made from preparation method described in claim 10.
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| CN112444466B (en) * | 2019-09-05 | 2023-02-28 | 上海新型烟草制品研究院有限公司 | Method for evaluating in-vitro absorption of nicotine buccal cigarette |
| CN117625420B (en) * | 2024-01-25 | 2024-05-03 | 天津科技大学 | Method for preparing essence and spice by composite microorganism liquid state fermentation of tobacco leaves and saccharomyces cerevisiae |
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| CN101262786B (en) * | 2005-05-25 | 2015-04-08 | 美国无烟烟草有限责任公司 | Tobacco compositions |
| CN101548797B (en) * | 2008-03-31 | 2011-12-07 | 湖北中烟工业有限责任公司 | Cigarette and preparation method thereof |
| US9039839B2 (en) * | 2010-04-08 | 2015-05-26 | R.J. Reynolds Tobacco Company | Smokeless tobacco composition comprising tobacco-derived material and non-tobacco plant material |
| CN102715647B (en) * | 2012-07-02 | 2014-06-18 | 湖北中烟工业有限责任公司 | Novel buccal cigarette |
| CN102920013B (en) * | 2012-11-19 | 2015-02-11 | 湖南中烟工业有限责任公司 | Tobacco extractive microcapsule and preparation method thereof |
| US20160044955A1 (en) * | 2014-08-13 | 2016-02-18 | R.J. Reynolds Tobacco Company | Smokeless tobacco products |
| CN105286080B (en) * | 2015-11-12 | 2021-05-28 | 贵州中烟工业有限责任公司 | Buccal smokeless tobacco product and preparation method thereof |
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